Available online at www.sciencedirect.com Composites: Part A 39 (2008) 176–187 www.elsevier.com/locate/compositesa Titanium matrix composite lattice structures Pimsiree Moongkhamklang *, Dana M. Elzey, Haydn N.G. Wadley Department of Materials Science and Engineering, University of Virginia, 140 Chemistry Way, P.O. Box 400745, Charlottesville, VA 22904-4745, USA Received 12 June 2007; received in revised form 31 October 2007; accepted 13 November 2007 Abstract Cellular materials made from high temperature composites with efficient load supporting lattice topologies and small cell sizes would create new options for light weight, high temperature structures. A method has been developed for fabricating millimeter cell size cellular lattice structures with a square truss topology from 240 lm diameter Ti–6Al–4V coated SiC monofilaments. The compressive stiffness of the lattice structures was well approximated by that of the monofilament fraction in the loading direction. The strength of the lattices was controlled by elastic buckling and the results were accurately represented by an elastic buckling model. The post peak compressive deformation was accommodated by elastic buckling of the SiC fibers and plastic deformation of the titanium coating until the onset of monofilament fracture. The specific stiffness and strength of the lattices were found to be between 2 and 10 times that of other cellular structures and thus appear to be promising candidates for high temperature, ultralight weight load supporting applications. Ó 2007 Elsevier Ltd. All rights reserved. Keywords: Cellular materials; A. Metal–matrix composites (MMCs); B. Mechanical properties 1. Introduction Lightweight, multifunctional load supporting structures based upon sandwich panel concepts have many applications [1–10]. Their cellular cores usually have either a prismatic (corrugations) or honeycomb topology and are usually adhesively bonded to the face sheets [2–10]. The cores are made of very low density materials such as Nomex [3,4], polymer foams [5], or light metal constructions [6–9] that maintain the face sheet separation needed for sandwich panel action at minimum parasitic mass [1]. Metallic core systems based upon light metals such as aluminum [6,7] and titanium [8,9] alloys are utilized where high compressive strengths are needed to avoid local indentation. They can also be used for higher temperature applications provided metallurgical bonding is used to attach the core to the face sheets [6–9]. The maximum use temperature of these structures is then limited by the creep rate of the alloy system. * Corresponding author. Tel.: +1 434 982 5035; fax: +1 434 982 5677. E-mail address: [email protected] (P. Moongkhamklang). 1359-835X/$ - see front matter Ó 2007 Elsevier Ltd. All rights reserved. doi:10.1016/j.compositesa.2007.11.007 While honeycomb topology systems usually offer significantly superior structural performance [1,2,10,11], their closed-cell topology limits some potential multifunctional applications [10]. They are also susceptible to corrosion and suffer from delamination problems [2,9]. Stochastic metal foam core systems with fully interconnected pores have attracted interest because they provide multifunctional capabilities such as cross flow heat exchange [11–14], dynamic load protection [11,15–17], and acoustic damping [11,18]. However, their use in structural applications is severely constrained by their low elastic moduli and indentation strengths [1,11]. Methods have recently begun to be developed for fabricating millimeter scale, open-cell metallic lattices from a range of light metals and high temperature alloys [19–31]. The truss members in lattice materials can be topologically configured to experience predominantly axial stresses (i.e. tension or compression) when they are used in sandwich panels that are loaded in bending (i.e. the cores are stretch dominated) [19,32–34]. This results in significantly superior mechanical performance compared to stochastic metal foams whose ligaments deform by bending [35]. P. Moongkhamklang et al. / Composites: Part A 39 (2008) 176–187 These lattice topologies also possess greater compressive strength and therefore better resistance to indentation. Numerous cell topologies have been fabricated including those with tetrahedral [19–23], pyramidal [21, 24–26], 3D-Kagomé [23,27], woven textile [28,29], and diamond or square collinear [30,31] structures. Examples of these lattices, configured as the cores of sandwich panels, are schematically illustrated in Fig. 1. The textile and collinear lattice structures exploit metallic wires for their fabrication by a simple lay-up and transient liquid bonding process [24,29–31]. The strength of lattice core sandwich panels is governed by the stress at which panel failure mechanisms are initiated under the various modes of loading (through thickness, longitudinal compression, bending, tension etc.) [37–40]. These failure mechanisms are well established for metallic materials and include face sheet yielding [34,36,38], face sheet wrinkling [34,36,38], core shear [28,37,38], core plastic yielding [34,36,38], fracture under tension [33], and plastic buckling [27,33,34] of compressively loaded core truss members. Although the most common loading environments for sandwich panels are shear and bending, the practical implementation of sandwich panels is often limited by concentrated compressive stresses at the loading points. In such cases, the core suffers local yield or crushing (indentation) and can be accompanied by face sheet stretching/tearing [11,36,37]. These are affected by the compressive strength of the core and the cell size (which controls the stretching periodicity) [34]. The compressive stiffness and strength of lattice structures could be significantly increased by the use of stiffer, higher strength core materials. The highest specific strength lattice structures fabricated to date have utilized Ti–6Al– 4V for the truss structures [26]. This alloy has a density of 4.43 g/cm3, Young’s moduli in the range of 100– 120 GPa, and yield strengths of 750–1250 MPa [39]. A Ti–6Al–4V coated SCS-6 SiC monofilament developed in the 1990’s for titanium matrix composite (TMC) manufac- 177 ture [40–42] appears to be an even stronger (but less ductile) candidate material for lattice structures. For a 35% fiber volume fraction, the axial Young’s modulus of the monofilament is about 215 GPa and its ambient temperature tensile fracture strength exceeds 1800 MPa. Both are approximately two times higher than that of Ti–6Al–4V alloy, while the density of such a monofilament would be 3.93 g/cm3, roughly 12% less than that of Ti–6Al–4V. These composite materials also offer much better creep resistance than their all-metallic counterparts [43]. With these considerations, cellular structures fabricated from such composites might be attractive for high temperature and/or weight sensitive structural applications. The aim of the current paper is to report a method for the fabrication of TMC lattice core sandwich panels. The out-of-plane compressive behavior of the lattice structure is investigated experimentally and the micromechanisms of lattice deformation as a function of lattice relative density are identified. The mechanical properties are then compared to analytic estimates based upon the observed failure modes. While these materials/structures have limited ductility, they appear to be one of the highest specific strength cellular structures fabricated to date. 2. Lattice truss fabrication Collinear lattice structures with a square orientation (Fig. 1f) and a relative density, q, in the range of 5–17% were fabricated from Ti–6Al–4V coated SCS-6 SiC monofilaments supplied by FMW Composite Systems, Inc. (Clarksburg, WV). Each monofilament was approximately 240 lm in diameter and consisted of a 140 lm diameter SiC (SCS-6) fiber surrounded by a 50 lm thick physical vapor deposited Ti–6Al–4V coating, Fig. 2. The SCS-6 fibers were made by chemical vapor deposition on carbon cylindrical substrates (33 lm diameter fibers) [44,45]. The densities of SCS-6 fiber, Ti–6Al–4V, and the composite monofilament are 3.00, 4.43, and 3.93 g/cm3, respectively. Fig. 1. Examples of sandwich panel structures with open-cell, lattice core topologies. Metallic pyramidal, tetrahedral and kagomé core structures are made by folding perforated metal sheets or by investment casting. The textile and collinear core structures are made by wire lay-up and brazing methods. 178 P. Moongkhamklang et al. / Composites: Part A 39 (2008) 176–187 Fig. 2. (a) Schematic and (b) cross-sectional micrograph of a Ti–6Al–4V coated SCS-6 SiC monofilament (35% fiber volume fraction). Lattice structures were assembled from the monofilaments using a simple fixture (constructed of stainless steel and spray coated with BN to prevent sticking) to align the monofilaments in collinear layers, Fig. 3a. The orientation of consecutive layers was alternated to create a square lattice truss topology structure. Fig. 4 shows a stacking sequence and a unit cell of the lattice structure. Once assembly of the TMC filament lay-up was complete, a dead weight was used to apply a force of 3.7 102 N (equiva- lent to an applied pressure of 1.5–5 MPa) to each contact (truss–truss node). The assembly was diffusion bonded by placing it in a vacuum furnace at a base pressure of 107 Torr. It was heated at 20 °C/min to 900 °C and then held for 4 h under pressure, Fig. 3b. The lattice structures were then removed from the tooling and cut, using wire electro-discharge machining, to create samples that were four cells high and six cells in length, Fig. 3c. The sample width was approximately the same as the sample height, Fig. 3. Fabrication of a TMC square lattice core sandwich panel: (a) assembly sequence to make a TMC lattice; (b) vacuum diffusion bonding of the core; (c) sandwich panel lay-up; and (d) brazing of face sheets to the square orientated core. P. Moongkhamklang et al. / Composites: Part A 39 (2008) 176–187 179 Fig. 5 shows nodal regions of the lattice structure after the diffusion bonding step. It can be seen that excellent metallurgical uniformity was achieved in the bonded region. Equiaxed a-grains and an intergranular b-phase microstructure was observed with an average grain size of 8 lm. During diffusion bonding, the spacing between consecutive layers and hence the macroscopic lattice width decreased as the titanium alloy coating at the contact points deformed and interdiffused. Fig. 4 schematically shows a unit cell of the square lattice before and after diffusion bonding. A diffusion bonding coefficient, b, can be introduced by assuming the titanium alloy coating was redistributed similarly in each collinear layer (see Fig. 4). The b coefficient is defined as w/wo, where w and wo are the unit cell widths prior to and after the diffusion bonding process (Figs. 4b and c), correspondingly. The unit cell volume of the diffusion bonded lattice can then be written: V c ¼ wl2 ¼ bwo l2 ¼ b4al2 : ð2Þ Even though the titanium alloy coating is deformed at the contacts, the volume occupied by the solid composite in the unit cell remains the same as for the as laid-up unit cell. The relative density of the diffusion bonded square lattice structure, q, is therefore: V s 2pa2 l 1 pa qo ð3Þ q¼ ¼ ¼ ¼ : V c b4al2 b 2l b Fig. 4. Representative unit cells of a square lattice: (a) three layer lattice; (b) unit cell before diffusion bonding; and (c) unit cell of the diffusion bonded structure (w < wo). i.e. W H = 4l, where l, W, and H are the unit cell length, the lattice width, and the lattice height, respectively. The relative density of the as laid-up lattice,qo , is simply the volume fraction of the unit cell occupied by solid truss material: qo ¼ V s 2pa2 l 2pa2 l pa ; ¼ ¼ ¼ 2l Vc wo l2 4al2 Table 1 summarizes cell parameters and corresponding relative densities of the square lattices prior to and after diffusion bonding. For the diffusion bonding conditions used here, b was 0.9–0.92, and the relative density of the lattices therefore increased by 8–10% during the bonding process. After being cut to size, the lattices were brazed to 2 mm thick Ti–6Al–4V face sheets using a TiCuNi-60Ò paste braze alloy supplied by Lucas-Milhaupt, Inc. (Cudahy, WI), Figs. 3c–d. This alloy powder had a nominal composition of Ti-15Cu-25Ni (wt%) and was held in a polymer binder. The solidus and liquidus temperatures of the brazing alloy are 890 °C and 940 °C, respectively. The sandwich panel samples were vacuum brazed by heating at 20 °C/min to 550 °C, holding for 5 min (to volatilize and remove the polymer binder), and finally heating to 975 °C for 30 min at a base pressure of 107 Torr. Micrographs of a trussface sheet node made by the brazing technique are shown in Fig. 6. It can be seen that the TiCuNi-60Ò braze provided good wettability to the SCS-6 fiber surface as well as good penetration to the Ti–6Al–4V alloy coating and face sheet. Photographs of sandwich panel samples of each core relative density are shown in Fig. 7. ð1Þ where Vc, Vs, wo, a, and l are the unit cell volume, the volume occupied by the solid trusses, the cell width, the filament radius, and the cell length, respectively. 3. Experimental compressive response The square lattice structures were tested at ambient temperature in compression with a displacement rate of 180 P. Moongkhamklang et al. / Composites: Part A 39 (2008) 176–187 Fig. 5. Diffusion bonded truss–truss nodes: (a) exterior deformation of the metal coating at the nodes; (b) cross-section of a pair of nodes; and (c) diffusion bonded region between a pair of monofilaments. Table 1 Cell/lattice parametersa and corresponding relative densities prior to and after core diffusion bonding (T = 900 °C, t = 4 h, P = 1.5–5 MPa) Center-to-center cell length, l (mm) 1.26 1.88 2.51 3.77 a Prior to diffusion bonding After diffusion bonding b (w/w0) Relative density, qo ð%Þ Core width, Wo (mm) Core width, W (mm) Relative density, q ð%Þ 15.0 10.0 7.5 5.0 6.03 9.05 12.06 18.10 5.43 ± 0.015 8.35 ± 0.025 10.91 ± 0.043 16.75 ± 0.147 16.7 ± 0.05 10.8 ± 0.03 8.3 ± 0.03 5.4 ± 0.05 0.90 ± 0.003 0.92 ± 0.003 0.90 ± 0.004 0.92 ± 0.008 The monofilament diameter was 240 lm for all samples. The center-to-center cell length l is unaffected by diffusion bonding. Fig. 6. Truss-face sheet interface for a square oriented lattice structure after the brazing treatment: (a) SEM micrograph; (b) optical microscope crosssectional micrograph; and (c) SEM cross-sectional micrograph. Fig. 7. Photographs showing TMC square lattice core sandwich structures. 0.02 mm/min (see Table 2 for corresponding strain rates). The measured load cell force was used to calculate the nominal stress applied to the sandwich, and the nominal through thickness strain was obtained from a laser extensometer positioned about the sample centerline. The gage length for strain measurement for the compression samples was the core height, H (see Table 2). The through thickness, compressive stress–strain responses for square lattice structures at each q are shown in Fig. 8. All the cellular structures deformed in an elastic– brittle manner with a variable degree of post peak strength retention that decreased with increasing relative density. The stiffnesses and peak strengths are plotted against q in Figs. 9a and b. The stiffness exhibited a linear dependence P. Moongkhamklang et al. / Composites: Part A 39 (2008) 176–187 181 Table 2 Compression test parameters Sample relative density, q ð%Þ Core height, H (mm) Strain rate, e_ (105 s1) 16.7 10.8 8.3 5.4 6.20 ± 0.031 9.38 ± 0.010 12.66 ± 0.015 19.26 ± 0.022 5.38 ± 0.027 3.56 ± 0.004 2.68 ± 0.003 1.73 ± 0.002 Fig. 8. Compressive stress–strain response for square lattice truss structures with q ¼ 16:7; 10:8; 8:3; and 5:4%. 3 upon q, while the strength appeared to depend on ðqÞ . Figs. 10 and 11 show stress–strain responses and photographs of the lattice taken during the compression of samples with high (q ¼ 16:7%) and low (q ¼ 5:4%) lattice relative densities, correspondingly. As the samples were compressed, trusses parallel to the loading direction deformed elastically and then buckled cooperatively as a consequence of being joined by the horizontal trusses. The peak stress in the stress–strain curve coincided with the onset of this buckling instability. Unload/reload tests indicated that prior to the peak compressive strength the strain was fully recoverable, indicating that the strength of these structures is controlled by elastic buckling of the vertical trusses. Note that Fig. 8 indicates that the lower the relative density (the more slender the trusses) the lower the strength and the smaller the core strain at the onset of elastic buckling. In the highest relative density lattice (with q ¼ 16:7%), the trusses had a relatively low aspect ratio, and fracture of the monofilament was observed instantaneously with buckling (Fig. 10). Fig. 11 shows clearly that for the lattices with lower relative densities (more slender trusses), the trusses continued to buckle cooperatively as the strain progressed beyond the load peak. The buckling half wavelength was equal to the core height. This bucklingaccommodated straining was accompanied by a significant decrease in applied stress, i.e. core softening. As compres- Fig. 9. Experimental data for (a) out-of-plane compressive stiffness and (b) out-of-plane compressive strength of the TMC square truss cores. sion continued, the truss nodes were subjected to increasingly significant shear forces and eventually debonded. Fig. 12 shows micrographs of a vertical truss after the compression test where shear debonding has occurred. In addition to debonding at the nodal contact, fracture of the metallic coating and fiber also occurred in this case. While the peak compressive strengths appear to be simply controlled by the elastic buckling instability, the post peak stress behavior is controlled by less obvious mechanisms. From Fig. 11, it is clear that the unloading paths were not parallel to the initial elastic response and did not return to zero strain. This is indicative of inelastic deformation of the metallic coating. It appears that after the onset of the buckling instability, the SCS-6 fiber contin- 182 P. Moongkhamklang et al. / Composites: Part A 39 (2008) 176–187 Fig. 10. Compressive stress–strain response and corresponding photographs of a square lattice truss structure with q ¼ 16:7%: (a) prior to initial loading; (b) prior to peak load; (c) immediately after the peak load; and (d) after the peak load. Events (b)–(d) occurred within a few seconds. Fig. 11. Compressive stress–strain response and corresponding photographs of a square oriented lattice truss structure with q ¼ 5:4%: (a) prior to initial loading; (b) after the peak load and prior to first unloading; (c) following first unloading; (d) prior to second unloading; (e) following second unloading; (f) prior to third unloading; (g) following third unloading; (h) prior to fourth unloading; and (i) following fourth unloading. P. Moongkhamklang et al. / Composites: Part A 39 (2008) 176–187 183 where Es is the axial Young’s modulus of the parent material. The axial Young’s modulus of the TMC monofilament can be estimated by the rule of mixtures: Es ¼ ð1 f ÞEm þ fEf ; ð5Þ where f is the volume fraction of the SCS-6 fiber, and Em and Ef are the Young’s moduli of the Ti–6Al–4V matrix and SCS-6 fiber, respectively. For Ef = 400 GPa [44,45], Em = 115 GPa [39], and f = 0.35, Eq. (5) gives Es = 215 GPa. A comparison between the measured and predicted stiffness (plotted as non-dimensional compressive stiffness, P ¼ Ec =ðEs qÞÞ as a function of the lattice relative density is shown in Fig. 13a. While most of the experimental data lie within 30% of the predicted value, some data lie well Fig. 12. Nodal shear and coating/fiber fracture near the nodes of a compressively loaded square lattice truss structure with q ¼ 10:8%. ued to buckle elastically, while Ti–6Al–4V coating deformed plastically to accommodate the bending strain and node shear. At the highest core strains, beyond the elastic limit of the SCC-6 fiber and ductility of the Ti alloy coating, truss node debonding, coating fracture, and eventually SCS-6 fiber fracture accommodated the imposed strain and were responsible for the core softening. The reloading behavior of these structures also revealed interesting effects, Fig. 11. In particular, it can be seen that when the lattice structure was reloaded, it followed a different stress–strain path to that during unloading. During unloading, the applied stress at a fixed core strain was less than that during the subsequent reloading cycle. This appears to be a result of elastic SiC fiber spring back and the release of the stored elastic energy in the fiber. 4. Discussion Simple micromechanical arguments can be used to rationalize the initial loading modulus and peak strength of the composite cellular materials tested here. 4.1. Compressive stiffness Under out-of-plane compression, only half of the trusses (the vertical trusses) carry load. Prior to buckling of the compressively loaded columns, the elastic modulus, Ec, of the collinear lattice is simply [46]: 1 Ec ¼ Es q; 2 ð4Þ Fig. 13. Analytical prediction and experimental data for (a) dimensionless stiffness and (b) strength of TMC square lattices. 184 P. Moongkhamklang et al. / Composites: Part A 39 (2008) 176–187 below the prediction. Such discrepancies have been frequently reported for cellular materials [20–31] and the origin of the effect appears to result from imperfections introduced in the fabrication process. The discrepancy observed here is believed to be a consequence of small variations in the length of the load–carrying trusses (core height) due to the cutting process. During initial loading the applied load would then be disproportionately shared between the trusses. The compressive platen would apply the load onto longer trusses first. Because the platen moved with a constant rate, lower load would then be required than if all the trusses were load carrying. As compression proceeds, the load would be applied onto more and eventually all trusses. This makes the initial slope of the stress–strain plot (where a constant load supporting area is assumed) relatively low, but it continues to increase until the applied load is proportionately shared among all the trusses. 4.2. Compressive strength The peak compressive strengths of the TMC square collinear cores can be estimated by analyzing the failure modes of truss members as individual axially loaded columns. It is assumed that the lattice collapses by elastic buckling of the constituent struts over the full height of the sandwich core as schematically illustrated in Fig. 14. If the vertical trusses are not joined together by horizontal trusses, the buckling stress acting on each vertical truss can be described by the elastic bifurcation stress, rcr, of a compressively loaded circular column [47,48]: 2 p2 k 2 E s a rcr ¼ ; ð6Þ lb 4 where Es is the column elastic modulus, a the column radius and lb the length of the column between two supporting ends. The factor k depends upon the rotational stiffness of the end nodes with k = 1 corresponding to a freely rotating pin-joint and k = 2 corresponding to built in nodes which cannot rotate [47,48]. For the square lattices, the trusses length was H (the core height) and we assume k = 2. Using this expression for the predicted critical strength of individual truss members, the mechanical properties of the sandwich panel that has no interaction among the truss members can be globalized and the compressive collapse strength of a core structure, r0pk , can be expressed by [21]: r0pk ¼ Rrcr q; ð7Þ where R is a lattice topology dependent scaling factor. The scaling factor R = 1/2(sin2x1 + sin2x2) accounts for the fact that trusses oriented in the loading direction are the most efficient for load bearing, while those that are inclined are limited by force resolution considerations [49]. For square truss samples, half of the trusses have x1 = 0° and another half have x2 = 90° so the effective value of R ¼ 0:5. By substituting Eq. (6) into Eq. (7), the peak compressive strength of a square lattice truss structure failing by elastic buckling is then: p2 E s a 2 r0pk ¼ q: ð8Þ 2 H Substituting H = nl (where n = number of unit cells along the height of the core), Eqs. (1) and (3) into Eq. (8) gives a relation between core strength, lattice relative density, and the number of cells in the principle loading direction: r0pk ¼ 2Es 3 2Es b2 3 q ¼ q: n2 b o n2 ð9Þ However, since the vertical trusses are joined together and hence are forced to buckle cooperatively, an additional shear stress at the truss nodes is also present (as suggested by experiment, see Fig. 12). This cooperative buckling mode is similar to the shear buckling mode of a fiber composite material modeled by Rosen [50]. In Rosen’s model, adjacent fibers buckle with the same wavelength and in phase with one another. The deformation of the matrix material between adjacent fibers is assumed to be primarily a shear deformation. Rosen found that the compressive strength of a fiber composite rc due to (cooperative) shear buckling is: rc ¼ Fig. 14. Sketches of (a) an undeformed square lattice core and (b) its expected buckling mode under compression. Gm þ vf rcr ; 1 vf ð10Þ where Gm, vf, and rcr are the shear modulus of the matrix, the volumetric fraction of the fibers, and the buckling strength of the fibers. The first term on the right-hand side of Eq. (10) is the contribution to the composite compressive strength from matrix shear and the remaining term is the contribution to the compressive strength associated P. Moongkhamklang et al. / Composites: Part A 39 (2008) 176–187 185 with the finite-bending resistance of the fibers. Fleck [51] subsequently argued that the matrix shear contribution, Gm/(1vf), should be replaced by the in-plane shear modulus of the composite when the compressive strength of the composite material is to be estimated. Using this composite analogy, the cooperative buckling strength of a square lattice is then controlled by the resistance to lattice buckling (Eq. (9)) and the resistance to lattice shear given by the in-plane shear modulus of the lattice structure, G: rpk ¼ G þ r0pk : ð11Þ An analytical expression of the in-plane shear modulus of square lattice G has been recently derived by Hutchinson [52]. He finds that the structure investigated here has a shear modulus: G¼ 1 Es q3 : 16 ð12Þ By substituting Eqs. (12) and (9) into Eq. (11), the peak compressive strength of a square lattice truss structure that fails by cooperative elastic buckling then becomes: 1 2b2 þ ð13Þ rpk ¼ Es q3 : 16 n2 A comparison between the measured and predicted compressive peak strength (plotted as non-dimensional peak compressive strength, R ¼ rpk =ðEs q3 Þ against qÞ of the TMC square collinear cores is shown in Fig. 13b. The cooperative elastic buckling model is seen to capture the peak compressive strengths of these square lattices well. The analytically predicted strength coefficient is 0.13. Most of the experimental data lie within 20% of this estimate. 4.3. Comparisons with other cellular structures The highest specific strength lattice structures previously reported [19–31] utilized a Ti–6Al–4V alloy for the truss structure. The specific strength of such lattices was found to be approximately 100 kN m/kg [26]. The specific strength of the titanium composite lattices studied here was 185 kN m/kg. These TMC lattices therefore appear to be the highest specific strength cellular materials reported to date. The titanium composite lattices investigated here are expected to retain good dimensional stability during loading at temperature up to 500 °C (above this, creep of the metallic component becomes significant). The stiffness and peak strength of the square TMC lattice structures can be compared with those of similar lattices made from stainless steel [30] and ceramic foams [53–62] whose service temperatures also extend to 500 °C and above, Fig. 15. Examination of the figure indicates that the higher relative density TMC lattices possess a higher specific stiffness and strength than any of the other structures/materials. These materials may therefore provide interesting high tempera- Fig. 15. (a) Stiffness and (b) compressive strength versus density for TMC and stainless steel collinear lattice structures. Data for ceramic foams having service temperature of 500 °C and above is also included. ture multifunctional opportunities provided their limited ductility is not a significant constraint. 5. Conclusions 1. A method for making titanium sandwich panels with millimeter-scale titanium matrix composite (TMC) lattice cores has been developed. The method involves laying up linear arrays of TMC monofilaments, alternating the direction of consecutive layers, and using diffusion bonding to join the nodes. The relative density of the 186 P. Moongkhamklang et al. / Composites: Part A 39 (2008) 176–187 lattice was controlled by the diameter of the TMC monofilaments, the spacing between the filaments in each collinear layer (cell length), and the degree of diffusion bonding. 2. The out-of-plane modulus of square TMC lattice structures has been shown to scale linearly with q. The compressive peak strength was controlled by cooperative elastic buckling and varied with ðqÞ3 . 3. The specific strength and stiffness of the lattices significantly exceeds that of other lattice structures fabricated to date. 4. These TMC lattices appear promising candidates for elevated temperature, multifunctional applications. Acknowledgements The authors are grateful to Norman Fleck at the University of Cambridge and Vikram Deshpande at the University of California at Santa Barbara for helpful discussions of the interpretation of this work. The study was supported by the Office of Navel Research (ONR) and monitored by Drs. David Shifler and Steve Fishman under Grant Number N00014-01-1-1051. References [1] Gibson LJ, Ashby MF. Cellular solids: structure and properties. 2nd ed. Cambridge: Cambridge University Press; 1997. [2] Bitzer T. Honeycomb technology: materials, design, manufacturing, applications and testing. Chapman & Hall; 1997. [3] Foo CC, Chai GB, Seah LK. Mechanical properties of Nomex material and Nomex honeycomb structure. Compos Struct 2007;80:588–94. [4] Kintscher M, Kärger L, Wetzel A, Hartung D. Stiffness and failure behaviour of folded sandwich cores under combined transverse shear and compression. Compos Part A – Appl S 2007;38:1288–95. [5] Jung WY, Aref AJ. A combined honeycomb and solid viscoelastic material for structural damping applications. Mech Mater 2003;35:831–44. [6] Paik JK, Thayamballi AK, Kim GS. The strength characteristics of aluminum honeycomb sandwich panels. Thin Wall Struct 1999;35:205–31. [7] Doyoyo M, Mohr D. Microstructural response of aluminum honeycomb to combined out-of-plane loading. Mech Mater 2003;35:865–76. [8] Wenbo H, Kaifeng Z, Guofeng W. Superplastic forming and diffusion bonding for honeycomb structure of Ti–6Al–4V alloy. J Mater Process Tech 2007;183:450–4. [9] Williams JM, Kelly RG. An analysis of corrosive species ingress into IM7/PETI-5 Ti honeycomb composites. Compos Sci Technol 2004;64:1875–83. [10] Wadley HNG. Multifunctional periodic cellular metals. Philos T R Soc A 2006;364:31–68. [11] Ashby MF, Evan AG, Fleck NA, Gibson LJ, Hutchison JW, Wadley HNG. Metal foams: a design guide. Boston: Butterworth Heinemann; 2000. [12] Evan AG, Hutchinson JW, Fleck NA, Ashby MF, Wadley HNG. The topological design of multifunctional cellular metals. Prog Mater Sci 2001;46:309–27. [13] Lu TJ, Stone HA, Ashby MF. Heat transfer in open-cell metal foams. Acta Mater 1998;46:3619–35. [14] Boomsma K, Poulikakos D, Zwick F. Metal foams as compact high performance heat exchangers. Mech Mater 2003;35:1161–76. [15] Deshpande VS, Fleck NA. High strain rate compressive behavior of aluminium alloy foams. Int J Impact Eng 2000;24:277–98. [16] Hall IW, Guden M, Yu CJ. Crushing of aluminum closed cell foams: density and strain rate effects. Scripta Mater 2000;43:515–21. [17] Paul A, Ramamurty U. Strain rate sensitivity of a closed-cell aluminum foam. Mater Sci Eng A 2000;281:1–7. [18] Jiejun W, Chenggong L, Dianbin W, Manchang G. Damping and sound absorption properties of particle reinforced Al matrix composite foams. Compos Sci Technol 2003;63:569–74. [19] Deshpande VS, Fleck NA. Collapse of truss core sandwich beams in 3-point bending. Int J Solid Struct 2001;38:6275–305. [20] Chiras S, Mumm DR, Evans AG, Wicks N, Hutchinson JW, Dharmasena K, et al. The structural performance of near-optimized truss core panels. Int J Solid Struct 2002;39:4093–115. [21] Wadley HNG, Fleck NA, Evans AG. Fabrication and structural performance of periodic cellular metal sandwich structures. Compos Sci Technol 2003;63:2331–43. [22] Kooistra GW, Deshpande VS, Wadley HNG. Compressive behavior of age hardenable tetrahedral lattice truss structures made from aluminium. Acta Mater 2004;52:4229–37. [23] Lim JH, Kang KJ. Mechanical behavior of sandwich panels with tetrahedral and Kagomé truss cores fabricated from wires. Int J Solid Struct 2006;43:5228–46. [24] Queheillalt DT, Wadley HNG. Pyramidal lattice truss structures with hollow trusses. Mater Sci Eng A 2005;397:132–7. [25] Kooistra GW, Wadley HNG. Lattice truss structures from expanded metal sheet. Mater Design 2007;28:507–14. [26] Queheillalt DT, Wadley HNG. Titanium alloy pyramidal lattice truss structures. Mater design, submitted for publication. [27] Wang J, Evans AG, Dharmasena K, Wadley HNG. On the performance of truss panels with Kagomé cores. Int J Solid Struct 2003;40:6981–8. [28] Sypeck DJ, Wadley HNG. Multifunctional microtruss laminates: textile synthesis and properties. J Mater Res 2001;16:890–7. [29] Tian J, Kim T, Lu TJ, Hodson HP, Queheillalt DT, Wadley HNG. The effects of topology upon fluid-flow and heat-transfer within cellular copper structures. Int J Heat Mass Tran 2004;47:3171–86. [30] Queheillalt DT, Wadley HNG. Cellular metal lattices with hollow trusses. Acta Mater 2005;53:303–13. [31] Rathbun HJ, Zok FW, Waltner SA, Mercer C, Evans AG, Queheillalt DT, et al. Structural performance of metallic sandwich beams with hollow truss cores. Acta Mater 2006;54:5509–18. [32] Wicks N, Hutchinson JW. Optimal truss plates. Int J Solids Struct 2001;38:5165–83. [33] Wallach JC, Gibson LJ. Mechanical behavior of a three-dimensional truss material. Int J Solids Struct 2001;38:7181–96. [34] Zok FK, Rathbun HJ, Wei Z, Evans AG. Design of metallic textile core sandwich panels. Int J Solids Struct 2003;40:5707–22. [35] Ashby MF. Properties of foams and lattices. Philos T R Soc A 2006;364:15–30. [36] McCormick TM, Miller R, Kesler O, Gibson LJ. Failure of sandwich beams with metallic foam cores. Int J Solids Struct 2001;38:4901–20. [37] Bart-Smith H, Hutchinson JW, Evans AG. Measurement and analysis of the structural performance of cellular metal sandwich construction. Int J Mech Sci 2001;43:1945–63. [38] Côté F, Fleck NA, Deshpande VS. Fatigue performance of sandwich beams with a pyramidal core. Int J Fatigue 2007;29:1402–12. [39] Boyer R, Welsch G, Collings EW. Material properties handbook: titanium alloys, Materials Park: ASM International, 1994. [40] Guo ZX, Derby B. Solid-state fabrication and interfaces of fibre reinforced metal matrix composites. Prog Mater Sci 1995;39:411–95. [41] Ward-Close CM, Loader C. In: Froes FH, Storer J, editors. Recent advances in titanium metal matrix composites, Warrendale: TMS, 1995. p. 19. P. Moongkhamklang et al. / Composites: Part A 39 (2008) 176–187 [42] McCullough C, Storer J, Berzins LV. In: Froes FH, Storer J, editors. Recent advances in titanium metal matrix composites, Warrendale: TMS, 1995. p. 259. [43] Yang J-M. Creep behavior. In: Mall S, Nicholas T, editors. Titanium matrix composites: mechanical behavior. Technomic Publishing Company: Lancester; 1998. p. 273–312. [44] SCS silicon carbide fibers technical data sheet, Specialty Materials, Lowell, MA. [45] DeBolt HE, Krukonis VJ, Wawner FE. High strength, high modulus SiC filament via CVD. In: Marshall RC, Faust JW, Ryan CE, editors. Silicon carbide. University of South Carolina Press; 1973. p. 68. [46] Queheillalt DT, Deshpande VS, Wadley HNG. Truss waviness effects in cellular lattice structures. J Mech Mater Struct 2007;2:1657–75. [47] Gere JM, Timoshenko SP. Mechanics of materials. Boston: PWS Engineering; 1984. [48] Shanley FR. Mechanics of materials. New York: McGraw-Hill; 1967. [49] Zupan M, Deshpande VS, Fleck NA. The out-of-plane compressive behavior of woven-core sandwich plates. Eur J Mech A-Solid 2004;23:411–21. [50] Rosen BW. Mechanics of composite strengthening. In: Fiber composite materials. American Society of Metals; 1965. p. 37–75. [51] Fleck NA. Compressive failure of fiber composites. Adv Appl Mech 1997;33:43–117. 187 [52] Hutchinson RG. Mechanics of lattice materials. PhD thesis. Cambridge University. Department of Engineering, 2004. [53] Hopper RW, Pekala RW. Low density microcellular carbon or catalytically impregnated carbon forms and process for their preparation. US Patent 4,806,290; 1989. [54] Ultrafoam technical data sheet: Ultramet, Pacoima, CA. [55] Duocel RVC foam technical data sheet, ERG Materials and Aerospace Corporation. Oakland, CA. [56] Hardcastle LA, Sheppard RG, Dingus DF. Process for making carbon foam induced by process depressurization. US Patent 6,576,168; 2003. [57] Maricle DL, Nagle DC. Carbon foam fuel cell components. US Patent 4,125,676; 1978. [58] Han Y, Li J, Wei Q, Tang K. The effect of sintering temperatures on alumina foam strength. Ceram Int 2002;28:755–9. [59] Han Y, Li J, Chen Y. Fabrication of bimodal porous alumina ceramics. Meter Res Bull 2003;38:373–9. [60] DuocelÒ SiC foams technical data sheet, ERG Materials and Aerospace Corporation, Oakland, CA. [61] Jun I, Koh Y, Kim H. Fabrication of ultrahigh porosity ceramics with biaxial pore channels. Mater Lett 2006;60:878–82. [62] Jun I, Koh Y, Song J, Lee S, Kim H. Improved compressive strength of reticulated porous zirconia using carbon coated polymeric sponge as novel template. Mater Lett 2006;60:2507–10.
© Copyright 2026 Paperzz