Suspended Core Microstructured Polymer Optical Fibre: Connecting to Reality Richard Lwin1,2, Geoff Barton2, Trungta Keawfanapadol2, Maryanne Large1, Leon Poladian3, Roger Tanner3, Martijn van Eijkelenborg1, and Shicheng Xue3 1. Optical Fibre Technology Centre, Australian Photonics CRC, University of Sydney, 206 National Innovation Centre, Australian Technology Park, Eveleigh NSW 1430, Australia, Phone: +61 (02) 9351 1929, Fax: +61 (02) 93511911, [email protected] 2. School of Chemical Engineering, University of Sydney NSW, Australia 3. School of Mathematics and Statistics, University of Sydney NSW, Australia 4. School of Aerospace, Mechanical and Mechatronics Engineering, University of Sydney NSW, Australia Abstract We use Suspended Core mPOF to experimentally test rheological predictions, and optically characterize fibres in terms of numerical aperture and loss. This fibre has thin bridges supporting the core, which help produce high NA, and low loss. We have obtained our lowest loss to date with this design at 0.2dB/m – a figure competitive with conventional POF. Introduction: Microstructured Polymer Optical Fibres (mPOFs), [1]-[3] are rapidly developing as alternative to conventional polymer optical fibre. They are potentially, cheaper and simpler to make, and offer a wide variety of new optical properties through tailorising the hole structure. The draw process for these fibres however is critical, because deformation of the hole structure can lead to a change in the optical properties. In order to study this, and allow a comparision of theoretical and experimental results, we chose to fabricate simple Suspended Core or ‘Grapefruit’ fibres (Figure 1). The simplicity of this structure makes it ideal for 3D viscoelastic rheological hole deformation analysis during the necking down to fibre [4]. This has been important to fabrication, since a calibrated rheological computational model of the draw process is required, in the aim to understand and predict the behaviour of hole deformation and hence determine the initial hole array drilled in the preform for a desired microstructure. The optical properties of such fibres have also been studied theoretically [5] and their large holes make them ideal for microfluidics and bio-sensing applications [6]. This paper will reveal the development of Suspended Core mPOF, from the challenges during fabrication, to the acceptance of the 3D rheological model. Fabrication Challenge: Suspended Core mPOF consists of a straightforward array of large holes with thin bridges, which is structurally weak for fabrication, since the large air fraction leads to the natural tendency for the microstructure to collapse due to surface tension and viscous forces [4]. Also the close proximity of the large holes lends itself to a high degree of hole size and shape deformation. Initial Suspended Core mPOFs were drawn Figure 1: SEM images of Suspended Core mPOFs. a) Left fibre from old convective heating tower. b) Right fibre from new radiative heating tower. in the convective heating draw tower, which was unable to give radially isothermal heating [7]. The large air fraction only heightened the temperature gradient, by insulating the core and thus restricting deformation. The Scanning Electron Microscope (SEM) image in Figure 1a shows holes still close to circular and the bridges only moderately thinning. Suspended Core mPOF drawn in the new commercial draw tower uses radiative IR heating, which produces a uniform temperature profile in the radial direction. With higher temperature at the core, more substantial hole structure deformation is experienced, resulting in hole expansion and bridge thinning (Figure 1b). Table 1 lists the bridge thickness for 400µm fibre drawn from both towers, revealing the bridges for the new tower around 3 times thinner. In some cases sleeving of the fibre has been used to increase the outer diameter [3]. Modeling Microstructure Behaviour: Recent investigation of mPOFs has centered at the behavior of the hole structure deformation as the preform transforms into fibre in the neckdown region [4]. A computational finite element analysis program, PolyFlow, has been used to predict both the neckdown profile and the various forms of hole deformation, due to complicated interactions between optimised fabrication conditions to the non-linear viscoelastic polymer properties. Figure 2: PolyFlow model of Suspended Core The uniform radial temperature profile associated with the radiative heating means a radially isothermal profile – a more accurate axial temperature profile of the furnace will be incorporated in later models. The isothermal profile greatly improves the computational efficiency, yet is still capable of determining the degree of deformation accurately. As seen in Figure 2 and comparing against Figure 1b, employing an isothermal profile to the Suspended Core mPOF model, agrees qualitatively well to the real fibre hole deformation due to radiative heating. Optical Performance: The large air fraction gives Suspended Core mPOFs the potential of exceptional loss and NA performance. For loss, the thin bridges reduce leakage through confinement losses to a minimal value. Thin bridges are expected to create high NA. However it should be noted that the NA for the simulation models consisted of bridges shaped as rectangular guides [5], rather than the circular hole profile associated with Suspended Core mPOFs. Suspended Core mPOFs produced from the convective heating tower had relatively thick bridges, so confinement losses became the dominant mechanism. By contrast, the fibre from the new tower had much thinner and straighter bridges, hence restricting confinement losses. Figure 3 shows the loss from the new tower being substantially lower than from the old tower. As indicated in Table 1, the loss for the new tower is over 20 times better than that of the old tower at 650nm. However it is interesting to note that slight increase in bridge thickness for fibre of around 12% can produce losses almost 90% higher, even though the fibre came from the same preform and drawn under similar temperature and tension conditions. The confinement loss argument is further emphasised since the unusually high loss profile for Figure 3: Loss curve for Suspended Core MPOF drawn in different towers, including conventional POF. the old tower occurs at low wavelength, where the effects of confinement losses are most felt. These loss figures are the lowest loss yet achieved for mPOFs, and a loss of 0.192dB/m for 650nm, makes mPOFs serious competitors to conventional POFs. The loss of a conventional POF at 650nm is 0.15dB/m [8]. The relationship of bridge thickness and loss in these fibres is such that it strongly suggests confinement loss is the dominant loss mechanism rather than surface scattering. Table 1: The optical performance for Suspended Core MPOFs produced using the old convective and new radiative furnaces Min. Bridge Loss (dB/m) @ Predicted NA @ Measured NA @ Thickness (µm) 650nm 650nm 650nm 1.79 3.85 0.23 0.18 Convective 0.55 0.192 0.38 0.27 Radiative e.g. 1 0.62 0.360 0.37 0.21 Radiative e.g. 2 Table 1 shows that using a Suspended Core mPOF of greater than 2m lengths, the measured NA varied from the predicted high NA when just thin bridges were considered. Issues concern confinement loss due to the single ring of holes. The hole geometry has an impact, since the fibre holes have rounded profiles with thicknesses varying along the bridge length, which is in contrast to straight constant thickness sides of waveguides used in the model. The latter factor is evident since the discrepancies in NA, has occurred for fibre from both towers, even though the bridges in the new tower are much straighter. Conclusion: Suspended Core mPOFs have been useful in attaining good qualitative agreement for rheological modeling, in the future aim to have a simulation model that predicts hole deformation behaviour prior to designing the microstructure array. This fibre has proved that it is acceptable to employ an isothermal profile for the model, which helps the computational efficiency. For NA, the measurements have varied from the model, however differences between the geometry of the real holes compared to the model have been the main reasons for this discrepancy. With regards to loss though, the thin bridges of Suspended Core mPOFs significantly reduced mPOF loss to now be competitive with conventional POF. References [1] [2] [3] [4] [5] [6] [7] [8] M.A. van Eijkelenborg et al., Optics Express 9 pp. 319-327, (2001) G. Barton et al., Journal of Optical Fibre Technology 10 pp. 325-335, (2004) G. Barton et al., Microstructured polymer optical fibres – from concept to reality, World Congress of Chemical Engineering (2005) S. C. Xue, et al., J. Lightwave Technology, accepted, (2005) N.A. Issa, Applied Optics, 43, 33. pp. 6191-6197, (2004) E.C. Mägi et al., Optics Express 13, 2 pp. 453-459, (2004) K. Lyytikainen et al., Heat transfer in a microstructured polymer optical fibre perform, International Conference for Polymer Optical Fibres (2002) T. Ishigure et al., Electronics Letters, 30, 14, pp. 1169-1171 (1994)
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