Electronic Supplementary Information
Ruthenium(II) carbonyl complexes containing benzhydrazone ligands:
Synthesis, structure and facile one-pot conversion of aldehydes to amides
Rupesh Narayana Prabhu, Rengan Ramesh*
School of Chemistry, Bharathidasan University, Tiruchirappalli 620 024, Tamil Nadu, India
Contents
1
H NMR of complexes
– Fig. S1 – S8
Pg. S2 – S5
1
H NMR of amides
– Fig. S9 – S18
Pg. S6 – S10
– Fig. S19 – S28
Pg. S11 – S15
13
C NMR of amides
S1
Fig. S1. 1H NMR spectrum of complex (1)
Fig. S2. 1H NMR spectrum of complex (2)
S2
Fig. S3. 1H NMR spectrum of complex (3)
Fig. S4. 1H NMR spectrum of complex (4)
S3
Fig. S5. 1H NMR spectrum of complex (5)
Fig. S6. 1H NMR spectrum of complex (6)
S4
Fig. S7. 1H NMR spectrum of complex (7)
Fig. S8. 1H NMR spectrum of complex (8)
S5
Fig. S9. 1H NMR spectrum of 4-nitrobenzamide
Fig. S10. 1H NMR spectrum of 4-bromobenzamide
S6
Fig. S11. 1H NMR spectrum of benzamide
Fig. S12. 1H NMR spectrum of 4-methylbenzamide
S7
Fig. S13. 1H NMR spectrum of 4-methoxybenzamide
Fig. S14. 1H NMR spectrum of thiophene-2-carboxamide
S8
Fig. S15. 1H NMR spectrum of 3-methyl thiophene 2-carboxamide
Fig. S16. 1H NMR spectrum of pyridine-2-carboxamide
S9
Fig. S17. 1H NMR spectrum of pyridine-4-carboxamide
Fig. S18. 1H NMR spectrum of indole-3-carboxamide
S10
Fig. S19. 13C NMR spectrum of 4-nitrobenzamide
Fig. S20. 13C NMR spectrum of 4-bromobenzamide
S11
Fig. S21. 13C NMR spectrum of benzamide
Fig. S22. 13C NMR spectrum of 4-methyl benzamide
S12
Fig. S23. 13C NMR spectrum of 4-methoxy benzamide
Fig. S24. 13C NMR spectrum of thiophene-2-carboxamide
S13
Fig. S25. 13C NMR spectrum of 4-methyl thiophene-2-carboxamide
Fig. S26. 13C NMR spectrum of pyridine-2-carboxamide
S14
Fig. S27. 13C NMR spectrum of pyridine-4-carboxamide
Fig. S28. 13C NMR spectrum of indole-3-carboxamide
S15