HAA je potpisnica multilateralnog sporazuma s Europskom organizacijom za akreditaciju (EA) HAA is a signatory of the European co-operation for Accreditation (EA) Multilateral Agreement. PRILOG POTVRDI O AKREDITACIJI br: 1049 Annex to Accreditation Certificate Number: Klasa/Ref. No.: 383-02/13-30/020 Urbroj/Id. No.: 569-02/6-14-25 Datum izdanja priloga /Annex Issued on: 2014-02-18 Norma: HRN EN ISO/IEC 17025:2007 Standard:(ISO/IEC 17025:2005+Cor.1:2006; EN ISO/IEC 17025:2005+AC:2006) Akreditacija istječe: 2019-02-(2014-02-26) Accreditation expiry: Prva akreditacija: 2004-02-27 Initial accreditation: Akreditirani laboratorij Accredited laboratory EUROINSPEKT CROATIAKONTROLA d.o.o. PC LABORATORIJ Karlovačka cesta 4L, HR-10000 Zagreb Područje akreditacije: Scope of accreditation: Ispitivanje hrane, hrane za životinje, voda, vina, mineralnih gnojiva, tla, eluata otpada, otpada, predmeta opće uporabe i mikrobiološke čistoće objekata Uzorkovanje voda Testing of food, animal feeding stuffs, waters, wine, mineral fertilizers, soil, waste eluates, waste, objects of common use and microbiological cleanliness of facilities Sampling of waters Važeće izdanje Priloga dostupno je na web adresi: www.akreditacija.hr / Valid issue of the Annex is available at the web address: www.akreditacija.hr Ravnateljica: Director General: mr. sc. Biserka Bajzek Brezak, dipl. ing. HAA-Ob-7/7-2/1 /Izdanje 4/Issue 4 stranica/page 1 od/of 23 Prilog potvrdi o akreditaciji Annex to the Accreditation Certificate Datum izdanja priloga/ Annex Issued on 1049 2014-02-18 PODRUČJE AKREDITACIJE / SCOPE OF ACCREDITATION Materijali/Proizvodi Materials/Products Vrsta ispitivanja/Svojstvo Type of test/Property Raspon/Range Metoda ispitivanja Test method 1. Određivanje vode i udjela drugih hlapivih komponenti Determination of moisture and other volatile matter content HRN ISO 6496:2001 (ISO 6496:1999) 2. Određivanje udjela masti Determination of fat content HRN ISO 6492:2001 (ISO 6492:1999) 3. Određivanje pepela Determination of crude ash HRN ISO 5984:2004 (ISO 5984:2002) 4. Određivanje udjela sirovih vlakana Determination of crude fibre content HRN EN ISO 6865:2001 (ISO 6865:2000; EN ISO 6865:2000) (modificirana za FIBER CAP) (modified for FIBER CAP) 5. Određivanje količine dušika i izračunavanje količine sirovih proteina Determination of nitrogen content and calculation of crude protein content HRN ISO 5983-2:2010 (ISO 5983-2:2008) 6. Određivanje udjela škroba Determination of starch content HRN ISO 6493:2001 (ISO 6493:2000) Određivanje broja padanja Determination of falling number HRN EN ISO 3093:2010 (ISO 3093:2009; EN ISO 3093:2009) Hrana za životinje Animal feeding stuffs 7. Žitarice Cereals HAA-Ob-7/7-2/1 / Izdanje 4/Issue 4 stranica/page 2 od/of 23 Prilog potvrdi o akreditaciji Annex to the Accreditation Certificate Datum izdanja priloga/ Annex Issued on Materijali/Proizvodi Materials/Products 8. Žitarice i proizvodi od žitarica Cereals and cereal poducts 9. Žitarice i proizvodi mljevenja žitarica Cereals and milled cereal poducts 10. Žitarice i mahunarke Cereals and pulses 11. Mirodije i začini Spices and condiments 12. Čaj Tea 13. 14. Sirova kava Green coffee 15. Pržena mljevena kava Roasted ground coffee 16. 17. Životinjske i biljne masti i ulja Animal and vegetable fats and oils 18. HAA-Ob-7/7-2/1 / Izdanje 4/Issue 4 Vrsta ispitivanja/Svojstvo Type of test/Property Raspon/Range Određivanje količine vode rutinska referentna metoda Determination of moisture content - routine reference method Određivanje ukupnog pepela Determination of total ash Određivanje količine dušika i izračunavanje količine sirovih proteina – Kjeldahl metoda Determination of the nitrogen content and calculation of the crude protein contentKjeldahl method Određivanje ukupnog pepela Determination of total ash Određivanje gubitka mase pri 103 °C Determination of loss in mass at 103 °C Određivanje ukupnog pepela Determination of total ash Određivanje gubitaka mase pri 105 °C Determination of loss in mass at 105 °C Određivanje gubitka mase pri 103 °C Determination of loss in mass at 103 °C Određivanje količine vode i hlapljivih tvari Determination of moisture and volatile matter content Određivanje kiselinskog broja i kiselosti Determination of acid value and acidity Određivanje peroksidnog broja Determination of peroxide value 1049 2014-02-18 Metoda ispitivanja Test method HRN EN ISO 712:2010 (ISO 712:2009; EN ISO 712:2009) HRN EN ISO 2171:2010 (ISO 2171:2007; EN ISO:2010) HRN EN ISO 20483:2008 (ISO 20483:2006; EN ISO 20483:2006) HRN ISO 928:2001 (ISO 928:1997) HRN ISO 1573:2001 (ISO 1573:1980) HRN ISO 1575:2001 (ISO 1575:1987) HRN ISO 6673:2008 (ISO 6673:2003) HRN ISO 11294:1999 (ISO 11294:1994) HRN EN ISO 662:2004 (ISO 662:1998; EN ISO 662:2000) HRN EN ISO 660:2010 (ISO 660:1996; EN ISO 660:1999) HRN ISO 3960:2010 (ISO 3960:1998) stranica/page 3 od/of 23 Prilog potvrdi o akreditaciji Annex to the Accreditation Certificate Datum izdanja priloga/ Annex Issued on Materijali/Proizvodi Materials/Products 19. Životinjske i biljne masti i ulja Animal and vegetable fats and oils 20. 21. Kukuruz Maize Vrsta ispitivanja/Svojstvo Type of test/Property Raspon/Range Određivanje apsorbancija u ultraljubičastom spektru izraženih kao UV ekstincija Determination of ultraviolet absorbance expressed as specific UV extinction Analiza metilnih estera masnih kiselina plinskom kromatografijom Analysis by gas chromatography of methyl esters of fatty acids Određivanje sadržaja vlage mljevenog zrna Determination of moisture content on milled grains 1049 2014-02-18 Metoda ispitivanja Test method HRN EN ISO 3656:2011 (ISO 3565:2011; EN ISO 3656:2011) HRN EN ISO 5508:1999 (ISO 5508:1990; EN ISO 5508:1995) HRN ISO 6540:2010 (ISO 6540:2010) Pravilnik o šećerima i metodama analiza šećera namijenjenih za konzumaciju (NN 39/09, 144/10), Prilog 2, Metoda 1 Određivanje gubitka mase sušenjem Determination of loss in mass 22. Šećer Sugar 23. HAA-Ob-7/7-2/1 / Izdanje 4/Issue 4 Određivanje polarizacije polarimetrom Determination of polarization - Polarimetric method Ordinance on sugar and methods of analysis of sugar intended for human consumption (Official gazette of the Republic of Croatia No. 39/09, 144/10)), Annex 2, Method 1 Pravilnik o šećerima i metodama analiza šećera namijenjenih za konzumaciju (NN 39/09, 144/10), Prilog 2, Metoda 10 Ordinance on sugar and methods of analysis of sugar intended for human consumption (Official gazette of the Republic of Croatia No. 39/09, 144/10)), Annex 2, Method 10 stranica/page 4 od/of 23 Prilog potvrdi o akreditaciji Annex to the Accreditation Certificate Datum izdanja priloga/ Annex Issued on Materijali/Proizvodi Materials/Products Vrsta ispitivanja/Svojstvo Type of test/Property Raspon/Range Određivanje udjela amonijskog dušika Determination of ammoniacal nitrogen 24. Mineralno gnojivo Mineral fertilizer 1049 2014-02-18 Metoda ispitivanja Test method Pravilnik o mineralnim gnojivima, (NN 60/07), dodatak IV; B 2.1, 75-83 Ordinance on mineral fertilizer (Official gazette of the Republic of Croatia No.60/07), addition IV; B 2.1, 75-83 Uredba (EZ) br. 2003/2003 Europskog Parlamenta i Vijeća od 13. listopada 2003. o gnojivima, Prilog IV., Metoda 2.1., 153-161 Regulation (EC) No 2003/2003 of the European Parlament and of the Council od the 13 October 2003 relating to fertiliser (Official Journal of the European Union L 304, Annex IV, Method 2.1., 78-86 Pravilnik o mineralnim gnojivima (NN 60/07), dodatak IV; B 4.1, 126-129 Ordinance on mineral fertilizer (Official gazette of the Republic of Croatia No.60/07), addition IV; B 4.1, 126-129 25. Određivanje vodotopivog kalija Determination of the water soluble potassium content Uredba (EZ) br. 2003/2003 Europskog Parlamenta i Vijeća od 13. listopada 2003. o gnojivima, Prilog IV., Metoda 4.1., 209-212 Regulation (EC) No 2003/2003 of the European Parlament and of the Council od the 13 October 2003 relating to fertiliser (Official Journal of the European Union L 304, Annex IV, Method 4.1.,134-137 26. HAA-Ob-7/7-2/1 / Izdanje 4/Issue 4 Ekstrakcija vodotopivog fosfora Extraction of water soluble phosphorus Pravilnik o mineralnim gnojivima (NN 60/07), dodatak IV; B 3.1.6, 123-124 Ordinance on mineral fertilizer (Official gazette of the Republic stranica/page 5 od/of 23 Prilog potvrdi o akreditaciji Annex to the Accreditation Certificate Datum izdanja priloga/ Annex Issued on Materijali/Proizvodi Materials/Products Vrsta ispitivanja/Svojstvo Type of test/Property Raspon/Range 1049 2014-02-18 Metoda ispitivanja Test method of Croatia No.60/07), addition IV; B 3.1.6, 123-124 Uredba (EZ) br. 2003/2003 Europskog Parlamenta i Vijeća od 13. listopada 2003. o gnojivima, Prilog IV., Metoda 3.1.6., 205-206 Regulation (EC) No 2003/2003 of the European Parlament and of the Council od the 13 October 2003 relating to fertiliser (Official Journal of the European Union L 304, Annex IV, Method 3.1.6.,130-131 27. Mineralno gnojivo Mineral fertilizer Određivanje ekstrahiranog fosfora gravimetrijska metoda s kinolin fosformolibdatom Determination of extracted phosphorus (Gravimetric Method Using Quinoline Phosphomolybdate) Pravilnik o mineralnim gnojivima (NN 60/07), dodatak IV; B 3.2, 124-126 Ordinance on mineral fertilizer (Official gazette of the Republic of Croatia No.60/07), addition IV; B 3.2, 124-126 Uredba (EZ) br. 2003/2003 Europskog Parlamenta i Vijeća od 13. listopada 2003. o gnojivima, Prilog IV., Metoda 3.2., 206-209 Regulation (EC) No 2003/2003 of the European Parlament and of the Council od the 13 October 2003 relating to fertiliser (Official Journal of the European Union L 304, Annex IV, Method 4.1.,131-134 Pravilnik o mineralnim gnojivima (NN 60/07) dodatak IV; B 3.1.3., 117-118 28. HAA-Ob-7/7-2/1 / Izdanje 4/Issue 4 Ekstrakcija fosfora topivog u 2% limunskoj kiselini (20g/l) Extraction of phosphorus soluble in 2 % citric acid (20 g per litre) Ordinance on mineral fertilizer (Official gazette of the Republic of Croatia No.60/07), addition IV; B 3.1.3., 117-118 Uredba (EZ) br. 2003/2003 Europskog Parlamenta i Vijeća od 13. listopada 2003. o gnojivima, Prilog IV., stranica/page 6 od/of 23 Prilog potvrdi o akreditaciji Annex to the Accreditation Certificate Datum izdanja priloga/ Annex Issued on Materijali/Proizvodi Materials/Products Vrsta ispitivanja/Svojstvo Type of test/Property Raspon/Range 1049 2014-02-18 Metoda ispitivanja Test method Metoda 3.1.3., 198-199 Regulation (EC) No 2003/2003 of the European Parlament and of the Council od the 13 October 2003 relating to fertiliser (Official Journal of the European Union L 304, Annex IV, Method 3.1.3.,123-124 Mineralno gnojivo Mineral fertilizer 29. Uljarice Oilseeds 30. Horizontalna metoda za dokazivanje prisutnosti Salmonella spp Horizontal method for the detection of Salmonella spp 31. 32. Određivanje količine vode i hlapljivih tvari Determination of moisture and volatile matter content Određivanje količine ulja (Referentna metoda) Determination of oil content (Reference method) Hrana i hrana za životinje Food and animal feeding stuffs 33. 34. HAA-Ob-7/7-2/1 / Izdanje 4/Issue 4 Horizontalna metoda za brojenje mikroorganizama Tehnika brojenje kolonija na 30 °C Horizontal method for the enumeration of microorganismsColony count technique at 30 °C Horizontalna metoda za dokazivanje prisutnosti i brojenje Enterobacteriaceae – 2 dio: Metoda određivanja broja kolonija Horizontal methods for the detection and enumeration of Enterobacteriaceae – Part 2: Colony count method Brojenje kvasaca i plijesni Enumeration of yeasts and moulds HRN EN ISO 665:2004 (ISO 665:2000; EN ISO 665:2000) HRN EN ISO 659:2010 (ISO 659:2009; EN ISO 659:2009) HRN EN ISO 6579: 2003 (ISO 6579:2002; EN ISO 6579:2002) HRN EN ISO 6579:2003/Ispr1:2008 (ISO 6579:2002/Cor 1:2004; EN ISO 6579:2002/AC:2006) HRN EN ISO 4833:2008 (ISO 4833:2003; EN ISO 4833:2003) HRN ISO 21528-2:2008 (ISO 21528-2:2004) ISO 21527-1:2008 ISO 21527-2:2008 stranica/page 7 od/of 23 Prilog potvrdi o akreditaciji Annex to the Accreditation Certificate Datum izdanja priloga/ Annex Issued on Materijali/Proizvodi Materials/Products Vrsta ispitivanja/Svojstvo Type of test/Property Raspon/Range 35. Horizontalna metoda za dokazivanje prisutnosti i određivanje broja stanica Listeria monocytogenes – Metoda dokazivanja Horizontal method for the detection and enumeration of Listeria monocytogenes Detection method 36. Horizontalna metoda za dokazivanje prisutnosti i određivanje broje Listeria monocytogenes - Metoda brojenja Horizontal method for the detection and enumeration of Listeria monocytogenes – Enumeration method Hrana i hrana za životinje Food and animal feeding stuffs 1049 2014-02-18 Metoda ispitivanja Test method HRN EN ISO 11290-1:1999 (ISO 11290-1:1996; EN ISO 11290-1:1996) HRN EN ISO 112901:1999/A1:2008 (ISO 11290-1:1996/Amd 1:2004; EN ISO 112901:1996/A1:2004) HRN EN ISO 11290-2:1999 (ISO 11290-2:1998; EN ISO 11290-2:1998) HRN EN ISO 112902:1999/A1:2008 (ISO 11290-2:1998/Amd 1:2004; EN ISO 112902:1998/A1:2004) Horizontalna metoda brojenja beta –glucoronidasa pozitivne Escherichia coli- 1.dio: Brojenje kolonija pri 44 °C uporabom membrane i 5bromo-4-chloro-3-indolyl beta-D-glucuronida 37. HAA-Ob-7/7-2/1 / Izdanje 4/Issue 4 Horizontal method for the enumeration of betaglucoronidase- positive Escherichia coli-Part 1: Colony count at44 °C using membranes and 5-bromo-4chloro-3-indolyl beta-Dglucoronide HRN ISO 16649-1:2001 (ISO 16649-1:2001) stranica/page 8 od/of 23 Prilog potvrdi o akreditaciji Annex to the Accreditation Certificate Datum izdanja priloga/ Annex Issued on Materijali/Proizvodi Materials/Products 38. 39. Hrana i hrana za životinje Food and animal feeding stuffs 40. 41. HAA-Ob-7/7-2/1 / Izdanje 4/Issue 4 Vrsta ispitivanja/Svojstvo Type of test/Property Raspon/Range Horizontalna metoda brojenja beta – glucoronidasa pozitivne Escherichia coli 2.dio: Brojenje kolonija pri 44 °C uporabom 5-bromo-4chloro-3-indolyl beta-Dglucuronide Horizontal method for the enumeration of betaglucoronidasepositiveEscherichiacoli - Part 2: Colony count at44 °Cusing 5-bromo-4-chloro-3-indolyl beta-D-glucuronide Horizontalna metoda za brojenje Bacillus cereusa – tehnika brojenja kolonija pri 30°C Horizontal method for enumeration of presumptive Bacillus cereus – Colonycount tehnique at 30°C Vodoravni postupak brojenja koagulaza-pozitivnih stafilokoka (Staphylococcus aureus i druge vrste)– 1. dio: Postupak primjene BairdParkerove hranjive podloge na agaru Horizontal method for the enumeration of coagulase – positive staphylococco (Staphylococcus aureus and other species) – Part.1: tehnique using Baird –Parker agar medium Horizontalna metoda za brojenje sulfitreducirajućih bakterija u anaerobnim uvjetima Horizontal method for the enumeration of sulfitereducing bacteria growing under anaerobic condition 1049 2014-02-18 Metoda ispitivanja Test method HRN ISO 16649-2:2001 (ISO 16649-2:2001) HRN EN ISO 7932:2005 (ISO 7932:2004; EN ISO 7932:2004) HRN EN ISO 6888-1:2004 (ISO 6888-1:1999+Amd 1:2003; EN ISO 68881:1999+A1:2003) HRN ISO 15213:2004 (ISO 15213:2003) stranica/page 9 od/of 23 Prilog potvrdi o akreditaciji Annex to the Accreditation Certificate Datum izdanja priloga/ Annex Issued on 1049 2014-02-18 Vrsta ispitivanja/Svojstvo Type of test/Property Raspon/Range Metoda ispitivanja Test method 42. Određivanje ukupnog arsena (As) - GF-AAS tehnika Determinationof total arsenic (As) - GF-AAS technique Vlastita metoda/ In House method RU-MET-62 Izdanje/Edition 3/2013 43. Određivanje kadmija (Cd) - GF-AAS tehnika Determinationof cadmium (Cd) - GF-AAS technique Vlastita metoda/ In House method RU-MET-63 Izdanje/Edition 3/2013 44. Određivanje olova (Pb) - GF-AAS tehnika Determinationof leadin (Pb) - GF-AAS technique Vlastita metoda/ In House method RU-MET-64 Izdanje/Edition 3/2013 45. Određivanje deoksinivalenola (ELISA tehnika) Determination of deoxynnivalenol (ELISA technique) Vlastita metoda/ In House method RU-MET-60 Izdanje/Edition 3/2013 46. Određivanje fumonizina (ELISA tehnika) Determination of fumonisine (ELISA technique) Vlastita metoda/ In House method RU-MET-61 Izdanje/Edition 3/2013 47. Određivanje ukupnih aflatoksina (B1+B2+G1+G2) i aflatoksina B1 (LC-MS/MS) Determination of total aflatoxins (B1+B2+G1+G2) i and aflatoxin B1 (LC-MS/MS) Vlastita metoda In House method RU-MET-84 Izdanje/Edition 3/2013 Materijali/Proizvodi Materials/Products Hrana i hrana za životinje Food and animal feeding stuffs HAA-Ob-7/7-2/1 / Izdanje 4/Issue 4 stranica/page 10 od/of 23 Prilog potvrdi o akreditaciji Annex to the Accreditation Certificate Datum izdanja priloga/ Annex Issued on Materijali/Proizvodi Materials/Products 48. Žitarice i hrana za životinje Cereals and animal feeding stuffs 49. 50. Voda za ljudsku potrošnju, prirodne izvorske, prirodne mineralne, stolne vode Water for human consumption, natural spring water, natural mineral water, table water 51. HAA-Ob-7/7-2/1 / Izdanje 4/Issue 4 Vrsta ispitivanja/Svojstvo Type of test/Property Raspon/Range Određivanje ostataka pesticida (α-endosulfan, βendosulfan, heptaklor, heptaklor epoksid aldrin, dieldrin, lindan, αHCH, β-HCH, 2,4-DDT, 4,4DDT)-(GC ECD) Determination of pesticide residues(α-endosulfan, βendosulfan, heptachlor, heptachlor epoxide, aldrin, dieldrin, lindane, α-HCH, βHCH, 2,4-DDT, 4,4-DDT) – (GC ECD) Brojenje uzgojenih mikroorganizama- Broj kolonija nacjepljivanjem na hranjivi agar Enumeration of culturable micro-organisms - Colony count by inoculation in a nutrient agar culture medium Detekcija i brojenje crijevnih enterokoka- 2.dio: Metoda membranske filtracije Detection and enumeration of intestinal enterococci - Part 2: Membrane filtration method Detekcija i brojenje Escherichia coli i koliformnih bakterija -1. dio: metoda membranske filtracije Detection and enumeration of Escherichia coli and coliform bacteria - Part 1: Membrane filtration method 1049 2014-02-18 Metoda ispitivanja Test method Vlastita metoda/ In House method RU-MET-50 Izdanje/Edition 4/2013 HRN EN ISO 6222:2000 (ISO 6222:1999; EN ISO 6222:1999) HRN EN ISO 7899-2:2000 (ISO 7899-1:1998; EN ISO 7899-1:1998) HRN EN ISO 9308-1:2000 (ISO 9308-1:2000; EN ISO 9308-1:2000) HRN EN ISO 93081:2000/Ispr. 1:2008 (ISO 9308-1:2000/Cor. 1:2007; EN ISO 93081:2000/AC:2008) stranica/page 11 od/of 23 Prilog potvrdi o akreditaciji Annex to the Accreditation Certificate Datum izdanja priloga/ Annex Issued on Materijali/Proizvodi Materials/Products 52. 53. 54. Voda za ljudsku potrošnju, prirodne izvorske, prirodne mineralne, stolne vode, površinska, otpadna voda, podzemna voda, eluat otpada Water for human consumption, natural spring water, natural mineral water, table water, surface water, waste water, ground water, waste eluate 55. 56. 57. 58. Voda za ljudsku potrošnju, prirodne izvorske, prirodne mineralne, stolne vode, otpadne, površinske i podzemne vode, eluat otpada Water for human consumption, natural spring water, natural mineral water, table water, waste water, surface water and ground water, waste eluat Voda za ljudsku potrošnju, prirodne izvorske, prirodne mineralne, stolne vode, otpadna, površinska i podzemna voda Water for human consumption, natural spring water, natural mineral water, table water, waste water, surface water and ground water HAA-Ob-7/7-2/1 / Izdanje 4/Issue 4 Vrsta ispitivanja/Svojstvo Type of test/Property Raspon/Range Uzorkovanje za određivanje odabranih fizikalno-kemijskih i mikrobioloških pokazatelja Sampling for determination of selected physical-chemical and microbiological parameters 1049 2014-02-18 Metoda ispitivanja Test method HRN ISO 5667-5:2011 (ISO 5667-5:2006) HRN EN ISO 19458:2008 (ISO 19458:2006; EN ISO 19458:2006) Određivanje mutnoće Determination of turbidity HRN EN ISO 7027:2001 (ISO 7027:1999; EN ISO 7027:1999) Određivanje električne vodljivosti Determination of electrical conductivity HRN EN 27888:2008 (ISO 7888:1985; EN 27888:1993) Određivanje pH vrijednosti Determination of pH HRN EN ISO 10523:2012 (ISO 10523:2008; EN ISO 10523:2012) Određivanje klorida volumetrijskom metodom sa srebrnim nitratom uz kromatni indikator (Mohrova metoda) Determination of chloride by silver nitrate titration with chromate indicator (Mohr's method) HRN ISO 9297:1998 (ISO 9297:1989) Određivanje amonija spektrometrijskom metodom Determination of ammonium using manual spectrometric method HRN ISO 7150-1:1998 (ISO 7150-1:1984) Određivanje nitrita – Molekularna apsorpcijska spektrometrijska metoda Determination of nitite – Molecular absorption spectrometric method HRN EN 26777:1998 (ISO 6777:1984; EN 26777:1993) stranica/page 12 od/of 23 Prilog potvrdi o akreditaciji Annex to the Accreditation Certificate Datum izdanja priloga/ Annex Issued on Materijali/Proizvodi Materials/Products 59. 60. Otpadne, površinske i podzemne vode Waste water, surface water and ground water 61. 62. Otpadne, površinske i podzemne vode Waste water, surface water and ground water 63. 64. Vrsta ispitivanja/Svojstvo Type of test/Property Raspon/Range Određivanje suspendiranih tvari filtriranjem kroz filtar od staklenih vlakana Determination of suspended solids by filtration through glass fibre filters Određivanje nitrata – Spektrometrijska metoda s sulfosalicilnom kiselinom Determination of nitrate – Spectrometric method using Sulfosalicylic acid Određivanje fosfora spektrometrijskom metodom s amonijevim molibdatom Determination of phosphorus using ammonium molybdate spectrometric method Određivanje biokemijske potrošnje kisika nakon n dana (BPKn) metodom razrjeđivanja i nacjepljivanja uz dodatak aliltiouree Determination of biochemical oxygen demand after n days (BODn)using dilution and seeding method with allylthiourea addition Određivanje BPK5 nerazrijeđeni uzorci Determination BOD5, undiluted samples Određivanje otopljenog kisika – elektrokemijska metoda Determination of dissolved oxygen – electrochemical method 65. Otpadne, površinske i podzemne vode, eluat otpada Waste water, surface water, ground water, waste eluate HAA-Ob-7/7-2/1 / Izdanje 4/Issue 4 Određivanje kemijske potrošnje kisika Determination of the chemical oxygen demand 1049 2014-02-18 Metoda ispitivanja Test method HRN EN 872:2008 (EN 872:2005) HRN ISO 7890-3:1998 (ISO 7890-3:1988) HRN EN ISO 6878:2008 (ISO 6878:2004; EN ISO 6878:2004) HRN EN 1899-1:2004 (ISO 5815:1989, modified; EN 1899-1:1998) HRN EN 1899-2:2004 (ISO 5815:1989, modified; EN 1899-2:1998) Vlastita metoda In House method RU-OTV-24; Izdanje/Edition 3/2013 HRN ISO 6060:2003 (ISO 6060:1989) stranica/page 13 od/of 23 Prilog potvrdi o akreditaciji Annex to the Accreditation Certificate Datum izdanja priloga/ Annex Issued on Materijali/Proizvodi Materials/Products 66. Otpadna voda Waste water 67. Riba i proizvodi od ribe Fish and fish products 68. 69. 70. Med Honey Vrsta ispitivanja/Svojstvo Type of test/Property Raspon/Range Uzorkovanje Sampling Vlastita metoda In House method RU-MET-108 Izdanje/Edition 3/2013 Određivanje aktivnosti dijastaze (Phadebas) Determination of diastase activity (Phadebas) Određivanje električne vodljivosti Determination of electrical conductivity Vlastita metoda/ In House method RU-MET-57 Izdanje/Edition 2/2013 Vlastita metoda/ In House method RU-MET-58 Izdanje/Edition 2/2013 Vlastita metoda/ In House method RU-MET-59 Izdanje/Edition 2/2013 72. 73. Određivanje olova (Pb) Determination of lead (Pb) 75. HAA-Ob-7/7-2/1 / Izdanje 4/Issue 4 HRN ISO 5667-10:2000 (ISO 5667-10:1992) Određivanje histamina (HPLC) Determination of histamine (HPLC) Određivanje hidroksimetilfurfurala (HMF) tehnikom HPLC Determination of hydroxymethylfurfural (HMF) by HLPC Okolišni uzorci u proizvodnji hrane Enviormental samples in food production Metoda ispitivanja Test method Vlastita metoda/ In House method RU-MET-72 Izdanje/Edition 2/2013 Određivanje kiselosti meda Determination of free acidity 74. 2014-02-18 Određivanje histamina (ELISA tehnika) Determination of histamine (ELISA technique) 71. Vino i alkoholna pića Wine and alcoholic drinks 1049 Odredivanje kadmija (Cd) Determination of cadmium (Cd) Horizontalna metoda za postupke uzorkovanja s površina upotrebom otiska Horizontal method for sampling techniques from surfaces using swabs Vlastita metoda/ In House method RU-MET-56 Izdanje / Edition 3/2013 Vlastita metoda In House method RU-MET-99 Izdanje/Edition 2/2013 Vlastita metoda In House method RU-MET-141, Izdanje/edition 3/2013 HRN ISO 18593:2008 (ISO 18593:2004) stranica/page 14 od/of 23 Prilog potvrdi o akreditaciji Annex to the Accreditation Certificate Datum izdanja priloga/ Annex Issued on Materijali/Proizvodi Materials/Products 76. 77. 78. Kozmetika i površinski aktivne tvari Cosmetics and surface active agents Stakleno posuđe Glass hollowware Određivanje pH Determination of pH Brojenje i dokazivanje aerobnih mezofilnih bakterija Enumeration and detection of aerobic mesophilic bacteria Određivanje migracije kadmija (Cd) i olova (Pb) Glass hollowware in contact with food - Release of cadmium (Cd) and lead (Pb) Određivanje sadržaja vode Determination of moisture content 79. 80. 81. Meso i mesni proizvodi Meat and meat products 82. Mjerenje pH Measurement of pH Određivanje količine hidroksiprolina i izračun količine kolagena Determination of quantity of hydroxiprolyne an calculation of quantity of collagen Određivanje količine dušika i izračun sirovih proteina Determination of nitrogen content and calculation of raw proteins Određivanje ukupne količine masti Determination of total fat content 83. 84. Vrsta ispitivanja/Svojstvo Type of test/Property Raspon/Range Hrana i hrana za životinje Food and animal feeding stuffs HAA-Ob-7/7-2/1 / Izdanje 4/Issue 4 Opće upute za brojenje koliformnih bakterijaPostupak određivanja broja kolonija Horizontal method for the enumeration of coliforms – Colony count technique 1049 2014-02-18 Metoda ispitivanja Test method Vlastita metoda In House method RU-MET-87 Izdanje/Edition 2/2013 HRN EN ISO 21149:2010 (ISO 21149:2006, EN ISO 21149:2009) HRN ISO 7086-1:2000 (ISO 7086-1:2000) Vlastita metoda/ In House method RU-MET-76 Izdanje/Edition 3/2013 AOAC 950.46, 16 izdanje/edition HRN ISO 2917:2000 (ISO 2917:1999) Vlastita metoda/ In House method RU-MET-75 Izdanje/Edition 3/2013 AOAC 990.26, 16 izdanje/edition HRN ISO 937:1999 (ISO 937:1978) HRN ISO 1443:1999 (ISO 1443:1973) HRN ISO 4832:2008 (ISO 4832:2008) stranica/page 15 od/of 23 Prilog potvrdi o akreditaciji Annex to the Accreditation Certificate Datum izdanja priloga/ Annex Issued on Vrsta ispitivanja/Svojstvo Type of test/Property Raspon/Range Određivanja sladila (acesulfama K, aspartama i saharina), konzervansa (benzoata i sorbata) i kofeina Bezalkoholna 85. osvježavajuća pića Determination of artificial Soft drinks sweeteners (acesulfame K, aspartame and saccharin), preservatives (benzoate and sorbate) and caffeine Određivanje sadržaja Mlijeko i mlijeko u prahu aflatoksina M1(HPLC) 86. Milk and milk powder Determination of aflatoxin M1 content (HPLC) Materijali/Proizvodi Materials/Products 87. Sol Salt 88. Voda za ljudsku potrošnju Water for human consumption 89. Voda za ljudsku potrošnju, prirodne izvorske, prirodne mineralne, stolne vode Water for human consumption, natural spring water, natural mineral water, table water Materijali i predmeti koji dolaze u kontakt s hranom - Keramika 90. Materials and articles in contact with foodstuffs – Ceramics HAA-Ob-7/7-2/1 / Izdanje 4/Issue 4 Određivanje kalijheksacijanoferata Determination of Potassium Hexacyanoferrate Detekcija i brojenje Legionella 2. dio: Izravna metoda membranske filtracije za vode s malim brojem bakterija Detection and enumeration of Legionella – Part 2: Direct membrane filtration method for waters with low bacterial counts Detekcija i brojenje Pseudomonas aeruginosa Metoda membranske filtracije Detection and numeration of Pseudomonas aeruginosa Membrane filtration method Keramičko posuđe u dodiru s hranom - Otpuštanje olova (Pb) i kadmija (Cd) Ceramic ware in contact with food – Release of lead and cadmium – Part 1: Method of test 1049 2014-02-18 Metoda ispitivanja Test method HRN EN 12856:2000 (EN 12856:1999) HRN EN ISO 14501:2008 (ISO 14501:2007; EN ISO 14501:2007) Vlastita metoda In House method RU-MET-111 Izdanje/edition 2/2013 (EuSalt/AS 004-2008) HRN ISO 11731-2:2008 (ISO 11731-2:2004; EN ISO 11731-2:2008) HRN EN ISO 16266:2008 (ISO 16266:2006; EN ISO 16266:2008) HRN ISO 6486-1:1999 (ISO 6486-1:1981) stranica/page 16 od/of 23 Prilog potvrdi o akreditaciji Annex to the Accreditation Certificate Datum izdanja priloga/ Annex Issued on Materijali/Proizvodi Materials/Products Određivanje sulfata – turbidimetrijska metoda Determination of Sulfate – Turbidimetric Method 91. 92. Vrsta ispitivanja/Svojstvo Type of test/Property Raspon/Range Otpadna, površinska, podzemna voda i eluat otpada Waste water, surface water, ground water and waste eluate 93. 94. 95. Otpadna, površinska, podzemna voda, eluat otpada i tlo Waste water, surface water, ground water, waste eluate and soil 96. Otpad Waste 97. Otpadna, površinska, podzemna voda Waste water, surface water, ground water HAA-Ob-7/7-2/1 / Izdanje 4/Issue 4 1049 2014-02-18 Metoda ispitivanja Test method Standard methods 21th Ed. 2005:4500-SO42- E Standard methods 21th Ed. 2005:4500- SO42- E Određivanje ukupno rastopljenih krutina u vodi i eluatima Determination of total dissolved solids (TDS) in water and eluates HRN EN 15216:2008 (EN 15216:2007) Određivanje fluorida Determination of fluoride RU-OTV-045 izdanje/Edition 01/2013 (Kivetni test/ Cuvette test HACH LANGE, LCK 323) Određivanje električne vodljivosti Determination of electrical conductivity Određivanje kroma (VI) Spektrometrijska metoda s 1,5-difenilkarbazidom Determination of chromium (VI) -- Spectrometric method using 1,5 - diphenylcarbazide Izračunavanje suhe tvari određivanjem suhog ostatka ili sadržaja vode Calculation of dry matter by determination of dry residue or water content Određivanje anionskih tenzida mjerenjem indeksa metilenskog modrila (MMAT) Determination of anionic surfactants by measurement of the methylene blue index MBAS HRN EN 27888:2008 (ISO 7888:1985; EN 27888:1993) HRN ISO 11083:1998 (ISO 11083:1994) HRN EN 14346:2007 (EN 14346:2006) Metoda/Method A HRN EN 903:2002 (EN 903:1993) stranica/page 17 od/of 23 Prilog potvrdi o akreditaciji Annex to the Accreditation Certificate Datum izdanja priloga/ Annex Issued on Materijali/Proizvodi Materials/Products 98. 99. 100. Otpadna, površinska, podzemna voda Waste water, surface water, ground water 101. 102. 103. HAA-Ob-7/7-2/1 / Izdanje 4/Issue 4 Vrsta ispitivanja/Svojstvo Type of test/Property Raspon/Range Određivanje alkaliteta – 1.dio: Određivanje ukupnog i pojedinačnog alkaliteta Determination of alkalinity -Part 1: Determination of total and composite alkalinity Određivanje sume kalcija i magnezija (ukupna tvrdoća) Volumetrijska metoda s EDTA Determination of the sum of calcium and magnesium -EDTA titrimetric method Određivanje sadržaja kalcija EDTA titrimetrijska metoda Determination of calcium content -- EDTA titrimetric method Određivanje volumnog dijela istaložene tvari u vodi i otpadnoj vodi Determination of the settleable matter by volume in water and waste water Određivanje natrija i kalija 3. dio: Određivanje natrija i kalija metodom plamene emisijske spektrometrije Određivanje natrija i kalija -3. dio: Određivanje natrija i kalija metodom plamene emisijske spektrometrije Ispitivanje i određivanje boje Examination and determination of colour 1049 2014-02-18 Metoda ispitivanja Test method HRN EN ISO 9963-1:1998 (ISO 9963-1:1994; EN ISO 9963-1:1995) HRN ISO 6059:1998 (ISO 6059:1984) HRN ISO 6058:2001 (ISO 6058:1984) DIN 38 409:1980 dio/part 9 HRN ISO 9964-3:1998 (ISO 9964-3:1993) HRN EN ISO 7887:2012 Dio/Part 2 (ISO 7887:2011; EN ISO 7887:2011) stranica/page 18 od/of 23 Prilog potvrdi o akreditaciji Annex to the Accreditation Certificate Datum izdanja priloga/ Annex Issued on Materijali/Proizvodi Materials/Products Voda za ljudsku potrošnju, prirodne izvorske, prirodne mineralne, stolne vode, otpadna, površinska i podzemna voda 104. Water for human consumption, natural spring water, natural mineral water, table water, waste water, surface water and ground water 105. Podzemna voda Ground water 106. Voda za ljudsku potrošnju, prirodne izvorske, prirodne mineralne, stolne vode Water for human consumption, natural spring water, natural mineral water, table water 108. Tlo Soil 109. HAA-Ob-7/7-2/1 / Izdanje 4/Issue 4 2014-02-18 Vrsta ispitivanja/Svojstvo Type of test/Property Raspon/Range Metoda ispitivanja Test method Određivanje permanganatnog indeksa Determination of permanganate index HRN EN ISO 8467:2001 (ISO 8467:1993; EN ISO 8467:1995) Uzorkovanje Sampling Ispitivanje i određivanje boje Examination and determination of colour Određivanje pH-vrijednosti Determination of pH 107. 1049 Određivanje specifične električne vodljivosti Determination of the specific electrical conductivity Određivanje suhe tvari i sadržaja vode na osnovi mase – Gravimetrijska metoda Determination of dry matter and water content on a mass basis -- Gravimetric method HRN ISO 5667-11:2011 (ISO 5667-11:2009) HRN EN ISO 7887:2012 Dio/Part 4 (ISO 7887:2011; EN ISO 7887:2011) HRN ISO 10390:2005 (ISO 10390:2005) HRN ISO 11265:2004 (ISO 11265:1994+Cor 1:1996) HRN ISO 11465:2004 (ISO 11465:1993+Cor 1:1994) stranica/page 19 od/of 23 Prilog potvrdi o akreditaciji Annex to the Accreditation Certificate Datum izdanja priloga/ Annex Issued on Materijali/Proizvodi Materials/Products 110. Tlo i otpad Soil and waste 111. HAA-Ob-7/7-2/1 / Izdanje 4/Issue 4 Vrsta ispitivanja/Svojstvo Type of test/Property Raspon/Range Karakterizacija otpada – Izluživanje – Provjera izluživanja zrnatoga otpadnog materijala i muljeva – 1. dio: Jednostupanjski postupak kod omjera tekuće-čvrsto od 2 l/kg za materijale s visokim sadržajem krutina i veličinom čestica manjom od 4 mm (sa smanjenjem veličine čestica ili bez smanjenja) Characterization of waste Leaching -- Compliance test for leaching of granular waste materials and sludges -- Part 1: One stage batch test at a liquid to solid ratio of 2 l/kg for materials with high solid content and with particle size below 4 mm (without or with size reduction) Karakterizacija otpada – Izluživanje – Provjera izluživanja zrnatoga otpadnog materijala i muljeva – 2. dio: Jednostupanjski postupak kod omjera tekuće-čvrsto od 10 l/kg za materijale s visokim sadržajem krutina i veličinom čestica manjom od 4 mm (sa smanjenjem veličine čestica ili bez smanjenja Characterization of waste -Leaching -- Compliance test for leaching of granular waste materials and sludges -- Part 2: One stage batch test at a liquid to solid ratio of 10 l/kg for materials with particle size below 4 mm (without or with size reduction) 1049 2014-02-18 Metoda ispitivanja Test method HRN EN 12457-1:2005 (EN 12457-1:2002) HRN EN 12457-2:2005 (EN 12457-2:2002) stranica/page 20 od/of 23 Prilog potvrdi o akreditaciji Annex to the Accreditation Certificate Datum izdanja priloga/ Annex Issued on Materijali/Proizvodi Materials/Products 112. Tlo i otpad Soil and waste 113. Voda za ljudsku potrošnju, prirodne izvorske, prirodne mineralne, stolne vode, otpadna, površinska, podzemna voda i eluat otpada 114. Water for human consumption, natural spring water, natural mineral water, table water, waste water, surface water, ground water and waste eluate HAA-Ob-7/7-2/1 / Izdanje 4/Issue 4 1049 2014-02-18 Vrsta ispitivanja/Svojstvo Type of test/Property Raspon/Range Karakterizacija otpada – Izluživanje – Provjera izluživanja zrnatoga otpadnog materijala i muljeva – 4. dio: Jednostupanjski postupak kod omjera tekuće-čvrsto od 10 l/kg za materijale s veličinom čestica manjom od 10 mm (sa smanjenjem veličine čestica ili bez smanjenja) Characterization of waste -Leaching -- Compliance test for leaching of granular waste materials and sludges -- Part 4: One stage batch test at a liquid to solid ratio of 10 l/kg for materials with particle size below 10 mm (without or with size reduction) Određivanje suhog ostatka i sadržaja vode Determination of dry residue and water content HRN EN 12457-4:2005 (EN 12457-4:2002) Određivanje elemenata u tragovima GF-AAS tehnikom - (ukupni arsen (As), ukupni krom (Cr), olovo (Pb) i kadmij (Cd)) Determination of trace elements using atomic absorption spectrometry with graphite furnace - total arsenic (As), total chrome (Cr), lead (Pb), cadmium (Cd) HRN EN ISO 15586:2008 (ISO 15586:2003; EN ISO 15586:2003) Metoda ispitivanja Test method HRN EN 12880:2005 (EN 12880:2000) stranica/page 21 od/of 23 Prilog potvrdi o akreditaciji Annex to the Accreditation Certificate Datum izdanja priloga/ Annex Issued on Materijali/Proizvodi Materials/Products 115. Površinska i otpadna voda, tlo Surface water, waste water, soil HAA-Ob-7/7-2/1 / Izdanje 4/Issue 4 Vrsta ispitivanja/Svojstvo Type of test/Property Raspon/Range Određivanje lipofilnih tvari i ugljikovodika metodom infracrvene spektroskopije Determination of lipophilic substances and hydrocarbons, using infrared spectroscopy method 1049 2014-02-18 Metoda ispitivanja Test method Vlastita metoda/ In House method MET-OTV-054 Izdanje/Edition 1/2013 stranica/page 22 od/of 23 Prilog potvrdi o akreditaciji Annex to the Accreditation Certificate Datum izdanja priloga/ Annex Issued on 1049 2014-02-18 FLEKSIBILNO PODRUČJE AKREDITACIJE/FLEXIBLE SCOPE OF ACCREDITATION Oznaka/ Identification A Materijali/Proizvodi Materials/Products Hrana biljnog porijekla Foods of plant origin Vrsta ispitivanja/Svojstvo Type of test/Property Raspon/Range Određivanje ostataka pesticida Determination of pesticide residues Tehnika ispitivanja Test technique Metoda ispitivanja Test method LC-MS/MS GC-MS/MS HRN EN 15662:2008 (EN 15662:2008) LC-MS/MS - tekućinske kromatografije i višestruke spektrometrije masa/ LC-MS/MS - coupled method liquid chromatography tandem massSpectrometry GC-MS/MS - plinske kromatografije i višestruke spektrometrije masa/ GC-MS/MS - coupled method gas chromatography tandem massSpectrometry Fleksibilnim područjem akreditacije dopušta se laboratoriju primjena metoda ispitivanja na materijale/proizvode, vrstu ispitivanja/svojstvo i raspone unutar područja, u skladu s dokumentiranim i odobrenim postupcima laboratorija. / Flexible scope allows laboratory application test of methods for materials/products, type of test/property and ranges within the scope, in accordance with the laboratory’s documented and approved procedures. Važeći popis akreditiranih metoda iz fleksibilnog područja akreditacije dostupan je na / The valid list of accredited methods in the flexible scope is available on www.croatiakontrola.hr HAA-Ob-7/7-2/1 /Izdanje 4/Issue 4 stranica/page 23 od/of 23
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