International Journal of Applied Engineering Research ISSN 0973-4562 Volume 11, Number 15 (2016) pp 8507-8510 © Research India Publications. http://www.ripublication.com Experimental Investigation of Electrical Discharge Machining using Dielectric Fluid with Surfactant and Different Carbon Additives Pay Jun Liew a*, Muhammad Raziman Abdul Razak b, Nur Izan Syahriah Hussein c and Qumrul Ahsan d a,b,c Manufacturing Process Department, Faculty of Manufacturing Engineering, d Engineering Materials Department, Faculty of Manufacturing Engineering, Universiti Teknikal Malaysia Melaka, Hang Tuah Jaya, 76100 Durian Tunggal, Melaka, Malaysia. *Corresponding author. Abstract In this paper, Electrical Discharge Machining of Reaction Bonded Silicon Carbide (RB-SiC) was carried out using dielectric fluid with different surfactant concentrations and different type of carbon additives. Surfactant concentrations and types of carbon additives were varied and the machining performances such as material removal rate (MRR), electrode wear ratio (EWR), surface roughness and spark gap were investigated. The experiment results show that the surfactant and carbon additives added dielectric fluid not only increases the MRR and spark gap, but also reduces the EWR. In the case of surface roughness, only 0.4 wt.% surfactant with CNF produced smoother surface compared to the one obtained with no surfactant. Among three carbon additives, CNF was more effective to improve the machining efficiency of RB-SiC with the optimum surfactant concentration at 0.6 wt.%. fluids has been investigated extensively, all the previous works have focused on the high conductivity materials. Surprisingly, there is no report on a comparative study of different size and shape of carbon additive on low conductivity RB-SiC by EDM process. Therefore, the primary aim of this paper is to compare the machinability of RB-SiC using different types of carbon additives, such as carbon nanofiber (CNF), carbon nano powder (CNP) and carbon powder (CP) on the MRR, EWR, surface roughness and spark gap. Based on the present author’s work [8], the addition of surfactant span 80 can improve the machining efficiency of RB-SiC, especially on the MRR. Thus, in this study, surfactant span 80 was used to disperse the various types of carbon additives and its concentrations were also investigated. Keywords: EDM, RB-SiC, Dielectric fluid, Surfactant, Carbon additives EXPERIMENTAL DETAILS Sodick AQ35 EDM machine, type die-sinker was used to conduct the experiments. The workpiece material was RB-SiC with dimensions of 30 mm x 30 mm x 13 mm, and the tool was copper electrode with a diameter of 6 mm. Span 80 was used as a surfactant and mixed into EDM oil type Low Smell (LS) to disperse the carbon additive. Four different concentrations of surfactant were investigated, such as 0 wt.%, 0.4 wt.%, 0.6 wt.% and 0.8 wt.%. There are three different carbon additives, namely carbon nanofiber (CNF), carbon nano powder (CNP) and carbon powder (CP) were added into dielectric fluid. The differences between these three powders lay in their shape and size. Figure 2 indicates the field emission scanning electron microscopy (FE-SEM) micrograph of the CNF, CNP and CP, respectively. Before the EDM experiment, the required amount of surfactant, carbon additive and EDM oil were measured and mixed together. The process started by mixing the EDM oil with surfactant for 5 minutes to dissolve the surfactant using ultrasonic homogenizer. Then, carbon additive was added to the mixture and subjected to ultrasonication process for another 30 minutes. During the ultrasonic process, the sample was immersed into ice bath to minimize the temperature rise. Table 1 shows the experimental conditions and Figure 1 shows the EDM experimental setup. After the machining process, MRR, EWR, surface roughness and spark gap were measured as machining responses. An average of four measurements for each parameter setting was taken. INTRODUCTION Electrical Discharge Machining (EDM) is one of the most promising unconventional machining processes to fabricate products with high hardness and complex geometrical profiles. In this process, the workpiece material is removed by means of repetitive spark discharges between the electrode and workpiece that submerge in a dielectric fluid [1-2]. To improve the machining capabilities of EDM, powder mixed EDM (PMEDM) has emerged as one of the advance method in the past thirty years. In this process, the fine particles in the powder form are mixed into dielectric fluid to reduce the insulating strength of dielectric fluid [3]. Many previous researches have been done using PMEDM method and pioneer work can be traced to Jeswani [4], who reported that addition of 10 µm graphite powder can increase the material removal rate (MRR) and reduce the electrode wear rate (EWR). Tan and Yeo [5] added 45-55 nm silicon carbide powders into dielectric fluid, and confirmed the reduction of recast layer thickness on stainless mould steel. Liew et al. [6] also tried suspending carbon nanofiber (CNF) in dielectric fluid and they found that machining efficiency of reaction bonded silicon carbide (RB-SiC) was improved significantly. Recently, Marashi et al. [7] observed that after adding Ti nano-powder to dielectric, the surface morphology, surface roughness and material removal rate were notably enhanced. Although the effect of powder additive in various dielectric 8507 International Journal of Applied Engineering Research ISSN 0973-4562 Volume 11, Number 15 (2016) pp 8507-8510 © Research India Publications. http://www.ripublication.com Table 1: Experimental conditions Working Parameter Workpiece Material Description Reaction Bonded Silicon Carbide (RB-SiC) Electrode Material Copper Diameter Electrode [mm] 6 Polarity Positive (Workpiece) Negative (Tool/electrode) Voltage [V] 22 Peak Current, Ip [A] 6 Pulse On Time, Ton [µs] 10 Pulse Off Time, Toff [µs] 40 Machining Time [min] 15 Additive Carbon nanofiber (CNF) Carbon nano powder (CNP) Carbon powder (CP) Surfactant Span 80 Concentration of 0, 0.4, 0.6 and 0.8 Surfactant [wt. %] Figure 1: EDM experimental setup RESULT AND DISCUSSION Material Removal Rate (MRR) Figure 3 shows the effect of three different additives on the MRR of RB-SiC. It is clearly seen that the MRR increased with the increasing of surfactant concentration, except for the additive CP where there were no significant changes for all surfactant concentrations. With the presence of a surfactant in the dielectric fluid, the carbon particles were surrounded by surfactant molecules which can reduce the electrostatic force [9]. Due to this phenomenon, the particles can disperse evenly and cause a better distribution of discharge energy, leading to a higher MRR. The highest MRR was achieved at a concentration of 0.6 wt.%, whereby this only occurred for the additives CNF and CNP. However, the MRR tended to decrease at the surfactant concentration of 0.8 wt.%. For comparison, CNF was more effective at improving the MRR for machining RB-SiC compared to CNP and CP. In this case, the high electrical conductivity CNF might help to increase the frequency of discharge, and resulting in an improvement of MRR [6]. The addition of CNP, which has a nano size, also induced a higher MRR compared to the CP, which has a micro size. This result is consistent with that reported by Chow et al. [10]. Due to the small machining gap during the EDM process, it is difficult for the larger particles to enter the gap between the electrode and the workpiece. Therefore, the material removal rate is lower using the micro powder grain size than that obtained when applying the nano powder grain size. (a) (b) (c) Figure 2: FE-SEM micrographs of different types of additives (a) carbon nanofiber (CNF), (b) carbon nano powder (CNP) and (c) carbon powder (CP). 8508 International Journal of Applied Engineering Research ISSN 0973-4562 Volume 11, Number 15 (2016) pp 8507-8510 © Research India Publications. http://www.ripublication.com Surface Roughness Figure 5 illustrates the effect on surface roughness using different concentrations of the surfactant Span 80 and different additive powders. The graph shows that without the use of a surfactant, the value for surface roughness with CNF was high. However, when a suitable amount of surfactant was added (0.4 wt.% in this experiment), the surface roughness showed a decrease. According to Wu et al. [13], when a surfactant is added to the dielectric fluid, the hydrophilic head group absorbs on the surfaces of the particles and the hydrophobic tail will extend to the dielectric, causing these agglomerated particles separated and well distributed within the dielectric fluid. Therefore, the electrical discharges are more distributed and lead to a better surface finish on the machine surface. When comparing the types of additives, it can be seen that lower surface roughness can be achieved using CP particles. This might be due to the fact that the material is removed slowly (low MRR) through melting and evaporation, causing a decrease in crater size; thus the surface finish is improved. Figure 3: Effect of different carbon additive using different concentrations of the surfactant Span 80 on the MRR Electrode Wear Ratio (EWR) The effect of different concentrations of the surfactant Span 80 with different carbon additives on EWR is shown in Figure 4. For all three additives used in this experiment, the EWR tended to reduce with the addition of surfactant until a concentration of 0.6 wt.%. Nevertheless, when the surfactant further increased to 0.8 wt.%, the EWR tended to increase again. As known from Rehbein et al. [11], during the machining, the electron movement is intense, whereby a small arc that is produced during machining may reverse the direction of the feed to maintain a larger gap and, as a result, most negative ions move easily through the machining gap, resulting in a lower EWR. In terms of additive powder, it was noticed that the EWR was lowest when CNF was added to the dielectric fluid, compared to CNP and CP. This might be related to the good dispersion of CNF inside the dielectric fluid, producing a higher MRR, thus decreasing the EWR. The addition of CNF might also have prevented the ions that were produced by the ionization of the dielectric fluid from hitting the tool electrode with a high momentum and high energy, which causes a rapid erosion of the tool electrode [6]. Moreover, CNP with a smaller size also shows a lower EWR compared to that of the micro sized CP. This is attributed to the combined effect of a low MRR and a high tool wear by large particles [12]. Figure 5: Effect of different carbon additives using surfactant Span 80 on surface roughness Spark Gap The results for the spark gap using different additive powders and different surfactant Span 80 concentrations are illustrated in Figure 6. The graph clearly shows that using a surfactant affected the spark gap in contrast to a dielectric fluid without surfactant. When surfactants were used, the spark gap increased significantly. The addition of a surfactant might prevent the agglomeration of particles, and cause the particles to be well dispersed within the dielectric fluid. Therefore, bigger spark gap was obtained. Moreover, it is worth noting that the highest spark gap was obtained using the CNF additive compared to CNP and CP. Presumably, when CNF was added to the dielectric fluid, the long and thin shape of its particles might be able to more significantly bridge the gap between the electrode and the workpiece by interlocking with each other, in contrast to round-shaped particles of CNP and CP. In addition, when the CNF was added to the dielectric fluid, the additive reduced the insulating strength of the dielectric fluid [6] and due to this, a bigger spark gap was produced between the electrode and the workpiece. Figure 4: Effect of different carbon additive using different concentrations of the surfactant Span 80 on the EWR 8509 International Journal of Applied Engineering Research ISSN 0973-4562 Volume 11, Number 15 (2016) pp 8507-8510 © Research India Publications. http://www.ripublication.com [2] [3] [4] [5] Figure 6: Effect of different carbon additives using surfactant Span 80 on the spark gap [6] CONCLUSION In this experimental works, EDM machining of RB-SiC was carried out using dielectric fluid with surfactant and different carbon additives. The effect of carbon additives in the presence of different surfactant Span 80 concentrations on the material removal rate, electrode wear ratio, surface roughness and spark gap was investigated. The following conclusions can be drawn: MRR increases with the increasing of surfactant concentration and the optimum MRR was achieved at 0.6 wt.% of surfactant concentration using CNF as an additive. Surfactant concentration strongly effects the EWR. The higher the concentration is, the lower the EWR. However, there was only a marginal reduction of EWR using CP additives. Dielectric fluid with the addition of CNF and 0.4 wt.% of surfactant concentration can lower the surface roughness of machined surface. For the additive comparison, both CNF and CNP produced rougher surfaces than CP. Adding surfactant in the dielectric fluid can significantly improve the spark gap, particularly using CNF additive. [7] [8] [9] [10] [11] [12] ACKNOWLEDGEMENT The authors would like to thank the Ministry of Higher Education Malaysia and Universiti Teknikal Malaysia Melaka (UTeM) for technical, educational and financial support through the grant FRGS/1/2014//TK01/FKP/02/F00220. [13] REFERENCES [1] Kibria, G., Sarkar, B. R., Pradhan, B. B. and Bhattacharyya, B., 2010, “Comparative Study of Different Dielectrics for Micro-EDM Performance during Microhole Machining of Ti-6Al-4V Alloy,” The Int. J. Adv. Manuf. Tech., 48(5-8), pp. 557-570. 8510 Zeid, O. 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