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K*. 04
Continuous vs. Segmented Second Dimension
System Gradients for Comprehensive TwoDimensional Liquid Chromatography of Sugarcane (Saccharum SPP.)
Francesco Cacciola 1,2, Gabriel Mazzi Leme 1, Paola
Donato 3,4, Alberto Jose Cavalheiro 5, Paola Dugo 3,4,
Luigi Mondello 3,4
1 Dipartimento di Scienze dell‘Ambiente, della
Sicurezza, del Territorio, degli Alimenti e della
Salute, University of Messina, Italy
2 Chromaleont s.r.l. A start-up of the University
of Messina, Italy
3 Centro Integrato di Ricerca (C.I.R.), University
Campus Bio-Medico of Rome, Italy
4 Dipartimento di Scienze del Farmaco e dei Prodotti
per la Salute, University of Messina, Messina, Italy
5 Institute of Chemistry, São Paulo State University,
Araraquara, Brazil
K*. 05
Increase the Separation Power of Two-Dimensional Liquid Chromatography Through the
Use of Shifted Gradients for Polyphenol Determination in Red Wine
Cacciola 1,2,
Donato 3,4,
Francesco
Paola
Francesca
Rigano 4, Paola Dugo 3,4, Luigi Mondello 3,4
1 Dipartimento di Scienze dell‘Ambiente, della
Sicurezza, del Territorio, degli Alimenti e della
Salute, University of Messina, Italy
2 Chromaleont s.r.l. A start-up of the University
of Messina, Italy
3 Centro Integrato di Ricerca, University Campus
Bio-Medico of Rome, Italy
4 Dipartimento di Scienze
K*. 06
The On-Line Hyphenation of Comprehensive
Liquid Chromatography to Triple Quadrupole
Mass Spectrometry for the Elucidation of the
Carotenoid Content in Foodstuffs with High
Orthogonality and Sensitivity
Please visit our booth # 8 on
ISCC to see our latest technology
and discuss with our experts.
Paola Donato 1,2, Francesco Cacciola 3,4, Francesca
Rigano 2, Daniele Giuffrida 3, Paola Dugo 1,2,
Luigi Mondello 1,2
1 Centro Integrato di Ricerca (C.I.R.), University
Campus Bio-Medico of Rome, Italy
2 Dipartimento di Scienze del Farmaco e dei Prodotti
per la Salute, University of Messina, Italy
3 Dipartimento di Scienze dell‘Ambiente, della
Sicurezza, del Territorio, degli Alimenti e della
Salute, University of Messina, Italy
4 Chromaleont s.r.l. A start-up of the University
of Messina, Italy
K*. 07
Coupling of New Silver Thiolate and Monodisperse Materials in Comprehensive TwoDimensional Liquid Chromatography for Truly
Orthogonal Lipid Separation
INVITATION
Company Seminar at the 38th ISCC
Giuseppe Sullini 1, Paola Donato 1,2, Marco
Beccaria 1, Francesco Cacciola 3,4, Paola Dugo 1,2,
Luigi Mondello 1,2
1 Dipartimento di Scienze del Farmaco e dei Prodotti
per la Salute, University of Messina, Italy
2 Centro Integrato di Ricerca (C.I.R.), University
Campus Bio-Medico of Rome, Italy
3 Dipartimento di Scienze dell‘Ambiente, della
Sicurezza, del Territorio, degli Alimenti e della
Salute, University of Messina, Italy
4 Chromaleont s.r.l. A start-up of the University
of Messina, Italy
Presentation of two World Premieres
Smart & powerful tools for comprehensive analysis
Wednesday, May 21st, 3.45 - 4.45 pm, Palazzo Dei Congressi, Room 1000
Shimadzu Europa GmbH
Albert-Hahn-Str. 6-10 · D-47269 Duisburg
Tel.: +49 - (0)203 - 76 87-0
Fax: +49 - (0)203 - 76 66 25
[email protected]
www.shimadzu.eu
Presenters:
Haruhiko Miyagawa: New Smart technologies to
enhance GC-MS/MS productivity, operation and
performance
Megumi Hirooka: ChromSquare – Power of
GCxGC-MS analysis with ease of data handling
Dr. Paola Donato: Novel powerful MS strategies in
comprehensive 2D LC
Dr. Flavio A. Franchina: Double-oven comprehensive
2D GC combined with a rapid triple-quadrupole mass
spectrometer
Poster Presentations
38th ISCC
E. 08
Analytical Comparison of the Determination
of Bisphenol A in Paper for Food Packaging
Andrea Jurek, Erich Leitner
Institute of Analytical Chemistry and Food
Chemistry, Graz University of Technology, Austria
I. 04
Maximizing Efficiency in UHPLC-MS/MS Method
Development for Multi Component Analysis
Anja Grüning, Julia Sander, Ute Potyka,
Stéphane Moreau
GCMS-TQ8040
Improving precision and throughput, the new
GCMS-TQ8040 is the most accurate, cost effective, easy-to-use, triple quadrupole GCMS ever.
The system combines Ultra-Fast Mass Spectrometry (UFMS) and Smart Multiple Reaction Monitoring (MRM) based on Shimadzu’s patented
UFsweeper™ technology.
Shimadzu Europa GmbH, Duisburg, Germany
P. 10 – Fast GC-MS/MS Analysis of Multicomponent Pesticides Residue (>300) in Food Matrices
Using of MS Technology
Hendrik J. Schulte, Hans-Ulrich Baier,
Stéphane Moreau
Shimadzu Europa GmbH, Duisburg, Germany
Through smart technologies, the triple quadrupole GCMS provides a new level in routine work:
• Smart Productivity
means high efficiency and sample throughput
and is based on simultaneous multi-component
analysis.
• Smart Operation
facilitates rapid and easy method development.
• Smart Performance
enables Scan/MRM for low detection limits and
simultaneous target compound confirmation.
J. 18
Isolation of Bioflavonoids from Citrus ByProducts by Means of Multidimansional LC
Preparative System Coupled with a Mass
Spectrometer
Marina Russo1, Veronica Inferrera1, Paola Dugo1,2,
Luigi Mondello1,2
1D
ipartimento di Scienze del Farmaco e dei Prodotti
per la Salute, University of Messina, Italy
2 Centro Integrato di Ricerca (C.I.R.), University
Campus Bio-Medico of Rome, Italy
J. 19
The On-Line Combination of Liquid Chromatography-Large Volume Injection-Comprehensive
Two-Dimensional Gas Chromatography-Triple
Quad Mass Spectrometry: a Powerful FourDimensional Separation-Science Tool
Mariosimone Zoccali1, Peter Q. Tranchida1,
Paola Dugo1,2, Luigi Mondello1,2
1D
ipartimento di Scienze del Farmaco e dei Prodotti
per la Salute, University of Messina, Italy
2 Centro Integrato di Ricerca (C.I.R.), University
Campus Bio-Medico of Rome, Italy
J. 22
Rapid Isolation of High Solute Amounts by
Using an On-Line Fourdimensional Preparative
System: Normal Phase-Liquid Chromatography
Coupled to Methyl Siloxane-Ionic Liquid-Wax
Phase Gas Chromatography
Sebastiano Pantò1, Danilo Sciarrone1, Mariarosa
Maimone1, Peter Q. Trachida1, Paola Dugo1,2,
Luigi Mondello1,2
1D
ipartimento di Scienze del Farmaco e dei Prodotti
per la Salute, University of Messina, Italy
2 Centro Integrato di Ricerca (C.I.R.), University
Campus Bio-Medico of Rome, Italy
J. 24
Collection of Enantiomeric Pure Components by
Using a Multidimensional Gas Chromatographic
Preparative System
Danilo Sciarrone 1, Sebastiano Pantò 1, Paola Dugo 1,2,
Luigi Mondello 1,2
1D
ipartimento di Scienze del Farmaco e dei Prodotti
per la Salute, University of Messina, Italy
2 Centro Integrato di Ricerca (C.I.R.), University
Campus Bio-Medico of Rome, Italy
L. 06
Multi-Component Quantitative Analysis
of Pharmaceuticals in the Environment by
UHPLC-MS/MS with Online Spe
Anja Grüning 1, Julia Sander 1, Ute Potyka 1,
Stéphane Moreau 1, Mikael Levi 2
1 S himadzu Europa GmbH, Duisburg, Germany
2 Shimadzu France, Marne-la-Vallée, France
Anja Grüning 1, Julia Sander 1, Ute Potyka 1,
Stéphane Moreau 1, Mikael Levi 2
O. 15
Throughout Investigation of Fused-Core
Stationary Phases Coupled to Ion Trap-Time
of Flight Mass Spectrometry Detection for a
Comprehensive Elucidation of the Total Lipid
Profile of Human Plasma
1 S himadzu Europa GmbH, Duisburg, Germany
2 Shimadzu France, Marne-la-Vallée, France
Nermeen Girgis 1, Paola Donato 1,2, Francesco
Cacciola 3, Paola Dugo 1,2, Luigi Mondello 1,2
M. 05
Fast GC-MS/MS Analysis of 76 VOC Compounds
Using Headspace-Trap Sampling
1D
ipartimento di Scienze del Farmaco e dei Prodotti
per la Salute, University of Messina, Italy
2 Centro Integrato di Ricerca (C.I.R.), University
Campus Bio-Medico of Rome, Italy
3 Dipartimento di Scienze dell‘Ambiente, della
Sicurezza, del Territorio, degli Alimenti e della
Salute, University of Messina, Italy
L. 07
Analysis of Doping Agents Using Ultrafast
LC-MS/MS with Scheduled MRM
Hendrik J. Schulte, Hans-Ulrich Baier,
Stéphane Moreau
Shimadzu Europa GmbH, Duisburg, Germany
O. 07
Comprehensive Analysis of NaphthoylindoleType Synthetic Cannabinoids by GC-MS/MS
Using Simultaneous EI-Scan, MRM and Precursor Ion Scan Mode
Hendrik J. Schulte 1, Haruhiko Miyagawa 2,
Yuki Sakamoto 2, Tooru Kamata 3, Shuntaro
Matsuta 3, Hiroshi Nishioka 3, Munehiro Katagi 3,
Kei Zaitsu 4, Akira Ishii 4, Kento Tsuboi 5, Hitoshi
Tsuchihashi 5, Koichi Suzuki 5
1 S himadzu Europa GmbH, Duisburg, Germany
2 Shimadzu Corporation, Kyoto, Japan
3 Forensic Science Laboratory, Osaka Prefectural
Police Headquarters, Japan
4 Department of Legal Medicine & Bioethics, Nagoya
University Graduate School of Medicine, Japan
5 Department of Legal Medicine, Osaka Medical
College, Japan
P. 10
Fast GC-MS/MS Analysis of Multicomponent
Pesticides Residue (>300) in Food Matrices
Using of MS Technology
Hendrik J. Schulte, Hans-Ulrich Baier,
Stéphane Moreau
Shimadzu Europa GmbH, Duisburg, Germany
P. 11
The Use of Linear Retention Indices in
Pesticide Residue Analysis Using a Tandem
GCMS with MRM Database
Hendrik J. Schulte, Hans-Ulrich Baier,
Stéphane Moreau
Shimadzu Europa GmbH, Duisburg, Germany
Poster Presentations
11th GCxGC Symposium
K. 12
Characterization Of Sebum Lipids Using
Comprehensive Two-Dimensional Gas Chromatography Combined With Rapid-Scanning
Quadrupole Mass Spectrometry
Laurent Boisaubert 1, Valeria Manzin 1, Peter
Tranchida 2, Luigi Mondello 2
1A
dvanced Research, L‘OREAL R&I, Aulnay sous
bois, France
2 University of Messina, Italy
K. 66
Characterization of Organic Sulfur Compounds
in Fossil Fuels Using Flow-Modulated Comprehensive Two-Dimensional Gas Chromatography
and Tandem Mass Spectrometry
Maria E. Machado 1, Flavio A. Franchina 2, Claudia
Zini 1, Elina B. Caramao 1,3, Peter Q. Tranchida 2,
Luigi Mondello 2,4
1 Instituto de Quimica, Universitade Federal do Rio
Grande do Sul, Porto Alegre, Brazil
2 Dipartimento di Scienze del Farmaco e Prodotti
per la Salute, University of Messina, Italy
3 Instituto Nacional de Ciencia e Tecnologia em
Energia e Ambiente, INCT E&A, Campus
Universitário de Ondina, Salvador, Brazil
4 Centro Integrato di Ricerca (C.I.R.), University
Campus Bio-Medico of Rome, Italy
K. 71
The Off-Line Combination of High Performance
Liquid Chromatography and Comprehensive
Two-Dimensional Gas Chromatography-Mass
Spectrometry: a New Powerful Approach for
Highly-Detailed Essential Oil Analysis
Mariosimone Zoccali 1, Peter Q. Tranchida 1, Paola
Dugo 1,2, Giovanni Dugo 1, Luigi Mondello 1,2
1D
ipartimento di Scienze del Farmaco e Prodotti
per la Salute, University of Messina, Italy
2 Centro Integrato di Ricerca (C.I.R.), University
Campus Bio-Medico of Rome, Italy
K. 87
Monodimensional (GC-FID And GC-MS) and
Comprehensive Two-Dimensional (GC×GC)
Gas Chromatography for the Assessment
of Volatiles and Fatty Acids from Ruta
Chalepensis L. Plants
Selenia De Grazia 1, Rosaria Costa 1, Laura Tedone 1,
Salvatore Ragusa 2, Luigi Mondello 1,3
1D
ipartimento di Scienze del Farmaco e Prodotti
per la Salute, University of Messina, Italy
2 Dipartimento di Scienze della Salute, University
of Catanzaro, Italy
3 Centro Integrato
K*. 01
Comprehensive HPLC Analysis of Alkaloids and
Permitted Additives in Dark Chocolate Products
Gesa Schad, Björn T. Erxleben, Robert Ludwig,
Brigitte Richrath
Shimadzu Europa GmbH, Duisburg, Germany
ChromSquare V2
ChromSquare V2, the latest generation of
Shimadzu’s software solutions, provides an
easy-to-use GCxGCMS data handling for
Comprehensive Chromatography applications.
ChromSquare V2 meets the needs of the Comprehensive GCxGCMS separation power of the
GCMS-QP2010 Ultra. Users of food, environmental, flavor & fragrance industries as well
as analytical chemistry benefit from convenient
features such as view of chromatogram, spectra
and contour plot in one user interface, blob
assembling also by MS spectra, and easy quantification through method and schedule icons.
K. 71 – The Off-Line Combination of High Performance Liquid Chromatography and Comprehensive Two-Dimensional Gas Chromatography-Mass Spectrometry: a New Powerful
Approach for Highly-Detailed Essential Oil
Analysis
Mariosimone Zoccali 1, Peter Q. Tranchida 1, Paola
Dugo 1,2, Giovanni Dugo 1, Luigi Mondello 1,2
1D
ipartimento di Scienze del Farmaco e Prodotti
per la Salute, University of Messina, Italy
2 Centro Integrato di Ricerca (C.I.R.), University
Campus Bio-Medico of Rome, Italy
Oral Presentations
11th GCxGC Symposium
Monday, May 19 th, 10.10 am, Room 300 + 100
Thursday, May 22 nd, 9.50 am, Room 1000
Microfabricated Reactors for Volatiles Analysis
by GC×GC-C-IRMS
Comprehensive 2D-LC: a Rapid Evolution
of a Powerful Technique
Tom Brenna, Herbert Tobias
Cornell University, Savage Hall, United States
Paola Dugo 1,2, Paola Donato 1,2, Francesco
Cacciola 2,3, Luigi Mondello 1,3
1U
niversity of Messina, Italy
2 University Campus Bio-Medico of Rome, Italy
3 Chromaleont s.r.l. A start-up of the University
of Messina, Italy
Monday, May 19 th, 11.40 am, Room 1000
Flow-Modulated GC×Low-Pressure GC: a Novel
Approach for High Resolution/Sensitivity GC
Separations
LCMS-8050
The LCMS-8050 triple quadrupole mass spectrometer is perfect for definitive identification and
reproducible quantification of trace level analytes
in complex samples. Through its world-class
features it gives access to an expanded range of
LC-MS/MS applications such as pharmacokinetics
in pharma, food, environmental, forensics and
toxicology.
The system provides a dramatically increased
analytical throughput with ultra-high speed
performance. In addition, the newly improved
ion source and collision cell, Heated ESI and
UFsweeper™ III collision cell technology, yield
higher sensitivity.
The LCMS-8050 again features the world’s fastest polarity switching time of 5 msec – three
times faster than the predecessor version.
The leading UHPLC system and proprietary
ultrafast technologies support are the backbones of resolving power.
L. 07 – Analysis of Doping Agents Using Ultrafast LC-MS/MS with Scheduled MRM
Anja Grüning 1, Julia Sander 1, Ute Potyka 1,
Stéphane Moreau 1, Mikael Levi 2
1 S himadzu Europa GmbH, Duisburg, Germany
2 Shimadzu France, Marne-la-Vallée, France
Thursday, May 22 nd, 5.00 pm, Room 300
Peter Q. Tranchida, Flavio A. Franchina, Paola Dugo,
Luigi Mondello
University of Messina, Italy
Analysis of Principal Flavonoids in Citrus
Juices by Nano-LC and Determination of
their Antioxidant Activity
Monday, May 19 th, 4.00 pm, Room 300 + 100
Chiara Fanali 1, Anna Rocco 2, Laura Dugo 1,
Paola Dugo 1,3, Luigi Mondello 1,3
1C
ampus Bio-Medico University of Rome, Italy
2 CNR, Rome, Italy
3 University of Messina, Italy
Comprehensive Two-Dimensional Gas Chromatography Combined with a Fast-Scanning
Quadrupole Mass Spectrometer: Suitable for
Metabolomics?
Christoph H. Weinert 1, Bjoern Egert 1, Hans-Ulrich
Baier 2, Sabine E. Kulling 1
1M
ax Rubner-Institut, Karlsruhe, Germany
2 Shimadzu Europa GmbH, Duisburg, Germany
38th ISCC
Tuesday, May 20 th, 5.10 pm, Room 300 + 100
On-Line Liquid Chromatography-Comprehensive 2D Gas Chromatography-Triple Quad
Mass Spectrometry: a Powerful and Flexible
4D Separation-Science Tool
Mariosimone Zoccali 1, Flavio A. Franchina 1, Maria
E. Machado 2, Claudia Zini 2, Elina B. Caramao 2,3,
Peter Q. Tranchida 1, Luigi Mondello 1,4
1U
niversity of Messina, Italy
2 Universidade Federal do Rio Grande do Sul,
Porto Alegre, Brazil
3 INCT E&A, Salvador, Brazil
4 University Campus
Friday, May 23 rd, 9.30 pm, Room 1000
New Vacuum Ultraviolet Detector for
Gas Chromatography
Kevin A. Schug 1, Doug D. Carlton Jr. 1, Ian Sawicki 1,
Harold M. McNair 2, Chao Zheng 3, Phillip Walsh 4,
Dale Harrison 4
1U
niversity of Texas at Arlington, Arlington,
United States
2 Virginia Tech, Blacksburg, United States
3 The Dow Chemical Company, Freeport,
United States
4 VUV Analytics, Inc, Austin, United States

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