Application Note 3. Routine Core Analysis Free fluid, bound fluid and T2cutoff Knowing the value of T2cutoff enables the amount of mobile and bound fluids to be calculated from log data. The T2cutoff is the size boundary between small pores containing bound fluid and larger pores where the fluid is free. While various rock types have standard T2cutoff values, the geometry of the pores and the rock’s mineralogy may shift the T2 spectrum, so laboratory core analysis experiments are used to determine the value of T2cutoff. This application note demonstrates how the total porosity, free fluids and bound fluids are used to calculate T2cutoff. magritek www.magritek.com Concept called the bound volume irreducible (BVI). The quantity of unbound or mobile fluid in large pores is called the free fluid index (FFI). NMR measurements of a core are used to determine BVI and FFI, which are then used to calculate T2cutoff. The T2cutoff can be used to find the amount of free and bound fluids in a well log. NMR detects a decaying signal from excited fluid molecules in a rock sample. The decay time constant is proportional to the size of the pores in which the fluids are contained (see Application Notes 1 and 2). Very small pores bind the fluids tightly with capillary forces; the amount of fluid bound in these pores is Sample preparation To determine a T2cutoff in a laboratory, two NMR measurements of a core sample are made – the first when it is saturated with brine and the second when it has been desaturated. When a core is saturated, fluids occupy the entire pore space but when desaturated, water remains bound only in the small pore spaces between the grains, and in clays. FluidC Grains Clay bound water In Figure 1, a Berea sandstone core has been saturated, then desaturated by centrifugation. More details of these preparation methods can be found in the American Petroleum Institute’s Recommended Practices for Core Analysis. apillary bound water Figure 1: T2 distributions of saturated (blue) and bound (red) cores plotted as incremental porosity. NMR measurements Both brine-saturated and desaturated rock cores can be analyzed in a benchtop NMR instrument. Following analysis of the saturated sample, the raw data is processed to give a T2 incremental porosity spectrum (as described in Application Note 2). The core is then desaturated to remove all mobile water and reanalyzed. The T2 distributions of the saturated (blue) and bound (red) are shown in Figure 1. Note that both traces have signals from the bound water, but only the saturated sample has signals from the free fluid. FFI and BVI determination To determine BVI using NMR, the total volume of water in the desaturated sample is first measured by integrating the incremental porosity spectrum to produce a cumulative porosity spectrum (Figure 2, red line). BVI is then the fraction of water bound in pores below a certain size. The saturated sample is also integrated to determine the total porosity of the core (blue line). As shown in Equation 1, FFI is the difference between the total porosity and the BVI. In this example using a sandstone sample (Figure 2), total porosity is 18.8 p.u., BVI is 3.4 p.u. and FFI is 15.4 p.u. (1 p.u. = 1 porosity unit = 1 per cent of the bulk volume). Equation 1 FFI = Total porosity – BVI Saturate Core BVI Total Porosity FFI Saturated T2 Distribution Centrifuge Core Bound T2 Distribution BVI and FFI Determination Figure 2: A cumulative porosity spectrum is produced by integrating an incremental porosity spectrum. Total porosity, FFI, and BVI are determined from the cumulative porosity spectrum. T2cutoff determination Figure 3: A cumulative porosity plot, showing the calculation of T2cutoff as 40 ms. BVI FFI black line indicates that the saturated sample has a cumulative porosity of 3.4 p.u. at 40 ms. T2cutoff therefore equals 40 ms for this sample. Total Porosity The T2cutoff is defined as the value of T2 where the cumulative porosity of the saturated sample is equivalent to the BVI. For the example in Figure 3, BVI = 3.4 p.u., the dotted T2cutoff How T2cutoff is used Free fluid is in larger pores where T2 is greater than the T2cutoff, therefore the T2cutoff is used by well log analysts to determine the quantity of free fluid in a reservoir. Figure 4 shows the use of T2cutoff to differentiate between bound and free fluids in a saturated sample. It is impossible to measure the BVI of a reservoir in situ, but it can be calculated from the T2 spectra of a well log using the T2cutoff determined from NMR analysis of a core sample in a laboratory. Figure 4: An incremental porosity plot divided into bound and free fluids with T2cutoff. T2cutoff Summary The T2cutoff is a very important measurement for the interpretation of well log data. Using NMR in a laboratory, the T2cutoff is calculated by measuring the total porosity and the bound For further information please contact: [email protected] GERMANY Pauwelsstr 19 52074 Aachen, Germany Tel +49 241 963 1420 Fax +49 241 963 1429 and free fluids in the pores of core samples. The NMR experiment simply requires measuring the same core sample when saturated with brine and desaturated. NEW ZEALAND 32 Salamanca Road Wellington 6012, NZ Tel +64 4 920 7671 Fax +64 4 471 4665 US +1 (415) 287 0727 HK +852 8176 7196 magritek www.magritek.com
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