Permanent-magnet helicon sources for etching, coating, and thrust Francis F. Chen, UCLA Low Temperature Plasma Teleseminar, June 14, 2013; originally prepared for (but not given at): 2013 Workshop on Radiofrequency Discharges, La Badine, La Presqu’ile de Giens, France, 29-31 May 2013 Helicons are RF plasmas in a magnetic field Density increase over ICP Prf 200 400 600 800 1000 % 16% 21% 35% 38% 42% UCLA Helicon sources usually use heavy magnets The MØRI source of Plasma Materials Technologies, Inc. UCLA Size of the MØRI source UCLA The source has been simplified to this This uses a commercially available 2 x 4 x 0.5 inch NeFeB magnet The discharge is 5 cm high and 5 cm in diameter UCLA How did we get here? First, the HELIC code of Arnush Loop antenna Helical antenna h B0 a b Lc D. Arnush, Phys. Plasmas 7, 3042 (2000). UCLA Examples of HELIC results: Pr , Pz 5000 -3 n (cm ) 2.5E+11 4.0E+11 6.3E+11 1.0E+12 P(r) (arb.) 4000 3000 2000 1000 0 0.000 0.005 0.010 0.015 r (m) 0.020 0.025 6 13 MHz, 80G 5 1.6E+12 2.5E+12 4.0E+12 6.3E+12 1.0E+13 P(z) 4 3 2 1 0 0 5 10 15 20 25 30 z (cm) UCLA Most important, RnB: power deposition UCLA RnB results organized in matrices Matrix A: B-field D = 7.4" 100W 300W 500W Folder D7W100 Folder D7W300 Folder D7W500 1 mTorr, ei = -1 D = 11" D = 13" Folder D11W100 Folder D11W300 Folder D11W500 Folder D13W100 Folder D13W300 Folder D13W500 Matrix C: pressure D = 0, 300W D=0 1 mTorr 10 mTorr conductor Folder P1cond Folder P10cond insulator Folder P1ins Folder P10ins Folder D0W100 Folder D0W300 Folder D0W500 Similar matrices for tube size determined the tube design. After that, there are matices for the experimental results. UCLA Optimized discharge tube: 5 x 5 cm GAS INLET (optional) 1. Diameter: 2 inches 2. Height: 2 inches 3. Aluminum top 5 cm ANTENNA 4. Material: quartz 5. “Skirt” to prevent eddy currents canceling the antenna current 5.1 cm 10 cm The antenna is a simple loop, 3 turns for 13 MHz, 1 turn for 27 MHz. The antenna must be as close to the exit aperture as possible. Antenna: 1/8” diam tube, water-cooled UCLA Design of matching circuit (1) N loads R, L Z2 - short cables R, L Z2 R, L R, L Z1 - long cable Z1 Matching ckt. (standard) C2 C1 50W PS Distributor Matching ckt. (alternate) C2 C1 UCLA Design of 50W matching circuit (2) Let the load be RL + jXL : R and X have first to be transformed by cable length k = wR0C, R0 = 50W UCLA Forbidden regions of L, R, and Z (N = 8) 2000 800 N N 8 6 4 2 1 1000 200 0 0 0.5 1 L (mH) 1.5 2 0 2.5 0.5 1 L (mH) 1600 2000 C1(S) C2(S) 1400 1200 C1(S) C2(S) 1500 1000 C (pF) C (pF) 400 500 0 8 6 4 2 1 600 C2 (pF) C1 (pF) 1500 800 1000 600 500 400 200 0 0 0 50 100 Z2 (cm) 150 200 0.5 1.5 2.5 R (ohms) 3.5 4.5 UCLA Instead, we can use annular PMs 8 PM Permanent magnet 6 4 2 NdFeB ring magnet 3” ID, 5” OD, 1” high 0 -2 Stagnation point The far-field is fairly uniform -4 -6 Put plasma here -8 -10 or here, to adjust B-field -12 -14 -16 -10 -8 -6 -4 -2 0 2 4 6 8 10 UCLA Experimental chamber 19 cm The magnet height is set for optimum B-field 6.8 Port 1 16.9 WALL MAGNETS 27.2 Port 2 38 Langmuir probes at three ports Port 3 46 PUMP BAFFLE AND GROUND PLANE Gate Valve To Turbo Pump UCLA Optimization of the B-field Peak density in Port 2 vs. B and Prf @ 27 MHz 30-60 G is best UCLA Typical scan of “Low-field peak” UCLA Density of ejected plasma 5 n11, 65G n11, 280G 19 cm 3 n (10 /cm ) 4 11 3 6.8 2 Port 1 16.9 1 WALL MAGNETS 27.2 Port 2 0 38 -25 -20 -15 -10 -5 0 5 10 15 20 25 r (cm) Port 3 46 4.5 3.0 2.5 n (10 11 -3 PUMP BAFFLE AND GROUND PLANE 6.8 16.9 27.2 3.5 cm ) 62 G, 400W cm below source 4.0 2.0 1.5 1.0 Gate Valve 0.5 0.0 -20 -10 0 r (cm) 10 20 To Turbo Pump UCLA Vertical probe for inside plasma LANGMUIR PROBE PERMANENT MAGNET HEIGHT ADJUSTMENT GAS FEED UCLA Axial density profile inside the tube 16 400W, 13.56 MHz, 15 mTorr 16 Jan. 4 w. Mk2 Jan. 5 w. ESPion 14 12 10 Horiz. Probe point n11 n11 12 8 8 Bottom of tube 6 4 4 400W, 62G 2 0 0 0 2 4 6 z (cm) 8 10 12 0 2 4 6 z (cm) 8 10 Density inside the tube is low (<1013 cm-3) because plasma is efficiently ejected. UCLA 12 Downstream density: 6 x 1011 cm-3 7 15 mTorr Port 2 Helicon ICP 5 -3 cm ) 6 4 n (10 11 Density increase over ICP 3 2 1 0 0 200 400 600 Prf (W) 800 1000 1200 Prf 200 400 600 800 1000 % 16% 21% 35% 38% 42% UCLA Port 2 density is higher at 13 MHz 9 Port 2 8 n (10 11 -3 cm ) 7 13 MHz 6 5 4 27 MHz 3 2 1 0 0 200 400 600 Prf (W) 800 1000 1200 This was a surprise and is contrary to theory. UCLA Cause and location of the “double layer” F.F. Chen, Phys. Plasmas 13, 034502 (2006) ne = ni = n ns ni n PRESHEATH ne v = cs PLASMA + SHEATH xs x ne n0e , where eV /KTe vis cs ( KTe / M )1/2 Wis ½Mvis2 ½KTe s ½, ns / n0 e1/2 B / B0 n / n0 (r0 / r )2 r / r0 e1/4 1.28 Maxwellian electrons Bohm sheath criterion A sheath must form here Single layer forms where r has increased 28% Where a diffuse “double layer” would occur 250 B (G) 200 150 100 Approx. location of "double layer" 50 0 5 10 15 20 25 30 z (cm) UCLA Ion energy distribution by Impedans SEMion UCLA IEDFs vs. Prf in Port 1 2E-06 600W 500W 400W 400W repeat 300W 200W 100W Vs IEDF 2E-06 1E-06 5E-07 0E+00 0 5 10 V 15 20 25 30 UCLA Conditions at Port 1 (r = 0) at 400W 7 100 6 Ii squared Ii squared (OML) 10 Ie (mA) 2 3 1 2 0.1 1 0 0.01 -100 -80 -60 V -40 -20 0 20 -5 0 5 V 10 15 20 6 Port 1 400W 5 -3 3 cm ) 4 11 n11 n (10 I (mA) 4 2 5 Ie Ie(fit) Ie (0) 2 Te eVs iVs n11 2.14 15.9 27 4.21 Te (eV) Plasma potential 1 0 -20 -10 0 r (cm) 10 20 UCLA Mach probe (in Port 2) 0.50 Hutchinson: v flow vf cs Result: vf cs 0.14 cs I up 1 Iup ln 0.75ln K I down I down ( K 1.34) 0.14 This seems very low. It should be much higher in Port 1 UCLA helicon ARRAY sources DISTRIBUTOR SUBSTRATE TO PUMP MEDUSA MEDUSA 1 UCLA The Medusa 2 large-area array UCLA An array source for roll-to-roll processing 165 cm Height can be adjusted electrically if desired Aluminum sheet 15 cm 30 cm Z1 Probe ports Z2 The source requires only 6” of vertical space above the process chamber. Two of 8 tubes are shown. UCLA Top view of Medusa 2 3.5" 29" 7" 7" 21" 7" 7" 65" Possible positions shown for 8 tubes. Tubes set in deeply (½ inch) 7" 3/4” aluminum 12" 1/2" aluminum Endplates: gas feed and probe port at each end. Substrate motion Two arrangements of the array 35.6 cm y 17.8 Staggered array x 53.3 cm 17.8 17.8 Covers large area uniformly for substrates moving in the y-direction 165 cm Top view 53.3 cm 17.8 y x 17.8 17.8 17.8 165 cm Compact array Gives higher density, but uniformity suffers from end effects. Operation with cables and wooden magnet tray It’s best to have at least 3200W (400W per tube) to get all tubes lit equally. Details of distributor and discharge tube The top gas feed did not improve operation. UCLA A rectangular 50W transmission line 50-W line with ¼” diam Cu pipe for cooled center conductor Operation with rectangular transmission line Radial profile at Z2 across rows 3.5 3 n KTe -3 cm ) 2.5 n (10 11 2 1.5 1 0.5 0 -25 -20 -15 -10 -5 0 r (cm) 5 10 15 20 25 Density profiles with staggered array Staggered configuration, 2kW Bottom probe array 5 Staggered, 2kW, D=7", 20mTorr Argon n (1011 cm-3) 4 y (in.) -3.5 0 3.5 3 2 1 0 -8 -6 -4 -2 0 2 4 6 x (in.) 8 10 12 14 16 Density profiles with compact array Compact configuration, 3kW Bottom probe array 10 Compact, 3kW, D=7", 20mTorr y (in) 3.50 3.5 n (1011 cm -3) 8 6 Data by Humberto Torreblanca, Ph.D. thesis, UCLA, 2008. 4 2 0 -8 -6 -4 -2 0 2 4 6 x (in.) 8 10 12 14 16 UCLA Plans for an 8-tube array for round substrates Distributor RG 393 teflon coax cable to each antenna. No center is necessary! Antennas aretube water-cooled in pairs, so that Antennas are 1/8" OD copper tubing. water enters and leaves the system at ground potential. UCLA
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