Lines and Components for making Carbon Fiber Dipl.-Ing. Erwin Glawion, Sales Manager and Dr. Dieter Zenker, Managing Director, both Trützschler Nonwovens GmbH In recent years carbon fiber came increasingly into the focus of the industry making parts and machinery for extreme standards regarding sustainability and energy saving. Also the automotive industry has already increased the share of carbon fiber composites, which could result in huge demands in the next years, even the price per kg is much higher than other construction materials. Trützschler has successfully started to participate in this market 3 years ago by building optimized machinery for production lines, based on experience of almost 50 years in building man-made fiber equipment. The Production of Carbon Fibers: A sensitive phase to phase Process As in the past the development of carbon fiber equipment and machines often took place independently from machine and equipment builders, it was not always easy for this industry, to find reliable, high-sophisticated units or even complete lines. Following this idea Trützschler and the companies Eisenmann, well known for material flow automation, environmental technology and high temperature technology like oxidation ovens and Ruhstrat, manufacturer of high-temperature furnaces like carbonization furnaces found each other more than two years ago and started to work on the upper mentioned goal. All together, complete carbonization lines, having a total length up to 250 m, can be engineered and delivered as required by the market. The Process Steps and the required Equipment The prepositions for a perfect carbon fiber however are created in the polymerization and the subsequent spinning of a suitable PAN precursor. Also these steps can be offered together with EPC Industrial Engineering, a family-owned engineering company, specialized in engineering of polymerization plants including utility and civil engineering. Trützschler has developed new optimized spinning components, based on the former delivery of many PAN textile lines and concepts, taken over from other spinning technologies. For the so-called wet spinning process PAN powder is dissolved in solvents continuously to get a spinning dope. The degassed dope is fed to the Trützschler Precursor Line consisting of innovative spinning units, which assure a homogenous consistency and shape of the tows. An even and uniform fluid flow and concentration in all coagulation and washing steps, reliably smooth-running rollers, and the prevention of friction points are realized by Trützschler through an intelligent combination of drive management, fluid circulations and temperature control. In all process steps, the modular machine system allows a high flexibility for the line configuration, exactly adaptable to the requirements. Through the whole processing on the Precursor Line, the tows are guided by the FiberLogistic-System, a combination of surface treatment bathes, drive and process control. The Precursor Line ends with the winding on 300 kg bobbins or plaiting of the precursor in big cans, as the following carbonization process runs at significantly lower speed. After unwinding or taking out from the cans again, the precursor tows are kept separately in a wide band and are subsequently transformed into carbon fiber tows. Trützschler’s knowledge of tow handling and the central HMI assure exactly parallel tow guiding and the overall process control in the following steps. The first fiber-modifying process step is the oxidation or stabilization of the PAN-precursor in the ovens of Eisenmann. The subsequent carbonization is executed in two process steps in the furnaces of Ruhstrat. The first step of the carbonization is done in a furnace around 700°C (LT-furnace). This furnace is directly followed by the high temperature furnace (HT), which heats up to 1800°C. For special CFapplications graphitization is possible in an optional ultra high furnace (UHT), which works at temperatures up to 2600°C. After the Carbonization the tows, each consisting of several thousand fibers, each having less than 8 microns, have to be electrolytically roughened to get a sufficient adhesion in the final product. Subsequently a sizing has to be applied before winding on easily manageable bobbins. Conclusion Trützschler and his alliance partners are the only one worldwide, which can offer complete lines for the whole process chain, in lab-scale up to industrial production lines with an output up to 2000 tons of carbon fiber per year. First orders are under manufacturing and the feedback from the market is still very encouraging.
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