Experimental Design of Beer Foam Height IEE572 Term Project Instructor: Dr. Douglas C. Montgomery Project Team: Serhan Alshammari (1:30pm), Jinsung Cho (4:30pm), Tracy Lenz (1:30pm) IEE 572 Project Height of Beer Foam EXECUTIVE SUMMARY Brewing and serving beer is a cultural and social subject in the United States. The chemistry and quantitative subject matter is organized by the American Society of Brewing Chemists, an organization ASBC is a professional organization of scientists and technical professionals in the brewing, malting, and allied industries. There was interest on behalf of a local brewer, BJ’s Brewery, to determine if an additive Biofoam CL could increase the foam head of a beer and if so, under what conditions. BJ’s Brewery also wanted data on temperature and pressure. The above photo is the “laboratory” for BJ’s Brewery. There are 5 major steps in the brewing process. 1. 2. 3. 4. Malted barley is mixed with hot water to 65 to 75 Celcius. This is called mashing. Lautering is a filter process to remove husks left over from the grains. Sparging is then completed. A liquid is sprinkled over the top not over 77 Celcius. At 100 Celcius, the hops is added at a boil and the liquid is quickly cooled and yeast is added in the line. 5. The yeast ferments at 20 Celcius. When the yeast is added to the wort, the fermenting process begins, where the sugars turn into alcohol, carbon dioxide and other components. Serhan Alshammari, Jinsung Cho, Tracy Lenz Page 2 IEE 572 Project Height of Beer Foam Biofoam CL is assumed to increase both the foam head at pour and the retention of foam. Biofoam should augment the natural foam components in beer. The experiment used four factors; the type of beer, the pressure in the draft line, the temperature, the use/nonuse of biofoam. The experiment also included a block factor since beer is typically served by many trained/experienced bartenders. Serhan Alshammari, Jinsung Cho, Tracy Lenz Page 3 IEE 572 Project Height of Beer Foam Table of Contents EXECUTIVE SUMMARY................................................................................................................... 2 Table of Contents .................................................................................................................................. 4 List of Figures: ...................................................................................................................................... 5 List of Tables: ....................................................................................................................................... 6 1. PROJECT STATEMENT & OBJECTIVES ........................................................................................ 7 2. INTRODUCTION ................................................................................................................................ 7 3. EXPERIMENTAL DESIGN ................................................................................................................ 8 3.1 Design Factors and Level .............................................................................................................. 8 3.2 Constant Factors............................................................................................................................ 8 4. EXPERIMENTAL PROCEDURE ....................................................................................................... 8 5. EXPERIMENTAL MATRIX ............................................................................................................... 9 6. RESULTS AND ANALYSIS ............................................................................................................. 10 6.1 Estimate Factor Effects ............................................................................................................... 10 6.2 Final Model: Model Adequacy Checking ................................................................................... 16 6.3 Final Model: One Factor Effects ................................................................................................. 19 6.4 Final Model: Interaction Effects ................................................................................................. 20 6.5 Final Regression Model .............................................................................................................. 24 7. CONCLUSIONS AND RECONMMENDATION ............................................................................. 25 8. REFERENCES ................................................................................................................................... 25 Serhan Alshammari, Jinsung Cho, Tracy Lenz Page 4 IEE 572 Project Height of Beer Foam List of Figures: Figure 1. Derek “Doc” Osborn ..................................................................................................................... 7 Figure 2 : Half Normal Plot ........................................................................................................................ 11 Figure 3 : Normal Plot of Residuals............................................................................................................ 12 Figure 4:Box-Cox Plot ................................................................................................................................ 13 Figure 5: Normal Plot of Residuals for the Final Reduction Model ........................................................... 16 Figure 6: Residuals Vs Run Order .............................................................................................................. 17 Figure 7: Residuals Vs Predicted ................................................................................................................ 18 Figure 8. Plot of Residuals vs Factors......................................................................................................... 19 Figure 9. Plots of One Factor Effect ........................................................................................................... 20 Figure 10: pressure and Biofoam Interaction .............................................................................................. 21 Figure 11: Temperature and Type of Beer Interaction................................................................................ 22 Figure 12: Temperature and Pressure Interaction ....................................................................................... 22 Figure 13: Biofoam and Type of Beer Interaction ...................................................................................... 23 Serhan Alshammari, Jinsung Cho, Tracy Lenz Page 5 IEE 572 Project Height of Beer Foam List of Tables: Table 1. Beer Chemistry ............................................................................................................................... 7 Table 2: Factor Levels and Codes ................................................................................................................. 8 Table 3: Test Matrix...................................................................................................................................... 9 Table 4: ANOVA for the Full Design ......................................................................................................... 10 Table 5: R Squared Values for Complete Design ....................................................................................... 12 Table 6: ANOVA Table without Outliers ................................................................................................... 14 Table 7. ANOVA Table without Outliers and Non-Significant Terms ...................................................... 15 Table 8. Comparison of R-Squared............................................................................................................. 15 Serhan Alshammari, Jinsung Cho, Tracy Lenz Page 6 IEE 572 Project Height of Beer Foam 1. PROJECT STATEMENT & OBJECTIVES The scope of the experiment is to analyze the factors affecting the amount of foam head created while pouring a draft beer. There are cosmetic and financial impacts regarding the serving of draft beer. Excessive foam is unacceptable to the consumer and the brewer. The consumer would not want excessive foam since they are paying for a beer. For the brewer, excessive foam at the pour of the draft beer may allow for a large quantity of foam, which is equivalent to 20% liquid, be wasted down the drain as the beer foam spills over the full glass. No foam, however, does not capture the aromatic and customer standards for a draft beer. The factors evaluated include pressure of the draft line, the type of beer (chemistry plays a role in foaming), the temperature of the beer in the draft line, use of a foaming agent, Biofoam CL, and a block factor of operator. BJ’s Brewery in Chandler, and their head brewer, Derek “Doc” Osborn, has been instrumental in assisting our team with this designed experiment. Derek wanted to determine if adding biofoam is a cost effective means of increasing foam head of a beer under the influence of various factors. 2. INTRODUCTION The objective of the experiment is to analyze the factors involved in the amount of foam head on a draft beer. Figure 1. Derek “Doc” Osborn Worldwide cultural traditions indicate that there are a variety of acceptable standards based on the type of beer, the history of beer brewing, and the customer expectations with relationship to the cost of a beer. Most American draft beers have the expectation of about .5 to 1 inches (1.27 to 2.54 cm) of head to fulfill a need for cosmetic looks and aromatic release of flavor as bubbles pop over the surface of the beer. At BJ’s Brewery, the standard draft is poured at 20 psi, at a temperature of 37 to 40 degrees Fahrenheit, without Biofoam CL. Our experimental design included a “type” of beer factor since the chemistry of the beer will affect its ability to foam at pour. Bartenders at breweries are trained to pour draft beers with specific guidelines. Despite training, there may be an uncontrollable variation from operator to operator that has been included is a block factor with two operators. The variation of pressure in this designed experiment, 11 and 24 psi, stood above and below the standard pour pressure of 20. The temperature levels, 37 and 58 degrees Fahrenheit, are the extremes of pouring and serving beer. Many beers are expected to warm and accentuate their flavors as the beer warms after the pour, especially the red beers. The two beers selected, Jeremiah Red and Lightswitch, were selected based on their chemistry. These beers elicit the spectrum of inherent foaming capability, red being the most and lightswitch being the least. Lights witch 2 row base malt (silo) Wheat Malt hops Water Yeast Jeremiah Red 2 row base malt (silo) 4 other malts hops Water Yeast Table 1. Beer Chemistry Serhan Alshammari, Jinsung Cho, Tracy Lenz Page 7 IEE 572 Project Height of Beer Foam The factors affecting the foaming ability in the chemistry make up of the beers is the larger quantity of 2 row base barley that is double of the amount in the red beer. The malt amount by weight is four times as much in the red beer. The other ingredients are the same in each beer; hops, water, and yeast. 3. EXPERIMENTAL DESIGN 3.1 Design Factors and Level In this experiment we have several controllable fixed factors that affect the height of the beer foam. The factors levels and code are listed in the following table. Factors + (High) - (Low) Keg Pressure (psi) 1 (24) -1 (11) Temperature at Keg (F) 1 (58) -1 (37) The use of Biofoam 1 (used) -1 (not used) Type of Beer 1 (Red) -1 (Light) Table 2: Factor Levels and Codes For each factor, we have two levels associated with it. The Keg pressure has been taken into consideration for the fact that the higher pressure you put on it the high level of CO2 you will have in the beer which makes it easily released. The same concept can be applied for the temperature factor the cooler the beer the more CO2 we will have in it. Low pressure is assumed to create a larger variation in data due to CO2 wanting to “break out” since there is no pressure to secure it. There may also be more variation in results with low pressure lines due to inconsistency in the line(actual pressure data). The Biofoam product is an additive substance that helps to increase foam head at the pour and to stabilize the foam from collapsing. The bartender (operator ) is a block to eliminate the nuisances created with this factor so we reduce its contribution for the experimental errors. 3.2 Constant Factors In the experiment three factors held constant; the mug shape, the room temperature, and the bar line. 4. EXPERIMENTAL PROCEDURE Looking at the factors, we have 4 fixed factors level and one nuisance factor we decided to run the experiment as full factorial 24 design with two blocks representing the two operators. There will be 32 runs for this designed experiment. Then we generate the randomized test matrix that reduces the variation caused by the pattern of the experiment. 1. After setting up the experiment we adjust the factor to the desired levels. 2. Pour the beer into the mug. 3. Measure the original foam height ( after 10sec from the pour step ) (20% of the foam is beer as per the expert background, hence a short delay in measuring ) 4. Repeat the previous steps with the next required levels. Serhan Alshammari, Jinsung Cho, Tracy Lenz Page 8 IEE 572 Project Height of Beer Foam 5. EXPERIMENTAL MATRIX We decided 24 full factorial design with 2 replicates depending on 2 blocks. Our experiment is total 32 runs that were divided into 2 blockings. This model used coded value for each factor. Std Run Block A:Pressure psi Factor Response C:Type of D:Type of B:Temperat Height of Biofoam Beer ure Beer Foam F cm 19 1 Operator1 1 -1 -1 1 3.7 13 2 Operator1 -1 1 1 -1 1.9 21 3 Operator1 -1 1 -1 1 2.5 9 4 Operator1 -1 -1 1 -1 0.9 15 5 Operator1 1 1 1 -1 1.8 25 6 Operator1 -1 -1 1 1 3.5 3 7 Operator1 1 -1 -1 -1 1.9 11 8 Operator1 1 -1 1 -1 2.9 17 9 Operator1 -1 -1 -1 1 4.5 23 10 Operator1 1 1 -1 1 3.6 29 11 Operator1 -1 1 1 1 6 27 12 Operator1 1 -1 1 1 7.2 7 13 Operator1 1 1 -1 -1 3 5 14 Operator1 -1 1 -1 -1 6.8 1 15 Operator1 -1 -1 -1 -1 1 31 16 Operator1 1 1 1 1 4.6 24 17 Operator2 1 1 -1 1 5.4 2 18 Operator2 -1 -1 -1 -1 1.4 12 19 Operator2 1 -1 1 -1 6 30 20 Operator2 -1 1 1 1 5.7 14 21 Operator2 -1 1 1 -1 4.7 26 22 Operator2 -1 -1 1 1 5.1 22 23 Operator2 -1 1 -1 1 4 4 24 Operator2 1 -1 -1 -1 4 18 25 Operator2 -1 -1 -1 1 2.5 6 26 Operator2 -1 1 -1 -1 8.9 28 27 Operator2 1 -1 1 1 8.2 20 28 Operator2 1 -1 -1 1 6.4 10 29 Operator2 -1 -1 1 -1 2.5 32 30 Operator2 1 1 1 1 7 8 31 Operator2 1 1 -1 -1 4.5 16 32 Operator2 1 1 1 -1 3.2 Table 3: Test Matrix Serhan Alshammari, Jinsung Cho, Tracy Lenz Page 9 IEE 572 Project Height of Beer Foam 6. RESULTS AND ANALYSIS 6.1 Estimate Factor Effects The main effects and the interaction effects were calculated, and in terms of checking normality of the model and ANOVA table, the model could be renovated by model refinement in order to obtain a better model. The half normal plot was utilized in finding the significant factors that affect the response. The following table is the experimental matrix that was utilized in our DOE project. This model was simulated by using Design-Expert 8.0. 6.1.1 Analysis of Variance First of all, ANOVA (analysis of variance) table was created based on the data that were obtained by 32 tests. The table below showed that this model is significant because of p-value. Source Block Model A-Pressure B-Biofoam C-Type of Beer D-Temperature AB AC AD BC BD CD ABC ABD ACD BCD ABCD Residual Cor Total Sum of Squares 17.5528 107.6697 4.1328 4.4253 1.5753 18.7578 21.6153 2.9403 5.3628 6.7528 8.5078 15.5403 0.0903 3.9903 1.7578 8.5078 3.7128 12.1422 137.3647 DF 1 15 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 15 31 Mean Squares 17.5528 7.1780 4.1328 4.4253 1.5753 18.7578 21.6153 2.9403 5.3628 6.7528 8.5078 15.5403 0.0903 3.9903 1.7578 8.5078 3.7128 0.8095 F-Value p-value Prob > F 8.8674 5.1055 5.4669 1.9461 23.1727 26.7027 3.6324 6.6250 8.3422 10.5102 19.1979 0.1116 4.9295 2.1715 10.5102 4.5867 < 0.0001 0.0392 0.0336 0.1833 0.0002 0.0001 0.0760 0.0212 0.0113 0.0055 0.0005 0.7430 0.0422 0.1613 0.0055 0.0490 significant Table 4: ANOVA for the Full Design Based on this table, the influential factors in this model are three main factors (A-pressure, Bbiofoam, D-temperature) except the factor C (Type of Beer). Beside AC, ABC, and ACD, almost of interaction factors were determined as a significant. This indicated that these factors have strong association with each other. Mostly, this model looks a strong model based on p-value. To find out influential factors of this model accurately, we utilized in half normal plot. Serhan Alshammari, Jinsung Cho, Tracy Lenz Page 10 IEE 572 Project 6.1.2 Height of Beer Foam Normal Plot Analysis 6.1.2.1 Half Normal Plot The figure below was the half normal plot of this model. Design-Expert?Software Height of Beer Foam Half-Normal Plot 99 H a lf-N o rm a l % P ro b a b ility Error estimates A: Pressure B: Biofoam C: Type of Beer D: Temperature Positive Effects Negative Effects AB 95 D CD 90 80 AD B A ABD ACABCD CACD 70 50 30 20 10 0 BC BCD BD ABC 0.00 0.41 0.82 1.23 1.64 |Standardized Effect| Figure 2 : Half Normal Plot This is the plot of the absolute value of the effect estimates against their cumulative normal probabilities. Except ABC, one of three-factor interactions, every factor seems to be significant. 6.1.2.2 Normal Plot of Residuals The figure below is the normal plot of residuals in this model. Serhan Alshammari, Jinsung Cho, Tracy Lenz Page 11 IEE 572 Project Height of Beer Foam Design-Expert?Software Height of Beer Foam Normal Plot of Residuals Color points by value of Height of Beer Foam: 8.9 99 N o rm a l % P ro b a b ility 0.9 95 90 80 70 50 30 20 10 5 1 -3.00 -2.00 -1.00 0.00 1.00 2.00 3.00 Internally Studentized Residuals Figure 3 : Normal Plot of Residuals There are obviously two outliers (std.17 and std.18 in the table) found in this plot. Based on the influential points from Design-Expert 8.0, these two points are turned out the outliers because studentized residuals and fitted value (DFFITS) of two points exceed the limits (|4.25|, |-4.25| > 3.85). DFFITS is the way to measure the influence of the ith observation on the fitted value in standard deviation units. However, except those outliers found, this plot has no severe problem for normality of the model. 6.1.3 R-Squared Various R-Squared values are presented in the table below. Std. Dev. 0.8997 R-Squared 0.8987 Mean 4.2281 Adj R-Squared 0.7973 C.V. % 21.2792 Pred R-Squared 0.5388 Table 5: R Squared Values for Complete Design The “R-Squared” is to confirm the proportion of total variability. This model has the RSquared of 0.8987, which is probably a good model. However, this model had significant difference between "Adj R-Squared" of 0.7973and "Pred R-Squared" of 0.5388. This means that this model could have a large block effect or possibility of model or data problem. We can try several ways (i.e. response transformation, model reduction, outliers, etc) to make a better model. Serhan Alshammari, Jinsung Cho, Tracy Lenz Page 12 IEE 572 Project 6.1.4 Height of Beer Foam Model Refinement 6.1.4.1 Box-Cox Plot For the most suitable transformation way, Box-Cox method is generally utilized. The figure below is the result of Box-Cox plot for this model. Design-Expert?Software Height of Beer Foam Box-Cox Plot for Power Transforms Lambda Current = 1 Best = 0.69 Low C.I. = -0.04 High C.I. = 1.5 9.00 L n (R e s id u a lS S ) 8.00 Recommend transform: None (Lambda = 1) 7.00 6.00 5.00 4.00 3.00 2.00 -3 -2 -1 0 1 2 3 Lambda Figure 4:Box-Cox Plot Lamda calculated in box-cox method is 1, meaning there is no recommended transformation of response to make a better model. So, for this model, transformation does not work well. 6.1.5 Model Reduction: Discarding Outliers Beside the transformation, the residual plots above indicated there are two outliers that could affect this model differently. There are two ways of controlling outliers. One suggestion is to substitute these oultiers for an estimate that is described by Chapter 4 for blocked designs (Motgomery, 2008). This will help keeping the orthogonality of the design, which makes analysis easy. The other way is to discard an outlier and analyzing the remining observations. This could make our model non-orthogonal, but the least squared does not need an orthogonal design so that this model could be analyzed regardless of orthogonality. Also, the correlation, which affects the normal probability plotting, is very small by a missing observation relatvely in 2k design having at least 4 factors or over. So, the researcher considered removing these outliers. The table below is shonw the ANOVA after deleting two outliers. Serhan Alshammari, Jinsung Cho, Tracy Lenz Page 13 IEE 572 Project Height of Beer Foam Sum of Squares Block 22.0163 Model 106.5387 A-Pressure 7.8400 B-Biofoam 8.1225 C-Type of Beer 5.0625 D-Temperature 2.8900 AB 21.6225 AC 0.0225 AD 9.0000 BC 10.24 BD 0.49 CD 17.2225 ABC 1.3225 ABD 0.0025 ACD 5.29 BCD 0.49 Residual 5.67866667 Cor Total 134.233667 Source DF 1 14 1 1 1 1 1 1 1 1 1 1 1 1 1 1 14 29 Mean Squares 22.0163 7.6099 7.8400 8.1225 5.0625 2.8900 21.6225 0.0225 9.0000 10.24 0.49 17.2225 1.3225 0.0025 5.29 0.49 0.40561905 F-Value p-value Prob > F 18.7612 19.3285 20.0249 12.4809 7.1249 53.3074 0.0555 22.1883 25.2453628 1.20803005 42.459791 3.26044846 0.00616342 13.0417938 1.20803005 < 0.0001 0.0006 0.0005 0.0033 0.0183 < 0.0001 0.8172 0.0003 0.0002 0.2903 < 0.0001 0.0925 0.9385 0.0028 0.2903 significant Table 6: ANOVA Table without Outliers The whole model was determined as a significant one. The significant factors found in this table are all main factors (A, B , C ,D), 4 two-factor interactions (AB, AD, BC, CD), and one three-factor interaction (ACD). Most factors are significant in this model. Also, like the same analysis from the original model, every factor is drastically interacted and influenced with each other. The table below is shown the varied R-Squared values. R-Squared significantly was improved after discarding the outliers. It seems that there is no problem for the big difference between Adj R-Squared and Pred R-Squared in this renovated model. This means discarding outliers would be a reasonable way for improving the model of this project. In addition, we tried to have a better R-Squared model deleting BD, ABD, and BCD, which is a non-significant term. The ANOVA table below is changed below after deleting nonsignificant terms. Serhan Alshammari, Jinsung Cho, Tracy Lenz Page 14 IEE 572 Project Height of Beer Foam Sum of Squares Block 22.0163 Model 105.6249 A-pressure 16.0023 B-biofoam 16.5123 C-type 10.9203 D-temperature 2.8623 AB 40.2003 AC 0.4202 AD 18.0903 BC 20.30625 CD 32.58025 ABC 3.66025 ACD 11.34225 Residual 6.59241667 Cor Total 134.233667 Source DF 1 11 1 1 1 1 1 1 1 1 1 1 1 17 29 Mean Squares 22.0163 9.6023 16.0023 16.5123 10.9203 2.8623 40.2003 0.4202 18.0903 20.30625 32.58025 3.66025 11.34225 0.38778922 F-Value p-value Prob > F 24.7616 41.2653 42.5805 28.1603 7.3809 103.6652 1.0837 46.6497 52.3641431 84.0153586 9.43876171 29.2484926 < 0.0001 < 0.0001 < 0.0001 < 0.0001 0.0147 < 0.0001 0.3124 < 0.0001 < 0.0001 < 0.0001 0.0069 < 0.0001 significant Table 7. ANOVA Table without Outliers and Non-Significant Terms Every term looks significant but AC, which was not discarded due to hierarchy issue. This model was proven as a better model because of the improved R-Squared below. Model Original Discarding Outliers Discarding Outliers + Non-significant terms R-Squared 0.8987 0.9494 0.9413 Adj R-Squared 0.7973 0.8988 0.9032 Pred R-Squared 0.5388 0.7676 0.8173 Table 8. Comparison of R-Squared The third column informed that we have a better Adj R-Squared and Pred R-Squared rather than only discarding outliers (second column). Adj R-Squared increases after deleting non-significant terms (BD, ABD, and BCD). This is actually a efficient improvement because R-Squared (94.13%) is almost same as the second column (94.94%). Serhan Alshammari, Jinsung Cho, Tracy Lenz Page 15 IEE 572 Project Height of Beer Foam 6.2 Final Model: Model Adequacy Checking 6.2.1 Plot of Residuals 6.2.1.1 Normal Plot of Residuals Design-Expert?Software height of foam Normal Plot of Residuals Color points by value of height of foam: 8.9 99 N o rm a l % P ro b a b ility 0.9 95 90 80 70 50 30 20 10 5 1 -3.00 -2.00 -1.00 0.00 1.00 2.00 3.00 Internally Studentized Residuals Figure 5: Normal Plot of Residuals for the Final Reduction Model Without outliers, the figure shows there is no doubt of normality assumption. Serhan Alshammari, Jinsung Cho, Tracy Lenz Page 16 IEE 572 Project Height of Beer Foam 6.2.1.2 Run Order Design-Expert?Software height of foam 0.9 3.00 In te rn a lly S tu d e n tiz e d R e s id u a ls Color points by value of height of foam: 8.9 Residuals vs. Run 2.00 1.00 0.00 -1.00 -2.00 -3.00 1 6 11 16 21 26 31 Run Number Figure 6: Residuals Vs Run Order This plot of residuals is good for checking correlation between residuals. There is no cause to consider this model as any violation of the independence or constant variance assumptions. 6.2.1.3 Predicted Value The next residual model with predicted value is to check another normality of model. This plot also proved there is no violation of normaility assumptions due to constant distribution and structureless model. However, there are two outliers found easily in this plot as well. These outliers were the same one found in the ANOVA table above. Serhan Alshammari, Jinsung Cho, Tracy Lenz Page 17 IEE 572 Project Height of Beer Foam Design-Expert?Software height of foam Residuals vs. Predicted Color points by value of height of foam: 8.9 In te rn a lly S tu d e n tiz e d R e s id u a ls 3.00 0.9 2.00 1.00 0.00 -1.00 2 -2.00 -3.00 0.00 2.00 4.00 6.00 8.00 10.00 Predicted Figure 7: Residuals Vs Predicted 6.2.1.4 Factors Figures below are shown the plot of residuals with each factor. Design-Expert?Software xpert?Software foam Residuals vs. biofoam of foam Residuals vs.height pressure Color points by value of height of foam: 8.9 In te rn a lly S tu d e n tiz e d R e s id u a ls 3.00 3.00 In te rn a lly S tu d e n tiz e d R e s id u a ls nts by value of foam: 0.9 2.00 1.00 0.00 -1.00 -2.00 2.00 1.00 0.00 -1.00 -2.00 -3.00 -3.00 -1.00 -0.50 0.00 0.50 A:pressure Serhan Alshammari, Jinsung Cho, Tracy Lenz 1.00 -1.00 -0.50 0.00 0.50 1.00 B:biofoam Page 18 IEE 572 Project Height of Beer Foam xpert?Software foam Design-Expert?Software Residuals vs. heighttype of foam In te rn a lly S tu d e n tiz e d R e s id u a ls Residuals vs. temperature Color points by value of height of foam: 8.9 3.00 3.00 In te rn a lly S tu d e n tiz e d R e s id u a ls nts by value of foam: 0.9 2.00 1.00 0.00 -1.00 -2.00 2.00 1.00 0.00 -1.00 2 -2.00 -3.00 -3.00 -1.00 -0.50 0.00 0.50 -1.00 1.00 -0.50 0.00 0.50 1.00 D:temperature C:type Figure 8. Plot of Residuals vs Factors From this plot, we know the variability of each factor with some levels. The residual plots from Factor B, C, D present there is little more variability at high level. The pressure (Factor A) has higher variability at low level. However, it can be concluded that there is no huge difference of variability at each level. At low pressure, variability is more likely due to inconsistency in pressure in the draft line.` 6.3 Final Model: One Factor Effects The plots of one factor below are shown respectively. Expert?Software oding: Actual foam Design-Expert?Software One Factor Factor Coding: Actual One Factor height of foam Warning! Factor involved in multiple interactions. 6 ressure actors m = 0.00 0.00 rature = 0.00 X1 = B: biofoam Actual Factors A: pressure = 0.00 C: type = 0.00 D: temperature = 0.00 5 h e ig h t o f fo a m h e ig h t o f fo a m 5 4 3 2 4 3 2 1 1 0 0 -1.00 -0.50 0.00 0.50 A: pressure Serhan Alshammari, Jinsung Cho, Tracy Lenz Warning! Factor involved in multiple interactions. 6 1.00 -1.00 -0.50 0.00 0.50 1.00 B: biofoam Page 19 IEE 572 Project Expert?Software oding: Actual foam Height of Beer Foam Design-Expert?Software One Factor Factor Coding: Actual One Factor height of foam Warning! Factor involved in multiple interactions. 6 ype X1 = D: temperature actors ure = 0.00 m = 0.00 rature = 0.00 Actual Factors A: pressure = 0.00 B: biofoam = 0.00 C: type = 0.00 5 h e ig h t o f fo a m h e ig h t o f fo a m 5 Warning! Factor involved in multiple interactions. 6 4 3 2 1 4 3 2 1 0 0 -1.00 -0.50 0.00 0.50 1.00 -1.00 C: type -0.50 0.00 0.50 1.00 D: temperature Figure 9. Plots of One Factor Effect This plot could explain how each factor affects the response at some levels. All the plots describe the height of beer foam is high at high level of each factor, and the gradient of each line is not fairly big. At high level (high temperature, pressure, using biofoam, and red beer) of each factor, we will have higher height of beer foam. 6.4 Final Model: Interaction Effects To check the interaction effects, two-factor interactions are only considered because threefactor interactions have small coefficients relatively. Also, two-factor interactions are good enough to describe how differently or significantly factors are interacted with each other. This plot is so important for our model conclusions because the effects of interaction factors are existing based on the ANOVA table. The first plot of interaction effect is the plot between pressure (factor A) and biofoam (factor B), which has highest sum of squares. Serhan Alshammari, Jinsung Cho, Tracy Lenz Page 20 IEE 572 Project Height of Beer Foam Design-Expert?Software Factor Coding: Actual height of foam Interaction Warning! Term involved in ABC interaction. 6 Actual Factors C: type = 0.00 D: temperature = 0.00 5 h e ig h t o f fo a m B- -1.00 B+ 1.00 B: biofoam 7 X1 = A: pressure X2 = B: biofoam 4 3 2 1 0 -1.00 -0.50 0.00 0.50 1.00 A: pressure Figure 10: pressure and Biofoam Interaction On the left hand side of this plot, two points represent levels of biofoam (factor B) at low pressure without any influence of the other factors (type of beer, temperature). This means biofoam affects the height of foam at low pressure. At low pressure, the existence of biofoam will highly multiply the size of beer foam. On the contrary, the size of beer foam is high at high pressure regardless of the existence of biofoam. The next figure is the interaction plot between type of beer (factor C) and temperature (factor D), which has the second highest sum of squares. Serhan Alshammari, Jinsung Cho, Tracy Lenz Page 21 IEE 572 Project Height of Beer Foam Design-Expert?Software Factor Coding: Actual height of foam Interaction Warning! Term involved in ACD interaction. 6 Actual Factors A: pressure = 0.00 B: biofoam = 0.00 5 h e ig h t o f fo a m D- -1.00 D+ 1.00 D: temperature 7 X1 = C: type X2 = D: temperature 4 3 2 1 0 -1.00 -0.50 0.00 0.50 1.00 C: type Figure 11: Temperature and Type of Beer Interaction This plot displays that the height of beer foam is large in red beer at high temperature. Red beer is influenced by temperature variation more than light beer. On the contrary, light beer is not much affected by temperature based on two points on the left hand of this plot. The next figure is the interaction plot for pressure (factor A) and temperature (factor D). Design-Expert?Software Factor Coding: Actual height of foam Interaction Warning! Term involved in ACD interaction. 6 Actual Factors B: biofoam = 0.00 C: type = 0.00 5 h e ig h t o f fo a m D- -1.00 D+ 1.00 D: temperature 7 X1 = A: pressure X2 = D: temperature 4 3 2 1 0 -1.00 -0.50 0.00 0.50 1.00 A: pressure Figure 12: Temperature and Pressure Interaction Serhan Alshammari, Jinsung Cho, Tracy Lenz Page 22 IEE 572 Project Height of Beer Foam At high pressure, there is big variation of beer foam size between temperature levels, meaning both high pressure and temperature produces large size of beer foam. Design-Expert?Software Factor Coding: Actual height of foam Interaction Warning! Term involved in ABC interaction. 6 Actual Factors A: pressure = 0.00 D: temperature = 0.00 5 h e ig h t o f fo a m C- -1.00 C+ 1.00 C: type 7 X1 = B: biofoam X2 = C: type 4 3 2 1 0 -1.00 -0.50 0.00 0.50 1.00 B: biofoam Figure 13: Biofoam and Type of Beer Interaction This plot is the interaction plot between biofoam and type beer. Interestingly, type of beer is highly influenced when beer has no biofoam. Without influence of biofoam, red beer produces more beer foam than light beer. However, all types of beer make greater beer foam using biofoam. This proves that beerfoam produces more beer foam. In summary, all main factors are significant in height of beer foam based on the ANOVA table. However, the interaction between main factors strongly affects this model more than only one factor effect. Also, this could be indicated by checking the size of coefficient in the next section (6.5). This conclusion resulted from the interaction plots that have been analyzed above. In short, the size of beer foam mostly increases at high pressure irrespective of any factors. Using biofoam (factor B) also produces higher size of beer foam relatively. Furthermore, temperature severely varies depending on pressure and type of beer. Temperature itself has lowest effects for the response relatively. Red beer generally has more foam than light beer. Serhan Alshammari, Jinsung Cho, Tracy Lenz Page 23 IEE 572 Project Height of Beer Foam 6.5 Final Regression Model The coded and actual final regression models are shown below. Final Equation in Terms of Coded Factors: height of foam = +3.80 +0.79 +0.80 +0.65 +0.33 -1.25 -0.13 +0.84 -0.89 +1.13 +0.38 -0.67 *A *B *C *D *A*B *A*C *A*D *B*C *C*D *A*B*C *A*C*D Final Equation in Terms of Actual Factors: height of foam = +3.79688 +0.79063 +0.80312 +0.65312 +0.33438 -1.25312 -0.12812 +0.84062 -0.89062 +1.12813 +0.37812 -0.66563 * pressure * biofoam * type * temperature * pressure * biofoam * pressure * type * pressure * temperature * biofoam * type * type * temperature * pressure * biofoam * type * pressure * type * temperature As looking at the coefficients of each factor, two-factor interactions have large number except AC, indicating each factor strongly influences beer foam height when they interact. Serhan Alshammari, Jinsung Cho, Tracy Lenz Page 24 IEE 572 Project Height of Beer Foam 7. CONCLUSIONS AND RECONMMENDATION The brewery has two objectives in draft beer service regarding foam height. The first is a foam that is adequate relative the mug size the mug size and beer foam that does not dissipate too quickly as the customer drinks the beer. From the analysis the observations find that red beer (due to its chemical composition) have more potential to create high foam (figure 18). That gives a clue to pay more attention when trying to reduce the foam it produces by controlling the factors that have a significant affect. However, the presence of biofoam for red beer does not have a huge affect in the foam height. On the other hand biofoam has a significant effect in keeping high foam in light beer so the same decision will be made for not using it. When looking at the interaction between beer type and temperature (figure 16) the temperature affects the red beer more significantly, so in order to reduce the beer foam height, have the line in cold temperature. Also, the biofoam does not have a big affect on the foam height when handling in high pressure. Moreover, the selection of pressure and temperature as factors affecting the process defines an overlap with each other since both factors help to increase the level of CO2 in the beer. When To observe the interaction between these factors, look for a combination of high pressure and low temperature to reduce the foam height (figure 16). Based on what Derek said about the suitable temperature for each beer type, the optimum temperature for red beer is between 37 and 40 Fahrenheit. The taste of red beer in these temperatures could be better as it warms up depending on customer preference. This temperature range is applied to light beer as well. This description is in accord with the analysis of this experiment because the temperature chosen in this experiment was 39 Fahrenheit, which is placed within this range (37 to 40 Fahrenheit). Figure 16 and 17 proved low temperature created a relatively small beer foam even though light beer has more foam with low temperature than red one. To summarize the result of the analysis and mention some recommendations consider that this model has very strong interactions of each factor. To achieve adequate beer foam for customers and managers, low pressure without biofoam is required regardless of temperature effect. In beer type, red beer produces more foam than light beer. However, most customers prefer red beer to light. For the red one, the best combination would be to pour in low temperature with low pressure. Keeping low temperature in transferring beer lines could mostly be recommended for relatively smaller beer foam. Generally, biofoam is utilized depending customer preference, because some customers want more beer foam. Thus, optimal condition to pour for beer height foam will be to control low pressure, not using biofoam, and keeping beer lines in low temperature (37 to 40 F). 8. REFERENCES Montgomery, C. Douglas, (2008), “Design and Analysis of Experiments.”, John Wiley & Sons, Inc., 7th edition. http://en.wikipedia.org/wiki/Brewing. http://www.asbcnet.org/ Serhan Alshammari, Jinsung Cho, Tracy Lenz Page 25
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