ARTICLE IN PRESS Composite Structures xxx (2006) xxx–xxx www.elsevier.com/locate/compstruct Low velocity impact induced damage evaluation and its effect on the residual flexural properties of pultruded GRP composites Z.Y. Zhang *, M.O.W. Richardson Advanced Polymer and Composites (APC) Research Group, Department of Mechanical and Design Engineering, University of Portsmouth, Portsmouth, Hampshire PO1 3DJ, UK Abstract Low velocity impact induced non-penetration damage in pultruded glass fibre reinforced polyester (GRP) composite materials was investigated using an instrumented falling weight impact test machine with a chisel shaped impactor. The characteristics of the impact event, force/time and force/deflection traces were determined. The internal damage was visualised and quantified by Electronic Speckle Pattern Interferometry (ESPI) in terms of the thickness, density and uniformity degradations of fringe patterns. There is a linear relationship between the impact energy and the identified damage areas. The post impact structural integrity of impacted specimens was evaluated by three point bending tests. It reveals that there is a significant reduction in flexural properties due to the impact-induced damage and that the residual flexural strength is more susceptible to damage than residual modulus. 2006 Elsevier Ltd. All rights reserved. Keywords: Polymer matrix composites (PMCs); Defects; Non-destructive testing; Impact behaviour 1. Introduction Fibre reinforced polymer composites exhibit distinct properties such as high specific modulus and strength, lightness, high productivity, environmental degradation resistance and cost effectiveness [1,2]. They have found ever-increasing applications as engineering components and structures in the fields of transportation, aircraft, aerospace, marine, military weapon system and nuclear energy industries. However, polymer composites can be susceptible to impact damage during manufacturing and in service. Unlike traditional materials such as metals and ceramics, polymer composites exhibit unique damage characteristics. When they are subjected to impact loading, there might be no damage indication on surfaces by visual evaluation but internal damage may have already occurred. This damage can have an adverse effect on material performances and structural integrity. It is referred to as Barely Visible Impact Damage (BVID) [3–5]. This could potentially lead * Corresponding author. Tel.: +44 23 92842360; fax: +44 23 92842351. E-mail address: [email protected] (Z.Y. Zhang). to catastrophic failure at any subsequent moment. Therefore, it is important to develop a good understanding of impact-induced damage non-destructively. Electronic Speckle Pattern Interferometry (ESPI) has made a significant contribution to engineering measurement and testing. It is capable of making whole-field and non-contact measurements of static and dynamic displacements with high sensitivity [6–9]. It can be extended to damage visualisation and quantification in non-destructive way [10–12]. The presence of either external or internal damage leads to mechanical degradations of GRP composite materials, which can be visualised by ESPI in terms of uniformity and continuity degradation and disruption of fringes. It is also important to establish a relationship between damage severity and residual properties by which the residual load bearing capabilities can be estimated [13–16]. The objectives of this study are to develop a good understanding of the characteristics of low velocity impact induced damage, including the damage formation and development features, to visualise and quantify the impact induced damage using ESPI and to evaluate the post impact load bearing capabilities. 0263-8223/$ - see front matter 2006 Elsevier Ltd. All rights reserved. doi:10.1016/j.compstruct.2006.08.019 Please cite this article as: Z.Y. Zhang, M.O.W. Richardson, Low velocity impact induced damage evaluation and its effect on ..., Composite Structures (2006), doi:10.1016/j.compstruct.2006.08.019 ARTICLE IN PRESS 2 Z.Y. Zhang, M.O.W. Richardson / Composite Structures xxx (2006) xxx–xxx 2. Experimental The pultruded GRP panels were provided by Euro-Projects (LTTC) Ltd. They have been used for bridge floors, marine and chemical plant decking where they are subjected to low velocity and non-penetration impact events. The lay-up was confirmed to be symmetrical by deplying the specimen. It consisted of roving in the centre, sandwiched with random glass fibre mat with woven fibre fabric and surface veil placed symmetrically on both sides. The fibre volume fraction was approximately 50%. The panel was cut into rectangular specimens with overall dimensions of 150 · 40 · 4 mm so that they could be accommodated into a purposely build fixture for ESPI testing. Impact testing was implemented using an Instrumented Falling Weight Impact Test (IFWIT) machine. The general features of the equipment are schematically shown in Fig. 1. A controlled impact is achieved by dropping a chisel shaped striker which is attached to a weight in a defined manner from prescribed impact heights as shown in Fig. 2. The probe is equipped with a pizeo-electric transducer for measurement of velocity and load interaction between the probe and specimen. The velocity and load transducer provides a complete profile of the deformation response of the specimen during the impact process. Discrete values provided by the load transducer are collected and stored in a computer for post processing. A pneumatically operated mechanism switches on when the impactor bounces back to prevent the repetitive strike on the specimen. The specimen was pneumatically clamped between a 65 mm circular ring and anvil. Parameters such as energy, time duration, load, deflection and velocity are generated to characterise the impact events. An ESPI system was based on a Helium Neon (He–Ne) continuous wave laser (k = 632.8 nm) interferometer in combination with a frame store, monitor, video recorder, clamping jig and excitation apparatus which are schematically illustrated in Fig. 3. Theoretical aspect of ESPI and detailed descriptions of the testing system are documented elsewhere [17]. ESPI is capable of making whole-field and non-contact measurements of deformations with high sensitivity and perturbations to the fringe patterns are corre- Striker length: 15 mm Striker radius: 2.5 mm Impact test configuration Diameter of supporter: 10mm Diameter of loading roller: 10 mm Span: 80 mm Flexure test configuration Fig. 2. Impact and flexure test configurations. Laser Mirror Mirror Beam Splitter Lens Lens Digital correlation Camera Impacted Sample Fig. 3. Schematic of electronic speckle pattern interferometry (ESPI). Fig. 1. Schematic of instrumented falling weight impact test machine. Please cite this article as: Z.Y. Zhang, M.O.W. Richardson, Low velocity impact induced damage evaluation and its effect on ..., Composite Structures (2006), doi:10.1016/j.compstruct.2006.08.019 ARTICLE IN PRESS Z.Y. Zhang, M.O.W. Richardson / Composite Structures xxx (2006) xxx–xxx 3. Results and discussion 3.1. Characteristics of low velocity impact events The impact performance of GRP composite materials depends upon many factors, including the nature of the fibre, matrix, interface, geometry and testing conditions. Impact testing is generally split into two categories. The first is impact testing under relatively low incident energy where the composites are partially damaged but still capable of performing their primary function to certain extent. The second is impact testing under high incident energy where composites are completely ruptured or penetrated by the striker. The former is generally simulated using a low velocity falling weight or a swing pendulum tester and the latter using a gas gun or some other ballistic launcher. The responses of composites to impact loading are extremely complicated and have already received considerable attention [19–22]. An investigation into the fracture toughness and impact resistance of GRP composite materials was not the main concern of this study. Instead, damage evaluation and the establishment of correlation between the various impact event parameters with post impact load bearing capabilities were the primary concern. In order to achieve these objectives, an instrumented low velocity falling weight impact machine was employed to introduce damage using a chisel shaped striker and the impact energy levels were pre-determined and controlled by varying the striker heights in order to incrementally introduce non-penetration damage in six specimens. Force/time traces at six different impact loading levels are illustrated in Fig. 4. They are indicative of load history, which is associated with the damage initiation and development. The force/time traces of six impact events exhibit similar trends with a complex series of peaks and troughs. The overall curves can be approximately divided into two parts at the maximum impact force. The first part is predominantly related to damage initiation. There is a linear increase of force with the time at the start of loading, indicating the purely elastic response of the specimen and no damage is expected to occur if the impact loading is terminated at this stage. When the impact loading in further increased, there are pronounced fluctuations in damage initiation regions. It suggests that the damage initiation occurs at different moments in different mechanisms. The second part is mainly associated with damage propagation in which the force has a monotonical decrease with increasing the time. It should be noted that force/time traces are similar to those in penetration impact testing but the implications are fundamentally different. In the case of penetration impact events, load drops are associated with major fracture processes such as fracture of fibre bundles or complete plies. As far as non-penetration impact events are concerned, the load drops are associated with both elastic and plastic deformation. The striker bounces upwards from the specimen surface due to elastic collision and is then caught by a second strike prevention mechanism. Force/deflection traces at six loading levels are illustrated in Fig. 5. They are indicative of the deformation and damage development history of specimens, which in turn have an analogous relationship with force/time traces. In general, force/deflection traces can be approximately 7 6.4 J 8.9 J 11.5 J 14 J 16.6 J 19 J 6 5 Force (kN) lated to the impact induced barely visible damage in this study. The specimens were firmly clamped onto a purpose build jig in which the rectangular specimen was clamped vertically at both ends for ESPI measurement. Care was taken to make sure that specimens were clamped in parallel to the jig for easy calibration and analysis. Matt paint was spread uniformly on the surfaces in order to enhance the reflectivity. The specimens were mechanically excited using a force transducer hammer. Live fringe patterns were recorded for post damage recognition and measurement [18]. Flexural modulus and strength of the impacted specimens were evaluated using a three-point-bending test. The testing was carried out according to the ISO 178, a test method for flexural strength and modulus of fibre reinforced plastics. The selected crosshead speed was 2 mm/ min so that specimens failed within 30–180 s intervals as required. The experimental results were normalised in order to achieve a straightforward interpretation and comparison of the post impact flexural strength and modulus. The orientation of the damage with respect to geometry of the flexure test specimens is illustrated in Fig. 2. Here the normalised flexural modulus is defined as the modulus of the sample experiencing the impact loading divided by the modulus of the sample without experiencing the impact loading. Similarly, the normalised flexural strength is defined as the strength of the sample experiencing the impact loading divided by the strength of the sample without experiencing the impact loading. 3 4 3 2 1 0 0 0.5 1 1.5 2 2.5 3 3.5 4 Time (ms) Fig. 4. Force/time traces of six impact events with incremental incident energies. Please cite this article as: Z.Y. Zhang, M.O.W. Richardson, Low velocity impact induced damage evaluation and its effect on ..., Composite Structures (2006), doi:10.1016/j.compstruct.2006.08.019 ARTICLE IN PRESS 4 Z.Y. Zhang, M.O.W. Richardson / Composite Structures xxx (2006) xxx–xxx 7 6.4 J 8.9 J 11.5 J 14.0 J 16.6 J 19.0 J 6 Force (kN) 5 4 3 2 1 0 0 0.5 1 1.5 2 2.5 3 3.5 4 4.5 Deflection (mm) Fig. 5. Force/deflection traces of six impact events with incremental incident energies. subdivided into different stages. The first stage is referred to as linear load/deflection deformation due to the elastic response to loading. No damage occurrence was expected at this stage. A complete recovery from the deformed state to the original specimen position is expected when the applied load is removed. With the increase of load, the specimen yielded, implying the onset of plastic or permanent deformation, lead to a sudden drop in load. Once the load reached its maximum, it decreased monotonically and the deflection decreased accordingly due to the gradual recovery of elastic deformation. Force/deflection traces of non-penetration impact events are substantially different from those of penetration impact events in which the decrease of force is related to further damage development when the striker passes through the specimen. The maximum depth corresponds to the termination of the impact event. In the case of non-penetration impact event, the peak forces approximately coincide with the maximum deflections in the force/deflection curves which are significantly different from the penetration impact events. The deflections are then contracted due to the elastic deflection recovery. The summarised impact testing results are shown in Table 1. Peak forces, peak energy, energy at failure and peak deflection increased linearly with increasing the striker height. The peak deflections exhibited similar trends which are characterised by a monotonical increase with the incident energy. However linearity substantially deteriorates in deflections at failure because damage develop- ment and elastic recovery in these specimens has an effect on this process in complicated ways that make it difficult to produce quantitative descriptions. Energy is the primary parameter for characterising damage tolerability, which is preferably employed to correlate with damage magnitude. It is inappropriate to correlate incident energy with damage magnitude because part of this energy is transformed into kinetic energy when the striker bounces upwards and dissipated in the form of vibration and noise during the testing process. These energy components have no direct relevance to damage initiation and development. Peak energy consists of the energy absorbed via elastic deformation of the specimen and the energy dissipated via damage initiation and propagation. For non-penetration impact events, peak energy is invariably higher than the energy at failure due to elastic recovery when the striker bounces upwards. It is different from penetration impact events when peak energy is invariably lower than energy at failure due to the complete rupture of specimens. It is obvious that failure energy is exclusively responsible for the damage initiation and propagation in the specimen. In this case it is significant to establish a correlation between energy at failure and damage magnitudes and to evaluate postimpact load bearing capabilities. The force/time and force/deflection traces can assist in understanding of impact damage initiation and propagation mechanisms. However, they hardly indicate the impact damage presence and severity. Under these circumstances, ESPI was employed in this study for impact induced damage evaluation and quantification. 3.2. Damage evaluation The representative features of impacted coupons on both front and back surfaces are shown in Fig. 6. There is usually no indication of damage presence on front sur- Table 1 Impact testing results at incremental incident energy levels Incident energy (J) Striker height (mm) Peak force (KN) Peak deflection (mm) Peak energy (J) Deflection at failure (mm) Energy at failure (J) 6.4 250 2.69 2.1 4.75 1.1 4.01 8.9 350 3.15 2.7 6.80 1.2 5.57 11.5 450 3.77 3.3 8.79 1.8 7.25 14.0 550 4.39 3.6 10.95 2.0 8.84 16.6 650 4.60 3.9 12.98 2.0 10.79 19.0 750 5.33 4.2 15.05 2.2 12.38 Fig. 6. Visual inspection of impacted coupons. Please cite this article as: Z.Y. Zhang, M.O.W. Richardson, Low velocity impact induced damage evaluation and its effect on ..., Composite Structures (2006), doi:10.1016/j.compstruct.2006.08.019 ARTICLE IN PRESS Z.Y. Zhang, M.O.W. Richardson / Composite Structures xxx (2006) xxx–xxx face, where the specimen is subjected to compressive loading. It implies no defects in the impacted specimen which is incorrect and misleading. By contrast, a crack can be visible on back surface, indicating the presence of damage. But this indication is invariably unhelpful due to the physical constraints and difficulties in accessing to the back surface such as tubular, cylindrical and hollow components. Visual inspection provides a certain indication of the damage presence but it can hardly provide complete and quantitative information because of its inability in detecting internal damage. Correlation fringe patterns generated by ESPI in combination with a force transducer hammer were employed to characterise the internal damage. The typical fringe patterns for the sample without damage are characterised by good symmetry and uniformity, which are associated with the rigid body movement of the sample under excitation loading. An interpretation of the fringe patterns requires 5 some knowledge in laser interferometry and observations of live fringe pattern during the test would make the damage identification and evaluation less demanding. The fringe patterns associated with six impact energy levels are illustrated in Fig. 7. These images have been processed to eliminate background noise and to highlight the damage features. The damage is characterised by the degradation and disruption of uniformity and continuity of fringe orientation, density and thickness. Damaged areas deform more than un-damaged ones because of stiffness differences. The deformation in damaged area is plastic in nature due to the debonding, fibre pullout, delamination and fibre breakage. Therefore the fringe patterns are frozen because the damage is unlikely to recover elastically. Comparatively the deformation in undamaged area is elastic so the fringe patterns would gradually disappear because of the elastic deformation. Although these differences can be very small in magnitude, ESPI can pick them up due Fig. 7. Damage visualisation by fringe patterns from ESPI. Please cite this article as: Z.Y. Zhang, M.O.W. Richardson, Low velocity impact induced damage evaluation and its effect on ..., Composite Structures (2006), doi:10.1016/j.compstruct.2006.08.019 ARTICLE IN PRESS Z.Y. Zhang, M.O.W. Richardson / Composite Structures xxx (2006) xxx–xxx to its high sensitivity. It can be seen that the magnitude and severity of damage increase with increasing incident impact energies. There are lineal relationships between the damaged areas and impact energies as illustrated in Fig. 8. The horizontal error bands illustrate standard variations of damage areas of five testing samples evaluated by ESPI. Linearity between the damaged areas and energy at failure was expected because it represents the energy dissipated or absorbed at the expense of damage occurrence. The similar linearity between the peak energy and the damaged areas implies that a similar percentage of energy is absorbed in the form of elastic deformation, which subsequently recovers elastically. It is expected that the damage related to different impact loading levels could be approximately predicted although an extrapolation might not be completely appropriate. A wider impact stressing range is recommended for future work in order to develop a further understanding of correlations between impact energy and damage magnitude. 3.3. Residual flexural strength Investigations into post-impact load bearing capabilities of GRP materials involving different modes of stressing have received a lot of attention. It is of particular interest to understand to what extent the impacted materials can sustain further loading. It has been found that tensile, compression and flexural properties are reduced when impact damage is present in specimens [23,24]. In this study flexural testing was carried out to evaluate post impact properties, namely flexural strength and modulus. It was anticipated that a correlation between the impact energies, the damage magnitudes and residual flexural properties would be established. The relationships of residual flexural properties with increasing impact damage energies are illustrated in Fig. 9. It indicates that impact events result in reductions in modulus and strength to varying degrees. The residual flexural modulus is slightly less reduced with increasing 1 Residual Modulus 0.95 Residual Strength Residual Properties (%) 6 0.9 0.85 0.8 0.75 0.7 0.65 0 2 4 6 8 10 12 14 Damage Energy (J) Fig. 9. Residual flexural properties as a function of absorbed impact energy. impact energies compared to residual strength. The maximum reduction is approximately 20%, indicating that flexural modulus is not particularly sensitive to the damage presence. Comparatively flexural strength is more severely affected by impact damage, leading to higher reductions. The maximum flexural strength reduction is approximately 30%. This higher sensitivity can be explained by the fact that the impact damage is localised in most cases and therefore it has less effect on global properties such as modulus. The calculation of modulus only involves the initial linear part of force/deflection curves. Conversely localised impact damage has adverse effect on the load bearing capability of materials, referred to as ‘‘residual strength’’ or ‘‘strength after impact’’. The flexural strength is calculated using the ultimate force that the specimens could sustain and this is dramatically reduced due to the presence of impact degradation. Similar experimental results were reported regarding post-impact performance [25,26]. The relationship between the residual properties and the damaged areas is similar to that in Fig. 9 and should be considered in the context of the linear relationship between impact energies and the damage areas as shown in Fig. 8. 4. Conclusion 16 Energy at Failure 14 Peak Energy Impact Energy (J) 12 10 8 6 4 2 0 0 200 400 600 800 1000 1200 1400 Damage Area (mm2) Fig. 8. A relationship between impact energy and damage area. A series of samples were incrementally impacted using an instrumented low velocity impact machine to introduce non-penetration damage and were then subjected to NDT and flexural testing. Force/time and force/deflection traces are indicative of the damage initiation and propagation. The impact events are characterised by the variations of force, energy and deflection. ESPI has been successfully employed to visualise and quantify the impact-induced damage. Post impact flexural property testing shows that flexural strength is more sensitive to the presence of localised impact damage than flexural modulus. The damage areas increase with an increase in the energy at failure. The successful evaluation of impact-induced damage using ESPI could be extended to investigation of different mechanical loading induced damage and performance Please cite this article as: Z.Y. Zhang, M.O.W. Richardson, Low velocity impact induced damage evaluation and its effect on ..., Composite Structures (2006), doi:10.1016/j.compstruct.2006.08.019 ARTICLE IN PRESS Z.Y. Zhang, M.O.W. Richardson / Composite Structures xxx (2006) xxx–xxx degradations. The established correlations between impact energy levels, damage severities and residual flexural properties can be employed to estimate post-impact load bearing capabilities for material design, selection and maintenance purposes. References [1] Shalin RE. Polymer matrix composite. London: Chapman & Hall; 1995. 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