CP620, Shock Compression of Condensed Matter - 2001 edited by M. D. Furnish, N. N. Thadhani, and Y. Horie 2002 American Institute of Physics 0-7354-0068-7 OUTPUTS OF SHOCK-LOADED SMALL PIEZOCERAMIC DISKS Jacques A, Charestl and Jonathan Lee Mace 2 President ofDynasen Inc, 20 Arnold Place, Goleta, CA 93117 DX-2, Los Alamos National Laboratory, Los Alamos, NM 87545 2 Abstract. Thin small-diameter polycrystalline Lead-Zirconate-Titanate piezoceramic disks were shock loaded in the DSS orientation over a stress range of 0.1-30 GPa. Their electrical outputs were discharged into 50 Q viewing resistors, producing typically 0.15 [is quasi-triangular impulses ranging from 50-700 V. The gas gun flat plate impact approach and the high explosives (HE) plane wave lens approach were used to load piezoceramic elements. These piezoceramic elements consisted of 0.25 mm thick and 1.32 mm diameter disks that were ultrasonically machined from 25 mm piezocrystal disks of type APC 850, commercially produced by American Piezo Ceramic Inc. To facilitate our experiments, the piezoceramic elements were coaxially mounted at the tip of a 2.35 mm diameter brass tube, an arrangement that is commercialized by Dynasen, Inc. under the name Piezopin of model CA-1136. Simple calculations on the electrical outputs produced by these piezoceramic disks reveal electrical outputs in excess of 3000 W. Such short bursts of electrical energy have the potential for numerous applications where critical timing is needed to observe fast transient events. capable of producing a short-duration high-output electrical signal when impacted by a fast moving object, a shock wave or a strong blast. INTRODUCTION The use of piezoceramic materials has virtually exploded over the past 20 years. Indeed, to describe all their applications would require numerous publications. This company, being a manufacturer and developer of shock sensors, has of course utilized various types of piezoelectric materials to construct many of its sensors. As several experimenters know, we have supplied our sensors to nearly all US DOE and DOD laboratories and to several oversea research organizations engaged in fundamental research of shock physics or ammunition testing. One of our particular products, which we call the Piezopin, has been used intensively by shock wave physicists over the past thirty years because of its low cost and high output performance reliability. To date, Piezopins have been utilized primarily for event timing and triggering of instrumentation. Despite their great popularity at many research laboratories, relatively little quantitative information has been published on their output performance under shock wave loading or on potential applications. This particular study is concerned with the highoutput short-duration impulse capability of small piezoceramic elements. The experiments presented in this paper focus on results obtained by utilizing Dynasen s Piezopin configuration when subjected to a wide range of dynamic loads. Two series of controlled tests were conducted to investigate the output of these Piezopins. The first series of tests was conducted at Dynasen s impact facility using gas gun-driven plane wave impact tests of 0-10 A Piezopin is a small and simple coaxial device that utilizes a thin piezoceramic disk as its detector. It is 1153 Eleven gas gun tests and six HE plane wave lens tests were performed, each consisting of six to eight Piezopins, plus several of Dynasen s Carbon Film or Low Impedance Manganin gauges, depending on the pressure range, for accurate recording of shock pressure and shock arrival times. Standard shock matching techniques were used to calculate pressure in Teflon gauge packages. GPa, whereas the second series of tests, 10-30 GPa, was conducted at Los Alamos National Laboratory (LANL) using HE lenses. The experimental approach for these tests is described next, followed by a brief data summary and some conclusions. EXPERIMENTAL APPROACH The intent of these experimental series was to develop well characterized small, passive gauge elements that can be used in applications where critical timing information from fast transient events is transmitted to a receiver from an antenna or wave guide. These experiments demonstrated that short, high power bursts of electrical energy from small dipolar piezoceramic disks potentially satisfied these requirements. Also, they provided Hugoniot data up to about 80 kbar. In the experiments reported Piezopins were oriented such that the surface of a small dipolar piezoceramic disk was parallel to an incident shock. When shock loaded, this dipolar separation of charge is compressed on the time scale of shock dynamics, thereby producing a large electrical impulse across 50 Q that is recorded onto various digitizers via coaxial cable. Figure 1 shows the basic construction of Dynasen s Piezopin, whereas Figures 2-3 illustrate the gas gun and HE testing approaches. Target Assembly FIGURE 2. Typical gas gun assembly; 0-10 GPa. A flyer, mounted on the front of a projectile, is fired from a gas gun into the target assembly at normal incidence to the piezopins. Each target assembly typically consisted of multiple Piezopins and Carbon Film gauges. Figure 2 illustrates the typical gas gun flyer and target assemblies utilized in experiments at Dynasen s impact facility. During initial experiments we began to observe large variations in (P9V) data points as successive tests in this experimental series produced higher impact pressures; where P is pressure and V is voltage across 50 Q. Thin wall nrass tube 0.093"xl" Our initial guess as to why this variation occurred had to do with the fact that a small copper film was vapor deposited over the front surface of the Piezopin in order to form a complete circuit (Fig. 1). The large voltage spikes that developed over the circuit (3000 W average power) caused us to believe that the integrity of this thin film of copper was questionable over the duration of the pulse. Therefore, this copper film was replaced by a thin copper disk. This resulted in only slightly better data. pei0ci*ramic disk " O.Q52"x0.01Q" FIGURE 1. Construction of the Dynasen Piezopin. The piezoceramic disk contains a dipolar charge separation and is the active element. The surface of this element is grounded to the brass tube via a thin Cu disk, and the backside is connected to the brass rod, thus providing a convenient arrangement for coaxial transmission of the electrical impulse induced by the incident shock. 1154 We now realize that this measured scatter in data (see Fig. 6) probably results from dipolar variations between individual piezoceramic disks. These small disks were ultrasonically machined from much larger piezoceramic crystals with no control over variations in dipolar properties. Nevertheless, the significant measured outputs of these small passive elements should be noted. Figure 4 is on the order of O.l-jJs. This time is related to shock transit time in the piezoceramic material. A simple Gaussian is fit to this data in order to illustrate the average power and frequency content (Fig. 5) of a typical pulse. These frequencies are such that electromagnetic transmission through air and time resolved reception should be viable. Typical Pube Voltage accrass 5K1 Gaussian Fit: Average Power: ; i p (£ ( t ) ) 2 t2 - ti jt; (R = 50 Q) ddt =2125 W FIGURE 4. Typical pulse from a shocked 0.052 inch x 0.010 inch piezoceramic element. A Gaussian is fit to the data and is used to illustrate the average power and frequency content of a typical pulse. | x 10~4 Fourier Transform of the Ganssian Fit FIGURE 3. HE plane wave assembly; 10-30 GPa. A 4 inch plane wave lens produces a flat detonation wave in the HE booster material, which in turn produces a flat shock in the attenuation package that becomes incident on the Teflon. The gauge plane consists of an array of piezoceramic elements and low impedance Manganin gauges. A Faraday cage is used to isolate the gauge plane and cables from electrical noise inherent in the detonation front. 1.25 1 0.75 0.5 0.25 0 Figure 3 illustrates the HE plane wave lens experimental arrangement. In each experiment both the 1/2 inch booster and the attenuation pack were chosen such that the shock matched pressure transmitted into the Teflon gauge package varied from 10 to 30 GPa. This pressure was verified using low impedance Manganin gauges. FIGURE 5. Frequency content of a typical pulse from a shocked piezoceramic element. Figures 6-7 provide a summary of measured peak output voltage across 50 Q and measured Hugoniot data. The data of Figure 6 demonstrate that peak pulse voltages from 300 to 700 V can be expected over a range of about 20 to 350 kbar. Notice the large scatter in data. We think this scatter is largely Figures 4-5 illustrate a typical pulse whereas Figures 6-7 provide a summary of measured data. Notice that the duration of the pulse illustrated in 1155 due to dipolar variations between piezoceramic elements. We expect that this scatter is due to polycrystaline nature of material, a property that is not detectable by the Hugoniot measurements of Figure 7. CONCLUSIONS These experiments demonstrate that a small, passive piezoceramic element can produce a highpower pulse over frequencies of up to 1-200 MHz when shock loaded. There are, of course, many potential applications that can be imagined for such small, non-intrusive, passive elements. In particular, electromagnetic transmission through air should be viable. APC 850: peak voltage across 50O Furthermore, we suspect that the development of a method for producing consistent dipolar characteristics between individual piezoceramic elements should eliminate much of the data scatter seen on Figure 6. Further investigations on the subject are expected to yield more insights on the process of shock loading APC 850 polycrystal piezopceramic. FIGURE 6. Peak voltage output of shock loaded 0.052 x 0.010 piezoceramic elements. Each point represents the output average of 6 or 8 piezopins. ACKNOWLEDGEMENTS This work was funded under Los Alamos National Laboratory contract numbers 100554-001, 100554009X and 16326-001-009X. REFERENCES 0.2 0.4 0.6 0.8 Particle Velocity (mm\jo,s) Stanley P. Marsh, Editor. LASL Shock Hugoniot Data, Publisher: University of California Press, 1980 FIGURE 7. APC 850 Lead-Zirconate-Titanate Hugoniot measurements (p=1.5 glee) and Lead-Zirconium-Titanate (p=l.H4 glee} data from the LASL Shock Hugoniot Data handbook. Figure 7 provides six measured Hugoniot points of APC 850 over a range of 0-80 kbar. The slope of the resulting line is about 268 kbarl(mml s ). These results were obtained from gas gun tests performed at Dyansen, and are the first published results for APC 850 that we are aware of (1). 1156
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