A New Method of Controlling Water in SelfCompacting Concrete Production Hai-Thong Ngo 1, Abdelhak Kaci 1, El-Hadj Kadri 1, Tien-Tung Ngo 1, Alain Trudel 2 , Sylvie Lecrux 2 1 Laboratory of Mechanics and Materials of Civil Engineering, University of CergyPontoise, France 2 Centre Technique National, Cemex France, France Abstract: Online water control is one of the most important processes to improve self-compacting-concrete (SCC) production regularity. This control is generally implemented during the mixing process based on the stabilisation of mixing power measurement. However, as for concrete with admixtures, typical SCC mixture takes a certain amount of time to recognise the stabilisation of mixing power which is sometimes difficult to achieve due to the effects of admixtures on concrete workability. In addition, for very fluid concrete like SCC, when the concrete water content is high, the variation of the power measurement becomes very small; thus, the water measurement precision becomes insufficient. In order to improve the control process based on the mixing power measurement and optimise the mixing time, this research proposes a criterion to determine the stabilisation of power curves by using power fluctuation over time. The stabilisation time estimated by this criterion is tested for measuring the concrete water content through an experimental program consisting of 14 SCC truck mixer productions of different compositions produced at an industrial batching plant. The results show that the new processing method allows obtaining a ±3.6 L/m3 precision of water content measurement. Besides, the reduction in mixing time can be made by considering the stabilisation time of power curves as an appropriate mixing time for each concrete batch production. Keywords: Mixing power; Stabilisation time, Concrete plant, Water control, Selfcompacting concrete production 265 K.H. Khayat, SCC 2016 - 8th International RILEM Symposium on Self-Compacting Concrete, ISBN: 978-2-35158-156-8 © RILEM 2016 266 Hai-Thong Ngo, Abdelhak Kaci, El-Hadj Kadri et al. Introduction With the growing popularity of self-compacting concrete (SCC), the requirement for adequate quality control in ready-mixed concrete plants has increased considerably. Compared with conventional concretes, SCC mixtures contain a greater dosage of admixture and a higher powder content which makes the concrete more difficult to mix and more sensitive to all kinds of disturbance. Field experience also shows that the industrial production of these new mix designs does not tolerate any approximation due to the sensitivity of SCC to compositional deviations, especially the variation of water dosage. The control of the water content is consequently crucial in SCC production. In the ready-mixed concrete plants, the application of online water measurements in quality control has become more and more common for an improvement of SCC production regularity [1-3]. These measurements assist the operator in the regulation of the batch composition by adjusting the water content for forthcoming batches of a same truck based on the information collected from the current batch [4]. The most current measurement method used to make water correction is based on the stabilisation of mixing power measurement. Some of the researches regarding the correlation between the concrete water content and the stabilisation power level have been found in the literature [4, 5]. Nevertheless, for very fluid concrete like SCC, an increase in water content of the mix does not affect the power level significantly. This leads to an insufficient accuracy of water measurement. Moreover, it takes several seconds to notice that the signal no longer changes. This waiting period results in a loss of time and thus productivity. Concrete mixtures influence the mixing time needed for complete dispersion of all the concrete components. As shown in [6], mixtures with higher viscosity tend to require longer mixing time and vice versa. In practice, batches of a given concrete design contain different water contents. Therefore, by monitoring their mixing power stabilisation, we realise that the mixing time varies from one batch to another. Considering these observations, the present study focuses on the use of the stabilisation time, which is probably linked with the deviation of water content in the batch, for improving the process of online water control. In order to evaluate the performance of this method in water content measurement, an experimental test campaign is performed in a full-scale concrete plant. Experimental Program The experimental campaign is conducted in a mixing plant equipped with a 2 m³ concrete pan-mixer. The power consumption vs. time evolution is recorded every 0.5 s. The power consumption is measured in percentage of the nominal mixing power of the mixer motor (37 kW). The order of constituent loading and the duration of the loading period set in this concrete plant are given as follows: A New Method of Controlling Water in SCC Production 267 - Coarse aggregates and sand (natural moisture) are first introduced into the mixer. - The loading of fines (cement and limestone filler) occurs after about 10 s. - Concrete admixtures pre-mixed with water are introduced after 20 s of dry mixing of coarse aggregates and fine elements. Liquid components are sprayed onto the upper part of the mixture in 9 to 11 s approximately, depending on the additional water amount. For each batch produced, the mixing time is set long enough to avoid incomplete mixing. As reported by RILEM [7], the mixing time was defined as the time between the loading of all constituents and the beginning of concrete discharge. In this study, 14 truck mixers have been filled with a total of 52 batches produced from 4 different SCC mix designs with several batch sizes. The analysis of all these batches is consistent. We present herein only 20 batches of two mix designs with a volume equals to 2 m³. These two concrete formulas are given in Table I. For each mix design, the water content was varied from one batch to the next. While SCC1, characterised by a lower workability, is used for horizontal applications, SCC2 with higher workability is employed for vertical applications. Table I. Concrete compositions. Component (kg/m³) Cement Limestone filler Sand 1 (0/4) Sand 2 (0/4) Gravel 1 (4/14) Gravel 2 (4/20) Superplasticizer Viscosity agent Total water Number of batches SCC1 295 85 300 552 886 4.37 187 8 SCC2 290 90 298 602 900 5.7 0.51 185 12 Total water in the mixture includes the moisture of aggregates, added water and water content in additives as well. The natural humidity of sand is measured online for each batch through the use of a microwave moisture probe. This moisture value is also checked and adjusted by drying before the fabrication. Coarse aggregate moisture is considered constant during the day of production. Both controls performed through the gravimetric method before and after production show close values. From typical fluctuations of moisture measurements, the measurement precision of water content in the batch concrete has been estimated at around 1.4 L/m3 (standard deviation), which is very high within an industrial environment. 268 Hai-Thong Ngo, Abdelhak Kaci, El-Hadj Kadri et al. Concrete fluidity is characterised by means of a test: slump-flow measurement at the batching plant at the end of each mixing. The slump-flow values vary between 62 and 75 cm for both two mix designs. Stabilisation Criterion of Power Curves The definition of a stabilisation criterion of power curves is likely linked to the determination of stabilisation time Ts which is the time needed to reach the stabilisation power level. Regarding concrete industrial production, this stabilisation time of the power consumption curve is generally considered as the shortest necessary mixing time after which the evolution of fresh concrete properties is negligible and the concrete can be discharged. The determination of Ts for each mix design can be made by using certain mathematical models suggested in the literature to fit the experimental power curves recorded during mixing. Many authors agreed that the power–time curves can be fitted by some exponential functions [6, 8]. These mathematical expressions mostly suit for the regular concrete and some SCC mix designs with high water to powder ratio (W/P). In these mixtures, the experimental mixing power evolution with respect to time shows that the power consumption increases with the constituents loading and then decreases during mixing until reaching a relative signal stabilisation. However, the power consumption curve of lower W/P ratio SCC cannot be treated with these models. Indeed, a second rise of power before the power final stabilisation for batch with low water dosage makes these models inappropriate. The highlight of this second power peak of high viscosity concrete, which marks the increase in material cohesion during mixing, was already mentioned in some works [1, 9, 10]. For this reason, one alternative method is to use the fluctuation in time of the power consumption, called "power fluctuation" associated with the filtered power consumption vs. time (Figure 1). This fluctuation is assessed herein by calculating the standard deviation of twenty consecutive power measurements (10 s after a given mixing time). The stabilisation time is then determined by the time needed for the power standard deviation to reach a defined limiting value. More specifically, by observing and analysing all experimental power curves, as soon as the power standard deviation decreases below the threshold value α set at 0.15% in absolute value, during at least 10 s, the stabilisation time of power curves is reached. The "end-point" of the stabilisation time in the power to time chart is called the "stabilisation point" after which there is no longer strong fluctuation in mixing power. The power measured at this point is called the "stabilisation power" Ps. The chosen value of α allows getting a minimum value of 55 s for Ts among the considered mixtures. Indeed, this time is the minimum mixing time recommended by the French standard for SCC mixtures [11]. Mixing power mixing power Power standard-deviation power standard-deviation Liquid loading 70 269 0.8 0.7 60 Stabilisation time 0.6 50 0.5 Stabilisation point 40 0.4 30 0.3 20 0.2 α = 0.15% 10 Power standard deviation (%) Percent of nominal mixing power (%) A New Method of Controlling Water in SCC Production 0.1 0 0.0 0 20 40 60 80 100 120 140 160 180 200 Time (s) Figure 1. Power consumption and its standard deviation during the mixing of a SCC2 batch with 171 L/m3 are used to determine the stabilisation time. Results and Discussion Stabilisation time versus total water content As already mentioned, the shortest necessary mixing time (i.e. stabilisation time Ts) depends on concrete composition, especially concrete water content [6, 8]. The correlation between stabilisation time Ts and total water content is confirmed in the Figure 2 for the two tested concrete mix designs. It can be noticed that the stabilisation time decreases with an increase in concrete water content. Furthermore, it could be observed that the plots fall into two groups depending on the use of viscosity agents in the mix. With the same water dosage, the presence of the viscosity agent leads to a higher stabilisation time. Consequently, mixtures with higher viscosity by using viscosity agents tend to require a longer mixing time. On the contrary, adding more water in the mix could reduce the friction between the particles and make them easier to be mixed. The diminution of stabilisation time is hence obvious. 270 Hai-Thong Ngo, Abdelhak Kaci, El-Hadj Kadri et al. 160 SCC1 (without viscosity agent) Stabilisation time (s) 140 SCC2 (with viscosity agent) 120 R² = 0.91 100 80 60 R² = 0.94 40 167 177 187 197 207 Total water content (L/m³) Figure 2. Relationship between water content and stabilisation time for the two SCC mix designs (with and without viscosity agent). Calculated water content L/m3) 205 195 185 175 165 165 175 185 195 205 3 Measured water content (L/m ) Figure 3. Measured versus Calculated water content for two SCC mix designs. A New Method of Controlling Water in SCC Production 271 The linear correlation between the stabilisation time and the water content observed in each mix design demonstrates that the stabilisation time of power curves could be a good indicator of concrete water content. The correspondence between the measured total water content and that calculated with the stabilisation time is given in Figure. For SCC mixtures tested here, water measurement precision based on the stabilisation time is better than ±3.6 L/m³ (standard deviation of 2.2 L/m3). Stabilisation line The experimental mixing power evolutions of seven SCC2 batches are shown in Figure which also represents the corresponding stabilisation points. It appears that the stabilisation points are located on a master curve called "stabilisation line" in the descending order of the water content. After the intersection of this line and the power curves, the variation of power consumption becomes negligible (power standard-deviation smaller than 0.15%). Thus, further mixing is not necessary when the stabilisation time is reached. Percent of nominal mixing power (%) 70 End of liquid loading Total water content (L/m³) 60 SCC2 (with viscosity agent) 171 50 175 177 Stabilisation line 40 186 189 30 192 20 200 10 Stabilisation point 0 0 50 100 150 200 Time (s) Figure 4. Power consumption vs. time for some SCC2 batches at different total water dosages. If the idea of setting an appropriate mixing time for each concrete batch is applied to the SCC production in the ready-mixed concrete plants, it would be possible to significantly reduce the mixing time and the energy consumption of the plant mixer. 272 Hai-Thong Ngo, Abdelhak Kaci, El-Hadj Kadri et al. When using the stabilisation time of power curves as the sufficient mixing time, at least 10 s can be reduced from the mixing time for each concrete batch production (see Figure 4). 30 Stabilisaation power (%) 25 Stabilisation line 20 15 SCC1 (without viscosity agent) 10 SCC2 (with viscosity agent) 5 40 60 80 100 120 140 160 Stabilisation time (s) Figure 5. The location of stabilisation points for the twenty batches of two SCC mix designs (with and without viscosity agent). For the pan-mixer investigated here, the stabilisation line of the twenty tested SCC batches can be fitted by a linear evolution of stabilisation power in stabilisation time (see Figure 5). For a given industrial mixing condition including mixer type and loading sequences, there exists a unique stabilisation line for each mix design (with a given batch volume). If several concrete mixtures have a similarity in the composition, it is possible to have one stabilisation line for all these mixtures (e.g., the two mix designs tested here). It should be also noted that the calibration of the stabilisation line is essentially influenced by modifying mechanical parts of the mixer or the loading sequences. Conclusions The proposed criterion of power consumption stabilisation in this paper allows determining the stabilisation time of power curves which can be used as a relative indication of SCC water content. With this new processing method, water measurement precision is estimated at ±3.6 L/m3 under real manufacturing conditions. In addition, the use of the stabilisation time as an indicator informing A New Method of Controlling Water in SCC Production 273 the end of the mixing time will allow avoiding unnecessary mixing time and increase the productivity in concrete plants. In the mixing power vs. mixing time chart, the stabilisation points corresponding to the mixing end-points of all SCC batches tested here are positioned on the stabilisation line in the decreasing order of the water dosage. For further applications, this line should be determined before being implemented in the concrete production process in order to optimise the mixing time and improve the online water control of SCC production. Thanks to industrial data processing, the intersection of the stabilisation line with the power consumption curve of the current batch may allow indentifying the actual water content and then making water adjustment for the next batch with the purpose of achieving the correct total water content of the mixed concrete. Acknowledgements The authors would like to thank Cemex Company for technical and financial support of the research work. References [1] Brunquet, E. and Cazacliu, B. (2007), In-situ on-line control of SCC production regularity, 5th International RILEM Symposium on Self-Compacting Concrete, Ghent, Belgium. [2] Wang, K. and Hu, J. (2005), Use of a moisture sensor for monitoring the effect of mixing procedure on uniformity of concrete mixtures, Journal of Advanced Concrete Technology, vol. 3, n. 3, pp. 371-383. [3] Cazacliu, B., Chopin, D., Shell, R., Château, E. and de Larrard, F. 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