SOURCE OF INTENSIVE OXYGEN PLASMA FLOWS OF LOW ENERGY FOR TECHNOLOGICAL A.FLICATICS Yury V. KYBAREV *, Vladimir N. CHERNIK ** Abstract The external magnetic field magnetoplasmadinamic accelerator cathode using. Double arc contraction by ferromagnetic intermediate with electrode material plasma reduces pumping electrode of The source produces the oxygen 4*10 . to up contamination jet plasma jet with ion current density 5 mA/cm2 the in range energy free lifetime is some lOOh. Its maintanance- 20-60eV. Ar-flow-hollow by adopted to produce low energy oxygen plasma jet is Introduction At present the interest has grown of the intensive in creation oxygen plasma or ion flows with the energy lower 100 eV[1]. 3aused the by structure to requirements make thin films with It is perfect and also the simulation of action of elemental oxygen on spacecraft materials. In the film fabrication technology the film proberties such as Irystalline structure, refractive index can be controlled by bombarding qrowing film with film density, inert or reactive qas ions. resistivity electrical and The interactions between ions and thin film surfaces are strongly-dependent on the incident kinetic energy Considering the energy dependences of damage creation, of the ions. the sticking probability, enhanced adatom migration, deposition and epitaxial the surface cleaning effect, the optimum kinetic energy growth of the films is and tne range between.a few eV and 100 eV [2]. *) - *) - Academy of Ingeneering Sciences of Russia. 84/32, Profsoyusnaya Str., Moscow, 117610, Russia Moscow State Informatics, I 20, Akademy of Stromynka Str., Instrument-making Moscow, for 107846, and Russia Spacecraft in low earth orbit (200-500Km height) are exposed to a rarefied atmosphere which is, atomic oxygen (ATOX). It can to a large extent, composed of interact with the spacecraft in a number of ways and in particular can cause undersirable erosion degradation of spacecraft materials. facilities are neened to investigate the erosion appropriate choice of Thus ground-based principal materials test mechanisms used in or of spacecraft construction[3]. The problem of material erosion in oxidative plasma is existed in fusion tecnology too. impurity oxygen wall material Under plasma-wall interaction the wall ions are produced intra- cavitarily and sputter of chemically. To predicate materials behavior the needed of simulative tests are requisite [1,4]. All technology high-intensivity branches oxygen energy lower 100eV. mentioned plasma flow are in source with ion translation Another common requiments are 1) density more of 1ma/cm 2 , ion current 2) long durability sufficient to material tests durations(lOOh). 3) minimal beam contaminants. Plasma or ion sources usually suitable for it in little degree. with one-grid hours) ion because of optics the used in the practice are Kaufman ion source of low energy (IO) possesses a small lifetime (a few rapid 10 destruction in the oxygen. In addition since most of the conventional high-current ion sources utilize metallic hight-discharge hot current cathodes and and are operated at considerably low gas pressure, a the liftime of the metallic hot cathodes is rather short and iL usually limits the lifetime of the ion source. In opposite a closed electron drift plasma accelerator supplied with Ar-gas-flow hollow cathode.That resultes in long operation in oxygen plasma 15), but the oxygen plasma flow is life energy is found to be too high (100eV and more). ions can be produced by Low translation energy magnetoplasmadinamic accelerator intended for a ground based ATOX simulation [6]. self-induced magnetic field MPD thruster type. Jet energy is expected (MPDA) The accelerator The oxygen to be in the range 3-15eV. oxygen gas operating the MPDA electrodes effects is plasma Howerer when limit pertormance duration (some minutes) and result in jet contaminations. Oxygen plasma source design and performance This paper concerns the oxygen plasma source advanced. Contrary to the truster above mentioned the source is based on external magnetic field MPDA configuration [7]. Inside the MPDA the regimes of acceleration flows with velocity of 5-20 km/s are known [7]. of this type you can create along the lines of conditions magnetic forces when and field and electron plasma air In the accelerator the electrons move their directions to a considerable extent coincide with the lines of electric wi.th plasma flows. The temperature are not great and it possible to make flows with energy not higher than ionization is one [8]. When developed the main difficult problems thermoelectron arc cathode were to design a with a long lifetime in the oxidative arc and to purify oxygen plasma jet of contaminants. The development working of directly durability to traditional in the MPDA oxidative scheme are with permited the filament the source be no more than a few hours due to cathode erosion. Zirconium or hafnium cathodes known as thermo chemical have a durability in atmospheric oxygen arc long owing to protective oxide layer creation and maintenance in oxidative plasma. The application of the thermochemical Hf emitter oxygen failed to increase the source lifetime because of the destruction 1 of the protective emissive layer by ion bombardment in low pressure arc of MPDA .e t'e [9]. long hollow emItter lifetime inert gas cathode prototype [10]. of 5-. th cathode was developed ,mp to lOOh) employed. The for the "FOBOS was ensured w en diaphragmed program LaS served as The finished cathode assembly of the source is mace in the form of a diaphragmed Mo pipe which is half filled with LaB6 grains. The pipe is surrounded with the spiral start-up electric heater. The cathode assembly is arranged inside the cylindrical thermoscreen. The inert gas fills the screen hollow flowing through the pipe, and in such a way it protects not only LaBg emitter but also the exterior pipe and heater surfaces inside the screen. In this way the source life time in between LaB 6 grains substitutions is found to be near 100 hours in dependence on cathode flow-Ar-gas Purity. The plasma jet contamination problem being minor is important for technology source. for thruster The cathode erosion products and inert gas are the impurities of the oxygen plasma jet of tne MPDA. The electrode material atoms are transported by plasma jet to an irradiated surface, are deposited and disturbed its behaviors. The inert gase is pumped poorly by some type of vacuum pumps as sputter-ion ones. To reduce the impurities yield employed magnetic and geometric arc intermediate electrode (IE) as in to the contraction the plasma by stream we ferromagnetic duoplasmatron [11]. The contraction creates potential barriers limiting cathode plasma ions (cum contaminants) moving towards the anode plasma in which the jet is formed. For the more complete decrease of the neutral impurities yield to the anode plasma, the IE hollow is pumped complementary. The pumping reduces pressure in the IE and maintains in the E' channel gas flow which is contrary the eiectrons[12]. ship between intracavity IE pressure and plasma jet The relationion currents I i27 1ratio of Xe-impurity to oxygen is shown in fig. 1. The schematic diagram of the source is shown in figure anode 1, IE 2, cathode inside the solenoid 4. XEOHW OXYGEN of * 4.2 S- magnetic distribution in hum distribution in the anode and to corresponds downstream the MPDA, its the IE and at The 3 are arranged The induction 2. and in front of is it channel its ana- 40 0 4 2 6 IE PRESSURF- Pa Fig. logous to the distribution in the duo- plasmatron. The plasmaforming gas oxygen is the in fed anode and the inert gas argon or xenon runs through by pipelines pumped through The source vacuume line performances 5 and 6. by 7. were investigated in two-probe technique, a the 1 vacuum m" /s and three-grid energy analyser and a monopolar mass-spectrometer [13]. The oxygen flow measured at a distance of 0.2 m from the anode had plasma ion current density up to 5 mA/cm with 3 cm diameter on level 0.7 max. Varying the you can magnetic field, gas and electric supply consumption, control the ion current density. Figure 3 shows density as current. 2 1 Ithe 6 O o' 5 Fig.2 a The the function ion of current discharge The average ion energy range + ratio 0 /Ois of 20-60 eV, in and the fluxes at the interval of indicated is 0.3-3. perfomances are obtained with oxygen gas flow equal to 0.5 cm /s, argon I cathode The IE cavity is facilities with differential diffusion pumping 2 and plasma diagnostics the or xenon flow equal to 0.1 cm/s, I 6-12 A are current. O-100 V arc voltage. 16 - The s ' 0 o 8 impurity materials 12 DISCHARGE CURRENT-A not construction cathode observed massspectrometry Fig.3 of inert and were 16 ions of 5*104 sensitivity gas (Xe) during the plasma flow with limit. Construction materials contaminates were measured by deposition probe with Rutherford Back Scattering method. The Fe atoms technique were found to be some 4 per million oxygen ions in plasma jet [14]. The described source was used in the degradation of spacecraft and thermonuclear investigations reactor of materials in oxygen plasma flows [15,16]. References 1. O.Auciello, D.E.Ibbotson, D.L.Flamm, of Reactive Etching of Materials in "Critical Comparison Microelectronics, Fusion and Space Technologies", Nucl. Instrum. Meth., Vol. B23, 1987 2. T.Takagi, "A Perspective of eV-MeV Ion Beams", Nuc. Instrum. Meth., Vol. B37/38, 1989 3. V.S.Voicenja, S.K.Gudgova, V.I.Titov, "The Action of Low-Temperature Plasma and Electromagnetic Radiation on Materials", Moscow,1991 4. E.Hechtl, Y.Bohdansky, Typycal Impurity Ions for I.Roth, Different "The Fusion Sputtering Yield of Reactor Materials", Y.Nucl.Mat., Vol. 103/104, 1981 5. S.K.Absoljamov, S.A.Khartov, "Development V.V.Egorov, and Reserch V.Kim, L.A.Latjshev, of Closed Electron Dlift Accelerator on Oxygen" and Its Technology Application, Abstr. 2nd All- Union Conf. Modification of Construction Materials by Charge Particles Beams", Vol.1, 1991 (in Russian) i S. 1.Y.Wood, Simulation of Amomic Oxygen", in a Space Proc. on Materials Symp. Sixth Inter. Noordwijk, ESTEC, Ihvironment, Ground-Based a for Source Accelerator "Development of a Plasma 166974, 8. 1963, (in S.D.Grishin, Moscow, 1982 (in 9. Presure Oxidative 10. Russian) L.V.Leskov, Vol.2, Y.Okumura, Impurities in "Plasma accelerators", "Performaces of Filaments in Low Proc.conf."Plasma Physics and Technology", Russian) L.A.Latjshev, "Reserch of Ion Trusters 11. N.P.Kozlov, V.N.Chernik, Arcs", V.N.Korovkin, Propul. Conf., Pat. USSR, Russian) Yu.V.Kubarev, Minsk, 1994 (in 1994 The Netherlands, 7. Yu.V.Kybarev, " Discharge plasma source", No . A R. SS.B.Gabriel, s, :: . * in V.A.Obukhov, the USSR", Proc. V.G.Grigoryan, 22th Intern. Elect. 1991 Y.Mizutani, Y.Ohara, T.Shibata," a long-puslse multiamper beam ", Rev. Measurements Sci. of Instrum. Vol.52, 1981 12. V.N.Chernik, No 1797448, 1993 (in 13. V.N.Chernik, "Duoplasmatron type plasma source", Pat. USSR; Russian) V.I.Titov, G.G.Solovyev, "Vacuum Facility for Investigations of Influence of Plasma Flows and Optical Radiations on Materials", Vacuum Science and Technology, Vol.1, 1991 14. A.I.Akishin, V.N.Chernik, "An Application of Rutherford Back Scatteaing Plasma Contamination Measuring", of Charge Particals I V.S.Kulikauskas, V.V.Zatekin, Technique to Oxygen Proc. 26th Inter.Conf. on Physics Interaction with Crystalls, 1995 (in Russian) I 15. V.I.Titov, LowEarth Orbital G.G.Solovyev, V.N.Chernik, et. all., Simulation Facility Evaliation", Proc.5th Intern. Symp.on for Materials "Complex-2 Durability Spacecraft Materials in Space Environment,Cannes, 1991 16. A.I.Akishin, of V.S.Kulikauskas, V.N.Chernik, "Investigation Graphite and Stainless Steel Sputtering by Oxygen Plasma Flow", Bull.Russ.Acad.Sci.,Vol.58,No. 3, 1994 (in Russian) I
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