EFFECTS OF BIAXIAL STRESS CONDITION FOR FATIGUE PROPERTIES OF TITANIUM Y. Itoha, b, A. Shimamotob, D. Y. Hwangb, T. Nemotoa and H. Matuuraa a National Institute for Longevity Sciences National Center for Geriatrics and Gerontology 36-3, Gengo, Morioka, Obu, Aichi, 474-8522, Japan b Advanced Science Laboratory Saitama Institute of Technology 1690 Fusaiji, Fukaya, Saitama, 369-0293, Japan a [email protected], [email protected] ABSTRACT Machines and structures, such as automobiles are usually subjected to biaxial or three-axial stresses instead of uniaxial stress. However, research on a fatigue failure under multi-axial stress has not been fully presented because such experiments are difficult. To solve this problem, we developed the servo biaxial fatigue-testing machine. Authors already investigated the fatigue crack progress behavior of the magnesium alloy under biaxial stress. As a result, it was suggested that existence of a stress parallel to a crack affects crack progress velocity in AZ31B. In this research, fatigue crack propagation tests of pure titanium were conducted under conditions of biaxial and uniaxial loading by using a cruciform specimen in a biaxial fatigue machine, in order to investigate the effect of non-singular stress cycling on the fatigue crack growth properties. It is because the crystal structure of titanium is the same as magnesium. As a result, we clarified effects of biaxial stress condition for fatigue properties of pure titanium. The fatigue characteristics of pure titanium found that there was little effect of biaxial load stress ratio as a result of this research. Introduction The density of pure titanium is about 3/5 of that of steel. Pure titanium is excellent also not only in specific strength but the difficulty of rusting, the heat conductivity, and bio-compatibility. Therefore, use of titanium to medical equipment, an assisted living instrument, and a life tool is increasing in recent years. When applied to such a purpose, the fatigue characteristics of titanium are indispensable in order to create the design which ensures the reliability and the safety in long-distance run. The effect of non-singular stress acting parallel to the crack plane on fatigue crack propagation is one of the basic problems of fatigue crack propagation in biaxial stress fields. According to linear fracture mechanics the crack growth rate is controlled by the stress intensity factor (SIF), so the non-singular stress has no effect on the growth rate. While several experimental data by Kitagawa et al. and Liu et al. more or less support this principle, some data indicate that the non-singular stress does influence the crack growth rate [1, 2]. For example, Tanaka et al. and Miller reported that the action of a stress parallel to a crack affects crack progress velocity [3-5]. Above results suggest that there is no general consensus how biaxial stress exerts on fatigue crack propagation. In this research, fatigue crack propagation tests of pure titanium were conducted under conditions of biaxial and uniaxial loading by using a cruciform specimen in a biaxial fatigue testing device, in order to investigate the effect of non-singular stress cycling on the fatigue crack growth properties. As a result, the authors obtained the fundamental data about the biaxial fatigue characteristics of pure titanium. Since validity of a servo biaxial fatigue-testing machine is essential for this study, we verified it before conducting the fatigue tests. We present this result as well as the results from the fatigue tests. Verification of the Performance and the Effectiveness of the Biaxial Fatigue Testing Machine A uniaxial and an equal biaxial tensile test were carried out to verify the effectiveness of the biaxial fatigue testing device shown in figure 1 which authors developed. The performance of the device is shown in table 1. The test specimens were fabricated as the shape and size shown in figure 2 (a) and (b). To create test specimens, we processed the plates (aluminum alloy 2024-T3, a thickness, t = 2.54mm, its mechanical properties are given in table 2.) with an end mill with a vertical machining center. The thin strain gauges (KFEL -5-120-C1L3M2R: Kyowa Dengyo) were adhered to the front and back of the center part of the uniaxial specimens as shown in figure 2 (a). In the case of the biaxial test specimens, we attached the thin strain gauges to the front and back of the center part and also at a position of 80 % coverage of the biaxial stress field (in the dotted lines in figure 2 (b)). For the experimental conditions, we set tension speed at 0.02 mm/s in both the uniaxial and the biaxial tests. Strain under each load was measured with a memory recorder analyzer (EDX-1500 A-16AD: Kyowa Dengyo). Figure 3-5 shows the results of the relationship between the load and the strain. As shown in figure 3 and figure 4, we confirm that the experimental values are very well in agreement with the FEM analysis values. Figure 5 shows the relationship between the load and the strain at the center, and in the 80 % coverage of the biaxial stress field of the test specimens. It shows that the relationships have good proportionality up to the measured strain though there are some small deviations. The result suggests that our testing device generates a uniformity biaxial stress field as intended. Figure 1. Biaxial fatigue testing device Table 1. Performance of examination machine Name Size AS2000 Ver1.0 Length 2433mm Side 2266mm The maximum load 50kN Displacement ±15mm Frequency range 0.001-10Hz The maximum velocity 1.5cm/s Size of test specimen 300mm×300mm Control method Feedback control of displacement Control software SAGINOMIYA tiredness examination Software Table 1. Mechanical properties of aluminum alloy Tensile strength [MPa] Proof stress [MPa] Elongation [%] 461 320 17.9 .2 Strain Gauge 0 R2 20 25 60 O6 17 70 120 160 300 70 Unit : mm (a) uniaxial test specimen CH3 30 36.5 140 CH2 Triaxial gauge Biaxial strain gauge CH1~CH6 : Strain Gauge CH6 CH5 23.3 5. 4 CH4 R2 280 CH1 12.7 12.7 44.5 12.7 46.7 140 280 t=3 Unit : mm (b) biaxial test specimen Figure 2. Shape of test specimen and Position of strain gauges Stress [MPa] 450 400 350 FEM Experiment 300 250 200 150 100 50 0 0 1 2 3 4 Strain [%] Figure 3. Relation between stress and strain under uniaxial loading condition 400 Stress [MPa] 350 FEM Experiment 300 250 200 150 100 50 0 0 0.1 0.2 0.3 0.4 0.5 Strain [%] Figure 4. Relation between stress and strain under biaxial loading condition 250 1ch 2ch 3ch 4ch 5ch 6ch Stress [MPa] 200 150 100 50 0 0 0.05 0.1 0.15 0.2 0.25 Strain [%] Figure 5. Measured stress-strain relation by strain gauges in biaxial loading test Experimental Procedure Pure titanium TP340C plates used for this research is 2.5mm thickness. The Chemical composition of TPC340C is shown in Table 2. The mechanical property of TPC340C is shown in Table 3, and the dimension and form of a specimen are shown in Figure 6. The radius of curvature of initial crack at the center of a specimen was set to 0.15mm. We made Y-axis of the specimen as the rolling direction. The fatigue tester used for this experiment was the biaxial, electrically operated, oil-pressure servo tension-compression fatigue tester. In the fatigue crack propagation tests, as shown in Figure 7, we put the stress, σx0 0 0 0 on X-axis and σy on Y-axis. The experiment was conducted on condition of the load stress ratio Rb = σx /σy =0, 0.25, 0.5, 0 0 0 0.75 and 1.0. The maximum values (σx max, σy max) of σx are shown in Table 4. We put stress with sinusoidal in shape, with the 0 0 stress ratio of σy min /σy max = 0, and the cycle speed of 10Hz. Table 2. Chemical compositions of pure titanium TP340C (mass, %) H O N Fe Ti 0.002 0.01 0.01 0.07 bal. Table 3. Mechanical properties of pure titanium TP340C Tensile strength [MPa] Proof stress [MPa] Elongation [%] Young’s modulus [GPa] Poisson’s ratio 408 265 36 102.9 0.321 13.5 154.879 35.5 Y 25 69 300 a=30 X 22.4 12 23 24 140 300 Unit : mm Figure 6. Shape and dimension of fatigue test specimen Figure 7. Stress condition of fatigue test specimen Table 4. Load stress in each biaxial load stress ratio Rb ( = σx0/σy0) 0 0.25 0.5 0.75 1.0 σx0max [MPa] 0 11.43 22.86 34.29 45.72 σy0max [MPa] 45.72 45.72 45.72 45.72 45.72 Results and Discussion As shown figure 8, in all experiments, cracks were propagated from the both ends of a pre-crack tip, and the fatigue crack progressed in the direction of a pre-crack, i.e., the extended direction of a pre-crack tip. Figure 9 shows the relationship between the half crack length a and the number of load cycles N obtained by fatigue tests. We used the laser beam microscope for measurement of half crack length. Figure 9 shows that generating and progress of a fatigue crack become slow in proportion to a stress parallel to a crack. However, in the case of Rb = 0.75, generating and progress of the fatigue crack were the slowest. Existence of such a special biaxial load stress ratio is reported about magnesium [6-9]. However, the special biaxial load stress ratio is not discovered with other materials. It is guessed that it is a phenomenon peculiar to a dense hexagonal lattice that generating and progress of a fatigue crack become slow greatly under a specific biaxial load stress ratio. Pre-crack Crack tip Crack tip Figure 8. Test specimen after a fatigue test 0.04 Rb= ▲R b= ○R b= ×R b= ●R b= Half crack length, a , m □ 0.03 0 0.25 0.5 0.75 1.0 0.02 0.01 0 100000 200000 300000 Number of cycles, N Figure 9. Crack growth curves 400000 500000 Conclusions The following knowledge was acquired as a result of verification of the performance of the biaxial fatigue-testing machine and examining fatigue crack generation and progress process of pure titanium under various biaxial stress ratios. 1. The result of verification of the performance of the biaxial fatigue-testing machine suggests that our testing device generates a uniformity biaxial stress field as intended. 2. It became clear that generating and progress of a fatigue crack become slow in proportion to the magnitude of a stress parallel to a crack. 3. In the case of Rb = 0.75, generating and progress of the fatigue crack were the slowest. It is guessed that it is a phenomenon peculiar to a dense hexagonal lattice that generating and progress of a fatigue crack become slow greatly under a specific biaxial load stress ratio. Acknowledgments This research was sponsored by High-Tech Research Center of Saitama Institute of Technology. References 1. 2. 3. 4. 5. 6. 7. 8. 9. H. Kitagawa, R. Yuuki, and K. Tohgo,“A Fracture Mechanics Approach to High-Cycle Fatigue Crack Growth under InPlane Biaxial Loads,” Fatigue of Engineering Materials and Structures, 2, 195-206 (1979). A. F. Liu, J. E. Allison, D. F. Dittner, and J. R. Yamane, “Effects of Biaxial Stresses on Crack Growth,” ASTM STP, 677, 522 (1979). K. J. Mille,“Fatigue under Complex Stress,” MetalSci., 11, 432-438 (1977). T. Hoshide, and K. 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