FTS systems with diode based referencing and auto-alignment capabilities James R. Engel and Rick Dorval OPTRA, Inc. 461 Boston Street, Topsfield, MA 01983 ABSTRACT Over the past two decades major advances in FTS have allowed process control engineers to more readily consider the use of this measurement technique. The most striking advance has been in the area of data processing facilitated by extraordinary increases in computing power. The development of improved optical fibers has provided a means for bringing the measurement to the factory floor while providing a remote "laboratory environment" site for the less-than-robust spectrometer optical systems. Recent advances in auto-aligned systems again permit consideration of moving the spectrometer system to locations in close proximity to the process itself. Generally, these systems are based on the use of HeNe lasers for the reference and autoalign mechanism. This results in large and expensive measurement heads to again argue against placement of the spectrometers proximate to the process. This paper describes the successful use of a solid state light source in place of the HeNe laser in an auto-aligned and referenced FTS system which allows consideration of small and inexpensive process control spectrometers. A review of a spectrometer system utilizing a combination of autoalign and referencing technologies utilizing diode sources is presented. DOD and NASA support enabled this dual-use technology to be developed. Keywords: Fourier Transform Spectrometer, Auto-Align Reference Systems, UV Spectrometer SYSTEM CONFIGURATION The spectrometer system is a self-contained assembly shown in Figure 1. The FTS system specifications are summarized in Table 1. The system is comprised of several subassemblies which include the thermally and electrically controlled diode laser based probe beam assembly, auto-align assembly, transducer assembly, exit optics assembly, silicon and photomultiplier detectors, and the associated electronics. The system was designed to be as modular as possible such that all the sub-assemblies can be removed and replaced with relative ease. All user selectable variables are externally accessed via the control panel located on the rear of the instrument. OPTRA, Inc FTS systems with diode based referencing and auto-alignment capabilities Page 2 Probe Beam Optical Assembly The laser diode assembly shown in Figure 1 consists of a GRIN lens, an optical isolator and a beam expander. The expanded laser beam is directed through the interferometer with a right angle mirror toward the beamsplitter/compensator below the clear aperture of the spectrometer. The probe beam is then split into two linearly polarized components at the beamsplitter. A λ/4 waveplate located in one arm of the interferometer in combination with the mirror rotates one of these polarizations by 90º. The now orthogonally polarized beams then exit the interferometer and are directed to the detector assembly with a fold mirror. Contained within this detector assembly is specially designed Wollaston prism and a PolarcorTM polarizer. This prism symmetrically introduces a small angle between the two orthogonal polarizations. This angle is chosen such that, when the polarizations are mixed with the PolarcorTM rotated 45º with respect to the orthogonal polarizations, the two beams form an interference fringe pattern. This pattern consists of parallel vertical fringes at a precisely known spacing at the detector plane which are used in the spatial heterodyning. Laser diode stability requirements Substitution of a laser diode for the more commonly used HeNe laser requires addressing several issues including: coherence length, wavelength stability, and a phase measurement technique. Diode lasers have more than adequate coherence lengths for use in a W-FTS System, typically greater than 1meter. Wavelength stability and phase measurement issues, however, require some new techniques. Since the location of the sinc2 function (the instrument line shape for boxcar apodization) in frequency (cm-l) space will be determined by the relationship of the sampling frequency and the signal frequency shift in the sampling frequency will cause the sinc2 function to change location in wavenumber space. This is shown in Figure 2 for two arbitrary sampling frequencies: (Note that for convenience σ1 can be set to zero). If one desires that a change in sampling frequency will produce a change in reported spectral amplitude of less than 1% a simple spreadsheet model can be used to numerically derive Table 2 which enumerates the maximum allowed center shift in the sinc2 (z/2) location to satisfy this condition. OPTRA, Inc FTS systems with diode based referencing and auto-alignment capabilities Page 3 The relative spectral shift between the sampling frequency and the spectrum are equal ∆σ(sampling) = ∆σ (spectrum) σ(sampling) σ(spectrum) (1) For the case where L = 10 cm ∆σ (spectrum) = 5.5 x 10-3 cm-l, ∆σ (spectrum) = 40,000 cm-l, and σ(spectrum) = 12,050 cm-l, ∆σ = σ 5.5 x 10-3 cm-l 40,000 cm-l = ___∆σ___ 12,050 cm-l (2) The sampling frequency stability is proportional to the signal frequency shift by the ratio of the wavelengths (0.25µm/0.83µm) ∆σ (sampling) = 1.66 x 10-3 cm-l which is the required wavelength stability of the laser. Thermal and drive current effects The spectral properties of commercially available laser diodes have been well documented in the literature123. Because of their broad gain curves (>>10 cm-l) laser diodes require wavelength stabilization for interferometric applications. The wavelength stability as a function of temperature and current of a Sharp model LT015MD laser diode was investigated at OPTRA. 1 C. Shin and M. Ohtsu, "Stable Semiconductor Laser with a 7-Hz Linewidth by an Optical-Electrical Double-Feedback Technique", Optics Letters, Vol. 15, pp. 1455-1457, 1990. 2 E. David and Jean-Made Gape, "Frequency Locking of Laser Diode Using Metallic Vapor Optogalvanic Spectrum: UI",Appl. Opt., Vol 29, pp. 4493-4498, 1990. 3 H. Furuta and M. Ohtsu, "Evaluations of Frequency Shift and Stability in Rubidium Vapor Stabilized Semiconductor Lasers", Appl. Opt. Vol. 28, pp. 3737-3743, 1989. OPTRA, Inc FTS systems with diode based referencing and auto-alignment capabilities Page 4 The wavelength stability of 0.095 cm-l/mA and 0.94 cm-l/ºC was experimentally determined and is consistent with that reported in the literature4. In order to achieve 1.66 x 10-3 cm-l stability, the RSS of the two errors for the current and temperature require that they be controlled to 0.012 mA and 1.2 m C, respectively. While this is not trivial, it is achievable for short term stability in a laboratory environment. The drive electronics used to control the laser diode utilize two servo loops, one to control the temperature (using a thermoelectric cooler) and one to control the drive current as shown in Figures 3 and 4. In order to implement the spatial heterodyning technique to determine phase from a single frequency laser diode, a series of straight line fringes have to be generated. This is accomplished through the use of a specially designed Wollaston prism. A Wollaston prism consists of two equal angle calcite prisms optically coupled with optic axes directions orthogonally crossed. The two output beams are orthogonally plane polarized and slightly unequally deviated (asymmetrical) with an angular separation. It is this angular separation in combination with a 4 A. Abou-Zeid, "Diode lasers for interferometry," Precision Engineering, Vol. 11 pp. 139-144, July 1999. OPTRA, Inc FTS systems with diode based referencing and auto-alignment capabilities Page 5 linear polarizer located 45º to the orthogonally plane polarized beams which causes interference to occur. The fringe spacing, D, is related to the laser wavelength, λ, and the angular separation by: D = λ/(2sinθ) (3) where θ is the half the angular separation of the diverging beams. For a laser wavelength of 830 nm this requires and a desired fringe spacing of 75 microns requires an angular separation of 0.63º. Noting that calcite has an ordinary index, no = 1.647237 and an extraordinary index, ne = 1.481564 yields a calcite wedge angle of 1.9º ±10'. The surfaces were polished flat to λ/4 @ 6328 nm, the wedges were bonded with an optical adhesive and the outer surfaces were AR "V" coated. The 3-Tri-Element Detector assembly consists of three multi-element arrays each located on the apex of an equilateral triangle, Figure 5. The detector assembly is positioned such that three adjacent detectors sample a single fringe at locations separated by 2π/3, Figure 45. Each of the detector arrays consists of 90 elements which has been designed such that every third element is wired in parallel. Therefore each detector provides a spatially averaged signal which generates the I(1), I(2), and I(3) needed for the phase recovery algorithm based on the technique described by Mertze6. The three signals from each of the detector arrays are then pre-amplified. Error signals proportional to tilt are generated at every fringe crossing. These three signals are then amplified, and delivered to appropriate piezo actuators in the auto-align mirror assembly. 5 6 Patent applied for. L. Mertz, "Complex Interferometry", Applied Optics, Vol. 22, pp. 1530-1534, 1983. OPTRA, Inc FTS systems with diode based referencing and auto-alignment capabilities Page 6 Auto-alignment technique The basic auto-align technique, Figure 7, consists of an expanded laser beam which traverses the interferometer and falls on a 3-tri-element detector. Each of the tri-element detectors provide the means for measuring the path length for three paths through the interferometer spatially separated by 120 degrees. A perfectly aligned interferometer will show three identical path lengths, while mirror tilt produces unequal path lengths. Each of the three segments path length information and error signals are generated and applied to piezo-ceramic actuators that sit under one of the mirrors and allow for tilt correction. Figure 8 shows additional system elements designed to accommodate phase offsets and amplitude changes in the laser diode output. Phase offsets between X1, Y1, X2, Y2, and X3, Y3 when tilt error is zero are very likely to occur due to the mechanical positioning of each of the Tri-Element detector arrays, to chromatic errors (since the auto-align wavelength is .830µ vs. .25µ wavelength of interest), as well as electrical phase offsets. The phase offsets of the Tri-Element detector arrays can be adjusted to ±60° maximum by designating which array outputs are, I1, I2, and I3. Then instead of measuring Y1, and Y2 directly, the difference between Y1, Y2, and an adjustable reference voltage will result in error signals proportional to the tilt errors. OPTRA, Inc FTS systems with diode based referencing and auto-alignment capabilities Page 7 The concept to handle phase offsets assumes the amplitudes Y1, and Y2 are constant. This may not be the case. To allow for this, two blocks are added. These circuits use the same sampling technique described earlier to sample X1, and X2, when Y1, and Y2 = 0 resulting in stored signals equal to the maximum amplitude of Y (assuming the amplitude of X1 = Y1 and X2= Y2). SPECTRA Figure 10 shoes a 0.4 resolution scan of a HeNe laser line source. ACKNOWLEDGEMENTS NASA/JPL OPTRA, Inc Contract Number NAS7-1109 (SBIR) FTS systems with diode based referencing and auto-alignment capabilities Page 8
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