Ballistic Response of Pyramidal Lattice Truss Structures A Thesis Presented to the faculty of the School of Engineering and Applied Science University of Virginia In Partial Fulfillment of the requirements for the Degree Master of Science (Engineering Physics) By Christian Joseph Yungwirth May 2006 APPROVAL SHEET The thesis is submitted in partial fulfillment of the Requirements for the degree of Master of Science (Engineering Physics) _______________________________ Author, Christian J. Yungwirth This thesis has been read and approved by the examining committee: _______________________________ Thesis advisor, Haydn N.G. Wadley _______________________________ Committee Chairperson, Dana M. Elzey _______________________________ Stuart A. Wolf Accepted for the School of Engineering and Applied Science: _______________________________ Dean, School of Engineering Applied Science May 2006 Abstract Cellular metal structures with periodic “lattice truss” topologies are being utilized for an expanding variety of multifunctional applications including mitigation of the high intensity dynamic loads created by nearby explosions. In these situations, the panels are also exposed to high velocity projectiles and their ballistic response is then pertinent. This thesis explores the ballistic resistance of a cellular pyramidal lattice truss structure fabricated from both a high ductility, high work hardening rate 304 stainless steel and an age hardened 6061 aluminum alloy with similar yield strength, but lower ductility and significantly smaller work hardening rate. Projectiles made of 1020 carbon steel, measuring 12.5 mm in diameter, made normal impact with these sandwich structures. The pyramidal lattice truss core sandwich panels had a core relative density of approximately 3% with cell sizes of approximately 2.54 cm x 2.54 cm x 2.54 cm and 1.5 mm thick faces that were 25.4 mm apart. The stainless steel structures were first penetrated at an impact velocity of approximately 450 m/s. Above this critical velocity, the exit velocity of the projectile was between 55 and 70% of the impact velocity. The sandwich structure outperformed a solid plate of similar composition, with an equivalent areal density of 28 kg/m2, exhibiting an exit velocity of the projectile that was between 67 and 70%. The aluminum alloy structures were penetrated at the lowest test velocity of approximately 200 m/s. The exit velocity of the projectile was between 60 and 92% of the impact velocity. The stainless steel lattice structures were then infiltrated with a polyurethane that had a Tg of -56 °C, a low tensile modulus of 2.76 MPa and a high elongation to yield of approximately 700%. Infiltration of the stainless steel lattice with this low Tg polyurethane exhibited a similar critical velocity of approximately 450 m/s, similar to the empty structure. Above the critical velocity, the exit velocity of the projectile was between 50 to 55% of the impact velocity at the expense of doubling the mass per unit area. Energy was mainly dissipated from the associated strain fields as the polymer was transiently displaced outwardly from the projectile. Methods were developed to fabricate other “hybrid” lattice truss structures with various materials infiltrated into the sandwich panel. These systems contained ballistic fabrics, a different polymer system and metal encased ceramics. Two of the systems prevented penetration by projectiles with velocities in the 600 m/s range. The first system was a polyurethane infiltrated lattice that had a Tg of 49 °C. The significantly higher Tg material had a higher tensile modulus of 1120 MPa and a lower elongation to fracture of 16%. A second system containing 304 stainless steel encased alumina prisms, with the surrounding space infiltrated with a high Tg polyurethane, also resisted penetration but at the expense of a four fold increase in mass per unit area. The success of the system can be attributed to the degree of energy absorption of the alumina prisms and the confinement of the fragments. After fracturing, the ceramic fragments were contained in steel tubes and frictionally dissipated a majority of the remaining kinetic energy while fracturing the projectile. The remainder of the kinetic energy appeared to be dissipated by the polyurethane and plastic dishing of the rear metal facesheet. These “hybrid” lattice systems show significant promise as multifunctional load-bearing structures that also possess high ballistic performance. Acknowledgements I want to express my gratitude to my advisor Professor Haydn N.G. Wadley. He has been instrumental in sharpening my analytical tools and assisting me in accomplishing my goals. Allowing a large degree of latitude, he gave me the opportunity to explore my ideas and provided the resources to see them until their conclusion. Along the journey, I gained an immense professional respect for him and forged a personal friendship that will continue after my graduate education. I want to extend my appreciation to the members of the IPM Laboratory, in particular Mrs. Sherri S. Thompson, Dr. Doug T. Queheillalt, Dr. Kumar P. Dharmasena and Mr. Rich T. Gregory. Without Sherri’s connection to the group members or her “greasing the wheels”, the IPM Laboratory would cease to function. I am indebted to Doug and Kumar for their tolerance of my innumerable questions and curiosities. Their breadth of knowledge was an invaluable resource that was not taken for granted. I owe Rich thanks for keeping the computers operating smoothly and maintaining my lifeline to the group over distances despite my occasional indoor headwear. Additionally, I would like to express my sincere gratitude to Dr. Mark T. Aronson and his group at the University of Virginia for conducting chemical characterizations, Dr. Alan M. Zakraysek at the Naval Surface Warfare Center for conducting ballistic testing, Dr. Steve G. Fishman at the Office of Naval Research for providing funding for my research and my other committee members Dr. Dana M. Elzey and Dr. Stuart A. Wolf. Dedication I would like to dedicate my efforts to my grandmother Agnes V. Sands, my deceased grandfather Joseph E. Sands, my mother Katherine M. Yungwirth, my aunt Joann M. Sands and my aunt Anne M. Sands. My accomplishments are a testimonial to the abyss of love and affection they have provided me from the day I was brought into this world. Every one of them has provided a safe haven where I could venture into the farthest expanses of my imagination and explore each crevice thoroughly. These explorations and their support have forged the man that stands today. Through the trials and tribulations, they have remained steadfast in their support even with the occasional mild opposition. Therefore, I extend my deepest, sincerest gratitude to each of them and wish that happiness and prosperity finds them on their continued journey through life. Additionally, I would like to make a dedication to all of my friends and the beloved people for who I care deeply, particularly Janet and the Conterelli’s. Janet has been a pillar of support that I have come to depend and I look forward to a future rich with joyous memories shared with her. She is an amazing woman that epitomizes beauty, intelligence and loyalty. The Conterelli’s have lovingly embraced me into their lives and their hearth, a deed that has earned my eternal gratitude and appreciation. Quotations Ad astra per aspera (A rough road leads to the stars) - Plaque dedicated to the crew of Apollo 1 at Launch Complex 34, Kennedy Space Center Γνώθι Σεαυτόν (Gnothi Seauton): “know thyself” Μηδέν Άγαν (Meden Agan): "nothing in excess" - Inscribed in golden letters at the lintel of the entrance to the Temple of Apollo at Delphi He who fights with monsters might take care lest he thereby become a monster. And if you gaze for long into an abyss, the abyss gazes also into you. - Friedrich Nietzsche, Beyond Good and Evil If you aspire to the highest place, it is no disgrace to stop at the second, or even the third, place. - Cicero i Table of Contents Table of Contents ............................................................................................................... i List of Figures................................................................................................................... iii List of Tables .................................................................................................................. viii List of Symbols ................................................................................................................. ix Chapter 1. Introduction........................................................................................................1 1.1 1.2 1.3 1.4 Multifunctional Cellular Materials ........................................................1 Ballistic Properties of Cellular Metals...................................................4 Goals of this Thesis................................................................................6 Thesis Outline ........................................................................................6 2. Impact and Plate Penetration Mechanics ........................................................7 2.1 2.2 Impact Mechanics ..................................................................................7 Plate Impact Mechanics .......................................................................11 3. Materials and Structures.................................................................................19 3.1 3.2 3.3 3.4 3.5 Sandwich Panel Fabrication.................................................................19 Relative Density Relations...................................................................22 Alloy Mechanical Properties................................................................23 3.3.1 304 Stainless Steel .......................................................23 3.3.2 Age Hardened 6061-T6 Aluminum Alloy ...................24 Polymer Infiltrated ...............................................................................25 3.4.1 Hybrid Lattice Fabrication...........................................25 3.4.2 Polymer ........................................................................26 Polymer Characterization.....................................................................28 3.5.1 DSC Analysis...............................................................28 3.5.2 DMA Analysis .............................................................29 4. Ballistic Testing ................................................................................................33 4.1 4.2 4.3 Stage One Powder Gun........................................................................33 Sabot and Projectile .............................................................................34 Test Fixture ..........................................................................................35 ii 5. Empty Lattice Resistance ................................................................................38 5.1 5.2 5.3 5.4 304 Stainless Steel Panel Response .....................................................38 304 Stainless Steel Plate Response ......................................................44 AA6061 Panel Response......................................................................49 Discussion ............................................................................................55 6. Polymer Infiltration Study ..............................................................................57 6.1 6.2 Ballistic Response................................................................................57 Discussion ............................................................................................63 7. Enhanced Ballistic Lattice Fabrication ...........................................................65 7.1 7.2 7.3 7.4 7.5 7.6 Concept Systems..................................................................................65 Lattice Structure Fabrication................................................................66 Double Layer Lattice Relative Density................................................67 Infiltration Materials and Methods ......................................................69 7.4.1 Polymers ......................................................................69 7.4.2 Fabric ...........................................................................70 7.4.3 Metal Encased Ceramic Prisms ...................................70 Hybrid Lattice Relative Density ..........................................................71 Material Properties...............................................................................71 7.6.1 Brazed 304 Stainless Steel ...........................................73 7.6.2 PU 2 .............................................................................74 7.6.2.1 DSC Analysis....................................74 7.6.2.2 DMA Analysis ..................................75 8. Ballistic Testing ................................................................................................78 8.1 8.2 8.3 Test Setup.............................................................................................78 Results..................................................................................................80 8.2.1 Single Layer Empty System............................................80 8.2.2 Soft Polymer Filled System ............................................82 8.2.3 Double Layer Filled with PU 1.......................................84 8.2.4 Hard Polymer Filled System...........................................85 8.2.5 Single layer filled with PU 1 plus Fabric........................87 8.2.6 Ceramic plus PU 2 Filled System ...................................88 Discussion ............................................................................................89 9. Discussion..........................................................................................................91 10. Conclusions.....................................................................................................96 References iii List of Figures Figure 1. a) Photograph and illustration of Alporas®, a stochastic closed cell aluminum foam manufactured by Foam Tech Co. Ltd. via titanium hydride particle decomposition. b) Photograph and illustration of Duocel®, a stochastic open cell aluminum foam manufactured by ERG Materials and Aerospace Corp. via pressure casting. Figure 2. Isometric view of a) Hexagonal honeycomb b) Square honeycomb c) Triangular honeycomb d) Triangular corrugation e) Diamond corrugation f) navtruss corrugation g) Tetrahedral lattice truss h) Pyramidal lattice truss and i) 3-D Kagomé lattice truss structures between solid face sheets. The tetrahedral lattice truss has three sets of triangular, prismatic voids (0°/60°/120°). The pyramidal lattice truss possesses similar geometrical voids running orthogonally (0°/90°) through the lattice. The 3-D Kagomé lattice truss possesses two sets of similar geometrical void orientations (0°/60°/120° and 30°/90°/150°). Figure 3. Bonded-interface test result showing section view with subsurface accumulated damage beneath the indentation (Left). Finite-element result showing extent of the plastic zone in terms of contours of maximum shear stress at τ Max / Y = 0.5 for indenter load P = 1000 N (Right). Distances are expressed in terms of the contact radius, a0 = 0.326mm , for the elastic case of P = 1000 N . The bold black line indicates the radius of the circle of contact, a0 = 0.437mm , as determined from the finite-element calculation [393H57]. Figure 4. Illustration of a thin target showing a) bulging b) dishing and c) cratering [407H69]. Figure 5. Perforation mechanisms [421H69]. Figure 6. Manufacturing process for making pyramidal lattice truss cored sandwich panels [465H3]. Figure 7. Illustration of the laser welding process for bonding the truss lattice to proximal and distal facesheet. Figure 8. Cross section of the single layer empty pyramidal truss lattice along a nodal line. Figure 9. Unit cell geometry used to derive the relative density for single layer pyramidal topology. Figure 10. Uniaxial tension data for as-received 304 stainless steel. Figure 11. Uniaxial tension data for the age hardened 6061-T6 aluminum alloy. Figure 12. Heat capacity (Rev Cp) of PU 1 as a function of temperature (°C). iv Figure 13. Storage modulus at a frequency of 1 Hz for PU 1 as a function of temperature. Figure 14. Predicted values for the storage and loss modulus of PU 1 at a reference temperature of 25 °C as a function of frequency. Figure 15. Tan δ ( E ′′ / E ′ ) of PU 1 as a function of frequency. Figure 16. Illustration of the single stage powder gun used for ballistic studies. The sabot carried a 12.5 mm spherical projectile. Figure 17. Illustration of the sabot used to carry the projectile. Figure 18. Illustration of setup used in the blast chamber to mount the samples, measure velocities and record via high-speed photography. Figure 19. Plot of exit velocity of the projectile (m/s) as a function of the impact velocity (m/s) for the 304 stainless steel pyramidal truss lattice. Figure 20. Plot of energy absorbed (J) as a function of the impact velocity (m/s) for the 304 stainless steel pyramidal truss lattice system. Figure 21. a) Cross section of the 304 stainless steel sample that was impacted at 339.2 m/s and was not fully penetrated, shot 1 b) Cross section of the entry hole of shot 1 c) Cross section of the exit hole of shot 1. Figure 22. a) Cross section of the 304 stainless steel sample that was impacted at 810.8 m/s, shot 3 b) Cross section of the entry hole of shot 3 c) Cross section of the exit hole of shot 3. Figure 23. a) Cross section of the 304 stainless steel sample that was impacted at 1206.1 m/s, shot 54 b) Cross section of the entry hole of shot 54 c) Cross section of the exit hole of shot 54. Figure 24. Plot of exit velocity of the projectile (m/s) as a function of the impact velocity (m/s) for the 304 stainless steel monolithic plate compared to the 304 stainless steel pyramidal truss lattice. Figure 25. Plot of energy absorbed (J) as a function of the impact velocity (m/s) for the 304 stainless steel pyramidal truss lattice system and solid plate. Figure 26. Cross section of the monolithic 304 stainless steel plate that was shot at 341.7 m/s, shot 58. Figure 27. Cross section of the monolithic 304 stainless steel plate that was shot at 509.6 m/s, shot 105. v Figure 28. Cross section of the monolithic 304 stainless steel plate that was shot at 1226.5 m/s, shot 108. Figure 29. Plot of exit velocity of the projectile (m/s) as a function of the impact velocity (m/s) for the age hardened AA6061 aluminum alloy pyramidal truss lattice compared to the 304 stainless steel pyramidal truss lattice system. Figure 30. Plot of the energy absorbed (J) as a function of the impact velocity (m/s) for the 304 stainless steel sandwich panel and AA6061 aluminum alloy sandwich panel. Figure 31. a) Cross section of the AA6061 sample that was impacted at 280.1 m/s, shot 114 b) Cross section of the entry hole of shot 114 c) Cross section of the exit hole of shot 114. Figure 32. a) Cross section of the AA6061 sample that was impacted at 493.3 m/s, shot 81 b) Cross section of the entry hole of shot 81 c) Cross section of the exit hole of shot 81. Figure 33. a) Cross section of the AA6061 sample that was impacted at 1222.2 m/, shot 55 b) b) Cross section of the entry hole of shot 55 c) Cross section of the exit hole of shot 55. Figure 34. Plot of exit velocity of the projectile (m/s) as a function of the impact velocity (m/s) for the 304 hybrid stainless steel pyramidal truss and the empty 304 stainless pyramidal truss lattice. Figure 35. Plot of projectile the energy absorbed (J) as a function of the impact velocity (m/s) for the 304 stainless steel pyramidal truss lattice infiltrated with PU 1 and the empty 304 stainless pyramidal truss lattice. Figure 36. a) Cross section of the 304 stainless steel sample infiltrated with PU 1 that was impacted at 370.9 m/s, shot 70 b) Cross section of the entry hole of shot 70 c) Cross section of the exit hole of shot 70. Figure 37. a) Cross section of the 304 stainless steel pyramidal truss lattice filled with PU 1 that was impacted at 515.7 m/s, shot 110 b) Cross section of the entry hole of shot 110 c) Cross section of the exit hole of shot 110. Figure 38. a) Cross section of the 304 stainless steel pyramidal truss lattice filled with PU 1 that was impacted at 984.5 m/s, shot 112 b) Cross section of the entry hole of shot 112 c) Cross section of the exit hole of shot 112. Figure 39. Schematic illustrations of pyramidal lattice truss concepts evaluated in the study. a) Empty pyramidal truss lattice b) Polymer filled in truss lattice c) Ballistic fabric interwoven between trusses with polymer filling remaining air space d) 304 SS encased alumina inserted in triangular prismatic voids and remaining air space filled with polymer vi Figure 40. Unit cell geometry used to derive the relative density for a double layer pyramidal topology. Figure 41. Uniaxial tension data for brazed 304 stainless steel. Figure 42. Heat capacity (Rev Cp) PU 2 as a function of temperature (°C). Figure 43. Storage modulus at a frequency of 1 Hz for PU 2 as a function of temperature. Figure 44. Predicted values for the storage and loss modulus of PU 2 at a reference temperature of 25 °C as a function of frequency. Figure 45. Tan δ ( E ′′ / E ′ ) of PU 2 as a function of frequency. Figure 46. Ballistic testing configuration. Ball bearing projectiles with a radius of 6 mm and weight of 6.9 g were used. An impact velocity of approximately 600 m/s was used for all the tests. Figure 47. Projectile impact location for a) Single and b) Double layer pyramidal lattice truss sandwich panels. Figure 48. Test 1: a) Cross section of the single layer empty pyramidal truss lattice along a nodal line b) Cross section of the single layer empty pyramidal truss lattice after a projectile impact of 598 m/s. Figure 49. High-speed photography of a projectile impact with the empty single layer pyramidal lattice (system 1). Each figure (a)-(h) depicts a frame of the high-speed photography. The time in microseconds (μs) is labeled from the initial impact of the projectile with the proximal facesheet. Figure 50. Position of a spherical projectile from the proximal facesheet of the empty single layer pyramidal lattice truss as a function of time. To the left of the time of impact is before the impact of the projectile and the right of the time of impact is after impact of the projectile. Figure 51. Test 2: a) Cross section of the single layer pyramidal truss lattice filled with PU 1 b) Cross section of the single layer pyramidal truss lattice filled with PU 1 after a projectile impact of 616 m/s. Notice the brass breech rupture disk (b) remaining in the polymer while the projectiles path resealed. Figure 52. Test 7: a) Cross section of the double layer pyramidal truss lattice filled with PU 1 b) Cross section of the double layer pyramidal truss lattice filled with PU 1 after an impact of 613 m/s. vii Figure 53. Test 4: a) Cross section of the single layer pyramidal truss lattice filled with PU 2 b) Cross section of the single layer pyramidal truss lattice filled with PU 2 after a projectile impact of 632 m/s showing approximately 8.5 mm deflection of the rear face panel. Note that the projectile is visibly arrested in (b). Figure 54. X-ray tomography of specimen 4. Side profile (Left). Elevated view above proximal face sheet (Right). Figure 55. Test 5: a) Cross section of the single layer pyramidal truss lattice filled with the interwoven fabric and the PU 1 b) Cross section of the single layer pyramidal truss lattice filled with interwoven fabric and the PU 1 after a projectile impact of 613 m/s. Figure 56. Test 6: a) Cross section of the single layer pyramidal truss lattice filled with 304 stainless steel prisms and PU 2 b) Cross section of the single layer pyramidal truss lattice filled with 304 stainless steel prisms and PU 2 after an impact of 613 m/s. viii List of Tables Table 1. Manufacturer reported properties for the polyurethane system. Table 2. The impact and exit velocities of the projectile, nodal disbonding of the distal facesheet and whether the projectile penetrated the distal facesheet for the 304 stainless steel pyramidal truss lattice sandwich structure. Table 3. The impact and exit velocities of the projectile for a 3 mm thick 304 stainless steel monolithic plate. Table 4. The impact and exit velocities of the projectile, nodal disbonding of the distal facesheet and whether the projectile penetrated the distal facesheet for the age hardened AA6061-T6 aluminum alloy pyramidal truss lattice sandwich structure. Table 5. The impact and exit velocities of the projectile, nodal disbonding of the distal facesheet and whether the projectile penetrated the distal facesheet for the 304 stainless steel pyramidal truss lattice sandwich structure with polyurethane. Table 6. Physical descriptions of composite lattice truss systems fabricated. Table 7. Manufacturer reported properties for the polyurethane system. Table 8. Physical properties of AD-94 Al2O3 triangular prisms. ix List of Symbols Δ δ ν π ρ ρ θ σ τ υ0 υr ω a b cp cpr ct d h h0 k l m pm p0 r t w x⎫ ⎪ y⎬ z ⎪⎭ E Ec Ed E* E′ E ′′ P R Tg V W distance of mutual approach between indenter and specimen parameter used to assess dissipative energy efficiency Poisson’s ratio pi mass density relative density petal rotation angle at the end of stages stress shear stress initial velocity of projectile residual velocity of projectile angle between truss and facesheet indenter contact area radius triangle base height heat capacity wave velocity of projectile dilatational wave velocity of target diameter height plate thickness mass ratio length mass mean contact pressure maximum contact pressure (Hertz stress) radial distance thickness width Cartesian coordinates Young’s modulus perforation energy of plate energy absorbed through plate dishing contact modulus storage modulus loss modulus indenter load force (reduced) radius of sphere glass transition temperature volume work x Subscripts θ a c cr f i m p pu r t tr u y z angular cylindrical coordinate aluminum oxide unit cell crack fabric intermediate plate base metal projectile polyurethane radial cylindrical coordinate target truss ultimate yield height cylindrical coordinate xi Page Left Intentionally Blank 1 Chapter 1 Introduction Cellular metals are a relatively new class of materials [1-2]. Using foaming or foam derived methods, various groups developed stochastic topology structures in the 1980’s [1]. Examples of closed and open cell systems are shown in Figure 1. More recently, methods have begun to be developed to create open cell topology structures with periodic, or lattice cells [3] and compliment closed cell periodic systems (e.g. honeycombs) that have been developed for weight sensitive structural applications [3-4]. 1.1 Multifunctional Cellular Materials Cellular metal structures with both stochastic (metal foams) [2-6], Figure 1, and periodic topologies [5,6], Figure 2, are being utilized for an expanding variety of structural [3-12], thermal [13-15], and acoustic damping [2] applications. a) Closed-cell Metal Foam b) Open-cell Metal Foam Figure 1. a) Photograph and illustration of Alporas®, a stochastic closed cell aluminum foam manufactured by Foam Tech Co. Ltd. via titanium hydride particle decomposition. b) Photograph and illustration of Duocel®, a stochastic open cell aluminum foam manufactured by ERG Materials and Aerospace Corp. via pressure casting. 2 Figure 2. Isometric view of a) Hexagonal honeycomb b) Square honeycomb c) Triangular honeycomb d) Triangular corrugation e) Diamond corrugation f) navtruss corrugation g) Tetrahedral lattice truss h) Pyramidal lattice truss and i) 3-D Kagomé lattice truss structures between solid face sheets. The tetrahedral lattice truss has three sets of triangular, prismatic voids (0°/60°/120°). The pyramidal lattice truss possesses similar geometrical voids running orthogonally (0°/90°) through the lattice. The 3-D Kagomé lattice truss possesses two sets of similar geometrical void orientations (0°/60°/120° and 30°/90°/150°). The periodic structures show significant promise as multifunctional structures when configured as the cores of sandwich panel structures. In these scenarios, functions such as structural load support and thermal management can be simultaneously exploited [11,13,15]. Periodic structures consisting of 3-D space filling unit cells with honeycomb [3,16-17], corrugation [18] or lattice truss topologies [3,7] are significantly more structurally efficient than equivalent relative density metal foams. The fabrication routes developed 3 for these periodic cellular systems [19] also enable much higher strength alloys to be used. As a result, periodic topology structures can be an order of magnitude, or more, stronger than metal foams of the same mass [12]. As the relative density decreases, lattice topologies have been shown to have higher strengths than honeycombs and simple corrugations [20]. The first proposed lattice structure was lattice block material [21-23]. More recently, structures based on the octet truss (i.e. a tetrahedral structure) [24], a pyramidal truss [25-26], the 3-D Kagomé [27-28] and various lattices created by weaving or laying up metal wires and tubes have all been developed [7]. Figure 2 showed examples. The cell size of these structures can be varied from several hundreds of micrometers to several centimeters using metal folding and either brazing or spot welding fabrication methods [29,16]. All cellular metals have been shown to possess excellent impact energy absorption characteristics [11,30-33]. Typically, these materials exhibit three regions of deformation [1]. The first region is an elastic region followed by a plateau stress region persisting to plastic strains of around 60-70%. It corresponds to a region where buckling and plastic collapse of the cell walls occurs. Finally, after the collapse of the cells, sufficient densification of the structure has occurred that cell wall/truss impingement causes a sharp rise in stress. This arises because of their very extensive crush strains at near constant flow stress. The mechanics of foam deformation and associated energy absorption have been reviewed by M. Ashby et al. [2], and includes expressions for foam elastic modulus, elastic collapse stress, plastic collapse, strength and densification strain etc. Recent experimental and numerical modeling studies indicate that periodic lattice truss and honeycomb core sandwich panels enable significant mitigation of explosion created shock waves [31-34]. These studies indicate that sandwich panels fabricated from high ductility metals (e.g. stainless steels and some aluminum alloys) with honeycomb, lattice truss or corrugated cores could provide multifunctional static load support and blast protection in air and underwater [36]. If cellular metal structures of this type were used for air blast mitigation applications, they would also be exposed to impact by high 4 velocity projectiles. Very little is known about the penetration resistance of these structures or ways to enhance it. 1.2 Ballistic Properties of Cellular Metals A study conducted by B. Gama et al. [37] has explored the ballistic characteristics of a cellular metal. It investigated metal foams made from low strength aluminum alloys in the context of integral armor concepts and reported only modest system performance enhancements. In this application, closed-cell aluminum foam delayed and attenuated stress wave propagation throughout the composite integral armor system. The cellular structure of the metal foam acted as small waveguides and a geometric dispersion of the stress waves occurred leading to propagation delays. Damping in these systems has been studied by D. Radford et al. at the University of Cambridge [31-34] and is associated with thermo-elastic effects. These studies provided little illumination of the performance of periodic lattice truss topologies, or sandwich panels constructed from them when exposed to high velocity projectiles. It is to be expected that the two solid faces of a sandwich panel will each individually provide some level of projectile propagation resistance. The penetration of a metal sheet such as rolled homogenous armor (RHA) [35] by a normal incidence projectile has been widely studied [38]. The critical velocity (i.e. the velocity at which the projectile penetrates the target) increases linearly with target thickness [32,35]. The depth of penetration (DOP) also increases linearly as the projectile velocity is increased [32, 35]. Experimental studies by A. Almohandes et al. [39] indicated that distributing the mass of a plate amongst a pair of plates of equivalent areal density resulted in a slight lowering of the ballistic resistance. Theoretical studies by G. Ben-Dor et al. [40] and experimental studies by J. Radin and W. Goldsmith [41] indicate that the distance between such a pair of plates has little or no effect upon the ballistic resistance of such systems. Other work conducted by R. Corran et al. [42] found that two plates in tight contact had a slightly higher ballistic limit than an identical pair that was not in contact. They tentatively attribute this small effect to a frictional interaction between layers. 5 The lattice truss structure itself might be anticipated to have some effect upon the propagation of a projectile provided the projectile impacts the lattice during penetration (i.e. the cell spacing is small compared to the projectile diameter). For example, it might increase the ballistic performance by deflecting (tipping) the projectile or causing some of its energy to be dissipated by plastic deformation/fracture of the trusses. Projectile kinetic energy losses during penetration of the face sheets and the truss structures are likely to be increased by utilizing metals with high strength, high fracture toughness (ductility) and high strain and strain rate hardening coefficients. Many austenitic and super austenitic stainless steels [43] have medium strength levels but high toughness and strain rate hardening coefficients. Analytical and experimental results from a study conducted by S. Shun-cheng et al. [44] showed that for 304 stainless steel, the yield stress increased with increasing strain rate until an upper limit of approximately 2500 s-1. Other materials, such as AA6061-T6 aluminum alloy, exhibit a decrease in strength as the strain rate is increased [45]. Recent developments in the fabrication of lattice structures from such alloys using perforated metal folding and brazing techniques [3,29] now enable an experimental assessment of the ballistic behavior of sandwich panels with lattice truss cores to be investigated. The voids in lattice truss structures provide easy access to the interior of the sandwich panel and enable materials to be added that might improve ballistic resistance. For example, the voids could be infiltrated with polymers to dissipate a projectiles kinetic energy [46], or with ballistic fabrics to arrest fragments [47,48] or with hard ceramics that fragment projectiles and impede their penetration [49,50]. The merits of these are also presently unclear and no experimental assessments of the ballistic properties and deformation mechanisms of these “hybrid” lattice truss structures have ever been reported. 6 1.3 Goals of this Thesis This thesis experimentally investigates the ballistic response of stainless steel and 6061 aluminum alloy pyramidal lattice truss core sandwich structures using spherical projectiles with impact velocities up to approximately 1200 m/s. The stainless steel sandwich panel structures response is compared to that of a monolithic plate of equivalent areal density (mass per unit area). The effects of filling the lattice void space with an elastomer are then investigated and the feasibility of fabricating more sophisticated “hybrid” sandwich structures containing ceramics and ballistic fabrics is added. The study finds significantly enhanced ballistic resistance can be achieved by this approach. 1.4 Thesis Outline The thesis is organized as follows: Chapter 2 presents the mechanisms of impact and plate penetration mechanics. Chapter 3 presents the materials and the fabrication methodology for the lattice truss sandwich structure. Chapter 4 describes the ballistic facility used to conduct the experiments and the sabot-projectile system. Chapter 5 presents the initial impact study of the 304 stainless steel and the age hardened AA6061T6 aluminum alloy mono-layer pyramidal lattice truss sandwich structures. Chapter 6 presents a study infiltrating the 304 stainless steel pyramidal lattice truss sandwich structure with an elastomer. Chapter 7 presents the fabrication of hybrid systems where various materials were infiltrated into the structure and Chapter 8 presents the results of the study. Chapter 9 summarizes the findings from the studies while Chapter 10 briefly lists the conclusions obtained. 7 Chapter 2 2.1 Impact and Plate Penetration Mechanics Impact Mechanics The impact of a hard projectile with a softer target causes local deformation (i.e. indent of both objects). The first attempt to develop a theory of the local indentation at the contact between two solid bodies was by Hertz [51], who likened the problem to an equivalent one in electrostatics. Hertzian contact mechanics is based on three key assumptions: i. The surfaces of the contacting bodies are both continuous, smooth, nonconforming and form a frictionless contact. ii. The strains associated with the deformations are small. iii. Each solid behaves as an elastic half-space in the vicinity of the contact zone. The size of the contact area (extent of the deformation field) is therefore small compared to the size of the bodies. According to Hertz, if two elastic spheres with radii R1 and R2 are pressed into contact with a force P, the resultant circular contact area has a radius, a, such that: 1 ⎛ 3PR ⎞ 3 a=⎜ * ⎟ ⎝ 4E ⎠ (1), where E* is the contact modulus defined by: 1 − ν 12 1 − ν 22 E = + E1 E2 * (2). In equation (2), E and ν are the Young’s modulus and elastic Poisson’s ratio of each sphere, respectively. In equation (1), R is the reduced radius of curvature and is related to those of the individual components by the relation: R= 1 1 + R1 R2 (3). Convex surfaces are taken as positive radii of curvature (concave surfaces are therefore taken as negative radii of curvature). If one of the solids is a plane surface then its effective radius is infinite so that the reduced radius of the contact is numerically equal to 8 that of the opposing sphere. This is then reduced to the half-space problem [52]. If we place a cylindrical coordinate system at the initial point of contact, the resulting radial pressure distribution, p(r), is axisymmetric and dependent only upon the radial distance from the initial point of contact. The pressure distribution is semi-elliptical, and of the form 1 ⎛ r2 ⎞2 p( r ) = p0 ⎜⎜1 − 2 ⎟⎟ ⎝ a ⎠ (4), where r 2 = x 2 + y 2 is the radial distance from the initial point of contact. The maximum pressure, p0, occurs on the axis of symmetry. This and the mean pressure, pm, are related: 1 ⎛ 6 PE *2 ⎞ 3 3 3P ⎟ ⎜ p0 = p m = = 2 2πa 2 ⎜⎝ π 3 R 2 ⎟⎠ (5). The maximum pressure, p0, is also sometimes known as the Hertz contact stress. Under this loading, the two spheres move together by a small displacement, Δ, given by: Δ= aπp0 ⎛ 9 P ⎞ a ⎟ = =⎜ 2 E * ⎜⎝ 16 RE *2 ⎟⎠ R 2 2 1 3 (6). Equation (6) is a quasi-static derivation of a sphere making contact with a sphere or plane 3 with a load placed on the axis of symmetry to cause a displacement in the direction of mutual approach. In a dynamical derivation of a sphere impacting a flat plane specimen in the elastic region [53], the second derivative of the displacement of the plane is related to the mass of the projectile, mp, and the force of the projectile impact, P: mp d 2 Δ (t ) = −P dt 2 where Δ is the displacement from the flat plane specimen. (7), 9 By rearranging equation (6) to give an expression for P(Δ) and equating it to equation (7), we obtain the indentation velocity: 1 3 dυ 4 R 2 Δ2 mp =− dt 3E * where υ = (8), dΔ . Multiplying both sides of equation (8) by velocity and integrating from dt the impact velocity of the projectile, υ 0 , to the final velocity, υ f = 0 , we obtain: 1 5 1 8 m pυ 02 = R 2 E * Δ2 2 15 (9). The left hand side of equation (9) equates the kinetic energy of the projectile to the strain energy stored in the specimen. Equation (9) can be arranged to give an expression for the depth of penetration, Δ, as a function of the mass, mp, and the impact velocity, υ 0 , of the projectile: 2 ⎛ 15m υ 2 ⎞ 5 p 0 ⎟ Δ = ⎜⎜ 1 ⎟⎟ ⎜ ⎝ 16 R 2 E * ⎠ (10). This relationship is limited to elastic impacts (i.e. when the impact velocity is low) and both objects are made of materials of high strength. It does not address the plasticity and fracture that can accompany projectile penetration [52, 53]. An elastic-plastic material will reach the limit of its elastic behavior at the point beneath the surface where the maximum contact pressure p0 at the instant of maximum compression has reached the von Mises flow criterion. The von Mises yield criterion for ductile materials can be written [53]: σ 1 (σ 1 − σ 2 )2 + (σ 2 − σ 3 )2 + (σ 3 − σ 1 )2 = k 2 = y 6 3 [ ] 2 (11), where σ y is the yield stress of the impacted (usually softer) material and σ i are the principal stress components (i.e. the stress components along the principal axes) [52]. For the axisymmetrical problem of a sphere impacting a flat plane, the principal axes are 10 with the cylindrical coordinate axes, and thus the principal stresses are σ z , σ r and σ θ with σ r = σ θ . Given the relation between the maximum contact pressure, p0, and the principal stress components [53], and assuming an elastic Poisson’s ratio, ν = 0.3 , the maximum value of stress in a thick plate, 0.62 p0 , and occurs at a depth (z-direction) below the surface of 0.48a . Thus by the von Mises yield criterion the value of p0 for the onset of plastic yield is given by p0 = 2.8k = 1.6σ y (12). Now by equating equation (6) and (10), we can obtain an expression for the maximum contact stress of an elastic impact: 4 1 ⎛ ⎞5 5 3 ⎜ 4E * ⎟ ⎛ 5 2⎞ p0 = m υ ⎜ ⎟ 0 in 3 2π ⎜⎜ 4 ⎟⎟ ⎝ 4 ⎠ ⎝ 3R ⎠ (13). By equating (13) to the von Mises critical contact pressure, equation (12), it is possible to obtain an expression relating the kinetic energy of the projectile to target materials mechanical properties [53]: 53R 3σ 5y 1 minυ 02 ≈ 2 E *4 (14). In the case of a rigid sphere impacting the planar surface of a large softer body, equation (14) reduces to υ0 = 26σ 5y ρE * 4 (15), where ρ is the density of the softer (target) material [53]. Analytical treatments of the stress indentation field for elastic-plastic contact are made complex by the plasticity zone underneath the impact. The analysis of the elastic-plastic stress field of a spherical impact with the surface of a half-space therefore requires the use of finite element analysis [54-56]. The actual size and shape of the plasticity zone depend on the mechanical properties of the target material, particularly the ratio of its Young’s modulus to yield strength, E/σy [57]. A section view of the subsurface damage for the Macor® glass-cermamic material is shown in Figure 3 together with the 11 corresponding finite-element solution. The residual impression in the surface made by the indenter is clearly visible as is the shear-driven accumulated subsurface damage resulting from the indentation. Figure 3. Bonded-interface test result showing section view with subsurface accumulated damage beneath the indentation (Left). Finite-element result showing extent of the plastic zone in terms of contours of maximum shear stress at τ Max / Y = 0.5 for indenter load P = 1000 N (Right). Distances are expressed in terms of the contact radius, a0 = 0.326mm , for the elastic case of P = 1000 N . The bold black line indicates the radius of the circle of contact, a0 = 0.437mm , as determined from the finite-element calculation [57]. 2.2 Plate Impact Mechanics In the 1960’s and early 1970’s, H. Hopkins and H. Kolsky [59], W. Goldsmith [60-63], M. Cook [64], A. Olshaker and R. Bjork [65], J. Rinehart and J. Pearson [66], L. Fugelso and F. Bloedow [67] and R. Sedgwick [68] conducted experimental studies to explore the impact processes and penetration mechanisms in plates. A compendium on the study of the mechanics of projectile penetration was published in 1978 by M. Backman and W. 12 Goldsmith [69]. A more recent review by G. Corbett et al. in 1996 [70] has incorporated copious amounts of experimental data and analytical interpretations that enable important penetration mechanisms to be identified. The analysis of failure mechanisms in finite thickness plates can be found in the aforementioned studies of M. Backman and W. Goldsmith and G. Corbett et al. [69,70]. Permanent deformations, possibly a convolution of two or more mechanisms, occur for both the non-penetrated and the penetrated cases. In the non-penetrated case, there are two failure modes that can be attributed to the transverse displacement of a thin1 target due to plastic deformation, Figure 4 (a) and (b). Figure 4. Illustration of a thin target showing a) bulging b) dishing and c) cratering [69]. 1 A plate is defined as ‘thin’ if stress and deformation gradients throughout its thickness do not exist [69] 13 The first mode is known as bulging in which the plate deforms to conform to the nose of the projectile. Bulging may be considered by the static and quasi-static methods of analysis used in metal processing problems [80]. The second failure mode is induced by bending, called dishing, and can extend far from the contact zone. Dishing, unlike bulging, requires a dynamical explanation of plastic bending, plastic hinge propagation and shear banding and/or other fracture modes [70,81-82]. As the target thickness and impact velocity increases, these two modes decrease and the deformation involves displacement that tends to involve the proximal and distal side of the target so as to thicken it with little or no deflection. This process is called cratering, Figure 4 (c), common in thick plates, and appropriately describes the effects of highly local deformations in targets of any thickness. As the velocity of the projectile increases, the ductile limit of target is approached, and penetration can begin to occur. In the penetrated regime, failure involving fracture occurs in plates of thin or intermediate 2 thickness. The fracture occurs from a combination of mechanisms with one often dominating the others depending on projectile/target material characteristics, geometry, velocity and angle of impact, etc. [69]. Figure 5 depicts the most common types of failure modes including that due to the initial compression wave, fracture in the radial direction, spalling, scabbing, plugging, front/rear petaling or fragmentation in the case of brittle targets and ductile hole enlargement [63-66, 69-70, 83-93]. 2 A plate is defined as ‘intermediate’ if the rear surface exerts considerable influence on the deformation process during all (or nearly all) of the penetrator motion [69]. 14 Figure 5. Perforation mechanisms [69]. 15 Fracture due to the initial stress wave can be caused by two different mechanisms depending on whether the tensile strength or compressive strength of the target is greater than the other. If the tensile strength of the target is greater than its compressive strength then failure occurs on the distal side, back side, of the plate from the dilatational wave, Figure 5 (a). Spalling, similar to the fracture on the distal side from the initial stress wave in Figure 5 (a), is a tensile material failure resulting from the reflection of the initial compressive transient off the distal side of the target, Figure 5 (c). Reflection of the wave changes the sign of the pulse thereby placing the target in tension from compression. The dilatational wave, produced by the impact, creates a fracture when the maximum shear stress of the reflected wave begins to exceed the materials yield stress [83]. A rough approximation for the velocity limit, the limit at which the projectile penetrates the distal side of the target, of fracture from compressive failure of the distal side due to impact is given by [69]: 1 υ Lim 2 2 ⎡ ⎤ ⎛ 1 − ν ⎞ ⎢ ⎛⎜ 2h0 ⎞⎟ ⎥ ⎛⎜ ρ t cd + ρ p c pr + = σY ⎜ 1 ⎟ ⎝ 1 − 2ν ⎠ ⎢ ⎜⎝ d p ⎟⎠ ⎥ ⎜⎝ ρ t cd ρ p c pr ⎣ ⎦ ⎞ ⎟ ⎟ ⎠ (16). where cd is the dilatational wave velocity of the target, cpr is the extensional wave velocity in the projectile, ρt is the target density, ρp is the projectile density, dp is the diameter of the projectile, h0 is the target thickness, σy is the yield stress of the target and ν is the Poisson’s ratio of the target. If the tensile strength of the target is lower than its compressive strength, then a radial fracture behind the initial stress wave will result, Figure 5 (b), based on the assumption that radial stress has exceeded the yield value in tension. A rough approximation for the velocity limit of this type of fracture is given by [69]: υ Lim = ⎛ ⎛ 2h 2σ y (1 − ν )⎜1 + ⎜ 0 ⎜ ⎜ dp ⎝ ⎝ ⎞ ⎟ ⎟ ⎠ 2 ⎞ ⎟ ⎟ ⎠ ⎛ ρ t c d + ρ p c pr ⎜ 1 ⎜ ρc ρ c ⎧ ⎫ 2 2 ⎝ t d p pr ⎡ ⎤ ⎛ 2h0 ⎞ ⎪ ⎪ ⎟ ⎥ ⎬ ⎨(1 − ν ) + 2ν ⎢1 + ⎜⎜ ⎟ ⎥ d ⎢ p ⎪ ⎠ ⎦ ⎪ ⎣ ⎝ ⎩ ⎭ ⎞ ⎟ ⎟ ⎠ (17). 16 In the ductile separation, voids nucleate through particle-matrix debonding or through particle cracking, then they grow by local plastic deformation, and finally coalesce by the onset of local instabilities or inhomogeneities [84,85]. A rough approximation for the velocity limit of this type of fracture is given by [69] υ Lim = ⎛ ⎛ 2h σ y ⎜1 + ⎜⎜ 0 ⎜ d ⎝ ⎝ p ⎞ ⎟ ⎟ ⎠ 1 ⎧ 2 2 ⎡ ⎤ ⎛ 2h0 ⎞ ⎪ ⎟ ⎥ ⎨ ⎢1 + ⎜⎜ ⎟ d ⎢ ⎪ ⎣ ⎝ p ⎠ ⎥⎦ ⎩ 2 ⎞ ⎟ ⎟ ⎠ ⎛ ρ t c d + ρ p c pr ⎜ ⎫ ⎜⎝ ρ t c d ρ p c pr ⎪ − 1⎬ ⎪ ⎭ ⎞ ⎟ ⎟ ⎠ (18). Plugging results as a cylindrical slug, nearly the size of the projectile is sheared from the target, Figure 5 (d). The failure occurs due to large shears around the moving slug. Generated heat is restricted to an annulus surrounding the slug and causes a reduction in material strength, resulting in instability; this is called an adiabatic shearing process [69]. This catastrophic shear results from interplay between thermal softening and the low work, and strain hardening rate of the plate material within the shear bands [86,87]. Plugging is most common for blunt projectiles impacting thin or intermediate, hard plates due to material being geometrically constrained to move ahead of the projectile. Analytical models describing the failure mechanism have been difficult to develop and tend to be complex, reaching five stages to adequately model the event [88]. Again, observed empirical relations have given a rough approximation for the velocity limit of this type of fracture [69] given by: υ Lim ⎡σ y =⎢ ⎢⎣ ρ t 1 1 ⎛ 2ρ h ⎞ ⎤2 ⎛ 2h0 ⎞⎤ 2 ⎡ ⎜⎜⎝ ρ Pt l 0 ⎟⎟⎠ ⎜ ⎟ ⎢e − 1⎥ ⎜ d ⎟⎥ ⎢ ⎥ ⎝ p ⎠⎥⎦ ⎣ ⎦ (19). where l is the length of the projectile. Petaling, both frontal and rear, is produced by high radial and circumferential tensile stresses after passage of the initial wave near the lip of the penetration [69,89], Figure 5 (e) and (f). This deformation is the result of bending moments created by the forward motion of the plate material being pushed ahead of the projectile and by inhomogeneities or weaknesses in the target. Petaling is usually accompanied by large plastic flows 17 and/or permanent flexure. As the material on the distal side of the plate is further deformed, the tensile stresses are exceeded and a star-shaped crack is initiated by the tip of the projectile [70]. Finally, the sectors are rotated back by the ensuing motion of the projectile, forming, often symmetric, petals. Petaling commonly occurs from ogival or conical shaped noses on projectiles penetrating thin ductile plates (h0 / dp < 1). B. Landkof and W. Goldsmith [91] expanding upon a study conducted by C. Calder and W. Goldsmith [93], carried out an experimental and theoretical investigation of petaling. In the study, they used an energy balance through multiple stages of impact to establish an expression for the final velocity of the projectile given by υ Lim ⎡ 2+k πσ y lcr h02 (θ1 − θ 2 ) 2 E d 2 − − υ ⎢ 2 0 m mp ( ) + 2 1 k p =⎢ 2 2 ⎢ πl h ρ cos θ 2 1 + cr 0 ⎢ 6m p ⎣⎢ 1 ⎤2 ⎥ ⎥ ⎥ ⎥ ⎦⎥ (20), where Ed is the energy absorbed through plate dishing [70], k is a mass ratio parameter, θ1 and θ2 are the petal rotation angles at the ends of the stages and lcr is the crack length. Fragmentation of the projectile and target occur in situations similar to radial fracture where the stress wave of the impact creates tensile and compressive stresses which exceed those of the projectile and target, Figure 5 (b). A study conducted by M. Kipp et al. [92] explores the effect of high-velocity impact fragmentation, both numerically and experimentally. Ductile hole enlargement seems to be a common failure of thick 3 plates of medium to low hardness common from ogival or small-angle conical shaped projectiles [69], Figure 5 (h). At the beginning of contact, the tip of the projectile begins displacing material radially and continues so that a hole in the target is enlarged along the trajectory of the projectile. Heavily dependent on projectile shape and projectile diameter to target thickness ratio, ductile hole enlargement is favorable instead of plugging if the following condition is satisfied with a ogival or small-angle conical shaped projectile [87] 3 A plate is defined as ‘thick’ if there is an influence of the distal boundary on the penetration process only after substantial travel into the target element [69]. 18 h0 > 3 dp 2 (21). A quasi-static analysis of the completely symmetrical enlargement of the hole that develops at the moving point of the sharp projectile was given in a classical paper for a thin infinite elastic-perfectly plastic sheet [69, 94]. This description was improved by G. Taylor [95] providing a more precise stress analysis in the region of significant target thickening. The work required to expand such a hole to a given radius R1 is W = 1.33πR12 h0σ y (22). A complex analytical solution to the radial stresses at the hole and the total resistance to penetration were formulated by W. Herrmann and A. Jones [96] and H. Bethe [94]. A rough approximation for the velocity limit can be found by equation (23). Several models describing impact upon plates with a finite thickness have been proposed [71-76] but the complexity of the impact event has limited general closed-form analytical solutions [77]. To supplement the lack of analytical solutions, empirical relations, neglecting plate bending, stretching or dynamic effects beyond the impact zone, have been proposed but are of limited utility. These relations are only applicable in a narrow set of velocity ranges for a particular type of projectile geometry. For example, the Standard Research Institute Formula (SRI) [70] proposes that for a cylindrical geometry the critical projectile impact energy, Ec, to penetrate a sample is given by: Ec = σ u d p3 13 (42.7h 2 0 + l p h0 ) (23), where σu is the ultimate stress, dp is the diameter of the projectile and h0 is the thickness of the target. This empirical expression is valid only for 0.1 < h0/dp < 0.6; 0.002 < h0/lp < 0.005; 10 < lp /dp < 50; 5 < lp /dp < 8; lp /h0 < 100 and 21 < v0 < 122 m/s. Other empirical formulas only make accurate predictions significantly greater than the target’s ballistic limit. For example the study conducted by W. Thomson [78,79] found υ r2 = υ 02 − 16πd p2 h0 ⎛ σ y ρυ 02 ⎜ + m p ⎜⎝ 2 3 where and υr is the residual velocity of the projectile. ⎞ ⎟⎟ ⎠ (24), 19 Chapter 3 3.1 Materials and Structures Sandwich Panel Fabrication A perforated sheet folding process [29] was used to create pyramidal truss sandwich panel structures with a core relative density ( ρ ) between 5 and 6%. A diamond perforation pattern was die stamped into a 1.9 mm thick (14 gauge) 304 stainless steel sheet, Figure 6. A similar thickness, 6061-T6 aluminum alloy was annealed to the Ocondition also die stamped in a similar manner to the 304 stainless steel. The Ocondition annealing was achieved by placing the assembly in a furnace at 500 °C for 30 minutes and allowed to furnace cool. Afterwards, the sheets were perforated to create a 2-D array of diamond perforations that were each 5.46 cm in length and 3.15 cm wide. Adjacent perforations were separated by 4.0 mm of metal. The patterned sheets were then bent as schematically illustrated in Figure 6, to create a single layer pyramidal truss lattice with trusses that were 31.75 mm in length and 1.9 x 4.0 mm2 in cross section. After bending, the annealed O-condition AA6061 trusses were artificially aged at 165 °C for 19 hours and then water quenched from the solutionizing temperature to return them to their peak strength condition (T6). 20 Figure 6. Manufacturing process for making pyramidal lattice truss cored sandwich panels [3]. The lattice truss panels were trimmed to form 3x3 pyramidal cell arrays. The 304 stainless steel structures were placed between a pair of 1.5 mm thick (16 gauge) 304 stainless steel (12.07 cm x 12.70 cm) facesheets and laser welded at the nodes, Figure 7. The AA6061 lattices were sandwich between 1.5 mm thick (14 gauge) AA6061 face sheets with similar dimensions 12.07 cm x 12.70 cm and laser welded, Figure 7. The 7axis CO2 laser was manufactured by LaserDyne (Champlin, MN), and used 600-1300 W to control the depth and size of the welds which were conducted on both alloys. 21 Figure 7. Illustration of the laser welding process for bonding the truss lattice to proximal and distal facesheet. Figure 8 shows a cross section of the single layer empty pyramidal truss lattice along a nodal line. Figure 8. Cross section of the single layer empty pyramidal truss lattice along a nodal line. 22 3.2 Relative Density Relations The relative density, ρ , is non-dimensional ratio defined as the volume fraction of truss members occupying a prescribed unit cell. Ignoring the detailed geometry located at the nodes, the relative density of the pyramidal lattice truss core can be calculated from a unit cell analysis of the single layer pyramidal unit cell, Figure 9. Figure 9. Unit cell geometry used to derive the relative density for single layer pyramidal topology. ° where ω = 54.7 is the included angle (the angle between the truss members and the base of the pyramid), w is the truss width, t is the truss thickness and l is the truss length. Based upon these considerations, the volume, Vtr , of the truss members occupying the single layer pyramidal unit cell shown in Figure 9 is: Vtr = 4lwt (25). The volume, Vc , of the single layer pyramidal unit cell is: Vc = ( 2l cos ω )( ) 2l cos ω (l sin ω ) = 2l 3 cos 2 ω sin ω (26), 23 Taking the ratio between the volume of the trusses, equation (25), and volume of the unit cell, equation (26), we obtain the single layer pyramidal relative density ( ρ ) expression: ρ= Vtr 2 wt = 2 Vc l cos 2 ω sin ω (27). 14 gauge thick 304 stainless steel and 12 gauge thick age hardened AA6061-T6 aluminum alloy panels are used here, with t = 1.9 mm, w = 4.0 mm, l = 31.75 mm and ω = 54.7° . Substituting these values into equation (27) yields a ρ = 5.5 ± 0.3% . The 304 stainless steel sandwich panel had an areal density of approximately 28 kg/m2 while that of the age hardened 6061-T6 aluminum alloy was approximately 10 kg/m2. 3.3 Alloy Mechanical Properties 3.3.1 304 Stainless Steel Uniaxial tension specimens were machined from 304 stainless steel with a 0.61 mm plate thickness, according to ASTM E-8 guidelines [97]. A servo-electric universal testing machine (Model 4208, Instron Corp., Canton, MA) with self-aligning grips was used to test each specimen at ambient temperature, approximately 25 °C. The applied nominal strain rate for the stainless steel was 0.3 mm/min (10-3 s-1), and the strain measurements were made using a linear variable differential transformer (LVDT) clip-on extensometer with an accuracy of ±0.5% of the gage length of 50 mm. The stress as a function of strain for the as received alloy is plotted in Figure 10. The elastic modulus measured approximately 200 GPa, the yield strength measured approximately 255 MPa, the ultimate yield strength measured approximately 1000 MPa and the strain to fracture measured approximately 0.39. The test results approximately agree with referenced values [98]. 24 Figure 10. Uniaxial tension data for as-received 304 stainless steel. 3.3.2 Age Hardened 6061-T6 Aluminum Alloy Uniaxial tension specimens were machined age hardened 6061-T6 aluminum alloy with a 6.35 mm plate thickness, according to ASTM E-8 guidelines [97]. The equivalent servoelectric universal testing machine as described in Chapter 3.4.1 was used for testing the mechanical properties of the alloy. The applied nominal strain rate for age hardened 6061-T6 aluminum alloy was 0.2 mm/min (10-3 s-1). The stress as a function strain response is plotted in Figure 11. The elastic modulus measured approximately 68 GPa, the yield strength measured approximately 268 MPa respectively, the ultimate yield strength measured approximately 310 MPa and the strain to fracture measured approximately 0.15. The test results approximately agree with referenced values [98]. 25 Figure 11. Uniaxial tension data for the age hardened 6061-T6 aluminum alloy. 3.4 Polymer Infiltrated Sandwich Panels In an attempt to add ballistic resistance to the sandwich panels, a low Tg polyurethane, designated PU 1, was infiltrated into the structure to create a hybrid lattice. This polyurethane was chosen due to its wide availability and customizable mechanical properties allowing a polymer with a high elongation to yield to be chosen easily. 3.4.1 Hybrid Lattice Fabrication Twenty five 304 stainless steel mono-layer pyramidal lattice truss structures, with equivalent dimensions as described in Chapter 3.1, were fabricated and assembled. The samples were taped on three sides. PU 1 was poured into the sandwich structure and the samples were allowed to cure for twenty four hours at ambient temperature, approximately 25 °C. 26 The relative density of the system can be calculated using a similar unit cell analysis, described in Chapter 3.2. Equation (28) shows the relative density for the 304 stainless steel pyramidal truss lattice with infiltrated PU 1, incorporating the different densities of the metal and the PU 1, ρ pu (2l 3 cos 2 ω sin ω − 4lwt ) + ρ tr (4lwt ) ρ= ρ m (2l 3 cos 2 ω sin ω ) (28), where ρ pu is the density of the polyurethane, ρ tr is the density of the trusses and ρ m is the density of the base metal system. With polyurethane density of ρ p = 1.3 g/cc, a truss density of ρ tr = 7.97 g/cc and a base metal density of ρ m = 7.97 . Compared to an all steel plate, the relative density of the system is approximately ρ = 27%. The areal density of the 304 stainless steel pyramidal truss lattice infiltrated with PU 1 is 55 kg/m2. 3.4.2 Polymer The PU 1 polymer chosen for the study was a type of polyurethane, designated PMC-780 Dry [100], formulated by Smooth-On (Easton, PA). PU 1 is a two component, pliable, castable elastomer with an approximate twenty-four hour cure time at room temperature. Part A is composed mostly of polyurethane prepolymer and a trace amount of toluene diisocyanate. Part B is composed of polyol, a proprietary chemical (NJ Trade Secret #221290880-5020P), di(methylthio)toluene diamine and phenylmercuric neodecanoate. This polyurethane has a low elastic modulus and tensile strength but a very high elongation to failure. The term elastomer is loosely applied to polymers that at room temperature can be stretched repeatedly to at least twice their original length and, immediately upon release of the stress, return with force to their approximate original length [101]. Table 1 lists the manufacturer’s specifications for the polyurethane. 27 Property PU 1 Manufacturer Product Name Tensile Modulus (MPa) Tensile Strength (MPa) Elongation to Break (%) Shore Hardness Smooth-On (Easton, PA) PMC-780 Dry 2.76 6.21 700 80 A Table 1. Manufacturer reported properties for the polyurethane system. The hardness testing of plastics is most commonly measured by the Shore (Durometer) test or Rockwell hardness test. Both methods measure the resistance of the plastic toward indentation by a spring-loader. Both scales provide an empirical hardness value that doesn't correlate to other physical properties or fundamental characteristics such as strength or resistance to abrasion. Shore hardness, either the Shore A or Shore D scale, is the preferred method for rubbers/elastomers and is also commonly used for 'softer' plastics such as polyolefins, fluoropolymers, and vinyls. The Shore A scale is used for 'softer' rubbers while the Shore D scale is used for 'harder' ones. The Shore A hardness is the relative hardness of elastic materials such as elastomers or soft plastics can be determined with an instrument called a Shore A Durometer. If the indenter completely penetrates the sample, a reading of 0 is obtained, and if no penetration occurs, a reading of 100 results. Shore hardness is a dimensionless quantity. A full description of the test method can be found in ASTM D2240, or the analogous ISO test method is ISO 868. 28 3.5 Polymer Characterization A characterization of the dynamical properties of the polymer is necessary due to their effect on the ballistic response. Three properties were characterized, the glass transition temperature, the storage modulus and the loss modulus. The glass transition temperature indicates the amount of crosslinking in the polymer and affects the elongation to yield. This property can be ascertained by measuring the heat capacity as a function of temperature with a differential scanning calorimeter (DSC). The storage modulus and loss modulus are related to a parameter, Tanδ , that indicates a materials ability to absorb and dissipate energy. These rheological properties can be ascertained by the use of a dynamic mechanical analyzer (DMA). 3.5.1 DSC Analysis A DSC analysis of PU 1 was conducted by M. Aronson et al. of the University of Virginia. The glass transition temperature, Tg, of the polyurethane was determined with modulated differential scanning calorimetry (MDSC®) using a Q1000 Modulated DSC (TA Instruments-Waters, LLC). The polymer was heated over a temperature range of -80 to 240 °C with a heating rate of 3 °C/min and a modulation of ± 0.5 °C/60 sec period. With traditional DSC, the heat flow curve is a superimposition of the Tg, endotherms and exotherms. Due to this superimposition, it is difficult to make an accurate determination of the Tg with traditional DSC. With modulated DSC, the reversing heat flow curve associated with the Tg is separated from the non-reversing heat flow curve associated with endotherms and/or exotherms, thus enabling an accurate determination of the Tg [103]. Figure 12 is a plot of the heat capacity, Rev Cp, of PU 1 as a function of temperature. The Cp of the polyurethane was determined by dividing its reversing heat flow value, J/(sec·g), by the heating rate, °C/sec. 29 Figure 12. Heat capacity (Rev Cp) of PU 1 as a function of temperature (°C). The Tg of each sample was taken to be the inflection point of the step-change in Cp. Based on this definition, and the information included in Figure 12, the Tg of PU 1 was -56 °C. The small step-change in Cp, around 70 °C, is believed to be an experimental artifact and not associated with a second Tg of this sample. 3.5.2 DMA Analysis A DMA analysis of PU 1 was also conducted by M. Aronson et al. of the University of Virginia. The rheological properties of PU 1 were characterized with dynamic mechanical analysis (DMA) using a Q800 DMA (TA Instruments-Waters, LLC). Measurements were made on each sample at three different frequencies, 1, 10 and 100 Hz, over a temperature range of -100 to 40 °C in 5 °C increments. The data over the entire temperature range were transformed using time-temperature superposition (TTS) with a reference temperature of 25 °C [106,107]. The result of this data manipulation is a 491H master curve of predicted storage modulus, E ′ , and loss modulus, E ′′ , values over a frequency range of 10-1 to 1010 Hz for each sample at the reference temperature. 30 Figure 13 is a plot of the storage modulus of PU 1 at a frequency of 1 Hz over a temperature range of -100 to 40 °C. As the temperature is increased from -70 to 0 °C, the storage modulus of PU 1 decreases by three orders of magnitude. This difference is due to the fact that the Tg of PU 1 is -56 °C, Figure 12. Figure 13. Storage modulus at a frequency of 1 Hz for PU 1 as a function of temperature. The predicted storage and loss modulus values for PU 1 over a frequency range of 1 to 106 Hz at a reference temperature of 25 °C was computed, Figure 14. As previously discussed, these predicted values were obtained by transforming the measured E’ and E” values obtained over the temperature range of -100 to 40 °C at the three different frequencies using TTS (data obtained at low temperatures corresponds to the high frequency data in Figure 14, while data obtained at high temperatures corresponds to the low frequency data). 31 Figure 14. Predicted values for the storage and loss modulus of PU 1 at a reference temperature of 25 °C as a function of frequency. The ratio of E ′ to E ′′ , which is referred to as Tan δ, is a parameter that is often used to assess the ability of a material to absorb and dissipate energy. For materials with comparable storage moduli, the greater the Tan δ value, the more efficient the material is able to absorb and dissipate energy. Figure 15 is a plot of Tan δ of PU 1 over the same frequency range covered in Figure 14. 32 Figure 15. Tan δ ( E ′′ / E ′ ) of PU 1 as a function of frequency. 33 Chapter 4 Ballistic Testing Fifteen pyramidal lattice truss structures of each alloy, with contrasting mechanical properties, were tested using impact velocities between approximately 225 m/s and 1225 m/s. Eleven 304 stainless steel monolithic plates, 3 mm thick, with an equivalent areal density to 304 stainless steel lattice truss sandwich panels, were tested as a comparison to evaluate the ballistic resistance of the lattice truss sandwich system. Both stainless steel systems had the same (as-received) mechanical properties and neither underwent heat treatment prior to testing. 4.1 Stage One Powder Gun Ballistic testing was conducted by A. Zakraysek et al. at the Indian Head Division, Naval Surface Warfare Center, MD, using a powder gun shown schematically in Figure 16. Figure 16. Illustration of the single stage powder gun used for ballistic studies. The sabot carried a 12.5 mm spherical projectile. 34 A cable connected the firing switch to an electric solenoid, Figure 16. Upon closing the circuit, the electric solenoid activated a firing pin. The firing pin then struck a 0.38 caliber blank cartridge supplied by Western Cartridge Company (East Alton, IL) which ignited a gun powder charge whose mass determined the projectile velocity. Gun powder 3031, manufactured by IMR (Shawnee Mission, KS), and cotton, placed in front of the gun powder, was contained in the middle region of the breech in Figure 16. The purpose of the cotton was to ensure the initiated shock wave remained uniform throughout propagation of the detonation. A sabot was located within the 2.54 cm bore gun barrel, Figure 16. A series of holes placed along the gun barrel were used to dissipate the shock wave and maintain a smooth acceleration of the sabot until it exited the barrel. 4.2 Sabot and Projectile The plastic sabot was composed of four quarters that, upon mating, surrounded a 12.5 mm diameter spherical projectile. The sabot plugs had an inner diameter of 1.25 cm, an outer diameter of 2.54 cm, a height of 3.50 cm and weighed 18.60±0.12 g. A 40° bevel at the sabot opening facilitated separation of the sabot from the projectile by air drag, shortly after initiation of free flight. Figure 17 shows a photograph of both the fully assembled and separated sabot. The projectiles had a diameter of 1.25 cm and weighed 8.42±0.02 g. The spherical projectiles were manufactured by National Precision Ball (Preston, WA). They were made from 1020 plain carbon steel with an ultimate tensile strength of 365 to 380 MPa [99]. 35 Figure 17. Illustration of the sabot used to carry the projectile. 4.3 Test Fixture The test sample fixture was located within a blast chamber, Figure 18. 36 Figure 18. Illustration of setup used in the blast chamber to mount the samples, measure velocities and record via high-speed photography. A square steel plate 41.28 cm long, 2.86 cm thick, was located one meter from the end of the barrel with a 3.8 cm diameter hole located in the center. A square wood plate 41.28 cm long, 2.22 cm thick, with a 6.35 cm diameter hole, was located 30.48 cm successively after the steel plate. On the back of the wood plate, covering the hole, was the first of four brake screens to measure entry and exit velocities. A brake screen is a piece of paper with a thin, silver mask that is connected into a circuit. These circuits were connected into a four channel oscilloscope. Upon penetration by the projectile, the circuit is broken. Using four brake screens, two for entry and two for exit, velocities can be calculated by knowing the distance between and the time difference between circuit closures. The oscilloscope was precise to ±1 μs therefore causing decreasing error in the velocity measurement as the projectile velocity was increased (i.e. time is inversely 37 proportional to length in velocity). The mounting steel plate, 2.86 cm thick, was located 30.86 cm after the wood plate. In the center of plate, was a 13.34 cm square aperture to house the sample. On each side of the sample, a brake screen was attached. An iron angle bracket 17.78 cm long, with 1.19 cm overlap over the top and bottom was used to clamp the sample into the fixture with bolts. Adjacent to the fixture, a Fresnel lens was used to collimate the light onto the sample to provide adequate contrast for the highspeed photography located on the opposing side. Located 30.48 cm, successively after the mounting steel plate, was another square wood plate 41.28 cm long, 2.22 cm thick, with a 12.7 cm diameter hole located in the center. On the back of this plate was the final brake screen in the series. A final square steel plate 41.28 long, 2.86 cm thick, was located 28.21 cm successively after the second wood plate. This plate was used as backstop to catch any fragments from the sample or remaining projectile remnants. 38 Chapter 5 Empty Lattice Resistance Both alloy systems, 304 stainless steel and AA6061 aluminum alloy, were fixtured as described in Chapter 4.3 and impacted using the aforementioned projectiles as described in Chapter 4.2. Exit velocity of the projectile through the target was recorded and the impact velocity was gradually increased from 200-1200 m/s. Fifteen sandwich structure samples of both alloy systems and eleven 304 stainless steel plate samples were tested. 5.1 304 Stainless Steel Panel Response Table 2 displays the data acquired for the 304 stainless steel pyramidal truss lattice sandwich structure. The mass of each 304 stainless steel sample was 432.2±1.1 g. Shot # Impact Velocity (m/s) Exit Velocity (m/s) Nodal Disbond of Distal FS Penetration of Distal FS 1 46 56 2 48 133 3 50 134 4 52 135 54 136 137 339.2±0.1 290.8±0.1 227.1±0.1 506.9±0.3 481.3±0.3 493.8±0.3 810.8±0.8 768.4±0.8 812.3±0.9 1029.9±1.4 992.4±1.3 1001.0±1.3 1206.1±1.9 1214.9±1.9 1221.9±1.9 N/A N/A N/A 310.0±0.1 266.1±0.1 276.5±0.1 551.1±0.4 491.9±0.3 653.5±0.6 721.5±0.7 744.0±0.7 653.5±0.6 868.4±1.0 882.7±1.0 851.9±0.9 No No No No No No No No No No No No No No No No No No Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Table 2. The impact and exit velocities of the projectile, nodal disbonding of the distal facesheet and whether the projectile penetrated the distal facesheet for the 304 stainless steel pyramidal truss lattice sandwich structure. Figure 19 depicts the exit velocity of the projectile (m/s) as a function of the impact velocity (m/s) for the 304 stainless steel pyramidal truss lattice sandwich structure. The error bars for the impact and exit velocities are not illustrated on the graph because they are smaller than the size of the plotted data points. 39 Figure 19. Plot of exit velocity of the projectile (m/s) as a function of the impact velocity (m/s) for the 304 stainless steel pyramidal truss lattice. The results for the system can be fitted to a linear equation after the critical velocity region (i.e. the velocity at which penetration begins to occurs), R2 = 0.98, y = −100.8 + 0.81x (29). Figure 20 depicts the energy absorbed (J) as a function of the impact velocity (m/s) for the 304 stainless steel pyramidal truss lattice system. As described previously, the error bars for the impact and exit velocities are not illustrated on the graph because they are smaller than the size of the plotted data points. 40 Figure 20. Plot of energy absorbed (J) as a function of the impact velocity (m/s) for the 304 stainless steel pyramidal truss lattice system. The left parabaloid in Figure 20 represents the target preventing penetration of the projectile. After the critical velocity, the energy absorbed begins to decrease until it reaches a minimum, and then begins to increase monotonically with the initial velocity. The first 304 stainless steel pyramidal truss lattice sandwich structure sample to be penetrated occurred with an impact velocity of 481.3 m/s. The projectile exited the lattice structure at 266.1 m/s, approximately 55% of the impact velocity. The critical velocity is approximately 400±25 m/s. Figure 21 shows a cross sectional view of a 304 stainless steel sample that was impacted by a spherical projectile at 339.2 m/s. 41 Figure 21. a) Cross section of the 304 stainless steel sample that was impacted at 339.2 m/s and was not fully penetrated, shot 1 b) Cross section of the entry hole of shot 1 c) Cross section of the exit hole of shot 1. Bulging and dishing are apparent on the distal facesheet and a crack began to initiate petaling as the energy from the impact was fully absorbed. Physical examination after the test indicated a center-cell impact (i.e. equidistant from four nodes), Figure 21. The projectile impacted a truss/distal facesheet node causing a truss to separate and plastically deform. Penetration of the proximal facesheet resulted in an entry hole of 12.5 mm wide and deflected 4.5 mm. Dishing was approximately 3 cm in diameter. Full penetration of the distal facesheet did not occur and fully arrested the projectile resulting in a deflection of 12.5 mm. A star-shaped crack began to initiate forming sectors, but no petaling occurred. There was no nodal disbonding of the trusses and facesheets except for the impact location. 42 Figure 22. a) Cross section of the 304 stainless steel sample that was impacted at 810.8 m/s, shot 3 b) Cross section of the entry hole of shot 3 c) Cross section of the exit hole of shot 3. A small amount of ductile hole enlargement occurred on the proximal facesheet and bending/dishing exceeded the ductile limit of the 304 stainless steel to form petaling. Figure 22 shows a center-cell impact on shot 3 of 810.8 m/s and brake screens recorded an exit velocity 551.1 m/s, approximately 68% of the impact velocity. The projectile impacted a truss/distal facesheet node causing trusses to separate and plastically deform. Penetration of the proximal facesheet resulted in an entry hole of 12.5 mm wide and deflected 1.5 mm displaying ductile hole enlargement in the immediate impact location. Penetration of the distal facesheet resulted in an exit hole of 22.0 mm wide and deflected 11.0 mm exhibiting three separate petals. There was no nodal disbonding of the trusses and facesheets except for the impact location. 43 Figure 23. a) Cross section of the 304 stainless steel sample that was impacted at 1206.1 m/s, shot 54 b) Cross section of the entry hole of shot 54 c) Cross section of the exit hole of shot 54. A small amount of ductile hole enlargement occurred on the proximal facesheet and bending/dishing exceeded the ductile limit of the 304 stainless steel to form petaling. Figure 23 shows a center-cell impact on shot 54 of 1206.1 m/s and an exit velocity of 868.4 m/s, approximately 72% of the impact velocity. The projectile impacted a truss/distal facesheet node causing trusses to separate and plastically deform. Penetration of the proximal facesheet resulted in an entry hole of 12.5 mm wide and deflected 0 mm. Similar to shot 3, ductile hole enlargement was evident surrounding the impact location. Penetration of the distal facesheet resulted in an exit hole of 26.0 mm wide and deflected 44 12.5 mm exhibiting four distinct petals. There was no nodal disbonding of the trusses and facesheets except for the impact location. 5.2 304 Stainless Steel Plate Response Table 3 displays the data acquired for the 3 mm thick 304 stainless steel monolithic plate. The mass of each plate was 367.2±13.8 g, an approximate areal density of 28 kg/m2. Shot # Impact Velocity (m/s) Exit Velocity (m/s) 104 57 58 59 105 60 106 61 107 62 108 177.4±0.0 377.0±0.2 341.7±0.2 477.3±0.3 509.6±0.3 805.0±0.8 806.2±0.8 989.4±1.3 985.7±1.3 1191.8±1.8 1226.5±1.9 N/A N/A N/A 323.1±0.1 302.4±0.1 617.8±0.5 574.9±0.4 794.0±0.8 725.7±0.7 1000.0±1.3 874.8±1.0 Table 3. The impact and exit velocities of the projectile for a 3 mm thick 304 stainless steel monolithic plate. Figure 24 depicts the exit velocity of the projectile (m/s) as a function of the impact velocity (m/s) for the 304 stainless steel monolithic plate compared to the 304 stainless steel pyramidal truss lattice. As described in Chapter 5.1, the error bars for the impact and exit velocities are not illustrated on the graph because they are smaller than the size of the plotted data points. 45 Figure 24. Plot of exit velocity of the projectile (m/s) as a function of the impact velocity (m/s) for the 304 stainless steel monolithic plate compared to the 304 stainless steel pyramidal truss lattice. The results for the systems can be fitted to a linear equation after the critical velocity region. Equation (29) gives the relation for the pyramidal truss lattice sandwich structure and the 304 stainless steel solid plate is given by, R2 = 0.98, y = −109.1 + 0.87 x (30). Figure 25 depicts the energy absorbed (J) as a function of the impact velocity (m/s) for the 304 stainless steel pyramidal truss lattice system and solid plate. As described in Chapter 5.1, the error bars for the impact and exit velocities are not illustrated on the graph because they are smaller than the size of the plotted data points. 46 Figure 25. Plot of energy absorbed (J) as a function of the impact velocity (m/s) for the 304 stainless steel pyramidal truss lattice system and solid plate. Similar to the sandwich panel, after the critical velocity of the solid plate, the energy absorbed begins to decrease until it reaches a minimum, and then begins to increase monotonically with the initial velocity. The first 304 stainless steel monolithic plate sample to be penetrated occurred at an impact velocity of 477.3 m/s. The projectile exited the plate at 323.1 m/s, approximately 68% of the impact velocity. Figure 26 shows a cross sectional view of the monolithic 304 stainless steel plate that was impacted by a spherical projectile at 341.7 m/s. There was no penetration of the projectile and plate was only deflected 9.5 mm. The bulging zone had a diameter of 12.5 mm and the dishing zone extended 4.5 cm in diameter. 47 Figure 26. Cross section of the monolithic 304 stainless steel plate that was shot at 341.7 m/s, shot 58. Significant bulging and dishing occurred without penetration. Figure 27 shows a cross sectional view of the monolithic 304 stainless steel plate that was impacted by the spherical projectile at 509.6 m/s. The exit velocity of the projectile was 302.4 m/s, approximately 59% of the impact velocity. The projectile penetrated the steel plate with a hole 12.5 mm in diameter and a deflection of 6.5 mm. Adiabatic shearing is apparent from the cross-sectional view and the dishing zone extended approximately 3.5 cm. Figure 27. Cross section of the monolithic 304 stainless steel plate that was shot at 509.6 m/s, shot 105. Significant bulging and dishing occurred reaching the ductile limit and penetrated the plate. Figure 28 shows a cross sectional view of the monolithic 304 stainless steel plate that was impacted by the spherical projectile at 1226.5 m/s. The exit velocity of the projectile was 874.8 m/s, approximately 71% of the impact velocity. The projectile penetrated the steel plate with a hole 15.9 mm in diameter and a deflection of 0 mm. The sample exhibited a high degree of ductile hole enlargement and displayed little or zero dishing. 48 Figure 28. Cross section of the monolithic 304 stainless steel plate that was shot at 1226.5 m/s, shot 108. No bulging or dishing occurred but significant ductile hole enlargement occurred. As can be seen from Figure 21-Figure 23 and Figure 26-Figure 28, the penetration mechanisms of the sandwich panel are different from those of the monolithic plate with a few similarities. Large amounts of deformation, bulging and dishing, occurred at the slower speeds in both the plate and the proximal and distal sides of the sandwich structure. In the sandwich structure, the trusses stretched and assisted in restraining the bending of the facesheets. But as the impact speeds increased, bulging and dishing began to diminish. The plate transitioned to larger degrees of ductile hole enlargement whereas the sandwich structure displayed this phenomenon transition only on the proximal face sheet. The distal side exhibited large degrees of petaling deformation, with the petals still attached to truss members, whereas the plate never exhibited signs of petaling. 49 5.3 AA6061 Panel Response Table 4 displays the data acquired for the AA6061-T6 pyramidal truss lattice sandwich structure. The mass of each AA6061-T6 sample was 155.0±0.3 g. Shot # Impact Velocity (m/s) Exit Velocity (m/s) Nodal Disbond of Distal FS Penetration of Distal FS 47 80 114 49 81 115 51 82 116 53 83 117 55 84 118 232.1±0.1 370.4±0.2 280.1±0.1 506.5±0.3 493.3±0.3 545.9±0.4 756.5±0.7 739.0±0.7 795.5±0.8 997.8±1.3 1006.2±1.3 1020.7±1.3 1222.2±1.9 1222.0±1.9 1209.5±1.9 144.7±0.0 270.8±0.1 196.4±0.0 411.1±0.2 395.4±0.2 433.0±0.2 670.7±0.6 639.1±0.5 685.3±0.6 922.2±1.1 889.0±1.0 898.1±1.0 1125.5±1.6 1102.4±1.6 1045.5±1.4 No Yes Yes Yes Yes No Yes Yes Yes Yes No Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Table 4. The impact and exit velocities of the projectile, nodal disbonding of the distal facesheet and whether the projectile penetrated the distal facesheet for the age hardened AA6061-T6 aluminum alloy pyramidal truss lattice sandwich structure. Figure 29 depicts the exit velocity of the projectile (m/s) as a function of the impact velocity (m/s) for the AA6061 pyramidal truss lattice compared to the 304 stainless steel pyramidal truss lattice sandwich structure. As described in Chapter 5.1, the error bars for the impact and exit velocities are not illustrated on the graph because they are smaller than the size of the plotted data points. 50 Figure 29. Plot of exit velocity of the projectile (m/s) as a function of the impact velocity (m/s) for the age hardened AA6061 aluminum alloy pyramidal truss lattice compared to the 304 stainless steel pyramidal truss lattice system. The results for the systems can be fitted to a linear equation after the critical velocity region. Equation (29) gives the relation for the pyramidal truss lattice sandwich structure and the AA6061-T6 truss lattice sandwich structure is given by, R2 = 0.99, y = −79.7 + 0.97 x (31). Figure 30 depicts the energy absorbed (J) as a function of the impact velocity (m/s) for the 304 stainless steel and AA6061 aluminum alloy sandwich panel. As described in Chapter 5.1, the error bars for the impact and exit velocities are not illustrated on the graph because they are smaller than the size of the plotted data points. 51 Figure 30. Plot of the energy absorbed (J) as a function of the impact velocity (m/s) for the 304 stainless steel sandwich panel and AA6061 aluminum alloy sandwich panel. Unlike the stainless steel, the critical velocity for the aluminum alloy could not be ascertained. The energy absorbed by the age hardened AA6061 aluminum alloy increased marginally as the entry velocity was increased. Penetration of the distal facesheet for the AA6061 empty pyramidal truss lattice occurred with an impact velocity of 232.1 m/s, the slowest projectile speed possible with the stage one powder gun. The exit velocity of the projectile was 144.7 m/s, approximately 62% of the impact velocity. The critical velocity of the structure is at some velocity less than 232.1 m/s but speeds below this were unattainable due to technical constraints. Figure 31 shows a cross sectional view of the AA6061 sample that was impacted by the spherical projectile at 280.1 m/s. 52 Figure 31. a) Cross section of the AA6061 sample that was impacted at 280.1 m/s, shot 114 b) Cross section of the entry hole of shot 114 c) Cross section of the exit hole of shot 114. Significant amount of bulging and dishing occurred on the proximal facesheet and petaling occurred as a result of penetration. Break screens indicated an exit velocity of 196.4 m/s, approximately 70% of the impact velocity. Post impact observation revealed a center-cell impact on the proximal facesheet, with an entry hole 12.5 mm in diameter and deflected 6.5 mm, and dishing approximately 3 mm in diameter. The projectile impacted a node-facesheet contact on the distal facesheet separating and plastically deforming two pairs of the trusses. The exit hole on the distal facesheet was 12.5 mm in diameter and deflected 8.0 mm. Additionally, the energy absorbed by the impact of the projectile fractured all of the nodal contacts on the distal facesheet and separated it from the truss structure. 53 Figure 32. a) Cross section of the AA6061 sample that was impacted at 493.3 m/s, shot 81 b) Cross section of the entry hole of shot 81 c) Cross section of the exit hole of shot 81. Significant amount of bulging and dishing occurred on the proximal facesheet and petaling occurred resulting in penetration. Figure 32 shows a slightly off center-cell impact on shot 81 of 493.3 m/s and brake screens recorded an exit velocity 395.4 m/s, approximately 80% of the impact velocity. The projectile only impacted one truss upon penetration as a result of the impact being slightly off the center of the cell. The truss did not separate upon impact but did plastically deform. Penetration of the proximal facesheet resulted in an entry hole of 12.5 mm wide and deflected 2.5 mm. Penetration of the distal facesheet resulted in an exit 54 hole of 14.5 mm wide and deflected 8.0 mm. There was nodal disbonding of two contact points on the distal facesheet adjacent to impact cell. Figure 33. a) Cross section of the AA6061 sample that was impacted at 1222.2 m/, shot 55 b) b) Cross section of the entry hole of shot 55 c) Cross section of the exit hole of shot 55. A significant amount of ductile hole enlargement occurred on the proximal facesheet with little to no bulging/dishing and petaling occurred on the distal facesheet. Figure 33 shows a center-cell impact on shot 55 of 1222.2 m/s and brake screens recorded an exit velocity 1125.5 m/s, approximately 92% of the impact velocity. The projectile impacted the trusses and plastically deformed them to adjacent cells. 55 Penetration of the proximal facesheet resulted in an entry hole of 12.5 mm wide and deflected 0 mm with a high degree of ductile hole enlargement. Penetration of the distal facesheet resulted in an exit hole of 17.5 mm wide and deflected 8.0 mm with three distinct petals. The impact energy completely fractured all nodal contacts on the distal facesheet, separating it from the truss lattice. 5.4 Discussion The 304 stainless steel lattice truss system and the 304 stainless steel plate both had approximately equivalent critical velocities of approximately 450 m/s. Both systems shared similar performance, with the lattice truss exhibiting greater success at higher speeds. Although Almohandes [39] found poorer performance of distributing a mass equally over a given distance compared to the solid plate; our increased performance can most likely be attributed to the lattice truss in the sandwich structure. As can be seen in Figure 21-Figure 23 and Figure 26-Figure 28, large amounts of deformation, bulging and dishing, occurred at the slower speeds in both the plate and the proximal and distal sides of the sandwich structure. The trusses occasionally separated and deformed thus absorbing the remainder of the kinetic energy accounting for the approximate equal ballistic performance. Additionally, the lattice truss core restrained the facesheets from bending and dishing absorbing additional energy. But as the impact speeds increased, the plate transitioned to larger degrees of ductile hole enlargement whereas the sandwich structure displayed this phenomenon transition only on the proximal face sheet because of reduced projectile velocity. The distal side did not exhibit any phenomenon transition and continued displaying larger degrees of petaling deformation, with the petals still attached to truss members. The projectile would be forced to deform the distal face sheet to the point of fracture, maximal bulging, and then push each of the sectors out thus forming the petals. This additional deformation, in addition to the plastic deformation of the trusses, most likely accounts for greater energy absorption and thus lower exit speeds than the solid plate. 56 The AA6061 aluminum alloy structures were penetrated at the slowest possible speeds attainable at the facility, approximately 200 m/s. Similar to the 304 stainless steel, the aluminum alloy exhibited a large degree of bulging and dishing on the proximal and distal facesheets at the lower velocities. Petaling was prominent on the distal facesheet in addition to the bulging and dishing. As the velocity was increased, bulging and dishing diminished, transitioning to ductile hole enlargement on the proximal facesheet. On the distal facesheet, the degree of petaling became more pronounced with larger sectors. The vast difference in critical velocity and reduction in impact velocity between the AA6061 aluminum alloy and the 304 stainless steel can most likely be attributed to the aluminum alloy having lower ductility and a significantly lower work hardening rate. Given that these two materials have similar yields strengths, it is a possibility that lowering these properties drastically reduces the amount of energy absorbed through plastic deformation. Additionally, the density of the stainless steel is approximately two and a half times that of the aluminum alloy. Given the projectile diameter and cell size ratio (i.e. approximately 0.5), this drastic difference in density reduces the amount of momentum transfer from the projectile to the structure, thereby decreasing the amount of energy transferred to the system. All of these properties enable the 304 stainless steel to absorb more energy than the AA6061 aluminum alloy lattice truss sandwich structure. Therefore, the 304 stainless steel has a superior ballistic resistance compared to the age hardened AA6061 aluminum alloy with the same dimensions and relative density. 57 Chapter 6 6.1 Polymer Infiltration Study Ballistic Response Table 5 displays the data acquired for the 304 stainless steel pyramidal truss lattice sandwich structure filled with PU 1. The mass of each hybrid, polymer and 304 stainless steel sample was 857.1±6.4 g. Shot # Impact Velocity (m/s) Exit Velocity (m/s) Nodal Disbond of Distal FS Penetration of Distal FS 6 26 70 109 128 7 27 71 110 129 8 28 72 111 130 29 63 73 112 131 10 30 74 113 132 364.8±0.2 341.4±0.2 370.9±0.2 299.0±0.1 340.2±0.1 545.3±0.4 530.4±0.4 540.7±0.4 515.7±0.3 571.5±0.4 781.2±0.8 791.0±0.8 804.7±0.8 819.0±0.9 746.5±0.7 999.7±1.3 1057.7±1.4 1006.1±1.3 984.5±1.3 986.9±1.3 1316.7±2.2 1197.6±1.8 1229.6±1.9 1220.4±1.9 1232.0±2.0 N/A N/A N/A N/A N/A 273.7±0.1 245.7±0.1 213.7±0.1 275.8±0.1 251.8±0.1 466.3±0.3 467.6±0.3 473.4±0.3 468.2±0.3 456.0±0.3 622.1±0.5 573.3±0.4 670.6±0.6 557.5±0.4 589.2±0.4 779.1±0.8 719.3±0.7 692.2±0.6 680.0±0.6 675.1±0.6 No No No No No No No No No No No No No No No No No No No No No No No No No No No No No No Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Table 5. The impact and exit velocities of the projectile, nodal disbonding of the distal facesheet and whether the projectile penetrated the distal facesheet for the 304 stainless steel pyramidal truss lattice sandwich structure with polyurethane. Figure 34 depicts the exit velocity of the projectile (m/s) as a function of the impact velocity (m/s) for the 304 stainless steel pyramidal truss lattice infiltrated with PU 1 and the empty 304 stainless pyramidal truss lattice. As described in Chapter 5.1, the error 58 bars for the impact and exit velocities are not illustrated on the graph because they are smaller than the size of the plotted data points. Figure 34. Plot of exit velocity of the projectile (m/s) as a function of the impact velocity (m/s) for the 304 hybrid stainless steel pyramidal truss and the empty 304 stainless pyramidal truss lattice. The results for the systems can be fitted to a linear equation after the critical velocity region. Equation (29) gives the relation for the pyramidal truss lattice sandwich structure and 304 stainless steel truss lattice sandwich structure infiltrated with PU 1 is given by, R2 = 0.97, y = −72.2 + 0.65 x (32). Figure 35 depicts the energy absorbed (J) as a function of the impact velocity (m/s) for the 304 stainless steel pyramidal truss lattice infiltrated with PU 1 and the empty 304 stainless pyramidal truss lattice. As described in Chapter 5.1, the error bars for the 59 impact and exit velocities are not illustrated on the graph because they are smaller than the size of the plotted data points. Figure 35. Plot of projectile the energy absorbed (J) as a function of the impact velocity (m/s) for the 304 stainless steel pyramidal truss lattice infiltrated with PU 1 and the empty 304 stainless pyramidal truss lattice. Similar to the empty truss lattice sandwich structure, the energy absorbed by the PU 1 infiltrated sandwich structure decreases after the critical velocity until it reached a minimum and then increased monotonically with the impact velocity. The first sample of the 304 stainless steel pyramidal truss lattice filled with PU 1 to be penetrated occurred with an impact velocity of 530.4 m/s. The projectile exited the distal face sheet with an exit velocity of 245.7 m/s, approximately 46% of the impact velocity. Figure 36 shows a cross sectional view of a 304 stainless steel sample filled with PU 1 that was impacted by the spherical projectile at 370.9 m/s, shot 70. 60 Figure 36. a) Cross section of the 304 stainless steel sample infiltrated with PU 1 that was impacted at 370.9 m/s, shot 70 b) Cross section of the entry hole of shot 70 c) Cross section of the exit hole of shot 70. Physical examination after the test indicated a center-cell impact (i.e. equidistant from four nodes), Figure 36. The projectile impacted a truss/distal facesheet node causing a truss to separate and plastically deform. Penetration of the proximal facesheet resulted in an entry hole of 12.5 mm wide and deflected 3.0 mm with significant bulging. Penetration of the distal facesheet did not occur but displayed significant bulging and dishing. The projectile was fully arrested resulting in a deflection of 10.0 mm in the 61 bulge zone. The projectile’s path through the polyurethane resealed after penetration leaving no air space. The dishing zone diameter was approximately 65.0 mm and the impact caused a separation of the polyurethane/distal facesheet. There was no nodal disbonding of the trusses and facesheets except for the exit location. Figure 37. a) Cross section of the 304 stainless steel pyramidal truss lattice filled with PU 1 that was impacted at 515.7 m/s, shot 110 b) Cross section of the entry hole of shot 110 c) Cross section of the exit hole of shot 110. Figure 37 shows an impact that was approximately 12.5 mm off of the center of the cell, shot 110. The projectile impacted at 515.7 m/s and brake screens recorded an exit 62 velocity 275.8 m/s, approximately 53% of the impact velocity. The projectile did not impact any truss or nodal contact due to the off axis impact. Penetration of the proximal facesheet resulted in an entry hole of 12.5 mm wide and deflected 3.0 mm, displaying only minor bulging. Penetration of the distal facesheet resulted in an exit hole of 12.5 mm wide and deflected 8.0 mm. No petaling occurred on the distal facesheet, but significant dishing and bulging were observed. Similar to the rest of the shots infiltrated with polyurethane, there was separation of the polyurethane/distal facesheet interface with a diameter of 54.0 mm and a resealing of the projectile’s path through the polyurethane. There was only one nodal contact that began to disbond and separate, but that was adjacent to the exit location of the projectile. 63 Figure 38. a) Cross section of the 304 stainless steel pyramidal truss lattice filled with PU 1 that was impacted at 984.5 m/s, shot 112 b) Cross section of the entry hole of shot 112 c) Cross section of the exit hole of shot 112. Figure 38 shows a center-cell impact on shot 112 of 984.5 m/s and an exit velocity of 557.7 m/s, approximately 57% of the impact velocity. The projectile impacted a truss/distal facesheet node causing trusses to separate and plastically deform. Penetration of the proximal facesheet resulted in an entry hole of 12.5 mm wide and deflected 1.0 mm. The proximal face sheet separated from the polyurethane in the center of the entry hole by approximately 3.0 mm and the diameter of any separation of the interface was 74.0 mm. There was minor ductile hole enlargement of the proximal facesheet. Penetration of the distal facesheet resulted in a petaling exit hole of 27.5 mm wide and a deflection of 16.0 mm. The distal facesheet exhibited three distinct petals that terminated at each adjacent node. Similar to previously impacted polyurethane samples, the projectiles path resealed after penetration but showed signs of tearing due to the plastic deformation of the trusses. There was no nodal disbonding of the trusses and facesheets. 6.2 Discussion The 304 stainless steel lattice truss sandwich structure infiltrated with PU 1 and the 304 stainless steel empty sandwich structure both share approximate critical velocity regions 64 of 400 to 500 m/s. Although, the addition of the PU 1 to the 304 stainless steel truss lattice system marginally increased the first penetrated sample impact velocity by approximately 10%, from 481.3 m/s to 530.4 m/s. It also reduced the slope of the linear fit of the exit velocity by approximately 13%. Improvement of the ballistic resistance for the PU 1 infiltrated system compared to the empty truss lattice system was seen in Figure 34 as the entry velocity increased. This increase in performance was most likely attributed to the energy dissipated in the associated strain fields as the polymer was transiently displaced outward from the projectile. Additionally, reduction of the proximal facesheet deflection occurred at the lower speeds because of the physical restraint of the PU 1 inside the structure. The onset of petaling did not appear to change as the transition from dishing/bulging to fracture occurred. Another consideration for the improvement in ballistic efficiency was the constraint of the trusses and the energy absorbed through frictional dissipation as the trusses were plastically deformed from impact. With the 304 stainless steel empty truss lattice system possessing an areal density of 28 kg/m2 and the 304 stainless steel truss lattice infiltrated with PU 1 possessing an areal density of 54 kg/m2, a direct comparison between the normalized, first penetrated sample impact velocity yields 17 m3/kg·s and 10 m3/kg·s (first penetrated sample impact velocity divided by the areal density), respectively. The higher the normalized velocity indicates greater ballistic resistance efficiency. Therefore, accounting for areal density, the 304 stainless steel system has a higher ballistic efficiency than the PU 1 infiltrated system. Further improvement might have been attained if there was greater adhesion between the facesheet-PU 1 interfaces. The elastomeric properties of PU 1 allowing a large degree of elastic spring back, in addition with high velocities generating highly localized heat, may account for the resealing of the projectile path through the test samples. 65 Chapter 7 Enhanced Ballistic Lattice Fabrication Although the PU 1 did not increase the ballistic efficiency of the sandwich structure, there exists the possibility that other materials could be infiltrated or inserted into the structure to improve its resistance to penetration. This chapter conducts a preliminary investigation of several possibilities including a different polymer, ballistic fibers and metal encased ceramics with a polymer. Also investigated is the utility of a double layer pyramidal truss lattice. This preliminary investigation is a simple survey of six “hybrid” lattice truss systems at a fixed impact velocity of approximately 600 m/s with no recording capability of exit velocity. The investigation provides an insight for possible materials, with a high ballistic resistance, to be introduced into the truss lattice structure which future studies can explore. 7.1 Concept Systems Seven system concepts were constructed and evaluated. Six utilized a single layer system and one the double layer concept. Various materials were introduced into the structures void space. Table 6 summarizes the concepts evaluated. Figure 39 schematically illustrates these basic concepts. System Layer Polymer Fabric Encased Ceramic 1 2 3 4 5 6 7 Single Single Single Single Single Single Double None PU 1 PU 1 PU 2 PU 1 PU 2 PU 1 None None None None Yes None None None None None None None Yes None Areal Density (kg/m2) 27.7 54.8 54.6 55.9 53.7 105.1 53.1 Table 6. Physical descriptions of composite lattice truss systems fabricated. 66 Figure 39. Schematic illustrations of pyramidal lattice truss concepts evaluated in the study. a) Empty pyramidal truss lattice b) Polymer filled in truss lattice c) Ballistic fabric interwoven between trusses with polymer filling remaining air space d) 304 SS encased alumina inserted in triangular prismatic voids and remaining air space filled with polymer e) Double layer pyramidal truss lattice filled with PU 1. 7.2 Lattice Structure Fabrication Single layer pyramidal truss lattice sandwich structures were constructed according to the procedures described in Chapter 3.1. Double layer pyramidal truss lattice sandwich structures were created by stacking two layers of the lattice truss structure made from a 1.5 mm thick (16 gauge) 304 stainless 67 steel using an intermediate solid sheet of 0.5 mm thick (20 gauge) 304 stainless steel. The diamond perforation punch for the double layer lattice was 2.65 cm in length and 1.53 cm wide. The bent perforated sheets were then assembled to make nodal line contacts as shown in Figure 6. The double layer samples were cut to a 5x7 pyramidal cell array and also placed between identical 16 gauge thick 304 stainless steel facesheets 11.09 cm x 12.70 cm. In both systems, the lattice truss layer(s) were bonded to these facesheets using a transient liquid phase bonding process [111,112]. This involved spray coating the face and the intermediate solid sheets with a NICROBRAZ® alloy 51 (Wall Colmonoy, Dayton OH). This alloy is composed of 25 Cr, 10 P, 0.03 C (wt. %) with the balance consisting of Ni. The powder was contained in a polymer binder. These brazing alloys contain melting point depressants (e.g. boron, phosphorous, silicon) to achieve desirable liquid flow and adequate wetting behavior. The sandwich structure was placed in a high-temperature vacuum oven for brazing at 10 °C/min up to 550 °C, held for 20 minutes to remove any residual polymer binder, then heated to 1050 °C, for 60 minutes at 1.3 x 10-2 Pa before furnace cooling to ambient temperature at 25 °C/min. 7.3 Double Layer Lattice Relative Density Similar to the single layer pyramidal unit cell in Chapter 3.2, the relative density of the double layer pyramidal lattice truss core can be simply calculated from a unit cell analysis. Figure 40 shows the double layer pyramidal unit cell, 68 Figure 40. Unit cell geometry used to derive the relative density for a double layer pyramidal topology. where wi is the intermediate plate width, ti is the intermediate plate thickness and li is the intermediate plate length. We may write the volume of the truss members, in addition to the intermediate plate, occupying the double layer pyramidal unit cell shown in Figure 40 as Vtr = 8lwt + l i wi t i (33), where t is truss thickness, l is the truss length, w is the truss width, li is the intermediate plate length, wi is the intermediate plate width and ti is the intermediate plate thickness. From the unit cell geometry the volume of the double layer pyramidal unit cell, it can be shown that: Vc = ( 2l cos ω )( ) 2l cos ω (2l sin ω ) + l i wi t i = 4l 3 cos 2 ω sin ω + l i wi t i (34), Taking the ratio between the truss volume (33) and cell volume (34) we obtain the double layer pyramidal relative density expression: 69 ρ= Vtr 8lwt + l i wi t i = 3 V c 4l cos 2 ω sin ω + l i wi t i (35), with a truss length l = 14.7 mm, a truss width w = 1.5 mm, a truss thickness t = 1.5 mm, an intermediate length li = 25.4 mm, an intermediate width wi = 25.4 mm, an intermediate thickness of ti = 0.9 mm, yields a ρ = 10.2% (including the 20 gauge intermediate layer). The areal density of the double layer pyramidal truss lattice structure is 53.1 kg/m2. 7.4 Infiltration Materials and Methods 7.4.1 Polymers Two polyurethanes, PU 1 described in Chapter 3.4, and another polyurethane, designated PU 2, were inserted into six of the seven concept cellular sandwich systems. PU 2 was chosen to complement PU 1’s material characteristics. PU 2, model name CLC-1D078 [102], supplied by Crosslink Tech, Inc. (Mississauga, ON Canada), was chosen due to a high elastic modulus and high tensile strength but low elongation to failure. PU 2 is a two component, rigid, rapid prototyping polyurethane system with cure time of approximately five minutes at room temperature. Part A is composed of polyether polyol. Part B is composed of diphenylmethane-4,4’-diisocyanate. Table 7 shows the manufacture’s reported mechanical properties for the PU 2 system. Property Manufacturer Product Name Tensile Modulus (MPa) Tensile Strength (MPa) Elongation to Break (%) Shore Hardness PU 2 Crosslink Technology Inc. (Mississauga, ON Canada) CLC-1D078 1,120 68.9 16 78 D Table 7. Manufacturer reported properties for the polyurethane system. 70 7.4.2 Fabric A ballistic fabric was integrated into the one of cellular sandwich systems to investigate if it provided additional resistance to projectile penetration and fragment protection. The ballistic fabric chosen was a high strength ribbon composed of woven Spectra®, approximately 2.54 cm wide, and interwoven between every other cell in a 0-90° orientation. The ribbon was a 1200 denier 4 with a 21 x 21 plain weave impregnated with a 20 ± 2% resin. A single layer of interwoven ribbon was located inside the sandwich structure proximal to the distal face sheet. 7.4.3 Metal Encased Ceramic Prisms Metal encased alumina prisms were inserted in one of the single layer samples. The AD94 alumina rods were manufactured by CoorsTek (Golden, CO). They were equilateral triangular prisms with a base length of 2.54 cm, 12.07 cm long. The apexes of the prisms were ground to remove 0.32 cm of material so they could be slipped into 0.05 cm thick (20 gauge) 304 stainless steel triangular tubes. The 304 stainless steel equilateral triangular tubes had an interior base length of 2.54 cm. The AD-94 grade of alumina consists of 93.3 Al2O3, 4.1 SiO2, 0.8 BaO, 0.7 MgO, 0.7 ZrO2, 0.3 CaO, 0.2 Fe2O3 and 0.1 Na2O (wt. %). The mechanical properties for AD-94 alumina reported by CoorsTek are summarized in Table 8. Elastic Density Material Modulus (g/cc) (GPa) AD-94 3.97 303 Tensile Strength (MPa) 221 Comp. Strength (MPa) 2068 Fracture Toughness (MPa·m1/2) 4-5 Hardness (GPa) 11.5 Table 8. Physical properties of AD-94 Al2O3 triangular prisms. 4 Denier is a system of measuring the weight of a continuous fiber, numerically equivalent to the weight in grams of 9,000 m of a continuous fiber. Plain weave is one of the basic weaves utilizing a simple alternate interlacing of the fill and warp yarn, seriatim. 71 The 304 stainless steel tubes were then capped with 304 stainless steel plugs and sealed by brazing utilizing the NICROBRAZ® alloy 51 and an identical process to that used to fabricate the truss structures. 7.5 Hybrid Lattice Relative Density A unit cell analysis for polymer infiltration into the metal sandwich structure can be found in Chapter 3.4.1, with both polymer densities approximately equal, ρ = 1.3 g/cc. The relative densities of the systems are approximately ρ = 27-27.5%. The areal density of the 304 stainless steel pyramidal truss lattice infiltrated with PU 1 is approximately 55 kg/m2 and the truss lattice infiltrated with PU 2 is approximately 56 kg/m2. The relative density for the 304 stainless steel truss lattice infiltrated with PU 1 and ballistic fabric is given by: ρ= ρ pu (2l 3 cos 2 ω sin ω − 4lwt − l f w f t f ) + ρ tr (4lwt ) + ρ f (l f w f t f ) ρ m (2l 3 cos 2 ω sin ω ) (36). where ρ pu is the density of the polyurethane, ρ tr is the density of the trusses, ρ f is the density of the fabric and ρ m is the density of the base metal system. With a polyurethane density of ρ pu = 1.3 g/cc, a truss length of l = 31.75 mm, truss width of w = 1.9 mm, a truss thickness of t = 1.9 mm, an included angle of ω = 54.7° , a fabric length of l = 25.4 mm, a fabric width of w = 25.4 mm, a fabric thickness of t = 1.6 mm, a truss density of ρ tr = 7.97 g/cc, a fabric density of ρ t = 1.4 g/cc and a base metal density of ρ m = 7.97 , the relative density of the system is approximately ρ = 26.5%. The areal density of the 304 stainless steel pyramidal truss lattice infiltrated with PU 1 and fabric is approximately 54 kg/m2. The relative density for the 304 stainless steel truss lattice infiltrated with PU 1 and Al2O3 encased in 304 stainless steel tubes is given by: 72 ρ= ⎛ ⎝ 1 2 ⎞ ⎛1 [bo ho − bi hi ]⎞⎟ + ρ a ⎛⎜ 1 [bi hi ]⎞⎟ ⎠ ⎝2 ⎠ ⎝2 ⎠ ρ m (4l 3 cos 2 ω sin ω ) ρ pu ⎜ 2l 3 cos 2 ω sin ω − 4lwt − bo ho ⎟ + ρ tr (4lwt ) + ρ m ⎜ (37), where ρ pu is the density of the polyurethane, bo and bi are the bases of the triangle for the outer and inner tube respectively, ho and hi are the heights of the triangle for the outer and inner tube respectively ρ tr is the density of the trusses, ρ m is the density of the base metal system and ρ a is the density of the aluminum oxide. With a polyurethane density of ρ pu = 1.3 g/cc, a truss length of l = 31.75 mm, truss width of w = 1.9 mm, a truss thickness of t = 1.9 mm, an included angle of ω = 54.7° , triangle bases of bo = 2.54 cm and bi = 2.49 cm, triangle heights of ho = 2.20 cm and hi = 2.15 cm, a truss density of ρ tr = 7.97 g/cc, an aluminum oxide density of ρ a = 3.97 g/cc and a base metal density of ρ m = 7.97 , the relative density of the system is approximately ρ = 52%. The areal density of the 304 stainless steel pyramidal truss lattice infiltrated with PU 1 and fabric is approximately 105 kg/m2. Extending the cell analysis used to derive the relative density of the double layer truss lattice system in Chapter 7.3, the relative density for the double layer 304 stainless steel truss lattice infiltrated with PU 1 is given by: ρ= ρ pu (4l 3 cos 2 ω sin ω − 8lwt ) + ρ m (8lwt + li wi ti ) ρ m (4l 3 cos 2 ω sin ω + li wi ti ) (38), with a truss length l = 14.7 mm, a truss width w = 1.5 mm, a truss thickness t = 1.5 mm, an intermediate length li = 25.4 mm, an intermediate width wi = 25.4 mm, an intermediate thickness of ti = 0.9 mm, yields a relative density, compared to an all steel plate, of approximately ρ = 26% (including the 20 gauge intermediate layer). The areal density of the double layer pyramidal truss lattice structure is approximately 53 kg/m2. 73 7.6 Material Properties 7.6.1 Brazed 304 Stainless Steel The uniaxial tensile response of 304 stainless steel subjected to the same thermal history as the lattice truss structures has been previously measured and reported [7], Figure 41. The elastic modulus and 0.2% yield strength were 203 GPa and 176 MPa, respectively. Significant work hardening occurred in the plastic region. Figure 41. Uniaxial tension data for brazed 304 stainless steel. 74 7.6.2 PU 2 To contrast PU 1, another polyurethane system was chosen with a significantly higher glass transition temperature thus a higher elastic modulus and lower elongation to fracture. DSC analysis and DMA analysis were performed to characterize the mechanical properties of the polyurethane. 7.6.2.1 DSC Analysis The glass transition temperature, Tg, of PU 2 was determined with a similar modulated differential scanning calorimetry (MDSC®) technique using a similar Q1000 Modulated DSC described in Chapter 3.5.1. The polymer was heated over a temperature range of 80 to 240 °C with a heating rate of 3 °C/min and a modulation of ± 0.5 °C/60 sec period. Figure 42 is a plot of the heat capacity, Rev Cp, of PU 2 as a function of temperature revealing an approximate Tg of 49 °C. The Cp of each sample was determined by dividing its reversing heat flow value, J/(sec·g), by the heating rate, °C/sec. Figure 42. Heat capacity (Rev Cp) PU 2 as a function of temperature (°C). 75 7.6.2.2 DMA Analysis The rheological properties of PU 2 were characterized with dynamic mechanical analysis (DMA) using a similar Q800 DMA described in Chapter 3.5.2. Measurements were made at three different frequencies, 1, 10 and 100 Hz, over a temperature range of -100 to 40 °C in 5 °C increments. The data over the entire temperature range were transformed using time-temperature superposition (TTS) with a reference temperature of 25 °C [106,107]. The result of this data manipulation is a master curve of predicted storage modulus, E ′ , and loss modulus, E ′′ , values over a frequency range of 10-1 to 1010 Hz at the reference temperature. Figure 43 is a plot of the storage modulus of PU 2 at a frequency of 1 Hz over a temperature range of -100 to 40 °C. Figure 43. Storage modulus at a frequency of 1 Hz for PU 2 as a function of temperature. 76 The storage modulus of PU 2 did decrease by more than one order of magnitude as the temperature is increased to 40 °C. The observation that there was such a large decrease in the storage modulus of PU 2 more than 10 °C below its Tg was consistent with the observation that the temperature range over which the glass transition of this sample occurs was very large. Next, the predicted storage and loss modulus values for PU 2 over a frequency range of 1 to 106 Hz at a reference temperature of 25 °C were computed, Figure 14. As previously discussed, these predicted values were obtained by transforming the measured E’ and E” values obtained over the temperature range of -100 to 40 °C at the three different frequencies using TTS (data obtained at low temperatures corresponds to the high frequency data in Figure 14, while data obtained at high temperatures corresponds to the low frequency data). Figure 44. Predicted values for the storage and loss modulus of PU 2 at a reference temperature of 25 °C as a function of frequency. Figure 15 is a plot of Tan δ of PU 2 over the same frequency range covered in Figure 14. 77 Figure 45. Tan δ ( E ′′ / E ′ ) of PU 2 as a function of frequency. 78 Chapter 8 Ballistic Testing A preliminary study was conducted that initiates an exploration of 304 stainless steel hybrid pyramidal truss lattice structures ballistic response to moderate velocity impact by a spherical projectile. A full ballistic evaluation of each concept was not conducted; instead a comparison of relative performance was conducted against the impact of a spherical projectile 12 mm in diameter and constant velocity of approximately 600 m/s. 8.1 Test Setup A series of ballistics experiments with spherical projectiles were conducted using the University of Cambridge gas gun facility with samples whose fabrication was described in Chapter 7 [31]. Compressed nitrogen was used to accelerate the projectile which then impacted the samples normal to their surface, Figure 46. The gas gun fired 12 mm diameter, 6.9 g, 420 stainless steel ball bearings at the specimens at impact velocities of approximately 600 m/s. For these experiments, the gas gun was fitted with a 12 mm bore, 4.5 m long barrel designed for ballistic testing. The loading configuration, illustrated in Figure 46, shows that the projectile impacted the center of the panels, which were simply supported over an approximate 60 mm diameter hole located in a rigid backing plate (25 mm thick). A Hadland Imacon-790 image-converter high speed camera was used to monitor the responses of the (empty) system 1. It enabled observation of the projectile impact with the sandwich panel and the sequence of subsequent deformation. An inter-frame time of 10 µs and an exposure time of 2 µs was used. Additionally, x-ray tomography was performed on system concept 4. 79 Figure 46. Ballistic testing configuration. Ball bearing projectiles with a radius of 6 mm and weight of 6.9 g were used. An impact velocity of approximately 600 m/s was used for all the tests. The specimens were adhesively attached to a backing plate with double-sided tape as shown in Figure 46. Specimens used in evaluations of systems 1 through 6 were orientated such that impact occurred at the center of the proximal faceplate, which was supported centrally by the pyramidal core, as sketched in Figure 47 (a). The specimen used in evaluation of system 7, which consisted of the double-layered pyramidal core, was loaded in the configuration illustrated in Figure 47 (b). Figure 47. Projectile impact location for a) Single and b) Double layer pyramidal lattice truss sandwich panels. 80 8.2 Results 8.2.1 Single Layer Empty System Figure 48 shows cross sectional views of a truss sandwich panel (system 1) before and after impact by a spherical projectile with an incident velocity of 598 m/s. Figure 48. Test 1: a) Cross section of the single layer empty pyramidal truss lattice along a nodal line b) Cross section of the single layer empty pyramidal truss lattice after a projectile impact of 598 m/s. Examination after impact indicated buckling and plastic deformation of the trusses was limited to one cell in the lattice, as seen in Figure 48 (b). A fracturing of the nodes occurred at all four truss/facesheet contact points of the impacted cell, two of these contact points are shown in Figure 48 (b). The entry hole on the proximal facesheet was 15 mm in diameter and deflected 5 mm. The exit hole on the distal facesheet was approximately 18 mm in diameter and deflected 11 mm. The plastic deformation of both 81 facesheets is known as petaling, a phenomenon common among impacted thin, ductile metals. A time sequence of high-speed photographs was taken during the test and these are shown in Figure 49 (a)-(h). The time after impact is indicated for each frame, and it is seen that impact occurred between Figure 49 (b) and (c). Subsequent frames, Figure 49 (d)-(h), show the projectile penetrating the proximal face and propagating towards the distal face. Estimating the distance traveled from frames, Figure 49 (c)-(h), to be approximately 22.5 mm and knowing the time between these frames was 50 µs, the velocity of the projectile was approximately 450 m/s as it propagated between the proximal and distal faces. As the impact velocity was measured to be 598 m/s, the reduction due to penetrating the proximal face was approximately 148 m/s. Figure 49. High-speed photography of a projectile impact with the empty single layer pyramidal lattice (system 1). Each figure (a)-(h) depicts a frame of the high-speed photography. The time in microseconds (μs) is labeled from the initial impact of the projectile with the proximal facesheet. As indicated in Figure 49, the projectile impacted at a node-facesheet contact. There was no observable deflection of the projectile and no core compression could be detected. 82 The lack of core compression in the ballistic experiments is considerably different than that observed in beams [31,32] and plates [33,34] with pyramidal lattice cores, which were loaded with metal foam projectiles. Figure 50 shows the position of the projectile from the proximal facesheet as a function of time. As described in Chapter 5.1, the error bars for the graph are smaller than the plotted data points. Figure 50. Position of a spherical projectile from the proximal facesheet of the empty single layer pyramidal lattice truss as a function of time. To the left of the time of impact is before the impact of the projectile and the right of the time of impact is after impact of the projectile. 8.2.2 Soft Polymer Filled System Figure 51 shows the cross section of the single layer pyramidal truss lattice filled with PU 1 before and after impact with a spherical projectile whose contact velocity was 616 m/s. 83 Figure 51. Test 2: a) Cross section of the single layer pyramidal truss lattice filled with PU 1 b) Cross section of the single layer pyramidal truss lattice filled with PU 1 after a projectile impact of 616 m/s. Notice the brass breech rupture disk (b) remaining in the polymer while the projectiles path resealed. Examination after impact showed an entry hole on the proximal facesheet 12 mm in diameter and deflected 2 mm. The exit hole on the distal facesheet measured 15 mm in diameter and deflected 12 mm. Displaying less deflection of the proximal facesheet than the empty pyramidal lattice truss system indicates that the polymer constrained the movement of the structure. Approximately equal deflections and exit holes of the distal facesheets, with system 1, indicate similar exit velocities. A remnant of the brass breech rupture disk impacted the specimen also but did not penetrate the PU 1. The PU 1 resealed the remainder of the void space from the 84 projectiles penetration. These results further corroborated the data obtained in Chapter 6 which showed a penetration at approximately 600 m/s and a resealing of the projectile path. 8.2.3 Double Layer Filled with PU 1 The projectile impacted the double layer pyramidal truss lattice filled with PU 1 at 613 m/s. Figure 52 shows cross sections before testing (a), and after impact (b). Figure 52. Test 7: a) Cross section of the double layer pyramidal truss lattice filled with PU 1 b) Cross section of the double layer pyramidal truss lattice filled with PU 1 after an impact of 613 m/s. Examination after impact showed an entry hole 12 mm in diameter and a deflection of 2 mm. The exit hole was 16 mm in diameter and a deflection of 14 mm. The soft polymer, 85 at its apex, was displaced 5 mm. On the proximal facesheet, nodal failure was limited to the adjacent cells. On the distal facesheet, nodal failure extended to a radius of two to three cells in all directions. Differing from the other soft polymer infiltrations, only partial resealing of the PU 1 occurred due to the smaller dimensions of the cell size. Reducing the pyramidal unit cell size did not seem to improve ballistic efficiency given that penetration still occurred and approximately the same degree of deformation on the distal facesheet was exhibited. 8.2.4 Hard Polymer Filled System The projectile impacted the single layer pyramidal truss lattice filled with PU 2 at 632 m/s. Figure 53 shows cross sections before testing (a), and after impact (b). Figure 53. Test 4: a) Cross section of the single layer pyramidal truss lattice filled with PU 2 b) Cross section of the single layer pyramidal truss lattice filled with PU 2 after a projectile impact of 632 m/s showing approximately 8.5 mm deflection of the rear face panel. Note that the projectile is visibly arrested in (b). 86 Examination after impact showed the entry hole 12 mm in diameter and deflected by 1 mm, similar in performance to the soft polymer filled system. The rear facesheet was deflected by 8.5 mm and arrested the projectile. The projectile itself was intact with gashes equal in thickness to the trusses, shown in Figure 53 (b). Nodal failure occurred in multiple cells, including the impacted and adjacent cells. X-ray tomography was performed on this test specimen 4. Figure 54 depicts the sample after projectile impact. Figure 54. X-ray tomography of specimen 4. Side profile (Left). Elevated view above proximal face sheet (Right). The x-ray tomography reveals one of the pyramidal trusses severed and plastically deformed, without fragmentation. The projectile penetrated the PU 2/rear facesheet interface and the rear facesheet, in conjunction with complete nodal failure, absorbed the remaining kinetic energy. 87 8.2.5 Single layer filled with PU 1 plus Fabric The projectile impacted the single layer pyramidal truss lattice filled with fabric and PU 1 at 613 m/s. Figure 55 shows cross sections before testing (a), and after impact (b). Figure 55. Test 5: a) Cross section of the single layer pyramidal truss lattice filled with the interwoven fabric and the PU 1 b) Cross section of the single layer pyramidal truss lattice filled with interwoven fabric and the PU 1 after a projectile impact of 613 m/s. Examination after impact showed the entry hole 12 mm and deflected 2 mm. The exit hole was 12 mm in diameter and deflected 8 mm. Similar to the single layer pyramidal truss lattice filled with PU 1 only, the PU 1 resealed the void space left by the projectile. Additionally, there was complete nodal failure of the proximal facesheet but only partial nodal failure on the distal facesheet, limited to the impact cell. The addition of the fabric to the soft filled polymer system did alter its performance. 88 8.2.6 Ceramic plus PU 2 Filled System The projectile impacted the single layer pyramidal truss lattice filled with fabric and PU 1 at 613 m/s. Figure 56 shows cross sections before testing (a), and after impact (b). Figure 56. Test 6: a) Cross section of the single layer pyramidal truss lattice filled with 304 stainless steel prisms and PU 2 b) Cross section of the single layer pyramidal truss lattice filled with 304 stainless steel prisms and PU 2 after an impact of 613 m/s. Examination after impact showed the entry hole 12 mm in diameter and deflected by 3 mm. The projectile was arrested and fractured, as seen in Figure 56 (b), by the center 304 stainless steel tube containing the alumina. The tube was breeched and the alumina was fragmented. Damage was limited to the center tube with minimal fracturing of the surrounding hard polymer. There was no observable nodal disbonding. The rear facesheet was deflected by 3.5 mm, absorbing the remaining impact energy. Due to the large amount of 304 stainless steel in the specimen, an accurate x-ray tomographical analysis was unable to be performed. 89 8.3 Discussion The empty pyramidal lattice truss structure did not prevent the penetration of the projectile as expected from results obtained in Chapter 5. A fraction of the kinetic energy was absorbed in the plastic deformation of the trusses and the petaling of the face sheets, accounting for approximately a 25% reduction of the incoming velocity. There appeared to be no observable deflection of the projectile by the truss as previously theorized. The sample infiltrated with polyurethane, designated PU 2, was the only one of the four infiltrated with polymer, three single layer and one double layer, that successfully defeated the projectile. The possibility exists that the high tensile modulus and/or strength of the PU 2 facilitated the prevention of penetration. Additionally, the failure of all contact nodes with the rear face sheet may have also provided the necessary absorption of energy to prevent the projectile from penetrating and only deflecting the rear face sheet approximately 8.5 mm. All three samples infiltrated with PU 1 failed to prevent penetration of the projectile. A double layer pyramidal truss lattice with PU 1 infiltrated in the structure seems to offer no advantage to ballistic performance. Reducing the cell size and increasing the amount of layers offered an increased probability of an interaction with a truss thus deflecting the projectile but the evidence did not substantiate this assertion. As with the single layered samples, the PU 1 contributed minimally to the ballistic performance of the sample. Serendipitously, the elastomeric properties of PU 1 provided a unique side effect, a resealing of the projectiles path through the sample. Further studies could exploit this effect for maritime armoring. The addition of the ballistic fabric to the PU 1 system had no observable effect. This can most likely be attributed to the constraint of the fabric by the PU 1. A composite and/or ballistic fiber will absorb higher energy by either breaking a larger number of fibers or involving a larger area/volume of fibers. However, the fiber cannot fulfill its highest capability because of the constraints imposed by the matrix. Essentially, only a portion of the fibers is plastically deformed and fractured; a large portion of the fibers is not 90 stressed to their ultimate capability [113]. Penetration of the sample occurred with no deflection of the projectile. The sample containing the metal encased Al2O3 prisms was not penetrated by the projectile. Possessing the highest areal density, it outperformed all of the samples within the study by resisting penetration and having the smallest deflection of the distal facesheet. Not unexpected, the Al2O3 prisms were designed for ballistic impact and encasing them within 304 stainless steel prisms confined the fragmented ceramic pieces thus providing further resistance to penetration. Although an interior analysis of the sample was not conducted due to technical constraints, physical observation of the cross section revealed that the projectile breached the metal tubing and fractured the encased alumina. Also, the projectile fractured and remnants were visible in the cross sectioned sample. Plastic deformation was restricted by the back mounting, a 60 mm diameter circle cut from a sheet, thus allowing a permanent plastic deflection of 3.5 mm. 91 Chapter 9 Discussion Distributing the mass into the trusses and separate facesheets did not change the critical velocity of the 304 stainless steel system. The 304 stainless steel lattice truss system and the 304 stainless steel plate both had approximately equal critical velocities of 450 m/s based upon an extrapolation of the ballistic data. As the velocity was increased beyond the critical velocity, the sandwich structure exhibited superior performance to the plate by reducing the exit velocity to 55-70% of the impact velocity compared to the plate of 6770%. In the solid plate, the energy was absorbed through the dishing and bulging of the solid plate, with shear bands being created during the impact process. In the sandwich structure, the energy was absorbed through the dishing and bulging of the proximal facesheet, debonding of the truss-facesheet node, plastic deformation and bending of the trusses and minor petaling of the distal facesheet. At velocities significantly higher than the critical velocity (i.e. three times), the lattice truss system displayed an approximate 12% reduction in the exit velocity of the projectile and/or its fragments. As the projectile velocity increased, the failure mechanisms of the target altered. In the solid plate, dishing and bulging diminished, eliminating large shear band zones, and larger degrees of ductile hole enlargement began to dominate. In the lattice truss system, the proximal facesheet exhibited a similar transition between bulging and dishing to ductile hole enlargement. Additionally, a large degree of petaling still occurred on the distal facesheet but the size of the petals increased beyond the impacted unit cell thus causing further plastic deformation to the surrounding trusses still attached to the petals. This additional deformation could possibly explain the slight improvement of ballistic resistance for the lattice truss system compared to the solid plate. By comparing equivalent lattice truss systems composed of 304 stainless steel and age hardened 6061 aluminum alloy, we were able to gain an insight as to the role of the base metal’s effectiveness in ballistic resistance. These two systems were chosen due to their varied mechanical properties and their differing areal densities, 304 stainless steel truss 92 lattice panels having an areal density of 28 kg/m2 and AA6061 being 10 kg/m2. Although the critical velocity of AA6061 could not be ascertained directly due to technical constraints, it was linearly extrapolated to be approximately 60 m/s. By dividing the critical velocity of the system by the areal density, we can directly compare the systems. This normalization yields AA6061 being approximately 6 m3/kg·s compared to the 304 stainless steel being approximately 16 m3/kg·s. The higher the normalized velocity indicates greater ballistic resistance efficiency. Also, the AA6061 system exhibited similar failure mechanisms and similar transitions between mechanisms as the 304 stainless steel lattice truss system. The noticeable difference was the AA6061 petals formed at high velocities were considerably smaller. The lower performance of the ballistic resistance of the AA6061 compared to the 304 stainless steel can be attributed to the significantly lower work hardening rate, lower ductility and lower density of the former. The lower work hardening rate decreases the amount of energy dissipated through plastic deformation and therefore less bulging and dishing. Also, the lower density reduced the amount of energy absorbed through the momentum transfer of the projectile to the structure. The combination of these factors allowed fracture to initiate earlier and less energy to be absorbed causing penetration at lower speeds and higher exit velocities. The addition of the low Tg elastomer (PU 1) to the 304 stainless steel truss lattice system marginally increased the first penetrated sample impact velocity by approximately 10% (from 481.3 m/s to 530.4 m/s) and reduced the slope of the linear fit to the exit velocity by approximately 13%. This additional energy being absorbed can most likely be attributed to the associated strain fields dissipating energy as the polymer was transiently displaced outward from the projectile. The critical velocity was similar to the empty truss lattice sandwich structure of approximately 450 m/s. Another consideration for the improvement in ballistic efficiency was the physical constraint of the trusses by the surrounding polymer and the energy absorbed through frictional dissipation by the trusses as they were plastically deformed from impact. A possible improvement in ballistic performance might have been attained if there was 93 greater adhesion between the facesheet-PU 1 interfaces. The elastomeric properties of PU 1, in addition with high velocities generating highly localized heat, possibly account for the resealing of the projectile path through test samples. Similar failure mechanisms and trends were exhibited between the empty truss lattice system and the PU 1 infiltrated system with only one minor difference; the PU 1 physically restricted the proximal facesheet from bulging and dishing. The PU 1 infiltrated system exhibited the same progression to larger degrees of ductile hole enlargement on the proximal facesheet and larger degrees of petaling on the distal facesheet as the impact velocity of the projectile increased. With the 304 stainless steel empty truss lattice system possessing an areal density of 28 kg/m2 and the 304 stainless steel truss lattice infiltrated with PU 1 possessing an areal density of 54 kg/m2, normalizing the PU 1 infiltrated system yields 8 m3/kg·s compared to the empty truss lattice sandwich structure of 16 m3/kg·s (both systems having a critical velocity of 450 m/s). Therefore, accounting for areal density, the 304 stainless steel system has a higher ballistic efficiency than the PU 1 infiltrated system. The infiltration of polymers is only beneficial if their application exploits some other feature such as damping, leak plugging, thermal insulation, etc. The study investigating various hybrid truss lattice systems displayed some insight into the importance of polymer selection, in addition to other infiltrated materials. The sample infiltrated with PU 2 was the only one of the four infiltrated with polymer, three single layer and one double layer, that successfully defeated the projectile. The Tg of PU 2 was above room temperature therefore at ambient temperature (i.e. test conditions) the polyurethane was hard and brittle. Because of the differences in Tg, the possibility exists that the high tensile modulus and/or strength of the PU 2 facilitated the prevention of penetration as compared to the PU 1. This claim is substantiated by the fact that the temperature range over which the glass transition takes place is much larger with PU 2 than with PU 1, as can be seen from Figure 12 and Figure 42. This probably indicates that PU 2 has a greater molecular weight distribution and is more cross-linked and/or crystalline than PU 1 [104,105]. Additionally, the failure of all contact nodes with the 94 rear face sheet may have also provided the necessary absorption of energy to prevent the projectile from penetrating and only deflecting the rear face sheet approximately 8.5 mm. A double layer pyramidal truss lattice with PU 1 infiltrated in the structure seems to offer no advantage to ballistic performance. Reducing the cell size and increasing the amount of layers offered an increased probability of an interaction with a truss thus deflecting the projectile but the evidence did not substantiate this assertion. As with the single layered samples, the PU 1 contributed minimally to the ballistic performance of the sample. Increasing the projectile diameter to cell size ratio above 0.5 could possibly alter the intensity and extent of the damage zone. Further study is necessary to ascertain the relationship between the projectile diameter and cell size ratio to damage and/or penetration. It was anticipated that the addition of a ballistic fabric would delocalize the impact zone and lessen the degree of deformation by spreading it over a larger area. Unfortunately, the addition of the ballistic fabric to the PU 1 system had no observable effect. Penetration of the sample occurred with no deflection of the projectile. By containing the ballistic fabric within the PU 1 system, it was unable to bend and flex freely thus inhibiting it from absorbing the incoming energy of the projectile/fragments over a large area. To properly utilize the ballistic fabric in future studies, it would be beneficial to place the fabric on the distal side outside of the structure. In this situation, structural and projectile fragments would eject out of the structure and the fabric would be free to absorb energy without constraint. Additionally, a weak adhesion between the fabric/metal interface would allow the fabric to disbond upon structural failure. The sample containing the metal encased Al2O3 prisms was not penetrated by the projectile. Possessing the highest areal density of approximately 105 kg/m2, it outperformed all of the samples within the hybrid study by resisting penetration and having the smallest deflection of the distal facesheet. Not unexpected, the Al2O3 prisms were designed for ballistic impact and encasing them within 304 stainless steel prisms confined the fragmented ceramic pieces thus providing further resistance to penetration. Although an interior analysis of the sample was not conducted due to technical 95 constraints, physical observation of the cross section revealed that the projectile breached the metal tubing and fractured the encased alumina. Also, the projectile fractured and remnants were visible in the cross sectioned sample, Figure 56. The elastic bending of the samples motion was restricted by the back mounting, a 60 mm diameter circle cut from a sheet, thus allowing a permanent plastic deflection of 3.5 mm. With only one data point for this system, we are unable to linearly extrapolate a critical velocity to obtain a direct comparison between other systems. Further studies will have to be conducted to evaluate its ballistic efficiency, incorporating its high areal density. 96 Chapter 10 Conclusions This thesis attempted to experimentally investigate the ballistic response of stainless steel and 6061 aluminum alloy pyramidal lattice truss core sandwich structures using spherical projectiles with impact velocities up to approximately 1200 m/s. We compared the stainless steel sandwich panel structures response to that of a monolithic plate of equivalent areal density (mass per unit area). We then explore the effect of filling the lattice void space with an elastomer. Finally, we investigate the feasibility of fabricating more sophisticated “hybrid” sandwich structures containing ceramics and ballistic fabrics and find significantly enhanced ballistic resistance can be achieved by this approach. • The failure mechanisms for the 304 stainless steel monolithic plate and the truss lattice system transitioned as impact velocity increased. In the solid plate, dishing and bulging diminished, while ductile hole enlargement began to dominate. In the truss lattice, a similar transition occurred for the proximal facesheet and the degree/size of the petaling on the distal facesheet increased. • The 304 stainless steel monolithic plate and the truss lattice system both had similar extrapolated critical velocities but as impact velocity increased, the truss lattice exhibited better ballistic performance by reducing to the exit velocity of the projectile from 55-70% of impact velocity rather than 67-70%. • The 304 stainless steel truss lattice and the age hardened 6061 aluminum alloy truss lattice exhibited similar failure mechanisms and transitions with varying degrees, ductile hole enlargement and petaling. • The 304 stainless steel truss lattice system has a better ballistic efficiency than the age hardened 6061 aluminum alloy truss lattice system based on the normalized critical velocities of 16 m3/kg·s and 6 m3/kg·s, respectively. • The failure mechanisms for the 304 stainless steel empty truss lattice and the PU 1 infiltrated truss lattice system are similar, ductile hole enlargement and petaling, except for the PU 1 physically restricted the proximal facesheet from bulging and dishing. 97 • The 304 stainless steel truss lattice has a better ballistic efficiency than the PU 1 infiltrated into the 304 stainless steel truss lattice system based on the normalized, first penetrated sample impact velocities of 16 m3/kg·s and 10 m3/kg·s, respectively. • PU 2 outperformed PU 1 by preventing penetration at an approximate velocity of 600 m/s which can possibly be attributed to either and/or both: the PU 2 has a high tensile modulus and strength compared to the PU 1, the PU 2 has a storage modulus of approximately 100 times than PU 1. • Decreasing cell size and increasing the amount of pyramidal truss lattice layers in the 304 stainless steel system did not prevent penetration indicated by a single data point. • The addition of a ballistic fabric into the PU 1 infiltrated truss lattice system did not prevent penetration indicated by a single data point. • The addition of metal encased Al2O3 tubes into 304 stainless steel truss lattice system prevented penetration in a single data point but at a cost of increasing the areal density from 28 kg/m2 to 105 kg/m2. 98 References 1. L. Gibson and M. Ashby, Cellular Solids. Pergamon Press, 1988. 2. M. Ashby, A. Evans, N. Fleck, L. Gibson, J. Hutchinson and H. Wadley, Metal Foams: A Design Guide. Butterworth-Heineman, 2000. 3. H. Wadley, N. Fleck, and A. Evans, “Fabrication and Structural Performance of Periodic Cellular Metal Sandwich Structures”. Composite Science and Technology, 2003, 63, pp. 2331-2343. 4. S. Chiras, D. Mumm, A. Evans, N. Wicks, J. Hutchinson, K. Dharmasena, H. Wadley and S. Fichter, “The Structural Performance of Near-Optimized Truss Core Panels”. International Journal of Solids and Structures, 2002, 39, pp. 40934115. 5. D. Queheillalt, Y. Katsumura and H. Wadley, “Synthesis of Stochastic Open Cell Ni-based Foams”. Scripta Materialia, 2004, 50, pp. 313-317. 6. A. Brothers, R. Scheunemann, J. DeFouw and D. Dunand, “Processing and Structure of Open-Celled Amorphous Metal Foams”. Scripta Materialia, 2005, 52, pp. 335-339. 7. D. Queheillalt and H. Wadley, “Cellular Metal Lattices with Hollow Trusses”. Acta Materialia, 2005, 53, pp. 303-313. 8. H. Rathbun, Z. Wei, M. He, F. Zok, A. Evans, D. Sypeck and H. Wadley, “Measurement and Simulation of the Performance of a Lightweight Metallic Sandwich Structure with a Tetrahedral Truss Core”. Journal of Applied Mechanics, 2004, 71, pp. 368-374. 9. G. Kooistra, V. Deshpande and H. Wadley, “Compressive Behavior of Age Hardenable Tetrahedral Lattice Truss Structures Made from Aluminum”. Acta Materialia, 2004, 52, pp. 4299-4237. 10. R. Hutchinson, N. Wicks, A. Evans, N. Fleck and J. Hutchinson, “Kagomé Plate Structures For Actuation”. International Journal of Solids and Structures, 2003, 40, pp. 6969-6980. 11. J. Tian, T. Lui, H. Hodson, D. Queheillalt and H. Wadley, “Thermal-Hydraulic Performance of Sandwich Structures With Crossed Tube Truss Core and Embedded Heat Pipes”. 13th International Heat Pipe Conference, Shanghai, China, September 21-25, 2004. 99 12. A. Evans, J. Hutchinson and M. Ashby, “Multifunctionality of Cellular Metal Systems”. Program Material Science, 1999, 43, pp. 171-221. 13. S. Gu, T. Lu and A. Evans, “On the Design of 2D Cellular Metals For Combined Heat Dissipation and Structural Load Capacity”. International Journal of Heat and Mass Transfer, 2001, 44, pp. 2163-2175. 14. T. Kim, H. Hodson and T. Lu, “Fluid-Flow and Endwall Heat-Transfer Characteristics of an Ultra Light Lattice-Frame Material”. International Journal of Heat and Mass Transfer, 2004, 47, pp. 1129-1140. 15. J. Tian, T. Kim, T. Lu, H. Hodson, D. Queheillalt and H. Wadley, “The Effects of Topology Upon Fluid-Flow and Heat-Transfer within Cellular Cooper Structures”. International Journal of Heat and Mass Transfer, 2004, 47, pp. 317318. 16. N. Wicks and J. Hutchinson, “Optimal Truss Plates”. International Journal of Solids and Structures, 2001, 38, pp. 5165-5183. 17. W. Goldsmith and D. Louie, “Axial Perforation of Aluminum Honeycombs By Projectiles”. International Journal of Solids and Structures, 1995, 32, pp. 10171046. 18. F. Côté, V. Deshpande, N. Fleck and A. Evans, “The Compressive and Shear Responses of Corrugated and Diamond Lattice Materials”. International Journal of Solids and Structures, In Press, Corrected Proof, Available online 21 September 2005. 19. H. Wadley, “Multifunctional Periodic Cellular Materials”. Philosophical Transactions of the Royal Society A, 2006, 364, pp. 31-68. 20. H. Wadley, N. Fleck and A. Evans, “Fabrication and Structural Performance of Periodic Cellular Metal Sandwich Structures.” Composites Science and Technology, 2003, 63, pp. 2331-2343. 21. S. Brittain, Y. Sugimura, O. Schueller, A. Evans and G. Whitesides, “Fabrication and Mechanical Performance of a Mesoscale Space-Filling Truss System”. Journal of Microelectromechanical Systems, 2001, 10, pp. 113-120. 22. J. Wallach and L. Gibson, “Mechanical Behavior of a Three-dimensional Truss Material”. International Journal of Solids and Structures, 2001, 38, pp. 71817196. 23. J. Zhou, P. Shrotiriya and W. Soboyejo, “On the Deformation of Aluminum Lattice Block Structures from Struts to Structure”. Mechanics of Materials, 2004, 36, pp. 723-737. 100 24. V. Deshpande, N. Fleck and M. Ashby, “Effective Properties of the Octet-Truss Lattice Material”. Journal of Mechanics and Physics of Solids, 2001, 49, pp. 1747-1769. 25. A. Evans, J. Hutchinson, N. Fleck, M. Ashby and H. Wadley, “The Topological Design of Multifunctional Cellular Metals”. Progress in Materials Science, 2001, 46, pp. 309-327. 26. F. Zok, S. Waltner, Z. Wei, H. Rathbun, R. McMeeking and A. Evans, “A Protocol for Characterizing the Structural Performance of Metallic Sandwich Panels: Application to Pyramidal Truss Cores”. International Journal of Solids and Structures, 2004, 41, p. 6249-6271. 27. J. Wang, A. Evans, K. Dharmasena and H. Wadley, “On the Performance of Truss Panels with Kagomé Cores”. International Journal of Solids and Structures, 2003, 40, p. 6981-6988. 28. H. Karlsson, S. Torquato and A. Evans, “Simulated Properties of Kagomé and Tetragonal Truss Core Panels”. International Journal of Solids and Structures, 2003, 40, p. 6989-6998. 29. H. Wadley, "Cellular Metals Manufacturing". Advanced Engineering Materials, 2002, 10, pp. 726-733. 30. A. Hanssen, L. Enstock and M. Langseth, “Close-Range Blast Loading of Aluminum Foam Panels”. International Journal of Impact Engineering, 2002, 27, pp. 593-618. 31. D. Radford, V. Deshpande and N. Fleck, “The Use of Metal Foam Projectiles to Simulate Shock Loading on a Structure”. International Journal of Impact Engineering, 2005, 31, pp. 1152-1171. 32. D. Radford, V. Deshpande and N. Fleck, “The Response of Clamped Sandwich Beams Subjected to Shock Loading.” International Journal of Impact Engineering, 2006, 32, pp. 968-987. 33. H. Rathburn, D. Radford, Z. Xue, J. Yang, V. Deshpande, N. Fleck, J. Hutchinson, F. Zok and A. Evans, “Performance of Metallic Honeycomb-Core Sandwich Beams Under Shock Loading”. International Journal of Solids and Structures, 2004, 43, pp. 1746-1763. 34. D. Radford, G. McShane, V. Deshpande and N. Fleck, “The Response of Clamped Sandwich Plates with Lattice Core Subjected to Shock Loading”. International Journal of Solids and Structures, 2006, 43, pp. 2243-2259. 101 35. Military Specification, Armor Plate, Steel, Wrought, Homogenous, MIL-A12560H. 36. Z. Xue and J. Hutchinson, “A Comparative Study of Impulse-Resistant Metal Sandwich Plates”. International Journal of Impact Engineering, 2004, 30, pp. 1283-1305. 37. B. Gama, T. Bogetti, B. Fink, C. Yu, T. Claar, H. Eifert and J. Gillespie. “Aluminum Foam Integral Armor: A New Dimension in Armor Design”. Composite Structures, 52, p. 381-395. 38. U.S. Army Research Laboratory Technical Report ARBRL-MR-03097, “ArmorPenetrator Performance Measures”, Konrad Frank, 1981. 39. A. Almohandes, M. Abdel-Kader and A. Eleiche, “Experimental Investigation of the Ballistic Resistance of Steel-Fiberglass Reinforced Polyester Laminated Plates”. Composites Part Part B, 1996, 27B, pp. 447-458. 40. G. Ben-Dor, A. Dubinsky and T. Elperin, “On the Ballistic Resistance of MultiLayered Targets with Air Gaps”. International Journal of Solids and Structures, 1998, 35, pp. 3097-3103. 41. J. Radin and W. Goldsmith, “Normal Projectile Penetration and Perforation of Layered Targets”. International Journal of Impact Engineering, 1988, 7, pp. 229–259. 42. R. Corran, P. Shadbolt and C. Ruiz, “Impact Loading of Plates – An Experimental Investigation”. International Journal of Impact Engineering, 1983, 1, pp. 2-22. 43. ASM Metals Handbook, Vol. 1, 10th ed., ASM International, 1990. 44. S. Shun-cheng, D. Gui-bao and D. Zu Ping, “Martensitic Transformation under Impact with High Strain Rate”. International Jounral of Impact Engineering, 2001, 25, pp. 755-765. 45. W. Lee, J. Shyu and S. Chiou, “Effect of Strain Rate on Impact Response and Dislocation Substructure of 6061-T6 Aluminum Alloy”. Scripta Materialia, 2000, 42, pp. 51-56. 46. S. Yadav and G. Ravichandran, “Penetration Resistance of Laminated Ceramic/Polymer Structures”. International Journal of Impact Engineering, 2003, 5, pp. 557-574. 47. N. Naik and P. Shrirao, “Composite Structures under Ballistic Impact”. Composite Structures, 2004, 66, pp. 579-590. 102 48. G. Zhu, W. Goldsmith and C. Dharan, “Penetration of Laminated Kevlar by Projectiles-I Experimental Investigation”. International Journal of Solid and Structures, 1992, 29, pp. 399-419. 49. R. Subramanian and S.J. Bless, “Penetration of Semi-Infinite AD995 Alumina Targets By Tungsten Long Rod Penetrators From 1.5 to 3.5 km/s”. International Journal of Impact Engineering, 1995, 17, pp. 807-816. 50. R. Woodward, W. Gooch, R. O’Donnell, W. Perciballi, B. Baxter et al., “A Study of Fragmentation In the Ballistic Impact of Ceramics”. International Journal of Impact Engineering, 1994, 15, pp. 605-618. 51. H. Hertz, Miscellaneous Papers. Jones and Scotts, 1965. 52. A. Fischer-Cripps, Introduction to Contact Mechanics. Springer, 2000. 53. K. Johnson, Contact Mechanics. Cambridge University Press, 1985. 54. C. Hardy, C. Baronet and G. Tordion, “The Elastic-Plastic Indentation of a HalfSpace by a Rigid Sphere”. International Journal of Numerical Methods, 1971, 3, pp. 451-462. 55. P. Follansbee and G. Sinclair, “Quasi-Static Normal Indentation of an ElasticPlastic Half-Space by a Rigid Sphere”. International Journal of Solids and Structures, 1981, 20, pp. 81-91. 56. K. Kimvopoulos, “Elastic-Plastic Element Analysis of a Layered Elastic Solid in Normal Contact with a Rigid Surface”. Journal of Tribology, 1988, 111, pp. 477485. 57. G. Care and A. Fischer-Cripps, “Elastic-Plastic Indentation Stress Fields Using the Finite Element Method”. Journal of Material Science, 1997, 32, pp. 56535659. 58. C. Jackson and S. Yang, “Impact on Plates and Shells”. Journal of Solids and Structures, 1971, 7, pp. 445-458. 59. H. Hopkins and H. Kolsky, In: Proceeding of the 4th Hypervelocity Impact Symposium. APGC-TR-60-39, 1, 1960. 60. W. Goldsmith, NAVWEPS Report 7812, NOTS TP 2811. U.S. Naval Ordnance Test Station, China Lake, California, 1962. 61. W. Goldsmith, In Kurzzeitphysik (High-Speed Physics), pp. 620-658. SpringerVerlag, Berlin, 1967. 103 62. W. Goldsmith, Impact. Arnold, New York, 1960. 63. W. Goldsmith, Sciènces et Techniques de l’Armement, Memorial de l’Artillerie française, 1974, 48, pp. 849-853. 64. M. Cook, Journal of Applied Physics, 1959, 20, pp. 725. 65. A. Olshaker and R. Bjork, Proc. 5th Symposium on Hypervelocity Impact. 1962, 1, pp. 225-239. 66. J. Rinehart and J. Pearson, Behavior of Metals under Impulsive Loads. Dover, New York, 1965. 67. L. Fugelso and F. Bloedow, DDC. Ad 636 224, 1966. 68. R. Sedgwick, Tech. Rpt. AFATL-TR-68-61. Air Force Armament Laboratory, Eglin Air Force Base, 1968. 69. M. Backman and W. Goldsmith, “The Mechanics of Penetration of Projectiles into Targets”. International Journal of Engineering Science, 1978, 16, pp. 1-99. 70. G. Corbett, S. Reid and W. Johnson, “Impact Loading of Plates and Shells by Free-Flying Projectiles: A Review”. International Journal of Impact Engineering, 1996, 18, pp. 131-230. 71. P. Shadbolt, R. Corran and C. Ruiz, “A Comparison of Plate Perforation Models in the Sub-Ordnance Velocity Range”. International Journal of Impact Engineering, 1983, 1, pp. 23-49. 72. J. Awerbuch and S. Bodner, “Analysis of the Mechanics of Perforation of Projectiles in Metallic Plates”. International Journal of Solids and Structures, 1974, 10, pp. 671-684. 73. M. Langseth and P. Larsen, “The Behavior of Square Steel Plates Subjected to a Circular Blunt Ended Load”. International Journal of Impact Engineering, 1992, 12, pp. 617-638. 74. I. Marom and S. Bodner, “Projectile Perforation of Multi-Layered Beams”. International Journal of Mechanical Science, 1979, 21, pp. 489-504. 75. T. Wierzbicki and F. Hoo, MS. Deformation Perforation of a Circular Membrane Due to Rigid Projectile Impact. 76. M. Ravid and S. Bodner, “Dynamic Perforation of Viscoplastic Plates by Rigid Projectiles”. International Journal of Engineering Science, 1983, 21, pp. 577591. 104 77. T. Børvik, M. Langseth, O. Hopperstad and K. Malo, “Ballistic Penetration of Steel Plates”. International Journal of Impact Engineering, 1999, 22, pp. 855886. 78. W. Thompson, “An Approximate Theory of Armour Penetration”. Journal of Applied Physics, 1955, 26, pp. 80-82. 79. G. Corbett and S. Reid, “Quasi-Static and Dynamic Local Loading of Monolithic Simply-Supported Steel Plates”. International Journal of Impact Engineering, 1993, 13, pp. 423-441. 80. N. Wang, Journal of Applied Mechanics, 1970, 37, pp. 431. 81. N. Cristescu, Dynamic Plasticity. North-Holland, 1967. 82. P. Beynet and R. Plunkett, Experimental Mechanics, 1971, 11, pp. 64. 83. L. Fugelso and F. Bloedow, DDC. AD., 1966, 636, pp. 224. 84. P. Chevrier and J. Klepaczko, “Spall Fracture: Mechanical and Microstructural Aspects”. Engineering Fracture Mechanics, 1999, 63, pp. 273-294. 85. A. Dremin and A. Molodets, “On the Spall Strength of Metals”. In: Proceedings of the International Symposium on Intense Dynamic Loading and Its Effects. Beijing: Pergamon Press, 1986. pp. 13-22. 86. R. Recht, “Catastrophic Thermoplastic Shear”. Journal of Applied Mechanics, 1964, 31, pp. 189-193. 87. R. Woodward, “The Interrelation of Failure Modes Observed in the Penetration of Metallic Targets”. International Journal of Impact Engineering, 1984, 2, pp. 121129. 88. J. Liss, W. Goldsmith and J. Kelly, “A Phenomenological Penetration Model of Plates”. International Journal of Impact Engineering, 1983, 4, pp. 321-341. 89. G. Irwin, Fracture Dynamics in Fracturing of Metals, American Society of Metals, Cleveland, 1948. 90. H. Bethe, An Attempt at a Theory of Armor Penetration, Frankford Arsenal, 1941. 91. B. Landkof and W. Goldsmith, “Petaling of Thin, Metallic Plates during Penetration by Cylindro-Conical Projectiles”. International Journal of Solids and Structures, 1985, 21, pp. 245-266. 105 92. M. Kipp, D. Grady and J. Swegle, “Numerical and Experimental Studies of HighVelocity Impact Fragmentation”. International Journal of Impact Engineering, 1993, 14, pp. 427-438. 93. C. Calder and W. Goldsmith, “Plastic Deformation and Perforation of Thin Plates Resulting From Projectile Impact”. International Journal of Solids and Structures, 1971, 7, pp. 863-881. 94. H. Bethe, Report No. UN-41-4-23. Frankford Arsenal, Ordnance Laboratory, 1941. 95. G. Taylor, Q. Journal of Mechanics and Applied Mechanics, 1948, 1, pp.103. 96. W. Herrman and A. Jones, ASRL Report No. 99-1. Massachusetts Institute of Technology, Aeroelastic and Structures Research Laboratory, 1961. 97. ASTM International E8-01 Standard Test Methods for Testing of Metallic Materials, 2001. 98. MatWeb Material Data Property (Retrieved December 2005). December 30, 2005 from http://www.matweb.com Retrieved on 99. Metals Handbook, 10th Edition, Vol. 1, Properties and Selections: Irons, Steels and High Performance Alloys, ASM International, Materials Park, OH 44073, 1990. 100. PMC 780 Dry and PMC 780 Wet Industrial Liquid Rubber Compounds (January 2002). Retrieved on April 4, 2005, from http://www.smooth-on.com/ PDF/780. pdf 101. American Gas Association Engineering Glossary (February 2005). Retrieved on May 10, 2005, from http://www.aga.org/Content/NavigationMenu/About_ Natural_Gas/Natural_Gas_Glossary/Natural_Gas_Glossary_(E).htm#E 102. Crosslink Technology Inc. Formulated Epoxies, Urethanes - Custom Cast Parts (September 9, 2002). Retrieved on April 4, 2005, from http://66.146.131.130/data /PDFFiles/clc1d-078a_clc1d-078b.pdf 103. Modulated DSC Theory, TA Instruments Application Brief, TA-211. 104. F. Danusso, M. Levi, G. Gianotti, and S. Turri, “End Unit Effect on the Glass Transition Temperature of Low-Molecular Weight Polymers and Copolymer”. Polymer, 2003, 34, pp. 3687-3693. 105. T. Chen, J. Chui, and T. Shieh, Macromolecules, 1997, 30, pp. 5068-5074. 106 106. J. Ferry, Viscoelastic Properties of Polymers, 3rd Ed. Wiley, 1980. 107. A. Squires, A. Tajbakhsh and E. Terentjev, Macromolecules, 2004, 37, pp. 16521659. 108. Polypropylene Impact Resistance by Dynamic Mechanical Analysis, TA Instruments Application Brief, TA-130. 109. S. Jafari and A. Gupta, Journal of Applied Polymer Science, 2000, 78, pp. 962971. 110. D. Singh, V. Malhotra and J. Vats, Journal of Applied Polymer Science, 1999, 71, pp. 1959-1968. 111. Source book on brazing and brazing technology, American Society for Metals; 1980. 112. Brazing handbook. Miami: American Welding Society; 1991. 113. R. Zee and C. Hsieh, “Energy Absorption Processes in Fibrous Composites”. Materials Science and Engineering A, 1998, A246, pp. 161-168.
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