Proceedings of the ASME 2009 7th International Conference on Nanochannels, Microchannels and Minichannels ICNMM2009 June 22-24, 2009, Pohang, South Korea Proceedings of the Seventh International ASME Conference on Nanochannels, Microchannels and Minichannels ICNMM2009 June 22-24, 2009, Pohang, South Korea ICNMM2009-82249 MEASUREMENT OF HEAT TRANSFER IN THE ENTRANCE REGION OF SMALL DIAMETER TUBES Ting-Yu Lin Thermal Analysis, Microfluidics, and Fuel Cell Laboratory, Rochester Institute of Technology, 76 Lomb Memorial Dr., Rochester, NY 14623 [email protected] Chien-Yuh Yang Department of Mechanical Engineering, National Central University, Chung-Li, 32054, Taiwan [email protected] ABSTRACT Satish G. Kandlikar Thermal Analysis, Microfluidics, and Fuel Cell Laboratory, Rochester Institute of Technology, 76 Lomb Memorial Dr., Rochester, NY 14623 [email protected] The study of heat transfer performance in micro channels has become more important. There have been many studies, including Wu and Little [1984][1], Wang and Peng [1994] [2], Yu et al. [1995] [3] and Adam et al. [1998] [4], dealing with the single-phase forced convection heat transfer in micro tubes. Most of their tests results are significantly different from those of conventional forced convection heat transfer correlations, which were obtained for larger tubes. Yu et al. [1995] [3] studied the fluid flow and heat transfer characteristics of nitrogen gas and water in circular tubes with diameters of 19, 52 and 102 μm and Reynolds numbers ranging from 250 to 20,000. The measured friction factors were slightly lower than the Moody chart values for both laminar and turbulent flow regimes. However, the Nusselt numbers for cooling of water in the turbulent flow regime were considerably higher than would be predicted for larger tubes, suggesting that the Reynolds analogy does not hold for micro channel flow. Adams et al. [1998] [4] investigated turbulent single-phase forced convection of water in circular micro channels with diameters of 0.76 and 1.09 mm. The data suggested that the enhancement increases as the channel diameter decreases with increasing Reynolds number. Based on this data, along with earlier data for small circular channels by Yu et al. [1995] [3], a correlation was developed for the Nusselt number for turbulent, singlephase and forced convection in circular micro channels with diameters ranging from 0.102 to 1.09 mm. Adams et al. [1999] [4] investigated turbulent single-phase forced convection of water in non-circular micro channels with hydraulic diameter of 1.13 mm. The experimental results predicted by the Gnielinski correlation falls within ± 10%. From the results it was concluded that 1.2 mm was a lower limit for the applicability of standard turbulent single-phase correlations for non-circular Heat transfer coefficient in the entrance region of water flowing through micro-tubes with diameters of 962 μm and 123 μm was investigated in this study. Two temperature measurement methods, thermocouple and liquid crystal thermography (LCT), were used to measure the tube surface temperature. The experimental data showed that the Nu in the entrance region can be predicted well by conventional correlation while using the LCT to measure the temperature. Using the temperature measurements from the thermocouples attached to the surface, the Nu is found to be significantly higher than the prediction. This was believed to be due to the error in measurement of temperature. Simulation results also revealed that the measured temperature for a small diameter tube can be significantly decreased with a thermocouple attached to it. In transition flow, the wall temperature was also found to have a significantly fluctuation, as large as 2 oC, due to the unsteady flow conditions, while for fully established laminar as well as turbulent flow conditions, the fluctuation was measured to be less than 0.2 oC. The effect of viscous heating was negligible in the range of parameters investigated in this study. Keywords: heat transfer coefficient, micro-tubes, small diameter tubes, liquid crystal thermography (LCT), transition flow, transition to turbulent INTRODUCTION Owing to the fabrication technology development during the past decades, the so-called micro tubes with internal diameters smaller than 1 mm can be easily made and used to increase the compactness of heat exchangers. 1 Copyright © 2009 by ASME channels. Kandlikar et al. [2003] [5] investigated the pressure drop and heat transfer of laminar flow in smooth and rough circular tubes with diameters of 1.067 and 0.62 mm. The effect of the changes in the relative roughness on pressure drop was minimal but the heat transfer in the entrance region showed a distinct dependence on roughness. Some researches revealed the correspondence of experimental data and conventional correlations. Lelea etal [2004] [6], Owhaib and Plam [2004] [7], Muwanga and Hassan [2006] [8], Lin and Yang [2007] [9], Yang and Lin [2007] [10] indicated that the heat transfer coefficient can be predicted well by conventional correlations. Guo and Li [2003] [11] proposed that measurement accuracy of a tube is one of the most important factors to cause the discrepancy between experimental data and conventional correlations. The non-contact temperature measurement method of LCT was used to measure the temperature of small scale in some research. Hohmann and Stephen [2002] [12] used the non-encapsulated thermochromic liquid crystal (TLC) to investigate the heat transfer at an evaporating liquid meniscus. The measured surface area was 640 x 480 μm in a flat plate with a theoretical spatial resolution of less than 1 μm. The uncertainty of their measured temperature was 0.51 oC. Muwanga and Hassan [2006] [8] used non-encapsulated TLC to measure the local heat transfer coefficient in micro channel with 1.0668 mm inner diameter and outer diameter of 1.27 mm. The results indicated that the conventional correlation was adequate for predicting the heat transfer coefficient. Lin and Yang [2007] [9] and Yang and Lin [2007] [10] measured the convective heat transfer performance of micro-tubes with diameters from 123 to 962μm by LCT. Their results revealed that the experimental data was in a very good agreement with conventional correlation. Since the size of the normal commercial sensor for measuring micro-tubes surface temperature is comparable to the size of the micro tubes, it may not be accurate to measure the surface temperature by attaching a sensor on micro tube. Furthermore, since the size of the sensor and tube are extremely small, it is very difficult to have the sensor firmly contact the tube. In this study, the non-contact temperature measurement method, is applied to measure the micro tube surface temperature. Thermocouples with two attachment methods are compared to investigate the effect of the contact. This study is not intended to develop an accurate temperature measurement by thermocouple, but just to discuss the temperature measurement problems due to thermocouples. kf Water conductivity (W/m oC) L Tube length (m) LCT Liquid crystal thermography, dimensionless • m Mass flow rate (kg/s) Nud Nusselt number, dimensionless q Heat transfer rate (W) q” Heat flux (W/m2) r Radius (m) Red Reynolds number, dimensionless Ti Inlet water temperature (oC) Tx Local water temperature (oC) Twx Local tube inside wall temperature (oC) Velocity (m/s) u TLC Thermochromic liquid crystal, dimensionless x Axial position of tubes (m) μ Viscosity (N/m2 s) EXPERIMENTAL SETUP The schematic diagram of the test facilities is shown in Figure 1. A pressure vessel connected to high-pressure nitrogen was used to push the water through the test tube. The inlet water temperature was measured by a resistance temperature detector (RTD). DC power was clapped on both ends of the test tube to offer constant heat flux to the tube. The flow rate was measured by a programmable electronic microbalance. Power High pressure N2 Water reservoir Pressure vessel T P CCD Balance Figure 1. Schematic diagram of test loop The TLC usually reveals color from red to blue in the temperature from low to high active range. The temperature active range of TLC can be from 0.5 to 30 o C. TLC with lower active range usually has higher temperature resolution but less temperature detecting area. To increase the accuracy of temperature measurement, four TLCs with 5 oC band width from 28 to 33 oC, 33 to 38 oC, 38 to 43 oC and 45 to 50 oC were used in this study. A black paint was painted under the TLCs as the background for improving the color resolution by absorbing un-reflected light. The relation between the hue value and temperature was calibrated in a thermostat box. It was used to offer an environment for the calibration of the TLC. The box is made up of wooden plates having thickness of 10 mm with a 10 mm heat insulator on it, as shown in Figure 2. During the calibration process, electrical heating wires were attached to the inner surfaces of the box to maintain the entire box space at the designated temperature. The temperature inside the thermostat box can be adjusted by setting the input power on the heating wire. T-type thermocouples were placed on the test tube surface to measure its temperature distribution. The hue values of NOMENCLATURE A Ac cp di G Gz h Pump Test tube Filter Heat transfer area (m2) Tube cross section area (m2) Heat capacity (J/kg K) Tube inside diameter (m) Mass velocity (kg/m2 s) Graetz number, dimensionless Heat transfer coefficient (W/m2 oC) 2 Copyright © 2009 by ASME TLC and thermocouple temperature were recorded simultaneously. The temperature uniformity inside the box is within ±0.1 oC at different temperature settings. The thermal shunt problem can be neglected since the temperature between the test surface and the sensor is the same. the heat transfer coefficient h can be derived as: h= q A(Twx − Tx ) (3) Where A is the heat transfer area, A = πdiL and di is the tube inside diameter. Twx is the local inside tube surface temperature, derived from the measured outside surface temperature. The Reynolds number and Nusselt number are defined as Re d = Gd i and Nu d = hd i μ kf • Where G is the water mass flux, G = m /Ac and Ac is the tube cross-section area. Figure 2. Thermostat box A comparison test using a thermocouple to measure temperature was performed. This test was applied to qualitatively study the temperature measurement problem by thermocouple in a small tube. Figure 3 shows the 962 μm tube with a thermocouple attached. The external diameter of the tube is 1.26mm. Omega bond was used to cement the thermocouple joint and the tube surface after they were firmly connected. This connection method was commonly used to measure the surface temperature of large tubes. NUMERICAL SIMULLATION In this study, a 3D numerical model was formulated to solve the conduction heat transfer problem. Figure 4(a) shows the model of a rectangular solid 2 x 2 x 25 mm stainless steel (SS-304) test section with a thermocouple attached to it. The material of thermocouple was set as 0.05 x 0.05 x 12 mm copper. The attached location was in the center of the test section on the surface. The test section was used as heat source directly under natural convection situation. The ambient was set to be 25 oC air. The entire computational grids are 118,245 cells for the large test section and 1,001,388 cells for the small one. Figure 4(b) shows the model with dimension of 0.2 x 0.2 x 25 mm, and with the same size thermocouple attached as the large test section. The commercial software package Flotherm was used for the computations. Figure 3. The attachment of thermocouple on 962 μm test tube Test section Thermocouple DATA REDUCTION (a) The heat transfer rate was measured from the DC power input and is equal to the enthalpy of water flow increased. Since the electrical power was added uniformly on the tube surface, the local water temperature, Tx, at the position x from the heating entrance, can be estimated by: • x q = m c p (Tx − Ti ) L Figure 4. Simulation models RESULTS To reveal the stability of LCT in this study, hue versus temperature calibrations were performed for the 962 μm tube in different date, as shown in figure 5. Plotted data of “Cal-A # 1” was a calibration performed immediately after the TLC was sprayed on the tube. “Cal-B # 1, Cal-B # 2 and Cal-B # 3” were calibrations for another sprayed TLC. “Cal-B # 1” was also performed immediately after the TLC was sprayed, while “Cal-B # 2” and “Cal-B # 3” were performed after 3 days and 7 days, respectively. From “Cal-A # 1” and “Cal-B # 1” it is observed that (1) • Where m is the water flow rate, L is the tube length and Ti is the water inlet temperature. From the Newton’s Law of cooling, q" = q = h (Twx − Tx ) A (b) (2) 3 Copyright © 2009 by ASME lower than that measured by TLC. The difference is more than 1 oC, which is significantly higher than the experimental uncertainty. The lower temperature measured by thermocouple is due to the attachment, which is not a perfect match (3M tape), or the thermal shunt problem (Omega bond). In this case the temperature error caused by Omega bond is slightly higher than that of 3M tape. calibration curves for new TLC had no significantly difference. From “Cal-B # 1” and “Cal-B # 2” it is observed that the calibrated correlation after 3 days is still the same. At 45.8 oC the TLC started to appear clear in color and the hue value was about 60. After 7 days, “Cal-B # 2” showed the active temperature of TLC was about 46.4 oC with the hue value about 90. There was no detectable color which appeared with a temperature lower than 46.4 oC and hue value under 90. It was also observed that hue value in the lower temperature region was slightly lower than the other calibration. This situation means that the TLC started to decay. In this work, all the experiments were performed within 2 days. The temperature measurement error caused by the calibration correlation changes can be neglected in this study. In figure 5 it is also observed that the slope is higher in the higher hue value region. This means the resolution to temperature is lower and the uncertainty to measure temperature is higher in the higher hue value region. Figure 6. Color of TLC on a 250 μm external diameter tube with a thermocouple attached on it 50 52 TLC TC (3M Tape) TC (Omega bond) 49 Di=962μm Cal-A # 1 Di=962μm Cal-B # 1 Temperature (oC) 51 Di=962μm Cal-B # 2 Temperature (oC) 50 Di=962μm Cal-B # 3 49 48 47 46 48 47 45 46 44 44 45 40 45 46 47 48 49 50 o TLC temperature ( C) 60 80 100 120 140 160 Figure 7. Comparison of temperature measured by TLC and the thermocouple Hue Figure 5. Calibration of hue values versus temperature with 962 μm tube, performed on different dates The experimental values of the local Nu in the entrance region are compared with the correlation of Shan and Bhatti [1987] [13], as shown in Figure 8. Eight thermocouples were attached to the test tube to measure the temperature in equivalent distances from the entrance region to the fully developed region. The conventional correlation shows that the local Nusselt number decreases along the flow direction and asymptotically approaches the value of theoretical constant heat flux fully developed heat transfer coefficient, 4.36. Graetz number (Gz), which is defined as [(x/d)/RePr], was used to define the flow development situation. The lower Gz means the flow length is shorter or the Re is larger. Gz=0.05 was used to define the thermal developing situation. Gz higher than this value was considered to be fully developed. From Figure 8, it is observed that the data obtained from TLC can be well predicted by conventional correlation, while for the data from the thermocouples is significantly higher than the prediction. The departure increases with the increasing of Gz. This is because the thermocouple under estimates the wall Figure 6 shows the TLC color of the 123 μm tube. A thermocouple was attached to it by Omega bond. The external diameter of the tube was 250 μm and spread with 45 to 50 oC TLC. The tube was offered with uniform heat flux. It is observed that at the two ends of the tube the color is blue, which means the temperature is in higher temperature region. Near the bond the color is red, which means the temperature is in the lower temperature region of active range. The color showed of Omega bond was black, which means that the temperature is under than the active range. Figure 6 clearly reveals that the temperature was cooled down by the Omega bond and thermocouple. Figure 7 shows the comparison temperature measurements on 962μm tube, made by TLC and thermocouple. 3M tape and Omega bond were used to maintain the attachment between thermocouple sensor joint and test tube surface. It is observed that the temperature measured by thermocouple is significantly 4 Copyright © 2009 by ASME rate was steady state. Hence, for each test the heat flux and fluid temperature were steady. From equation 2 it can be observed that the wall temperature Twx changes while the heat transfer coefficient change. Agostini et al. [2004][14] investigated the convective heat transfer characteristics of R134a in multi-port extruded tubes. Tube wall temperature was measured by 0.5mm E-type thermocouple. Their experimental data reveal that in transition flow the tube wall temperature fluctuation is about 0.2 oC, which was three times higher than that of laminar or turbulent flow. From this study it was found that the fluctuation could be much higher than 0.2 oC. The response time of TLC is about 36 to 450 milliseconds, proposed by Hoffs [1992][15]. The transient temperature change was able to be observed clearly. The results indicated that the TLC can be further used to measure the transient temperature due to the shorter response time. temperature, as shown in the results in Figure 7. For the same Red, the lower Gz data means the temperature was measured in the entrance region. For constant heat flux heating, the fluid and wall temperature increases with the heating length. In the small Gz region (upstream entrance region of the tube) the wall temperature was lower. The temperature of tube wall and ambient were small, the under estimation of temperature was not significant. However, in the higher Gz region (downstream fully developed region of the tube) the wall temperature was high and the temperature difference between wall and ambient was much higher. The under estimate was significant. From equation (2) it can be observed that the underestimation of the wall temperature will cause the heat transfer coefficient to be higher. The higher underestimation in the fully developed region caused the Nu to be higher than that in the entrance region. 25 Shah and Bhatti [1987] Red=570-LCT 20 Red=620-LCT 0.00s 0.03 s 0.07s 0.10s 0.13s 0.17s 0.20 s 0.23s 0.27s 0.30s Red=590-thermocouples Red=640-thermocouples Nud 15 10 (a) Re=12078 (turbulent flow) 5 0 2 4 6 Gz X 0 8 10 12 14 0.53s 0.57 s 0.60s 0.63s 0.67s 0.70s 0.73 s 0.77s 0.80s 0.83s 100 Figure 8. Heat transfer coefficient in the entrance region by different measurement Transition flow (b) Re=2674 (transition flow) Figure 9. Frames of external diameter 1.26 mm tube with TLC at different time Figure 9 (a) shows 10 continuous pictures taken in 0.3 seconds of the tube of external diameter 1.26 mm. The tube has TLC on it, and has Reynolds number of 12,078. Images were taken 30 frames per second. There is no significantly color difference over time. However, in transition flow, Figure 9 (b) shows the tube color was changed significantly, especially for the pictures at 0.63 and 0.67s. After converting the color to temperature, the temperature fluctuation (difference between instant temperature Tinst and average temperature Tavg) with time was found to be high as shown in Figure 10. The fluctuation can be higher than 2 oC. In calibration, laminar and turbulent flow, the fluctuation was observed to be less than 0.2 oC. The higher temperature fluctuation in transition flow is due to the changing flow regimes. The heat transfer coefficient is low in laminar flow and is high in turbulent. In transition flow, the flow regime transits from laminar to turbulent and back to laminar continuously due to unsteadiness. Hence, the heat transfer coefficient changed continuously. In this study, uniform heat flux was applied for heating and the flow o Tinst-Tavg ( C) 2 Calibration Re=1884 (Laminar) Re=12078 (Turbulent) Re=2674 (Transition) 1 0 -1 0.0 0.2 0.4 0.6 0.8 1.0 Time (s) Figure 10. Transient tube surface temperature fluctuation 5 Copyright © 2009 by ASME on the test section was not significantly influenced by the thermocouple. The thermocouple temperature was higher near the test section and decreased with the distance. The temperature in the attachment of test surface was 60.4 oC which was slightly decreased by the attached thermocouple. For the 0.2 x 0.2 x 25mm test section the decrease was significant. The temperature distribution without attaching a thermocouple is shown in Figure 14. The input heat was set to be 0.037 W. The maximum temperature was 45.3 oC which was in the center of test section. By attaching the same size thermocouple the temperature was significantly decreased, as shown in Figure 15. The temperature in the attachment was 40.7 oC. The decrease was as high as 4.6 oC. The detailed simulation results are shown in Table 1. Viscous heating When compare to the flow in large tubes, the flow velocity in micro-tubes is relatively higher. Due to the high flow velocity, an evaluation of viscous heating in the fluid is necessary. In steady state, the energy balance for channel flow is generalized as follows: ρuπR 2 c p (Tx − Ti ) = ∫ L 0 ∫ R 0 ∂u ) 2πrdrdx ∂r 2 u( (4) with the assumptions of: circular cross-section, fully developed laminar (Poiseuille) velocity profile and constant fluid properties along the tube length. The fluid temperature difference between measuring position Tx and inlet position T i is as follows: Tx − Ti = 32μuL 2 ρd i c p Gnielinski Nu = 4.364 (4.2) d 100 (5) Nud From this equation it is observed that the temperature difference increases with the decreasing tube diameter. Considering the viscous heating the fluid temperature will be increased. The Nusselt number increases due to the fluid temperature increase. From equation (5) it is also observed that the fluid temperature increases with velocity and tube length. Figure 11 shows the effect of viscous heating on heat transfer coefficient for the 123 μm tube. Long length and high fluid velocity cases were plotted to clarify the effect of viscous heating. Both of the two cases show that there was no significant effect of viscous heating in this diameter. Considering the viscous heating, the Nu was increased with the increase of Red from 2.4 to 3.7% for 145 mm length tube. For the 29 mm length tube the increase was from 0.1 to 0.3%. Viscous heating was considered to be negligible in this research due to the high cp of water. It was also found that the Nu of 29 mm length tube was significantly higher than 4.364 and is a function of Red with Red higher than 1,000. It was because of the measuring length was too short for the flow to be fully developed. The flow was still in developing region hence the Nud was higher. For the 145 mm length tube the Nud corresponded to 4.364 and did not change with Red, since the tube length was long enough for the flow to be fully developed, even at high Red. Figure 12 shows the temperature distribution of the 2 x 2 x 25mm test section without a thermocouple attached to it. The input heat was set to be 0.12 W with uniform heating to the test section. The temperature distribution was uniform, and the minimum to maximum values ranged from 61.6 to 62.2 oC. In the edge region the temperature is lower due to more heat transfer area under natural convection. The maximum temperature 62.2 oC appeared in the center of the test section surface. Figure 13 shows the temperature distribution of the test section with a thermocouple on it. The temperature distribution Lm=29mm withount viscous heating Lm=29mm with viscous heating Lm=145mm withount viscous heating Lm=145mm with viscous heating 10 1000 10000 Red Figure 11. The effects of viscous heating in 123μm tube o C 62.2 61.9 61.6 Figure 12. temperature distribution of 2 x 2 x 25mm without thermocouple 6 Copyright © 2009 by ASME o heating were discussed. Based on the present study the following conclusions are drawn: 1. In a small tube the temperature can be significantly decreased by attaching a thermocouple on it. 2. Temperature measured by TLC revealed that Nu can be predicted well by conventional correlations, while for thermocouple measurements it was significantly higher. 3. Transient temperature phenomenon can be clearly observed by LCT. In transition flow the temperature was found to have high fluctuation larger than 2 oC. 4. Viscous heating effect was not significant in this study. C 61.5 50.9 35.0 Figure 13. temperature distribution of 2 x 2 x 25mm with thermocouple o C 45.3 44.4 43.0 Figure 14. temperature distribution of 0.2 x 0.2 x 25mm without thermocouple o C 44.6 42.6 39.7 Figure 15. temperature distribution of 0.2 x 0.2 x 25mm with thermocouple Table 1. Temperature in the center of test section surface Test section (mm) Input heat (W) Without TC (oC) With TC (oC) ΔT (oC) 2 x 2 x 25 0.2 x 0.2 x 25 0.12 0.037 62.2 45.3 60.4 40.7 1.8 4.6 Conclusions This study investigated the heat transfer in micro tubes. Temperature measurement, transient flow and viscous ACKNOWLEDGMENTS The work was conducted at National Central University, Chung-Li, Taiwan, and Rochester Institute of Technology, Rochester, NY, USA. REFERENCES 1. Wu, P., and Little, W. A., 1983, “Measurement of friction factors for the flow of gases in very fine channels used for microminiature Joule-Thomson refrigerators,” Cryogenics, pp. 273-277. 2. Wang, B. X., and Peng, X. 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Hoffs, A., 1992, “Lquid Crystal Technique For Heat Transfer Measurements Literature Study,” ECOLE POLYTECHNIQUE FEDERALE DELAUSANNE DEPARTEMENT DE MECANIQUE Rapport LTT92-45, pp. 1-40. 8 Copyright © 2009 by ASME
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