HFL14HydrangeaPhyto Objective: to compare three strategies to avoid or mitigate preemergence herbicide injury to container-grown Hydrangea macrophylla. Executive summary: Hydrangea macrophylla is one of the most popular landscape shrubs. In response to strong market demand, container nurseries have increased production of many varieties of Hydrangea macrophylla. However, weed management in hydrangea production is challenging because few herbicides are labeled for use on this species, and those which are labeled have been shown to cause crop injury when granules adhere to the foliage. In this experiment three methods to avoid or mitigate that injury were compared: (1) dislodge herbicide granules from the growing points by shaking plants before irrigation is applied; (2) spray-apply Tower herbicide followed immediately by irrigation; and (3) accept that bud damage would occur, but prune the damaged tissues to encourage regrowth. Results confirmed that severe crop damage results when granules are not manually removed before irrigation. Shaking plants to dislodge herbicide granules before irrigation prevented tip necrosis from Freehand and Snapshot treatments. Plants receiving this treatment were visually indistinguishable from the non-treated plants, but plant growth (as measured by canopy volume and fresh weight) was reduced by 10% to 15%. Despite this reduced growth, plants in these treatments were considered “marketable” based on visual quality assessments. Spray applications of Tower herbicide also caused about 10 to 15% reduction in overall plant growth with no tip necrosis. Shaking plants treated with OH2 reduced but did not eliminate tissue necrosis. Pruning plants to remove herbicide-damaged shoots did not promote plant quality or growth. In fact, regrowth of herbicide-damaged plants was significantly less compared to non-treated plants that were pruned at the same time. These results confirm that under the best of circumstances, growers should expect 10 to 15% growth reduction following herbicide treatments. Growers will need to understand and accept that when preemergence herbicides are applied to hydrangea it is likely that plant growth will be reduced. Acute injury can be avoided by following these guidelines: 1. Be sure the foliage is dry before application; 2. Utilize “non-burning” herbicides (such as the Freehand or Snapshot used in this trial); and 3. Physically remove granules from the growing points before irrigation is applied. Spray-applied herbicides, such as Tower, may also be an alternative. The other alternative is to rely on hand weeding and/or mulches for weed control in Hydrangea macrophylla production. Effects of herbicides and removal treatments on % marketable plants ~ 10 weeks after treatment 100 % marketable plants 90 80 70 60 Shaken 50 Irrigated 40 Pruned 30 20 10 0 Non-treated Freehand Snapshot OH2 Tower Title: Location: Substrate: HFL14HydrangeaPhyto Experiment #: Hydrangea Herbicide Injury Avoidance Comparisons Horticultural Field Laboratory, N. C. State University, Raleigh in a hoop house covered with 50% shade cloth. Parker Bark Company "Nursery Mix" minus minor elements; (hammer-milled pine bark amended with lime); top-dressed with Osmocote Pro 17-5-11 slow release fertilizer with minor elements @ 1 TBSP/pot CO2 pressurized 2L bottle sprayer and hand held shaker Application Equip. 2-8004 XR PSI: 36.5 Speed: 3 mph #/type of nozzle: 30 GPA: RCB 4 Experimental Design: Replicates: Plants/species/plot: 13 3 Treatments: 4’ x 4' 2013 Plot size: Potting Date: APPLICATION INFORMATION DATES Calibration: ml/15 sec (target 284) TREATMENTS APPLIED SOIL MOISTURE SOIL CONDITION TEMPERATURES (°F) air soil surface / 2 in / 6 in SKY: WIND SPEED & DIRECTION Date of first rain (R) or irrig. (I) Amount (in.) R or I 8/15/2014 282 12,13 8/15/2014 NA 1-11 moist moist outside of shade house 88 84/78/85 40% cloud cover 0-1 mph,W 8/15/2014 I ~0.4" inside shade house 80 80/79/78 50% shade cloth 0-1 mph,NW 8/15/2014 I ~0.4" CROP Status: Hydrangea macrophylla 'Endless Summer' 10-12" tall, w/many new shoots flushing; full canopy cover of pot; very uniform in size COMMENTS OR CORRECTIONS: all plants potted to 4-L pots in spring 2014. To encourage branching and new growth, plants were pruned to 4-6" in height 18 days prior to treatment. All treatments were applied on August 15th. On August 18th, treatments that included pruning were clipped with hand-held clippers to remove the damaged tips. This required pruning plants to about 6 - 8 inches in height. Hydrangea macrophylla is one of the most popular container-grown nursery crops. The species is relatively easily propagated and produced in container culture but is injured by most preemergence herbicides. Of the 25 preemergence herbicides labeled for use in container nursery crops, only 7 are labeled for use on Hydrangea macrophylla, including Freehand, OH2, Snapshot TG, Pennant Magnum, Regalkade G, Regal OO, and Surflan. However, grower experiences and research had demonstrated that each of these herbicides may injure Hydrangea macrophylla in container production. Below is a chart from our 2012 experiment illustrating that several of these herbicides cause significant foliar necrosis or stunting of Hydrangea macrophylla ‘Endless Summer’ when applied at labeled rates. Figure 1. Preemergence herbicide injury to Hydrangea macrophylla 3 and 10 weeks after treatment. It should be noted that each of these herbicides is labeled for use on hydrangea. PRE herbicide injury to Hydrangea macrophylla 2012 Data; NC State University % Injury / Stunting 100 3 WAT 80 10 WAT 60 40 20 0 Hand Weeded Freehand Tower Pendulum Snapshot TG . The injury generally consisted of necrosis of growing points where granules were “trapped” by the leaves or developing bud. See the photos below. Subsequent re-growth is also often delayed or stunted. Herbicide alternatives including various mulching materials have been investigated and can be effective, but these products often cost four to five times as much as an effective preemergence herbicide program. Consequently, weed management options for hydrangea production is routinely cited by growers as a high priority need. Since it appears that nearly all preemergence herbicides labeled for nursery crop production have the potential to injure this species, it is critical that we investigate methods to reduce the frequency and severity of injury following herbicide treatment. The crop injury observed appears to result primarily from “trapping” of granular treatments in the growing points, resulting in tip necrosis. In this research project we compared three strategies to mitigate this type of crop injury. Two strategies for removing granules from the growing points were irrigation immediately after treatment and manual shaking of the plants to dislodge granules. A third strategy was to accept that bud damage would occur, but prune the affected stems to remove the damaged tissues and encourage regrowth. This last strategy assumes that hydrangeas in container production require periodic pruning to stimulate branching. METHODS Hydrangea macrophylla ‘Endless Summer’ cuttings were rooted into cell trays. After rooting, plants were potted to 1-Gallon (classic 400) plastic pots using a pine bark-based substrate amended with recommended rates of lime and top dressed with slow-release nursery fertilizer. After potting, plants were allowed to grow to about 8 to 10 inches in height then were pruned to stimulate branching. This was done to increase the number of growing points on each plant that would be susceptible to herbicide damage. When plants had about 4 inches of new growth, labeled preemergence herbicides, including Freehand G, Snapshot TG, OH2, and Tower, were applied at labeled doses. Three treatment strategies were used to remove granular herbicides or mitigate the damage. 1. Physically shake plants to dislodge granules before irrigation; 2. Utilize a spray-applied herbicide, Tower, then irrigate immediately after treatment; 3. Treat, irrigate, then 3 days later (when it is possible to see which growing points were damaged) prune the injured stems. These treatments were compared to non-treated plants as well as plants receiving overhead irrigation after treatment. Herbicides were applied to dry foliage. Granular treatments included Freehand G, Snapshot TG, and Everris OH2, each applied at the manufacturer’s maximum recommended dose. Herbicides were applied in pre-weighed aliquots using a hand-held shaker jar. The one spray treatment, Tower, was applied at the high labeled dose using a CO2-pressurized sprayer calibrated to deliver 30 GPA. Herbicide treatments were applied on August 15, 2014. Plants were maintained under 50% shade cloth and received about 0.5 inches of overhead irrigation each day applied in 3 equal increments: morning, mid-day and late afternoon. Plant injury evaluations. Three days after herbicide application and before pruning, injury to the growing points was observed. Injury could be categorized into 4 points on a subjective bud injury rating scale (see images below): 0 = no discoloration; 1 = slight chlorosis; 2 = distinct chlorosis of new growth with some tissue necrosis; 3 = new growth necrotic (may or may not be accompanied by chlorosis); and 4 = necrotic growing points with necrotic symptoms spreading to adjacent leaves or stems. Additionally, an evaluation of the % of the leaf buds on the plant with necrosis (approximate # buds necrotic divided by total buds on the plant, multiplied by 100) was made. 0 2 1 3 4 Beginning 4 weeks after treatment, plant injury was evaluated on a 0 to 10 scale where 0 = no injury (visually equivalent to the non-treated) and 10 = dead. The evaluation scale is described below. To convert these data to % injury, multiply the means by 10. Value 0 1 to 2 3 to 4 5 6 to 9 10 Plant Symptoms No visual injury present. Minimal injury to desirable plant. Less than 10% of the plant leaf surface area showing chlorosis, necrosis or other symptoms. Or 10 to 20% reduction in growth. Greater than 20% discoloration or necrosis; generally associated with some stunting. Or 30 to 40% reduction in above-ground biomass. About 50% reduction in above-ground biomass; may also be stunting, necrosis or a combination thereof. A majority of the plant is necrotic or otherwise visibly damaged. Plant appears dead. No signs of regrowth. Plant quality and growth evaluations and measurements. Plant quality was visually evaluated using a subjective 0 to 10 scale where 10 = the best plants in the trial. In this “treatment-blind” evaluation, each plant (sub-sample) within a plot was assigned a separate number, then sub-sample data were averaged. Plants receiving a rating > 8 were considered “marketable”. To be deemed “marketable” plants had to be well formed, with lush growth and lack obvious signs of foliar damage. This was a subjective determination by the evaluator (Dr. Neal). From these data, an estimate of % marketable plants was calculated. Plant height and width in two directions were measured (to the nearest 0.5 inches) approximately 4, 7, and 10 weeks after treatment. Plant canopy volume was calculated using the formula for one-half of a sphere: canopy volume = 0.5(4/3πr3); where r = average of the height and one half of the width. At the termination of the experiment, about 10 weeks after treatment, the above-ground fresh weight of each plant was recorded. Additionally, visual evaluations of root quality were conducted using a 5 point scale (see image below): 0 = no roots; 1 = very few roots emerging from the original root ball; 2 = weakly rooted and root ball falls apart when handled; 3 = about half of the substrate exploited by white healthy roots; 4 = substrate fully exploited by roots but root ball not firm; 5= root ball firm when squeezed and fully exploited by healthy roots. Note: there were no root balls deemed to be a 0 or 1 in this experiment. RESULTS All granular herbicides caused chlorosis and necrosis of the growing points when granules were not physically removed before irrigation. Injury was observed as soon as 1 day after treatment. When granules were removed by manually shaking the plants, no injury was observed from Freehand or Snapshot treatments. OH2 injury was dramatically reduced when granules were removed by shaking, but plants still exhibited foliar necrosis. Growing points of hydrangea plants 1 day after herbicide treatment. No necrosis was observed on plants treated with Tower. Tower, irrigated Non-treated Bud necrosis in plants receiving overhead irrigation only vs. granules shaken off 1 day after herbicide treatment. OH2 treatments resulted in injury. Injury was less severe when granules were shaken off by hand. OH2, shaken off OH2, irrigated only In contrast, physically shaking the plants prevented bud damage from Freehand and Snapshot. Freehand, shaken off Snapshot, shaken off Freehand, irrigated only Snapshot, irrigated only Three days after herbicide application, plants were pruned to remove the damaged growing points. Before pruning After pruning About one month after herbicide treatment and pruning, plant quality evaluations were initiated. Plants treated with granular herbicides and receiving irrigation as the only removal technique were of lower quality – smaller and necrotic tissues still visible compared to plants which were shaken to dislodge granules before irrigation. When granules were shaken off, plants treated with Freehand or Snapshot were visually equivalent to the nontreated. Plants treated with OH2 were of lower quality despite having good regrowth; necrotic tissues were still visible on plants 10 weeks after treatment, resulting in a lower quality rating. Pruned plants were smaller in size (and thus lower in quality). Non-treated plants that were pruned resumed normal growth sooner than pruned herbicide-treated plants. A surprising observation was that regrowth following pruning was inhibited by prior herbicide treatments. Effects of preemergence herbicides and herbicide removal strategies on Hydrangea macrophylla ‘Endless Summer’ plant quality. Evaluations were on a 0 to 10 scale with 10 being the best plant quality in the test. Herbicide(s) Formulation na na Dose lbai/A 0 0 Removal method Irrigation Pruned 9/17 9.9 7.3 a b 9.8 7.6 a c 9.8 8.0 a cd 9.9 8.3 a cd dimethenamid-p + pendimethalin 1.75 GR 3.5 Irrigation Shaken Pruned 5.9 9.3 5.3 cd a de 6.0 9.3 6.3 de ab d 6.5 9.2 6.5 e ab e 6.6 9.4 6.7 e ab e isoxaben + trifluralin 2.25 GR 5 Irrigation Shaken Pruned 5.8 9.3 5.0 d a e 5.9 9.0 5.8 de b de 6.1 9.2 6.0 e ab ef 6.2 9.4 6.2 ef ab ef oxyfluorfen + pendimethalin 3G 3 Irrigation Shaken Pruned 5.1 7.2 4.1 e b f 5.3 7.4 5.0 ef c f 6.0 8.7 5.4 ef bc f 6.2 8.7 5.4 ef bcd f dimethenamid-p 6 EC 1.5 Irrigation Shaken Pruned 9.3 na 6.6 a 8.9 na 7.2 b 9.3 na 7.9 ab 9.2 abc d 7.8 d None None 9/30 bc 10/9 c 10/23 Means within a column followed by the same letter are not significantly different (LSD, p = 0.05). plant quality (0-10) Effects of herbicides and removal treatments on overall plant quality ~ 10 weeks after treatment 10 9 8 7 6 5 4 3 2 1 0 Shaken Irrigated Pruned Non-treated Freehand Snapshot OH2 Tower Freehand-treated and non-treated plants approximately 10 weeks after treatment. L to R: non-treated Freehand shaken Freehand irrigated Freehand pruned non-treated pruned Plant quality ratings included plant size, color, and presence or absence of injured tissues. The photos above illustrate OH2-treated plants that exhibit significant healthy growth and relatively good size, but the necrotic tissues damaged by herbicide treatment 10 weeks prior are still present and visible. Such a plant would have received a score of 7 on the quality scale and would have been classified as “not marketable” in the subjective classification. When individual plants were scored as “marketable” or “not marketable”, the treatment effects are clear. At the final evaluation, 10 weeks after treatment, Freehand- and Snapshot-treated plants which were shaken to remove granules were 100% marketable. Plants receiving irrigation to remove herbicide granules were less than 30% marketable. Pruning plants delayed overall marketability with about 80% of the non-treated plants being classified as “marketable” 10 weeks after pruning. In contrast, less than 10% of the herbicide-damaged plants which were pruned after treatment were considered marketable. These results soundly rejected our hypothesis that herbicide-damaged plants could be pruned to recover normal growth. Effects of herbicides and removal treatments on % marketable plants ~ 10 weeks after treatment % marketable plants 100 80 60 Shaken 40 Irrigated Pruned 20 0 Non-treated Freehand Snapshot OH2 Tower Plant canopy volumes were estimated using measurements of plant heights and widths. These data were highly correlated (R = 0.97) with plant quality evaluations. Plant volume increased dramatically in the first 4 to 6 weeks then slowed. Lack of growth in the last month may be related to shorter days and cooler nights in the month of October. Thus, had the trial been initiated earlier in the season it is possible that the pruned treatments would have continued growing and mitigated some of the growth inhibition observed in this trial. About 10 weeks after treatment, plants were cut off at ground level and weighed. Fresh weights were highly correlated with plant canopy volume and final plant quality evaluations. Analysis of plant canopy volume and fresh weight data identified treatment differences that were not apparent in visual evaluations. These data showed that all herbicide treatments reduced growth of hydrangea. The most severe reductions in growth resulted when granular herbicides were not physically removed from the growing points before irrigation. Shaking granules from the plants before irrigation mitigated herbicide damage, but plants were still about 10 to 15% smaller than the non-treated plants. Plants treated with the spray application of Tower then irrigated were similar in size to the plants treated with Freehand and Snapshot with granules removed before irrigation. Root ratings closely paralleled canopy growth and quality evaluations and measurements, suggesting that damage to the foliage reduced root development. fresh weight (g) Comparison of 3 herbicide removal methods on hydrangea fresh weight 1000 900 800 700 600 500 400 300 200 100 0 a b c d Nontreated Shaken Irrigated Pruned Comparison of preemergence herbicide injury mitigation methods on hydrangea fresh weights, measured 10 weeks after treatment. Data are averaged across herbicides. Pruning as a method to remove herbicide damaged tissues -- effects on plant regrowth (plant fresh weights) 800 a 700 b fresh weight (g) 600 bc 500 c 400 d 300 200 100 0 Nontreated Freehand Snapshot OH2 Tower Effects of preemergence herbicides on plant regrowth after pruning (as measured by plant fresh weight, 10 weeks after treatment). Conclusions: 1. OH2 caused more injury than Freehand, Snapshot TG or Tower. This suggests that the use of PPO inhibitor herbicides, such as oxyfluorfen, have a greater likelihood of foliar damage to hydrangea than herbicides with “non-burning” modes of action. 2. Normal overhead irrigation is insufficient to remove granular herbicides from the foliage and growing points. Bud necrosis was observed in hydrangea treated with all granular herbicides tested. 3. Manually shaking plants to dislodge herbicide granules eliminated tip burn and foliar necrosis. 4. Tower herbicide applications followed immediately by overhead irrigation caused only very slight and temporary chlorosis of the growing points. 5. Plants treated with Snapshot or Freehand and shaken to remove granules or plants treated with Tower were visually similar to the non-treated plants, and all were considered marketable. However, plant canopy volumes and fresh weights were reduced by 10 to 15% compared to the non-treated. Effects of preemergence herbicides and herbicide removal strategies on Hydrangea macrophylla ‘Endless Summer’ – plant volumes (in3) and final above-ground fresh weights (g). Herbicide(s) FormDose Removal Plant Plant Plant Fresh ulation lbai/A method Volume Volume Volume weight 9/19 10/10 10/23 10/23 None na 0 na 2170.5 a 6968.8 a 5272.8 a 930.8 a None na 0 Pruned 1057.6 d 4152.0 d 3399.8 de 736.8 b dimethenamid-p + pendimethalin (Freehand) 1.75 GR 3.5 Irrigation Shaken Pruned 727.4 e 1755.3 b 591.1 ef 2890.8 ef 5835.5 b 2224.5 fg 2418.8 f 4732.0 b 2133.8 fg 624.5 c 811.8 b 542.0 cd isoxaben + trifluralin (Snapshot) 2.25 GR 5 Irrigation Shaken Pruned 737.4 e 1594.6 bc 464.9 fg 2432.3 fg 4928.3 c 2043.3 gh 2247.8 fg 3905.0 cd 1741.5 g 620.0 c 743.0 b 451.5 d oxyfluorfen + pendimethalin (OH2) 3G 3 Irrigation Shaken Pruned 656.4 e 1560.4 c 346.7 g 2369.8 fg 5470.0 bc 1446.3 h 2202.5 fg 4149.5 c 1182.3 h 521.8 d 816.8 b 294.5 e dimethenamid-p (Tower) 6 EC 1.5 Irrigation Pruned 1679.3 bc 952.6 d 5303.3 bc 3538.0 de 4220.5 bc 3078.0 e 832.8 b 620.0 c Plant canopy volume was calculated using the formula for one-half of a sphere: canopy volume = 0.5(4/3πr3), where r = the average of the height and one half of the width measured in 2 directions (in inches). Means within a column followed by the same letter are not significantly different (LSD, p = 0.05). Appendix: ARM Data Summaries Hydrangea herbicide injury avoidance comparisons Trial ID: HFL14HydrangeaPhyto Location: HFL shade Crop Name Crop Variety Part Rated Rating Date Rating Data Type Rating Unit Days After First/Last Applic. Trt-Eval Interval Trt Treatment No. Name 1 Nontreated 2 Nontreated Pruned 3 Freehand Irrigated after treatment 4 Freehand Shaken after treatment 5 Freehand Pruned after irrigation 6 Snapshot TG Irrigated after treatment 7 Snapshot TG Shaken after treatment 8 Snapshot TG Pruned after irrigation 9 OH2 Irrigated after treatment 10 OH2 Shaken after treatment 11 OH2 Pruned after irrigation 12 Tower Irrigated after treatment 13 Tower Pruned after irrigation LSD (P=.05) Standard Deviation CV Replicate F Replicate Prob(F) Treatment F Treatment Prob(F) Protocol ID: HFL12HydrangeaPhyto Study Director: Neal Investigator: Joseph C. Neal, Ph.D. Hydrangea m> Hydrangea m> Hydrangea m> Hydrangea m> Endless Sum> Endless Sum> Endless Sum> Endless Sum> Bud Bud Plant Plant 08/18/14 08/18/14 08/18/14 08/29/14 BudInjury PHYNEC PHYGEN PHYGEN 0-4 % 0-10 0-10 3 3 3 3 3 3 14 14 3 DA-A 3 DA-A 3 DA-A 14 DA-A Form Form Rate Conc Type Rate Unit 1 2 3 7 0.0 d 0.0 d 0.0 d 0.0 d 0.5 cd 0.0 d 0.0 d 0.0 d 1.75 GR 200 lb/a 2.0 b 0.0 d 1.3 c 3.3 b Hydrangea m> Endless Sum> Hydrangea m> Hydrangea m> Hydrangea m> Endless Sum> Endless Sum> Endless Sum> 09/09/14 PHYGEN 0-10 25 25 25 DA-A 09/17/14 PHYGEN 0-10 33 33 33 DA-A 09/30/14 PHYGEN 0-10 46 46 46 DA-A 10/09/14 PHYGEN 0-10 55 55 55 DA-A 10 0.0 g 0.0 g 3.8 b 13 0.0 f 0.0 f 4.3 bc 21 0.0 e 0.0 e 4.8 ab 24 0.0 e 0.0 e 4.0 b 1.75 GR 200 lb/a 0.0 d 0.0 d 0.3 d 0.8 d 0.9 f 0.5 f 0.5 e 0.8 de 1.75 GR 200 lb/a 1.8 b 2.5 d 1.8 bc 1.8 c 3.0 cd 3.3 de 3.0 c 2.0 c 2.25 GR 200 lb/a 2.0 b 3.8 d 2.0 b 3.0 b 3.5 bc 4.3 bc 4.3 b 3.8 b 2.25 GR 200 lb/a 0.5 cd 0.0 d 0.3 d 0.8 d 1.0 f 0.5 f 0.5 e 0.8 de 2.25 GR 200 lb/a 1.8 b 15.0 c 1.8 bc 2.0 c 2.8 de 4.0 cd 4.3 b 3.3 b 3 GR 100 lb/a 3.0 a 95.0 a 3.8 a 4.5 a 4.8 a 5.0 ab 4.8 ab 5.0 a 3 GR 100 lb/a 1.8 b 23.8 b 1.8 bc 3.0 b 2.3 e 3.0 e 1.8 d 1.5 cd 3 GR 100 lb/a 3.0 a 90.0 a 3.8 a 4.8 a 4.5 a 5.3 a 5.3 a 3.8 b 6 EC 32 fl oz/a 0.8 c 0.0 d 0.3 d 0.8 d 0.6 fg 0.5 f 0.5 e 0.8 de 6 EC 32 fl oz/a 0.0 d 0.0 d 0.0 d 0.5 d 0.8 f 0.8 f 0.3 e 0.0 e 0.52 0.37 28.06 5.57 3.90 22.03 0.69 0.48 37.46 0.94 0.65 34.04 0.72 0.51 23.76 0.77 0.54 22.34 0.97 0.68 29.72 0.82 0.57 29.29 0.381 0.7673 34.714 0.0001 1.434 0.2489 304.107 0.0001 0.523 0.6693 30.743 0.0001 0.838 0.4820 25.130 0.0001 1.121 0.3532 44.364 0.0001 0.422 0.7382 58.289 0.0001 1.150 0.3421 38.626 0.0001 1.631 0.1993 37.971 0.0001 Means followed by same letter do not significantly differ (P=.05, LSD) 11/21/14 (HFL14HydrangeaPhyto) AOV Means Table Page 3 of 15 North Carolina State University Crop Name Crop Variety Part Rated Rating Date Rating Data Type Rating Unit Days After First/Last Applic. Trt-Eval Interval Trt Treatment Form Form Rate No. Name Conc Type Rate Unit 1 Nontreated 2 Nontreated Pruned 3 Freehand 1.75 GR 200 lb/a Irrigated after treatment 4 Freehand 1.75 GR 200 lb/a Shaken after treatment 5 Freehand 1.75 GR 200 lb/a Pruned after irrigation 6 Snapshot TG 2.25 GR 200 lb/a Irrigated after treatment 7 Snapshot TG 2.25 GR 200 lb/a Shaken after treatment 8 Snapshot TG 2.25 GR 200 lb/a Pruned after irrigation 9 OH2 3 GR 100 lb/a Irrigated after treatment 10 OH2 3 GR 100 lb/a Shaken after treatment 11 OH2 3 GR 100 lb/a Pruned after irrigation 12 Tower 6 EC 32 fl oz/a Irrigated after treatment 13 Tower 6 EC 32 fl oz/a Pruned after irrigation LSD (P=.05) Standard Deviation CV Replicate F Replicate Prob(F) Treatment F Treatment Prob(F) Hydrangea m> Endless Sum> Hydrangea m> Endless Sum> Hydrangea m> Hydrangea m> Endless Sum> Endless Sum> Hydrangea m> Endless Sum> Hydrangea m> Hydrangea m> Endless Sum> Endless Sum> 10/23/14 PHYGEN 0-10 69 69 69 DA-A 09/17/14 QUALITY 0-10 33 33 33 DA-A 09/30/14 QUALITY 0-10 46 46 46 DA-A 10/09/14 QUALITY 0-10 55 55 55 DA-A 10/23/14 QUALITY 0-10 69 69 69 DA-A 30 0.0 d 0.0 d 2.8 ab 11 9.9 a 7.3 b 5.9 cd 17 9.8 a 7.6 c 6.0 de 22 9.8 a 8.0 cd 6.5 e 28 9.9 a 8.3 cd 6.6 e 12 3.0 a 1.0 b 0.0 c 09/17/14 Marketable # 0-3 33 33 33 DA-A 09/30/14 Marketable # 0-3 46 46 46 DA-A 18 Hydrangea m> Endless Sum> 10/09/14 Marketable # 0-3 55 55 55 DA-A 3.0 a 1.8 b 0.0 c 23 3.0 a 2.8 ab 0.0 d 1.0 cd 9.3 a 9.3 ab 9.2 ab 9.4 ab 3.0 a 3.0 a 3.0 a 2.3 bc 5.3 de 6.3 d 6.5 e 6.7 e 0.0 c 0.0 c 0.3 d 3.5 ab 5.8 d 5.9 de 6.1 e 6.2 ef 0.0 c 0.0 c 0.0 d 0.0 d 9.3 a 9.0 b 9.2 ab 9.4 ab 3.0 a 3.0 a 3.0 a 3.0 ab 5.0 e 5.8 de 6.0 ef 6.2 ef 0.0 c 0.0 c 0.0 d 3.8 a 5.1 e 5.3 ef 6.0 ef 6.2 ef 0.0 c 0.0 c 0.0 d 0.8 d 7.2 b 7.4 c 8.7 bc 8.7 bcd 0.8 b 1.3 b 2.3 bc 4.0 a 4.1 f 5.0 f 5.4 f 5.4 f 0.0 c 0.0 c 0.0 d 0.3 d 9.3 a 8.9 b 9.3 ab 9.2 abc 2.5 a 2.5 a 2.8 ab 0.5 d 6.6 bc 7.2 c 7.9 d 7.8 d 0.5 bc 0.5 c 1.8 c 1.30 0.91 54.28 1.640 0.1973 11.891 0.0001 0.71 0.50 7.23 0.164 0.9199 60.814 0.0001 0.75 0.52 7.29 0.464 0.7092 37.749 0.0001 0.69 0.48 6.37 0.699 0.5586 41.295 0.0001 0.68 0.48 45.21 0.757 0.5256 29.916 0.0001 0.72 0.51 43.79 0.402 0.7526 27.176 0.0001 Means followed by same letter do not significantly differ (P=.05, LSD) 0.87 0.61 7.94 0.809 0.4971 25.857 0.0001 0.56 0.39 27.19 0.458 0.7131 50.417 0.0001 11/21/14 (HFL14HydrangeaPhyto) AOV Means Table Page 5 of 15 North Carolina State University Crop Name Crop Variety Part Rated Rating Date Rating Data Type Rating Unit Days After First/Last Applic. Trt-Eval Interval Trt Treatment Form Form Rate No. Name Conc Type Rate Unit 1 Nontreated 2 Nontreated Pruned 3 Freehand 1.75 GR 200 lb/a Irrigated after treatment 4 Freehand 1.75 GR 200 lb/a Shaken after treatment 5 Freehand 1.75 GR 200 lb/a Pruned after irrigation 6 Snapshot TG 2.25 GR 200 lb/a Irrigated after treatment 7 Snapshot TG 2.25 GR 200 lb/a Shaken after treatment 8 Snapshot TG 2.25 GR 200 lb/a Pruned after irrigation 9 OH2 3 GR 100 lb/a Irrigated after treatment 10 OH2 3 GR 100 lb/a Shaken after treatment 11 OH2 3 GR 100 lb/a Pruned after irrigation 12 Tower 6 EC 32 fl oz/a Irrigated after treatment 13 Tower 6 EC 32 fl oz/a Pruned after irrigation LSD (P=.05) Standard Deviation CV Replicate F Replicate Prob(F) Treatment F Treatment Prob(F) Hydrangea m> Endless Sum> Hydrangea m> Endless Sum> 10/23/14 Marketable # 0-3 69 69 55 DA-A 09/19/14 VOLUME CU IN 35 35 35 DA-A 29 3.0 a 2.5 abc 0.8 d Hydrangea m> Hydrangea m> Endless Sum> Endless Sum> 10/10/14 VOLUME CU IN 56 56 56 DA-A Hydrangea m> Endless Sum> Hydrangea m> Endless Sum> 10/23/14 VOLUME CU IN 69 69 69 DA-A 10/23/14 ROOT 0-5 69 69 69 DA-A 10/23/14 WEIFRE G 69 69 69 DA-A 16 6511.3 a 3172.8 d 2182.1 e 27 6968.8 a 4152.0 d 2890.8 ef 32 5272.8 a 3399.8 de 2418.8 f 31 4.9 a 4.3 ab 4.4 ab 33 930.8 a 736.8 b 624.5 c 3.0 a 5266.0 b 5835.5 b 4732.0 b 4.8 a 811.8 b 0.3 de 1773.1 ef 2224.5 fg 2133.8 fg 3.7 c 542.0 cd 0.3 de 2212.1 e 2432.3 fg 2247.8 fg 3.9 bc 620.0 c 3.0 a 4783.9 bc 4928.3 c 3905.0 cd 4.9 a 743.0 b 0.0 e 1394.8 fg 2043.3 gh 1741.5 g 3.6 cd 451.5 d 0.3 de 1969.1 e 2369.8 fg 2202.5 fg 3.9 bc 521.8 d 2.3 bc 4681.1 c 5470.0 bc 4149.5 c 4.3 ab 816.8 b 0.0 e 1040.0 g 1446.3 h 1182.3 h 3.0 d 294.5 e 2.8 ab 5038.0 bc 5303.3 bc 4220.5 bc 4.9 a 832.8 b 2.0 c 2857.8 d 3538.0 de 3078.0 e 4.3 ab 620.0 c 0.63 0.44 28.74 0.787 0.5091 33.852 0.0001 Means followed by same letter do not significantly differ (P=.05, LSD) 538.38 376.74 11.42 2.131 0.1134 86.408 0.0001 766.58 536.42 14.06 6.660 0.0011 42.336 0.0001 534.63 374.11 11.95 3.475 0.0258 45.063 0.0001 0.65 0.39 9.13 0.480 0.6244 7.064 0.0001 97.79 68.43 10.41 1.241 0.3090 26.911 0.0001 11/21/14 (HFL14HydrangeaPhyto) Plot Data Summary Page 6 of 17 North Carolina State University Hydrangea herbicide injury avoidance comparisons Trial ID: HFL14HydrangeaPhyto Location: HFL shade Crop Name Crop Variety Description Part Rated Rating Date Rating Data Type Rating Unit Days After First/Last Applic. Trt-Eval Interval Trt Treatment No. Name 1 Nontreated Protocol ID: HFL12HydrangeaPhyto Study Director: Neal Investigator: Joseph C. Neal, Ph.D. Hydrangea m> Hydrangea m> Hydrangea m> Hydrangea m> Endless Sum> Endless Sum> Endless Sum> Endless Sum> Bud 08/18/14 PHYNEC 0-3 3 3 3 DA-A Form Form Rate Conc Type Rate Unit 2 Nontreated Pruned 3 Freehand Irrigated after treatment 1.75 GR 200 lb/a 4 Freehand Shaken after treatment 1.75 GR 200 lb/a 5 Freehand Pruned after irrigation 1.75 GR 200 lb/a 6 Snapshot TG Irrigated after treatment 2.25 GR 200 lb/a 7 Snapshot TG Shaken after treatment 2.25 GR 200 lb/a Plot 108 202 304 408 1 Bud 08/18/14 PHYNEC % 3 3 3 DA-A 2 Plant 08/18/14 PHYGEN 0-10 3 3 3 DA-A 3 Plant 08/29/14 PHYGEN 0-10 14 14 14 DA-A 7 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 Mean = 107 210 303 404 0.0 0.0 1.0 0.0 1.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 Mean = 112 208 306 402 0.5 2.0 2.0 2.0 2.0 0.0 0.0 0.0 0.0 0.0 0.0 1.0 1.0 1.0 2.0 0.0 3.0 3.0 4.0 3.0 Mean = 105 212 309 411 2.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 1.3 1.0 0.0 0.0 0.0 3.3 2.0 1.0 0.0 0.0 Mean = 106 209 305 412 0.0 2.0 2.0 1.0 2.0 0.0 0.0 10.0 0.0 0.0 0.3 2.0 2.0 1.0 2.0 0.8 2.0 2.0 2.0 1.0 Mean = 110 213 311 410 1.8 2.0 2.0 2.0 2.0 2.5 5.0 10.0 0.0 0.0 1.8 2.0 2.0 2.0 2.0 1.8 4.0 3.0 3.0 2.0 Mean = 102 204 301 407 2.0 0.0 1.0 1.0 0.0 3.8 0.0 0.0 0.0 0.0 2.0 1.0 0.0 0.0 0.0 3.0 1.0 0.0 1.0 1.0 Mean = 0.5 0.0 0.3 0.8 11/21/14 (HFL14HydrangeaPhyto) Plot Data Summary Page 7 of 17 North Carolina State University Crop Name Crop Variety Description Part Rated Rating Date Rating Data Type Rating Unit Days After First/Last Applic. Trt-Eval Interval Trt Treatment No. Name 8 Snapshot TG Pruned after irrigation Hydrangea m> Hydrangea m> Hydrangea m> Hydrangea m> Endless Sum> Endless Sum> Endless Sum> Endless Sum> Bud 08/18/14 PHYNEC 0-3 3 3 3 DA-A Form Form Rate Conc Type Rate Unit 2.25 GR 200 lb/a Plot 109 201 302 413 1 Bud 08/18/14 PHYNEC % 3 3 3 DA-A 2 Plant 08/18/14 PHYGEN 0-10 3 3 3 DA-A 3 Plant 08/29/14 PHYGEN 0-10 14 14 14 DA-A 7 2.0 2.0 2.0 1.0 20.0 20.0 10.0 10.0 2.0 2.0 2.0 1.0 2.0 1.0 3.0 2.0 Mean = 103 207 313 405 1.8 3.0 3.0 3.0 3.0 15.0 100.0 100.0 90.0 90.0 1.8 4.0 4.0 4.0 3.0 2.0 4.0 5.0 5.0 4.0 Mean = 111 205 312 401 3.0 2.0 1.0 2.0 2.0 95.0 20.0 20.0 25.0 30.0 3.8 1.0 1.0 3.0 2.0 4.5 3.0 4.0 3.0 2.0 Mean = 104 203 310 406 1.8 3.0 3.0 3.0 3.0 23.8 90.0 90.0 100.0 80.0 1.8 4.0 3.0 4.0 4.0 3.0 5.0 5.0 5.0 4.0 Mean = 32 fl oz/a 113 211 307 403 3.0 0.0 1.0 1.0 1.0 90.0 0.0 0.0 0.0 0.0 3.8 0.0 0.0 0.0 1.0 4.8 0.0 0.0 1.0 2.0 Mean = 32 fl oz/a 101 206 308 409 0.8 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.3 0.0 0.0 0.0 0.0 0.8 0.0 1.0 0.0 1.0 Mean = 0.0 0.0 0.0 0.5 9 OH2 Irrigated after treatment 3 GR 100 lb/a 10 OH2 Shaken after treatment 3 GR 100 lb/a 11 OH2 Pruned after irrigation 3 GR 100 lb/a 12 Tower Irrigated after treatment 6 EC 13 Tower Pruned after irrigation 6 EC 11/21/14 (HFL14HydrangeaPhyto) Plot Data Summary Page 8 of 17 North Carolina State University Crop Name Crop Variety Description Part Rated Rating Date Rating Data Type Rating Unit Days After First/Last Applic. Trt-Eval Interval Trt Treatment No. Name 1 Nontreated Hydrangea m> Hydrangea m> Hydrangea m> Hydrangea m> Endless Sum> Endless Sum> Endless Sum> Endless Sum> combined combined combined Form Form Rate Conc Type Rate Unit 2 Nontreated Pruned 3 Freehand Irrigated after treatment 1.75 GR 200 lb/a 4 Freehand Shaken after treatment 1.75 GR 200 lb/a 5 Freehand Pruned after irrigation 1.75 GR 200 lb/a 6 Snapshot TG Irrigated after treatment 2.25 GR 200 lb/a 7 Snapshot TG Shaken after treatment 2.25 GR 200 lb/a 8 Snapshot TG Pruned after irrigation 2.25 GR 200 lb/a Plot 108 202 304 408 09/09/14 PHYGEN 0-10 25 25 25 DA-A 09/17/14 PHYGEN 0-10 33 33 33 DA-A 09/30/14 PHYGEN 0-10 46 46 46 DA-A 10/09/14 PHYGEN 0-10 55 55 55 DA-A 10 13 21 24 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 Mean = 107 210 303 404 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 Mean = 112 208 306 402 0.0 4.0 3.0 4.0 4.0 0.0 5.0 4.0 4.0 4.0 0.0 5.0 4.0 5.0 5.0 0.0 4.0 4.0 3.0 5.0 Mean = 105 212 309 411 3.8 1.5 1.0 0.0 1.0 4.3 1.0 1.0 0.0 0.0 4.8 1.0 1.0 0.0 0.0 4.0 2.0 0.0 1.0 0.0 Mean = 106 209 305 412 0.9 3.0 3.0 3.0 3.0 0.5 4.0 3.0 3.0 3.0 0.5 4.0 2.0 2.0 4.0 0.8 3.0 2.0 1.0 2.0 Mean = 110 213 311 410 3.0 4.0 4.0 3.0 3.0 3.3 5.0 4.0 4.0 4.0 3.0 4.0 5.0 5.0 3.0 2.0 4.0 4.0 4.0 3.0 Mean = 102 204 301 407 3.5 1.0 0.0 1.5 1.5 4.3 0.0 0.0 1.0 1.0 4.3 0.0 0.0 1.0 1.0 3.8 0.0 1.0 1.0 1.0 Mean = 109 201 302 413 1.0 3.0 2.0 3.0 3.0 0.5 4.0 3.0 4.0 5.0 0.5 4.0 4.0 4.0 5.0 0.8 4.0 2.0 3.0 4.0 Mean = 2.8 4.0 4.3 3.3 11/21/14 (HFL14HydrangeaPhyto) Plot Data Summary Page 9 of 17 North Carolina State University Crop Name Crop Variety Description Part Rated Rating Date Rating Data Type Rating Unit Days After First/Last Applic. Trt-Eval Interval Trt Treatment Form Form Rate No. Name Conc Type Rate Unit 9 OH2 3 GR 100 lb/a Irrigated after treatment Hydrangea m> Hydrangea m> Hydrangea m> Hydrangea m> Endless Sum> Endless Sum> Endless Sum> Endless Sum> combined combined combined Plot 103 207 313 405 09/09/14 PHYGEN 0-10 25 25 25 DA-A 09/17/14 PHYGEN 0-10 33 33 33 DA-A 09/30/14 PHYGEN 0-10 46 46 46 DA-A 10/09/14 PHYGEN 0-10 55 55 55 DA-A 10 13 21 24 5.0 5.0 5.0 4.0 5.0 6.0 5.0 4.0 5.0 5.0 5.0 4.0 5.0 5.0 5.0 5.0 Mean = 111 205 312 401 4.8 3.0 2.0 2.0 2.0 5.0 3.0 3.0 3.0 3.0 4.8 2.0 0.0 2.0 3.0 5.0 1.0 1.0 2.0 2.0 Mean = 104 203 310 406 2.3 5.0 4.0 4.0 5.0 3.0 5.0 5.0 6.0 5.0 1.8 5.0 5.0 6.0 5.0 1.5 4.0 3.0 4.0 4.0 Mean = 32 fl oz/a 113 211 307 403 4.5 0.0 0.0 1.5 1.0 5.3 0.0 0.0 1.0 1.0 5.3 0.0 0.0 1.0 1.0 3.8 1.0 0.0 1.0 1.0 Mean = 32 fl oz/a 101 206 308 409 0.6 0.0 1.0 1.0 1.0 0.5 1.0 1.0 0.0 1.0 0.5 0.0 0.0 0.0 1.0 0.8 0.0 0.0 0.0 0.0 Mean = 0.8 0.8 0.3 0.0 10 OH2 Shaken after treatment 3 GR 100 lb/a 11 OH2 Pruned after irrigation 3 GR 100 lb/a 12 Tower Irrigated after treatment 6 EC 13 Tower Pruned after irrigation 6 EC 11/21/14 (HFL14HydrangeaPhyto) Plot Data Summary Page 10 of 17 North Carolina State University Crop Name Crop Variety Description Part Rated Rating Date Rating Data Type Rating Unit Days After First/Last Applic. Trt-Eval Interval Trt Treatment No. Name 1 Nontreated Hydrangea m> Hydrangea m> Hydrangea m> Hydrangea m> Endless Sum> Endless Sum> Endless Sum> Endless Sum> combined Form Form Rate Conc Type Rate Unit 2 Nontreated Pruned 3 Freehand Irrigated after treatment 1.75 GR 200 lb/a 4 Freehand Shaken after treatment 1.75 GR 200 lb/a 5 Freehand Pruned after irrigation 1.75 GR 200 lb/a 6 Snapshot TG Irrigated after treatment 2.25 GR 200 lb/a 7 Snapshot TG Shaken after treatment 2.25 GR 200 lb/a 8 Snapshot TG Pruned after irrigation 2.25 GR 200 lb/a Plot 108 202 304 408 10/23/14 PHYGEN 0-10 69 69 69 DA-A 09/17/14 QUALITY 0-10 33 33 33 DA-A 09/30/14 QUALITY 0-10 46 46 46 DA-A 10/09/14 QUALITY 0-10 55 55 55 DA-A 30 11 17 22 0.0 0.0 0.0 0.0 10.0 9.7 10.0 10.0 9.3 9.7 10.0 10.0 9.3 10.0 10.0 10.0 Mean = 107 210 303 404 0.0 0.0 0.0 0.0 0.0 9.9 7.0 6.7 7.7 7.7 9.8 7.7 7.3 7.7 7.7 9.8 8.0 7.7 8.3 8.0 Mean = 112 208 306 402 0.0 3.0 3.0 1.0 4.0 7.3 6.0 6.0 6.3 5.3 7.6 6.0 6.3 6.3 5.3 8.0 6.3 6.7 7.0 6.0 Mean = 105 212 309 411 2.8 4.0 0.0 0.0 0.0 5.9 8.7 9.3 9.7 9.3 6.0 8.7 9.3 9.7 9.3 6.5 8.7 9.0 9.7 9.3 Mean = 106 209 305 412 1.0 3.0 1.0 3.0 2.0 9.3 5.3 5.3 5.0 5.7 9.3 6.3 6.3 6.7 5.7 9.2 6.7 6.3 7.0 6.0 Mean = 110 213 311 410 2.3 4.0 4.0 4.0 2.0 5.3 6.3 5.7 5.0 6.3 6.3 5.7 6.0 5.3 6.7 6.5 5.7 6.0 6.0 6.7 Mean = 102 204 301 407 3.5 0.0 0.0 0.0 0.0 5.8 9.7 9.0 8.7 9.7 5.9 9.0 9.0 8.7 9.3 6.1 9.3 9.3 9.0 9.3 Mean = 109 201 302 413 0.0 4.0 2.0 3.0 3.0 9.3 4.7 5.7 5.3 4.3 9.0 6.0 6.0 6.0 5.3 9.2 6.3 6.0 6.3 5.3 Mean = 3.0 5.0 5.8 6.0 11/21/14 (HFL14HydrangeaPhyto) Plot Data Summary Page 11 of 17 North Carolina State University Crop Name Crop Variety Description Part Rated Rating Date Rating Data Type Rating Unit Days After First/Last Applic. Trt-Eval Interval Trt Treatment Form Form Rate No. Name Conc Type Rate Unit 9 OH2 3 GR 100 lb/a Irrigated after treatment Hydrangea m> Hydrangea m> Hydrangea m> Hydrangea m> Endless Sum> Endless Sum> Endless Sum> Endless Sum> combined Plot 103 207 313 405 10/23/14 PHYGEN 0-10 69 69 69 DA-A 09/17/14 QUALITY 0-10 33 33 33 DA-A 09/30/14 QUALITY 0-10 46 46 46 DA-A 10/09/14 QUALITY 0-10 55 55 55 DA-A 30 11 17 22 5.0 4.0 4.0 2.0 5.3 4.7 4.7 5.7 5.3 5.0 5.0 6.0 6.0 5.7 6.0 6.3 Mean = 111 205 312 401 3.8 0.0 0.0 1.0 2.0 5.1 7.3 7.3 7.3 6.7 5.3 7.0 8.0 7.3 7.3 6.0 9.3 9.3 8.3 7.7 Mean = 104 203 310 406 0.8 4.0 4.0 4.0 4.0 7.2 4.3 4.0 4.3 3.7 7.4 4.7 5.7 4.7 5.0 8.7 5.3 6.3 4.7 5.3 Mean = 32 fl oz/a 113 211 307 403 4.0 0.0 0.0 0.0 1.0 4.1 9.7 10.0 8.3 9.0 5.0 9.7 9.7 8.0 8.0 5.4 9.3 10.0 8.7 9.0 Mean = 32 fl oz/a 101 206 308 409 0.3 1.0 1.0 0.0 0.0 9.3 6.7 6.3 7.3 6.0 8.9 6.7 6.7 8.3 7.0 9.3 8.0 7.3 8.7 7.7 Mean = 0.5 6.6 7.2 7.9 10 OH2 Shaken after treatment 3 GR 100 lb/a 11 OH2 Pruned after irrigation 3 GR 100 lb/a 12 Tower Irrigated after treatment 6 EC 13 Tower Pruned after irrigation 6 EC 11/21/14 (HFL14HydrangeaPhyto) Plot Data Summary Page 12 of 17 North Carolina State University Crop Name Crop Variety Description Part Rated Rating Date Rating Data Type Rating Unit Days After First/Last Applic. Trt-Eval Interval Trt Treatment No. Name 1 Nontreated Hydrangea m> Hydrangea m> Hydrangea m> Hydrangea m> Endless Sum> Endless Sum> Endless Sum> Endless Sum> 10/23/14 QUALITY 0-10 69 69 69 DA-A Form Form Rate Conc Type Rate Unit 2 Nontreated Pruned 3 Freehand Irrigated after treatment 1.75 GR 200 lb/a 4 Freehand Shaken after treatment 1.75 GR 200 lb/a 5 Freehand Pruned after irrigation 1.75 GR 200 lb/a 6 Snapshot TG Irrigated after treatment 2.25 GR 200 lb/a 7 Snapshot TG Shaken after treatment 2.25 GR 200 lb/a 8 Snapshot TG Pruned after irrigation 2.25 GR 200 lb/a Plot 108 202 304 408 28 09/17/14 Marketable # 0-3 33 33 33 DA-A 12 09/30/14 Marketable # 0-3 46 46 46 DA-A 18 10/09/14 Marketable # 0-3 55 55 55 DA-A 23 10.0 10.0 10.0 9.7 3.0 3.0 3.0 3.0 3.0 3.0 3.0 3.0 3.0 3.0 3.0 3.0 Mean = 107 210 303 404 9.9 7.7 8.0 9.0 8.7 3.0 0.0 0.0 2.0 2.0 3.0 2.0 1.0 2.0 2.0 3.0 3.0 2.0 3.0 3.0 Mean = 112 208 306 402 8.3 6.7 7.0 7.0 5.7 1.0 0.0 0.0 0.0 0.0 1.8 0.0 0.0 0.0 0.0 2.8 0.0 0.0 0.0 0.0 Mean = 105 212 309 411 6.6 8.7 9.7 9.7 9.7 0.0 3.0 3.0 3.0 3.0 0.0 3.0 3.0 3.0 3.0 0.0 3.0 3.0 3.0 3.0 Mean = 106 209 305 412 9.4 6.3 6.7 6.7 7.0 3.0 0.0 0.0 0.0 0.0 3.0 0.0 0.0 0.0 0.0 3.0 0.0 0.0 1.0 0.0 Mean = 110 213 311 410 6.7 6.0 5.7 6.0 7.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.3 0.0 0.0 0.0 0.0 Mean = 102 204 301 407 6.2 9.7 9.0 9.3 9.7 0.0 3.0 3.0 3.0 3.0 0.0 3.0 3.0 3.0 3.0 0.0 3.0 3.0 3.0 3.0 Mean = 109 201 302 413 9.4 5.7 6.7 6.7 5.7 3.0 0.0 0.0 0.0 0.0 3.0 0.0 0.0 0.0 0.0 3.0 0.0 0.0 0.0 0.0 Mean = 6.2 0.0 0.0 0.0 11/21/14 (HFL14HydrangeaPhyto) Plot Data Summary Page 13 of 17 North Carolina State University Crop Name Crop Variety Description Part Rated Rating Date Rating Data Type Rating Unit Days After First/Last Applic. Trt-Eval Interval Trt Treatment Form Form Rate No. Name Conc Type Rate Unit 9 OH2 3 GR 100 lb/a Irrigated after treatment Hydrangea m> Hydrangea m> Hydrangea m> Hydrangea m> Endless Sum> Endless Sum> Endless Sum> Endless Sum> 10/23/14 QUALITY 0-10 69 69 69 DA-A Plot 103 207 313 405 28 09/17/14 Marketable # 0-3 33 33 33 DA-A 12 09/30/14 Marketable # 0-3 46 46 46 DA-A 18 10/09/14 Marketable # 0-3 55 55 55 DA-A 23 5.3 6.3 5.3 7.7 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 Mean = 111 205 312 401 6.2 9.3 9.7 7.7 8.0 0.0 1.0 1.0 1.0 0.0 0.0 0.0 3.0 1.0 1.0 0.0 3.0 3.0 2.0 1.0 Mean = 104 203 310 406 8.7 5.3 6.0 5.0 5.3 0.8 0.0 0.0 0.0 0.0 1.3 0.0 0.0 0.0 0.0 2.3 0.0 0.0 0.0 0.0 Mean = 32 fl oz/a 113 211 307 403 5.4 9.3 10.0 8.3 9.0 0.0 3.0 3.0 2.0 2.0 0.0 3.0 3.0 2.0 2.0 0.0 3.0 3.0 2.0 3.0 Mean = 32 fl oz/a 101 206 308 409 9.2 8.0 7.7 8.0 7.7 2.5 0.0 0.0 2.0 0.0 2.5 0.0 0.0 2.0 0.0 2.8 2.0 1.0 2.0 2.0 Mean = 7.8 0.5 0.5 1.8 10 OH2 Shaken after treatment 3 GR 100 lb/a 11 OH2 Pruned after irrigation 3 GR 100 lb/a 12 Tower Irrigated after treatment 6 EC 13 Tower Pruned after irrigation 6 EC 11/21/14 (HFL14HydrangeaPhyto) Plot Data Summary Page 14 of 17 North Carolina State University Crop Name Crop Variety Description Part Rated Rating Date Rating Data Type Rating Unit Days After First/Last Applic. Trt-Eval Interval Trt Treatment No. Name 1 Nontreated Hydrangea m> Hydrangea m> Hydrangea m> Hydrangea m> Endless Sum> Endless Sum> Endless Sum> Endless Sum> 10/23/14 Marketable # 0-3 69 69 55 DA-A 09/19/14 VOLUME CU IN 35 35 35 DA-A 10/10/14 VOLUME CU IN 56 56 56 DA-A 10/23/14 VOLUME CU IN 69 69 69 DA-A 3.0 3.0 3.0 3.0 16 6268.4 6631.7 6548.3 6596.7 27 5915.0 7539.0 7789.0 6632.0 32 4607.0 5487.0 5861.0 5136.0 Mean = 107 210 303 404 3.0 2.0 2.0 3.0 3.0 6511.3 2849.8 3166.2 3652.8 3022.5 6968.8 3063.0 3831.0 4974.0 4740.0 5272.8 2984.0 3387.0 3444.0 3784.0 Mean = 112 208 306 402 2.5 1.0 1.0 1.0 0.0 3172.8 1865.9 2398.6 2462.0 2001.8 4152.0 2253.0 3465.0 3374.0 2471.0 3399.8 2267.0 2519.0 2741.0 2148.0 Mean = 105 212 309 411 0.8 3.0 3.0 3.0 3.0 2182.1 4271.6 5742.6 5351.1 5698.5 2890.8 4436.0 6553.0 5758.0 6595.0 2418.8 3654.0 5486.0 4882.0 4906.0 Mean = 106 209 305 412 3.0 0.0 0.0 0.0 1.0 5266.0 1625.1 1825.1 1948.8 1693.4 5835.5 1766.0 2344.0 2776.0 2012.0 4732.0 1763.0 2051.0 2786.0 1935.0 Mean = 110 213 311 410 0.3 1.0 0.0 0.0 0.0 1773.1 1632.3 2484.2 2187.8 2544.0 2224.5 1902.0 2437.0 2287.0 3103.0 2133.8 2006.0 2067.0 2287.0 2631.0 Mean = 102 204 301 407 0.3 3.0 3.0 3.0 3.0 2212.1 5058.4 4655.5 4805.7 4615.8 2432.3 5029.0 5029.0 4924.0 4731.0 2247.8 3828.0 4114.0 3439.0 4239.0 Mean = 109 201 302 413 3.0 0.0 0.0 0.0 0.0 4783.9 1319.6 1406.2 1436.0 1417.3 4928.3 1806.0 2012.0 2532.0 1823.0 3905.0 1563.0 1797.0 1876.0 1730.0 Mean = 0.0 1394.8 2043.3 1741.5 Form Form Rate Conc Type Rate Unit 2 Nontreated Pruned 3 Freehand Irrigated after treatment 1.75 GR 200 lb/a 4 Freehand Shaken after treatment 1.75 GR 200 lb/a 5 Freehand Pruned after irrigation 1.75 GR 200 lb/a 6 Snapshot TG Irrigated after treatment 2.25 GR 200 lb/a 7 Snapshot TG Shaken after treatment 2.25 GR 200 lb/a 8 Snapshot TG Pruned after irrigation 2.25 GR 200 lb/a Plot 108 202 304 408 29 11/21/14 (HFL14HydrangeaPhyto) Plot Data Summary Page 15 of 17 North Carolina State University Crop Name Crop Variety Description Part Rated Rating Date Rating Data Type Rating Unit Days After First/Last Applic. Trt-Eval Interval Trt Treatment Form Form Rate No. Name Conc Type Rate Unit 9 OH2 3 GR 100 lb/a Irrigated after treatment Hydrangea m> Hydrangea m> Hydrangea m> Hydrangea m> Endless Sum> Endless Sum> Endless Sum> Endless Sum> 09/19/14 VOLUME CU IN 35 35 35 DA-A 10/10/14 VOLUME CU IN 56 56 56 DA-A 10/23/14 VOLUME CU IN 69 69 69 DA-A 0.0 0.0 0.0 1.0 16 1666.5 1722.6 1669.6 2817.6 27 1746.0 2580.0 1968.0 3185.0 32 1797.0 1980.0 1911.0 3122.0 Mean = 111 205 312 401 0.3 3.0 3.0 1.0 2.0 1969.1 5001.7 4883.5 4731.2 4107.8 2369.8 5282.0 6003.0 5593.0 5002.0 2202.5 4360.0 4212.0 4201.0 3825.0 Mean = 104 203 310 406 2.3 0.0 0.0 0.0 0.0 4681.1 934.3 1144.8 1055.0 1025.9 5470.0 995.0 1576.0 1368.0 1846.0 4149.5 1099.0 1111.0 1151.0 1368.0 Mean = 32 fl oz/a 113 211 307 403 0.0 3.0 3.0 2.0 3.0 1040.0 5239.8 5866.2 4757.2 4288.7 1446.3 4997.0 6742.0 4757.0 4717.0 1182.3 4335.0 4657.0 3979.0 3911.0 Mean = 32 fl oz/a 101 206 308 409 2.8 2.0 2.0 2.0 2.0 5038.0 2613.4 2967.3 3306.4 2544.0 5303.3 3228.0 3423.0 4219.0 3282.0 4220.5 2650.0 3029.0 3462.0 3171.0 Mean = 2.0 2857.8 3538.0 3078.0 10 OH2 Shaken after treatment 3 GR 100 lb/a 11 OH2 Pruned after irrigation 3 GR 100 lb/a 12 Tower Irrigated after treatment 6 EC 13 Tower Pruned after irrigation 6 EC 10/23/14 Marketable # 0-3 69 69 55 DA-A Plot 103 207 313 405 29 11/21/14 (HFL14HydrangeaPhyto) Plot Data Summary Page 16 of 17 North Carolina State University Crop Name Crop Variety Description Part Rated Rating Date Rating Data Type Rating Unit Days After First/Last Applic. Trt-Eval Interval Trt Treatment No. Name 1 Nontreated Hydrangea m> Hydrangea m> Endless Sum> Endless Sum> combined 3 plants Form Form Rate Conc Type Rate Unit 2 Nontreated Pruned 3 Freehand Irrigated after treatment 1.75 GR 200 lb/a 4 Freehand Shaken after treatment 1.75 GR 200 lb/a 5 Freehand Pruned after irrigation 1.75 GR 200 lb/a 6 Snapshot TG Irrigated after treatment 2.25 GR 200 lb/a 7 Snapshot TG Shaken after treatment 2.25 GR 200 lb/a 8 Snapshot TG Pruned after irrigation 2.25 GR 200 lb/a Plot 108 202 304 408 10/23/14 ROOT 0-5 69 69 69 DA-A 10/23/14 WEIFRE G 69 69 69 DA-A 31 33 . 4.7 5.0 5.0 920.0 901.0 942.0 960.0 Mean = 107 210 303 404 4.9 . 4.7 4.3 4.0 930.8 627.0 700.0 906.0 714.0 Mean = 112 208 306 402 4.3 . 4.7 4.7 4.0 736.8 545.0 696.0 686.0 571.0 Mean = 105 212 309 411 4.4 . 5.0 4.7 4.7 624.5 781.0 840.0 896.0 730.0 Mean = 106 209 305 412 4.8 . 3.7 4.0 3.3 811.8 563.0 587.0 551.0 467.0 Mean = 110 213 311 410 3.7 . 4.3 3.3 4.0 542.0 559.0 646.0 589.0 686.0 Mean = 102 204 301 407 3.9 . 4.7 5.0 5.0 620.0 679.0 758.0 815.0 720.0 Mean = 109 201 302 413 4.9 . 3.3 3.7 3.7 743.0 414.0 479.0 495.0 418.0 Mean = 3.6 451.5 11/21/14 (HFL14HydrangeaPhyto) Plot Data Summary Page 17 of 17 North Carolina State University Crop Name Crop Variety Description Part Rated Rating Date Rating Data Type Rating Unit Days After First/Last Applic. Trt-Eval Interval Trt Treatment Form Form Rate No. Name Conc Type Rate Unit 9 OH2 3 GR 100 lb/a Irrigated after treatment Hydrangea m> Hydrangea m> Endless Sum> Endless Sum> combined 3 plants Plot 103 207 313 405 10/23/14 ROOT 0-5 69 69 69 DA-A 10/23/14 WEIFRE G 69 69 69 DA-A 31 33 . 3.7 3.3 4.7 467.0 484.0 500.0 636.0 Mean = 111 205 312 401 3.9 . 4.0 4.3 4.7 521.8 896.0 775.0 720.0 876.0 Mean = 104 203 310 406 4.3 . 3.3 3.0 2.7 816.8 262.0 319.0 296.0 301.0 Mean = 32 fl oz/a 113 211 307 403 3.0 . 5.0 5.0 4.7 294.5 901.0 940.0 748.0 742.0 Mean = 32 fl oz/a 101 206 308 409 4.9 . 5.0 4.0 4.0 832.8 600.0 664.0 610.0 606.0 Mean = 4.3 620.0 10 OH2 Shaken after treatment 3 GR 100 lb/a 11 OH2 Pruned after irrigation 3 GR 100 lb/a 12 Tower Irrigated after treatment 6 EC 13 Tower Pruned after irrigation 6 EC
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