NL-Petten: The supply, installation, warranty and maintenance of gas analyzer equipment for Quantitative Gas Analysis at the JRC-IE Lot II: Gas Chromatography (GC) analyzer equipment -TABLES - Page 2: Table Technical Requirements Page 5: Table 7: Gas-A H2 (from reforming of hydrocarbons) gas matrix Page 6 : Table 8: Gas-B air gas matrix Page 7 : Table 9: Gas-C Fuel gas matrix Page 8 : Table 10: Example of further gas impurities Page 10: Price table TABLES LOT II – GC Analyzer Equipment - CONTRACT 104703 1 Table technical requirements Lot II: Gas chromatography (GC) analyzer Contractor’s Comments/Data equipment 3.1 EQUIPMENT REQUIREMENTS The Equipments shall be modular and stand-alone with the following characteristics: a. The tables 7 to10 shall be reproduced in documentation of the offer. The empty cells in these tables shall be completely filled to inform the Commission about the characteristics of the Equipment. b. The layout of the Equipment and its features and working principles shall be described in detail in the documentation of the offer. This description shall contain the expected shifts in Equipment performance and the wear of its components and parts based on the intended operational life of the Equipment as specified in 3.3 a. for the performance of the contract. c. The documents mentioned in a. and b. and the maintenance calibration plan shall be part of the offer AND also be part of the Equipment documentation to be provided under stage 1b. d. Equipment spare parts and consumables shall be available for purchase during the expected life of the performance of the contract e. If the Equipment is assembled of more than one analyzer unit, ease of accessibility shall be assured for each part. f. Provided with multiple gas sampling of minimum six gas streams and a sufficient number of gas calibration lines, including automated switching via the Equipment’s operation software g. Prevent water condensation inside the Equipment in case of analysis of gas mixtures with residual humidity. h. Automated Equipment calibration. j. Computerized data acquisition and operation and processing software (spectrum visualization, search and libraries, etc) including computer and flat screen monitor with GPIB (IEEE 488.2) and ETHERNET communication interface or equivalent supporting the TCP/IP network protocol and input for external alarm signals (i.e. gas & fire alarms, panic buttons, etc). Operation and analysis software (incl. libraries and Gaussian/Non-Gaussian de-convolution) licenses shall apply to the entire period of the performance of the contract including any possible extended warranty. TABLES LOT II – GC Analyzer Equipment - CONTRACT 104703 2 k. The Equipment shall bear the CE mark; approval and calibration certificates shall accompany Equipment delivery. m. Emergency and safety buttons o. The Equipment shall be safely and easily movable within the laboratory area (i.e. mobile rack). p. Liquid’s injection apparatus to allow analysis of mixtures (see 3.2f.). q. Equipment sound level in dB at a distance of 1 meter from the equipment, shall not exceed 70 dB(A) as measured when in operation. 3.2 MEASUREMENT REQUIREMENTS a. Quantification (in μmol/mol) of binary gas mixtures A to H of table 11 subject to the Factory Acceptance Test (FAT) to be performed in stage 1a. b. Quantification (in μmol/mol) of ternary gas mixtures A2 to A5, A7, A8, G1, G8, H1 & H7 of table 11. c. Quantification (in μmol/mol) of quaternary gas mixture A7-A8 (see table 11). d. Quantification (in μmol/mol) of binary gas mixtures A to G of table 12 subject to the Factory Acceptance Test (FAT) to be performed in stage 1a. e. Quantification (in mg/l) of binary/ternary liquid mixtures A and C to E of table 13 subject to the Factory Acceptance Test (FAT) to be performed in stage 1a f. Ability for quantification (in mg/l) of binary/ternary liquid mixtures B and F to J of table 13 subject to the Factory Acceptance Test (FAT) to be performed in stage 1a. g. Time for sampling and analysis of the gas mixtures mentioned in a. to c. shall not exceed 20 minutes on average during 3 consecutive sampling intervals in one hour subject to the Factory Acceptance Test (FAT) to be performed in stage 1a. 3.3 OPERATIONAL REQUIREMENTS a. Upon completion of stage 1b, the Equipment shall operate during the performance of the contract of up to 1,000 hrs per year (corresponding to approximately 8 hours per working day) in performing quantitative and qualitative analysis. b. The Equipment shall be operational within 30 minutes from switch-on. c. Unattended operation including fail-safe shutdown d. Ability for Equipment calibration (see 3.1.d). The Equipment shall have the option of selecting an automatically calibration performed in intervals dependent, for example, on number of analyses TABLES LOT II – GC Analyzer Equipment - CONTRACT 104703 3 performed, elapse of operation hours, analyses value require so, etc. This information shall be given in the calibration plan. e. Handling of gas streams at elevated temperatures (e.g. up to 180°C) and 1-5 bar pressure. f. The software shall provide real time multi-tasking capabilities to support multiple activities concurrently including programmable measurement and analysis runs, programmable gas stream selection, spectrum visualization. The software shall also provide extended maintenance tools, such as statistical tracking of analyzer performance, reporting, maintenance logging, etc. g. Common data format (i.e. ASCII, Excel, etc) also for spectrum, libraries and data import and export and storage. h. Possibility to use libraries of different origin(s). 3.4 ADVANCED EQUIPMENT PERFORMANCE FEATURES (Non-mandatory but providing additional value) a. Quantification (in μmol/mol) of binary gas mixtures G and/or H of table 11 with LoDs below the mandatory requirements (see 3rd column of this table) subject to the Factory Acceptance Test (FAT) to be performed in stage 1a b. Quantification (in μmol/mol) of binary gas mixtures G and/or H of table 11 with accuracies at the LoDs concerned below the mandatory requirements (see 4th column of this table) subject to the Factory Acceptance Test (FAT) to be performed in stage 1a. TABLES LOT II – GC Analyzer Equipment - CONTRACT 104703 4 GASES FOR POTENTIAL ANALYSIS The anticipated gas mixtures used in the tests are listed in the tables below to be completed by tenderer: Table 7: Gas-A H2 (from reforming of hydrocarbons) gas matrix Impurities Gas concentration range Instrument model type/technique/detector (µmol/mol) Water THC O2 He; N2; Ar CO2 CO CH4 Methanol HCl Total Halogen. comp. Formaldehyde Formic acid 1-5000 1-10000 1-500 1-50000 1-10000 1-10000 1-50000 1-5000 0.1-10 0.1-50 NH3 H2S 20-5000 1-10 Instrument detection limit Precision (µmol/mol) % Relative detection limit/lower detection limit (µmol/mol) Accuracy (%) Operating range Response time Calibration frequency (s) 0.1-50 0.1-50 TABLES LOT II – GC Analyzer Equipment - CONTRACT 104703 5 Table 8: Gas-B air gas matrix Impurities Gas concentration range Instrument model type/technique/detector (µmol/mol) H2 THC O2 He; Ar N2 CO2 CO CH4 Methanol SO2 NOx Formaldehyde Formic acid NH3 Total Halogen. comp. Instrument detection limit Precision (µmol/mol) % Relative detection limit/lower detection limit (µmol/mol) Accuracy (%) Operating range Response time Calibration frequency (s) 10-10000 1-10000 Up to 100% 1-500 Up to 100% 1-5000 1-1000 1-10000 1-5000 0.5-5000 1-1000 1-500 1-500 0.1-5000 0.1-5000 TABLES LOT II – GC Analyzer Equipment - CONTRACT 104703 6 Table 9: Gas-C Fuel gas matrix Impurities Gas concentration range Instrument model type/technique/detector (µmol/mol) H2 THC O2 He; Ar N2 CO2 CO CH4 Methanol H2S NH3 Formaldehyde Instrument detection limit Precision (µmol/mol) % Relative detection limit/lower detection limit (µmol/mol) Accuracy (%) Operating range Response time Calibration frequency (s) Up to 99% 2-100 1-500 5-500 0.1%-50% 2-10 1-10 1-500000 1-5000 0.1-2 0.1-5000 0.1-50 Formic acid 0.1-50 Total Halogen. comp. 0.1-50 TABLES LOT II – GC Analyzer Equipment - CONTRACT 104703 7 Table 10: Example of further gas impurities Impurities Instrument type/technique/ detector Instrument detection limit Precision Relative detection limit/lower detection limit Accuracy Operating range Response time Calibration frequency Unsaturated hydrocarbons Ethene Cyclohexene Aromatic hydrocarbons Toluene Benzene Xylene Naphtalene Aliphatic hydrocarbons Propane n-hexane Cyclohexane Tar Sulfur containing compounds COS Tetrahydrotiophene Halogen containing compounds HCl HF Dichloromethane Trichlorethene Cis 1,2-Dichloethene TABLES LOT II – GC Analyzer Equipment - CONTRACT 104703 8 Impurities Instrument type/technique/ detector Instrument detection limit Precision Relative detection limit/lower detection limit Accuracy Operating range Response time Calibration frequency Trifluoromethane Dichlor Difluoromethane Si-containing compounds SiO2 Siloxanes (Hexamethyldisiloxane, Trimethylsilanol) Oxygenated organic compounds Ethylenglycol / Propyleneglycol Isopropanol Acetone Methyl-ethylketone Acetaldehyde Acetic acid Butyric acid MTBE ETBE Nitrogen containing compounds Pyridine Acrylates TABLES LOT II – GC Analyzer Equipment - CONTRACT 104703 9 Price table Lot II GC Analyzer Equipment STAGE 1a - MANUFACTURE and DELIVERY Price (€) 1b - INSTALLATION, COMMISSIONING and DOCUMENTATION 1c - TRAINING (based on 8 days) 1d - WARRANTY and PREVENTIVE MAINTENANCE SERVICE FOR 24 MONTHS SUBTOTAL STAGE 1 (1a+1b+1c+1d) 2a – PREVENTIVE MAINTENANCE FOR 12 MONTHS 2b – CORRECTIVE MAINTENANCE FOR 12 MONTHS SUBTOTAL STAGE 2 (2a+2b) TABLES LOT II – GC Analyzer Equipment - CONTRACT 104703 10
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