What the 2015 Methods Update Rule Means to You Presented by Wendy Schultz Ann Arbor Environmental Services Laboratory [email protected] 1 Compliance sample testing? EPA updates the list of approved methods used for compliance testing. 3 EPA updates the list of approved methods used for compliance testing. Methods Update Rule 4 5 Code of Federal Regulations (CFR) 6 Code of Federal Regulations (CFR) Title 40 – Protection of Environment 7 Safe Drinking Water Act (SDWA) 40 CFR Part 141 8 Clean Water Act (CWA) 40 CFR Part 136 9 2015 Methods Update Rule EPA proposed changes Feb. 2015 2015 2016 2017 10 2015 Methods Update Rule EPA proposed changes Comments closed Feb. 2015 May 2015 2015 2016 2017 11 2015 Methods Update Rule EPA proposed changes Comments closed Feb. 2015 May 2015 EPA reviewed comments 2015 2016 2017 12 2016 Methods Update Rule EPA proposed changes Comments closed Signed Final rule Feb. 2015 May 2015 Dec. 2016 EPA reviewed comments 2015 2016 2017 13 2017? Methods Update Rule EPA proposed changes Comments closed Signed Final rule Final rule withdrawn Jan. 2017 Feb. 2015 May 2015 Dec. 2016 EPA reviewed comments 2015 2016 2017 14 Wait, What? Will it apply to me? Clean Water Act (40 CFR Part 136) 18 Drinking Water Methods that: • Reference to 40 CFR Part 136 19 What are the changes? New and Revised Methods EPA ASTM New Revised X X Std. Methods X X USGS X 22 Approved Alternate Test Procedures (ATP) Idexx Colilert-18 with Quanti-tray for Fecal 23 Clarified the ATP procedures. Corrections to 40 CFR Part 136 25 Changes to required containers, preservation techniques and holding times. 26 New Method Detection Limit (MDL) procedure 40 CFR Part 136 Appendix B 27 MDL Sample Comparison Current MDL Revised MDL Spikes 7/year 2/quarter* Blanks 0 Use routine method blanks *less required if analysis is run infrequently 28 MDL Definition Change Current MDL Revised MDL 99% confidence that the measured concentration is greater than zero. 99% confidence that the measured concentration is greater than blank. 29 Day 1 Day 2 Day 3 blanks spikes 30 MDL Calculation MDLspike = tSspike MDLblank = X+tSblank MDL = whichever is greater 31 Ongoing Data Collection Quarterly Annually Spikes 2/quarter Blanks Use routine method blanks Recalculate MDL using ongoing data 32 Look at the annual data Ongoing Data Collection Compare annual data to the existing MDL • If within a factor of 2 – your choice to update • If outside a factor of 2 – you must update MDL 33 MDL Not Applicable to: • • • • • BOD Color pH WET testing others 34 MDL can be determined for TSS 35 What next? Start gathering data 37 Use data from multiple analysts. *not real analysts Use data from multiple instruments*. *not for SDWA Summary Contact Wendy Schultz Ann Arbor Environmental Services Laboratory [email protected] 41
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