Process Name: Fiji Acceptance Test Document Number / Version Number: 2011 One Kendall Square Cambridge, MA 02139 T: 617-674-8800 F: 617-674-8850 www.cambridgenanotech. Cambridge NanoTech Inc. Document Name: Fiji F202 Factory Acceptance Test Customer Name: UMASS Lowell Fiji F200 Date: 13 July 2017 Cambridge NanoTech Inc., 2010 Author: BK Issue Date: 0100217 Document Status: Approved 1 Process Name: Fiji Acceptance Test Document Number / Version Number: 2011 Processes and Procedures 1. Purpose This Acceptance document is to be used for Factory as well as when applicable Customer Site Acceptance of the Fiji Series Atomic Layer Deposition systems. 2. Vacuum Test Results Item Base Pressure Result Factory Results Initial and Date Base pressure BOC w/o Turbo 1.20E-03 Base pressure WRG w Turbo 2.38E-05 Customer Site Initial and Date MV 3/29/12 Base pressure to be checked at 250C after initial bake out, with 20sccm Ar, plasma gas flow, and 20sccm Ar carrier gas flow. Item Time to reach base pressure Result Less than 2 min Factory Results Initials and Date Customer Site Initials and Date MV 3/29/12 Method: Start at base pressure, vent with N2 or Ar, open chamber to atmosphere. Results shall be <3 mins, pump down chamber. Rate 0. 60. 120. 180. 240. 300. of rise (mTorr) 1.29 2.03 3.03 4.49 5.84 7.36 Cambridge NanoTech Inc., 2010 Author: BK Issue Date: 0100217 Document Status: Approved 2 Process Name: Fiji Acceptance Test Document Number / Version Number: 2011 3. Heater Functionality Results Item Spec Set point Factory site Actual Cust site Actual Factory Result Cust site Result Factory Results Initial and Date Chuck Heater Functional 250 250 Yes/ No Yes/ No MV 3/29/12 Chamber Wall Heaters Functional 250 250 250 250 Yes/ No Yes/ No MV 3/29/12 ALD Valve Heater Functional 150 149 Yes/ No Yes/ No MV 3/29/12 Prec. Del. Heater Functional 150 150 Yes/ No Yes/ No MV 3/29/12 Cone Heater Functional 250 250 Yes/ No Yes/ No MV 3/29/12 Prec. Jacket 1 Functional 75 75 Yes/ No Yes/ No MV 3/29/12 Prec. Jacket 2 Functional 75 74 Yes/ No Yes/ No MV 3/29/12 Prec. Jacket 3 Functional 75 75 Yes/ No Yes/ No MV 3/29/12 Customer Site Initial and Date Check the functionality of all available heaters. The actual temperature should be within 2C of the set point temperature. Note: Jalapeño valve heater is either on or off. Cambridge NanoTech Inc., 2010 Author: BK Issue Date: 0100217 Document Status: Approved 3 Process Name: Fiji Acceptance Test Document Number / Version Number: 2011 4. ALD Valve Functionality Results Item Spec Factory Result Cust. site Result ALD Valve 1 Functional Yes/ No Yes/ No MV 3/29/12 ALD Valve 2 Functional Yes/ No Yes/ No MV 3/29/12 ALD Valve 3 Functional Yes/ No Yes/ No MV 3/29/12 ALD Valve 4 Functional Yes/ No Yes/ No MV 3/29/12 Factory Results Initial and Date Customer Site Initial and Date Check the functionality of all available ALD valves by pulsing each valve. Observe the presence of the pulse. MFC Functionality Results Item Spec Set point Factory site Actual Cust site Actual Factory Result Cust site Result Factory Results Initial and Date MFC 1 Ar Functional 50 49.7 Yes/ No Yes/ No MV 3/29/12 MCF 2 Ar plasma Functional 50 50.4 Yes/ No Yes/ No MV 3/29/12 MFC 3 N2 (tested with Ar Functional 50 49.8 Yes/ No Yes/ No MV 3/29/12 MFC 4 O2 Functional 50 49.7 Yes/ No Yes/ No MV 3/29/12 MFC 5 H (tested with Ag) Functional 50 49.8 Yes/ No Yes/ No MV 3/29/12 Customer Site Initial and Date Check the flow functionality of all available MFCs by flowing gas from each MFC and verifying it is within 5% of the set point. @ 50 sccms MFC 0 (021782349) MFC 1 (021782939) MFC 2 (021783246) MFC 3 (021783244) MFC 4 (021783249) Cambridge NanoTech Inc., 2010 Author: BK 49.7 50.4 49.8 49.7 49.8 Issue Date: 0100217 Document Status: Approved 4 Process Name: Fiji Acceptance Test Document Number / Version Number: 2011 5. Functional Process Test Results Standard Al2O3 & HfO2 by thermal and plasma on 150mm Si substrates 150mm Si wafer measurements adjusted for native oxide F200 FAT Thermal Plasma HfO2 Al2O3 F200 CAT HfO2 Al2O3 Thermal Plasma 1 2 216.1 172.1 211.1 180.1 1 2 -13 -13 -13 -13 3 4 Thickness (Å) 217.1 208.1 176.1 176.1 3 4 Thickness (Å) -13 -13 -13 -13 5 227.1 180.1 5 -13 -13 Non-Unif (1-σ) GPC (%) (Å/cycle) 215.9 3.36% 1.08 176.9 1.89% 0.88 Ave. Non-Unif (1-σ) GPC (%) (Å/cycle) -13 0.00% -0.07 -13 0.00% -0.07 Ave. Note: The thermal HfO2 run above had a higher than normal growth at position 5. This is caused by a slightly high door purge value. It was corrected prior to the plasma run. Which shows a perfect value. The results will be rerun at your facility with less than 2% uniformity over the whole wafer. 6. Factory Acceptance and Shipment Authorization Based on the inspection and test results achieved on the Fiji F200 system the system has met the conditions for acceptance at the vendor site and/or the customer site. _________Bob Kane __________________ _______3/29/2012____________ Cambridge NanoTech Date __________________________________ ____________________________ Customer Representative Date 7. Customer Site Acceptance Authorization __________________________________ ____________________________ Cambridge NanoTech Cambridge NanoTech Inc., 2010 Author: BK Date Issue Date: 0100217 Document Status: Approved 5 Process Name: Fiji Acceptance Test Document Number / Version Number: 2011 __________________________________ ____________________________ Customer Representative Cambridge NanoTech Inc., 2010 Author: BK Date Issue Date: 0100217 Document Status: Approved 6
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