Summary Subject: MiKS project – WG3 meeting No 2 Date and time: Location: Participants: 29.04.2016, 10:00-15:00 Lyngby, DTU, Denmark Rolands Cepuritis, NTNU [RC] Stefan Jacobsen, NTNU [SJ] Evgeny Ramenskiy, NTNU [ER] Jon Spangenberg, DTU [JS] Sverre Smeplass, Skanska [SS] Distribution: Participants, Ernst Mørtsell Taken by: Evgeny Ramenskiy [ER] Summary MiKS WG3 meeting No 2 The primary objectives of WG3 established during the meeting No 2 are: 1. To obtain a matrix of data with rheological measurements performed with FlowCyl and mini-slump test methods on a set of filler-modified cement pastes where given composition parameters have been varied over a defined range. The obtained results shall be used in order to derive a practical model of predicting the influence on rheology of adding a specific crushed sand filler to a given cement paste and consequently concrete. 2. To correlate the FlowCyl test measurements with the results obtained by a rheometer. 3. To present the results on a series of the FlowCyl test simulations using the Flow 3D software and 4. To analyse the effect of the yield shear stress (according to the Bingham model) on the measured flow resistance ratio (λQ) acquired from both physical measurements and computer simulations. In order to meet the first objective, a setup of filler-modified cement paste composition parameters for the FlowCyl and mini-slump flow tests will be identified, as outlined in Table 1. The range/variants in the table are intentionally left out empty to be discussed during the consecutive meetings. The setup of parameters should also be designed with the following two considerations in mind: To identify and verify the FlowCyl test method as proficient in providing accurate information on the matrix rheology and To recognise the FlowCyl test suitability for matrices with high filler content when combined with low SP dosage in order to examine the inconsistency shown in [1]. 1 Table 1 - Overview of some of the possible composition variables for the FlowCyl and mini-slump flow tests. Parameter Range / Variants Cement type Norcem anlegg – CEM I 52.5 N Norcem standard – CEM I 42.5 R Norcem industry – CEM I 42.5 RR Norcem standard FA – CEM II/B-M 42.5 N Water – cement, w/c-ratio TBC Condensed silica fume, s/c-ratio TBC Pulverised fly ash, f/c-ratio TBC Ground-granulated blast-furnace slag, TBC - May be included as cement type GGBS/c-ratio Crushed fillers, grading TBC Crushed fillers, fi/c-ratio TBC Superplasticizer (EN934-2), SP/c-ratio TBC To fulfil the second objective, a test programme will continue with the rheometer analysis based on the parameter proposal in the Table 1. The time frame for the test programme is to be confirmed, however, the free access to the rheometer at SINTEF is until 12 Feb 2018. To accomplish the third objective, the FlowCyl test simulations using the Flow 3D software will initially require to select and confirm 10 data sets (along the line form Rolands thesis) to check λQ. Evgeny and Jon will perform these numerical simulations. Spreadsheet calculation of the flow resistance ratio λQ based on the FlowCyl test has been provided by Sverre. In order to correctly define parameters related to the numerical simulations, plastic viscosity (μ) and shear yield stress (0) will be examined using the Anton Paar viscometer at DTU by Jon and at NTNU by Evgeny. These parameters will be defined for mixes with the following constituents: T1 and T6 fillers used for the SCC2016 study; Norcem industry cement – CEM I-42.5 RR. The following materials to be sent by Evgeny to Jon: 0.5 kg of both T1 and T6 fillers used for the SCC2016 study; 0.5 g of Norcem industry cement – CEM I-42.5 RR. Geometry of the FlowCyl test cone will be updated in the computer simulations (see Figure 1). In addition, velocity profile plots of the FlowCyl cone cross-section simulation will be prepared. Simulation will be performed with length of matrix stream without bucket if it can be determined that a viscous liquid is not affecting the results. 2 Figure 1 - FlowCyl geometry. It is important to note that the FlowCyl setup diagram (see Figure 2) does not provide a reference distance form the cone to the container sitting on the weight. It would be advantageous to establish the reference distance as it determines the length of the stream, possibly affecting the results. Figure 2 - FlowCyl set up dimensions. Trondheim, May 14th 2016 Evgeny Ramenskiy 3 References 1. 2. 3. Kjos-Hansen, H.S., 2015. Mikroproporsjonering- Effekt av fillergradering og fillersammensetning. Prosjektoppgave, NTNU: Trondheim. Applicability of the particle-matrix model to LWAC. The European Union –Brite EuRam III. EuroLightCon BE96-3942/R12, March 2000. Mørtsell E., Smeplass S. and Maage, M., 1995. Karakterisering av flytegenskapene I betongens matriksfase. Instiutt for konstruksjonsteknikk, NTH. Betongindustrien okt 1995. 4
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