CP620, Shock Compression of Condensed Matter - 2001 edited by M. D. Furnish, N. N. Thadhani, and Y. Horie © 2002 American Institute of Physics 0-7354-0068-7/02/$ 19.00 THE STUDY OF INTERNAL DEFORMATION FIELDS IN GRANULAR MATERIALS USING 3D DIGITAL SPECKLE X-RAY FLASH PHOTOGRAPHY H,T. Goldrein, S.G. Grantham, W,G. Proud, J.E. Field Cavendish Laboratory, Madingley Road, Cambridge, CBS OHE. UK Abstract. Digital Speckle X~ray Flash Photography is a technique which combines Digital Speckle Photography with Flash X-Ray Photography to measure 2- and 3-D displacement fields within dynamically deforming specimens. Measurements are made throughout a plane within the specimen seeded with X-ray opaque particles. This technique has already been successfully applied to the study of polyester, cement1 and sand2, and is used here to study the influence of water on a sand bed under impact from a hemispherical-tipped copper rod travelling at 100 m s"1. Significant differences in the response of dry and wet sand beds were detected, and examples of the deformation fields measured are illustrated here. These results may be applicable in many spheres, for example, in the design of mechanisms to destroy buried ordnance. the "gauge" (the lead filings) is of the same dimension as the sand grains, introduces an insignificant perturbation in the sample, and no leads or power supply are required. The method provides very data rich results with x and y components of displacement obtained at every point on the plane to a resolution defined by the fourier sampling size chosen in the analysis. Here sand in both dry and saturated states has been subjected to an impact from a copper rod and the effect of the moisture in the sand studied. INTRODUCTION Being able to measure the internal response of sand to shock and ballistic impacts is of great use in many fields. One possible application is in the destruction of ordnance which are often buried in sand. There have been investigations into the penetration behaviour of shaped charges travelling through sand3, but it is very difficult to obtain dynamic measurements of the sand's response. The technique described here is known as digital speckle X-ray flash photography which uses digital speckle photography (DSP) combined with flash X-rays, Standard DSP algorithms are used4, but instead of producing the speckle pattern by white light or laser methods we instead seed a specimen with a sprinkled layer of X-ray opaque filings. A specimen such as sand lends itself naturally to this technique because of the granular nature of the material, and the relative ease of producing a specimen that incorporates a layer of lead filings at a chosen depth in the sample. The difficulty associated with mounting conventional gauges in a granular material also demonstrates the advantageous nature of this technique. In this case EXPERIMENTAL The sand used for this study was fraction C (David Ball Group pic, Huntingdon Road, Bar Hill, Cambridge, CBS 8HN, England), which has a grain size ranging from 300 to 600 |im. The projectile was a round ended copper (XM) rod with a diameter of 5.0 ± 0.1 mm, a length of 50.0 ± 0.5 mm and a mass of 8.6 ± O.lg. To find how much water was needed to achieve 100 % saturation of the sand, a volume of sand was placed in a measuring cylinder and a known volume of water 1105 Figure, la. 120 us delay, dry (displacement vectors x3). Figure.lb. 120 us delay, saturated (displacement vectors x3). Figure. 2a. 240 us delay, dry (displacement vectors x3). Figure. 2b. 240 us delay, saturated (displacement vectors x3). Figure. 3a. 360 us delay, dry (displacement vectors x3). Figure. 3b. 360 us delay, saturated (displacement vectors x3). 1106 added and left to soak through the sand. The volume of supernatant water could then be subtracted away from the total added, and the water/sand ratio and its density could then be calculated. The samples were prepared in PMMA (poly methyl methacry late) containers, with dimensions of 60 x 70 x 30 mm3, (the 60 x 30 mm2 face being the impact face) filled to a depth of 10 mm with sand. The lead layer was introduced at a depth of 5 mm. A sand depth of 10 mm was chosen to give the optimal exposure of the film using our ISOkeV X-ray heads. The X-ray flashes had a duration of 30 ns. The projectile was fired at 100 ± 3 m s"1, and X-ray photographs were taken at delays of 120 JLLS, 240 jus, and 360 jus after impact, for both the dry and saturated samples. To investigate more quantitatively the displacement ahead of the projectile, graphs have been plotted of the y-component of displacement 0.15 i . . . . . . . . . . X -a— Saturate i 1 '7 ; ': ^l> : N f ja ** -0.05 lw>"^^ -0.1 : y« : x*i^ Nfc j/ -n 1*5 5 10 15 • 20 25 Distance Ahead of Project: Fig. 4a. Displacements ahead of projectile, 120 ps. 0.5 a— 33ry 0.4 RESULTS -fl— Saturate 1 The results of these experiments can be seen in figures la to 3b. In each of these pictures, the bolts used to stop the sample container from moving backwards during the impact can be clearly seen, as can the fiducial marker region at the bottom of each picture below the bolts. This region enables the rigid body motions introduced by the scanning process to be calculated and subtracted. The displacement vectors in these images have been scaled up by a factor of three to make them more visible. A comparison of the 120 jis impacts shows that there is some movement away from the tip of the projectile in the dry case, but very little obvious movement in the saturated case with the displacements appearing quite noisy. This noisy displacement map is probably due to out-of-plane motions being comparable in magnitude to the inplane motion. By 240 jus after impact larger displacements occur ahead of the projectile in the saturated case than in the dry case. After 360 (is it is clear that there is more bulk motion occurring ahead of the projectile in the saturated case than in the dry case. In all of these images, the response of the sand to the impact is to flow away from the rod, both forward and to the sides, in a manner that is more hydrodynamic in behaviour than the response a solid would exhibit. It is also possible to see the effect of cavitation to the sides of the rod in all these results (indicated by "C" in Fig. 3a). It causes a change in density in the sand which is apparent as a lighter shade in the X-ray image. 5 10 15 20 25 Distance Ahead of ftrolect; Fig. 4b. Displacements ahead of projectile, 240 jis. Fig 4c. Displacements ahead of projectile, 360 |js. ahead of the projectile. In figure 4a to 4c, the result of averaging the 4 columns of the displacement vectors in the centre of the image, 21 mm in front of the projectile can be seen. The dry sample is represented by the solid line, and the saturated sample by the dashed line. From these graphs it is clear that in the 120 jis case there is very little 1107 difference between the two graphs, with the displacement reducing quite gradually further from the projectile tip. At 240 jus, the displacements in the dry sand have changed little, whereas in saturated sand the displacements are larger directly ahead of the projectile, and remain relatively constant at approximately 0.2 mm further into the target. By 360 jus the disparity between the two cases is quite pronounced. The dry sand has remained very similar to the 240 jus case with very little change, whereas the saturated sand has moved significantly further, the graph being relatively flat throughout. The behaviour seen in these plots can be explained by considering the effect that saturation has on the sand. The more open structure of the dry sand enables it to compact and move away from the projectile to the sides and even slightly backwards, this reduces the overall effect of bulk forward motion. In the saturated case, however, the sand cannot compact in the same way since the cavities are already filled with water, effectively an incompressible fluid at these pressures. Consequently the sand appears to move more like a rigid body ahead of the projectile. ACKNOWLEDGEMENTS The authors would like to thank Dr. I. G. Cullis (Defence Evaluation and Research Agency (DERA), UK, for his advice and encouragement. The research is supported, in part, by the Engineering and Physical Sciences Research Council. REFERENCES 1. Synnergren, P., Goldrein, H.T., Proud, W.G., Appl. Opt, 38,4030-4036 (1999). 2. Grantham, S.G., Proud, W.G., Goldrein, H.T., Field, J.E., "The Study of Internal Deformation Fields in Granular Materials Using 3-D Digital Speckle X-Ray Flash Photography," in Laser Interferometry X: Applications-2000, edited by G.M. Brown, W.P.O. Juptner, and RJ. Pryputniewicz, Proceedings of SPIE 4101, San Diego, USA, 2000, pp. 321-328. 3. Resnyansky, A.D., Wildegger-Gaissmaier, A.E., "Hydrocode Modelling of High-Velocity Jet Penetration Into Sand," in Proceedings 19lh International Symposium of Ballistics-200, edited by I.R. Crewther IBS Conference Proceedings, Interlaken, Switzerland, 2001, pp. 1561-1567. 4. Sjodahl, M., Benckert, L.R., AppL Opt. 32, 22782284(1993). 5. Goldrein, H.T., Synnergren, P., Proud, W.G., 'Three-Dimensional Displacement Measurements Ahead of a Projectile," in Shock Compression of Condensed Matter-1999, edited by M.D. Furnish, L.C. Chhabildas, and R.S. Hixson, AIP Conference Proceedings 505, Snowbird, Utah, 1999, pp. 10951098. CONCLUSION A series of experiments have been carried out on sand utilising the technique of digital speckle Xray flash photography. The measurements which have been made of the internal displacements of dry and moist sand would not have been possible using any other existing technique. It was shown that there was a measurable difference between the response of the dry and saturated sand when subjected to identical impacts. The purpose of this research was to validate the use of this technique when applied to granular materials, and its ability to make useful comparative studies. With this proven, the technique can now be used for more interesting and realistic situations, and we are currently in the process of scaling up the experiment to study impacts from shaped charge jets on sand beds and using a stereoscopic geometry with two X-ray heads5. This will allow out of plane motion to be measured as well, reducing the errors in the in-plane measurements. 1108
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