CP620, Shock Compression of Condensed Matter - 2001 edited by M. D. Furnish, N. N. Thadhani, and Y. Horie © 2002 American Institute of Physics 0-7354-0068-7/02/$ 19.00 MACRO - MESO ENERGY EXCHANGE IN DYNAMICALLY DEFORMED STEELS Yuri I. Mescheryakov Institute of Problems of Mechanical Engineering RAS, St.Petersburg 199178, Russia Abstract. Dependence of spall-strength on the intensity of the energy exchanges between macroscopic and mesoscopic scale levels is experimentally studied for four kinds of steels having different chemical composition and thermal treatments. For all the kinds of steel the spall-strength is shown to be maximum when velocity dispersion at the mesolevel equals velocity loss at the plateau of compressive pulse, which corresponds to equilibrium state of energy exchange between scale levels. structure re-arrangement of a dynamically deformed material reveals via the shock-induced change of the particle velocity dispersion D and velocity loss Au [3,4]: BACKGROUND Commonly used approaches to microstructure description of response of material to impact link the resulting macroscopic behavior with the microstructure data obtained after dynamic loading. In reality, adequate modeling of dynamic processes should be based on the microstructure kinetics data obtained in real time, i.e. during dynamic processes. To date the only possibility for obtaining in-sit data on the kinetics of microstructure is a measuring of time-dependent velocity dispersion at the free surface of targets in planar shock experiments. The velocity dispersion (or diffusion velocity) can be measured with the laser interference technique and has a statistical meaning [1,2]. In considering the microstructure aspects of dynamic deformation it should be ascertained that experimentally determinable kinetic characteristics obtained with interference technique are those belonging to the mesoscopic scale level which occupies an intermediate position between atomdislocation and macrolevel. In this connection it should be noticed that as distinct from the quasistatic situation, in a dynamically loaded medium mesolevel is not a completed structure. It is a specifically transient structure where both a scale of structure elements and energy capacity of mesolevel currently change. The specifics of Au= cm(dD/du) (1) Here cm = dE/ dD is the mesolevel specific energy capacity. This equation asserts that mass velocity loss is proportional to rate of change of the velocity dispersion in the velocity space. It disappears when the rate of change of dispersion is invariable. The "loss", or decrease of mass velocity, is a quantitative characteristic of the energy exchange between mesoscopic and macroscopic scale levels in non-equilibrium processes. The energy balance in this case [4]: = AuSU-cmD (2) Here AE is the change of internal energy due to non-equilibrium energy exchange between macrolevel and mesolevel. The first term on the right hand side is the energy proportional transportation of the velocity loss over the plastic front. When dispersion at the mesolevel grows faster than the mean mass velocity, AE goes on mesostructure formation. In this situation, energy balance supports owing to decrease of elastic stored energy and scheme of the process is thought to be: 267 W, m/s strain rate increase —+ velocity dispersion growth —» onset of energy exchange —> wave amplitude loss —> decrease of the elastic energy. In opposite situation initially large dispersion decreases and AE goes on increase of mean mass velocity. To check above consideration, four kinds of steel having different chemical composition and thermal treatment have been tested. They have been loaded under uniaxial strain conditions within impact velocity range of 200-550 m/s. < c>, u, m/s 250 248 246 10 EXPERIMENTS AND RESULTS Experiments on shock loading of plane targets were performed by using a light gas gun facility of 37 mm bore diameter. Thickness of targets and impactor were adjusted to provide a spallation. Free surface velocity profiles were recorded using a twochannel velocity interferometer [2]. The technique allows, besides the free surface velocity profile, to determine also a diffusion velocity (c) (or square root of the velocity dispersion) and velocity loss Au. 400 FIGURE 2. Pull-back velocity (1), diffusion velocity (2), velocity loss (3) versus impact velocity (40XCHMA steel, 2-set) a). Results of shock tests for the first set of targets are presented in Fig. 1 which shows that pullback velocity W = f (Uimp), diffusion velocity (c) = f (Uimp) and velocity loss Aw = / (Uimp) dependencies monotonically grow with the impact velocity. It is also seen that within impact velocity range 211-437 m/s diffusion velocity remains being smaller than velocity loss, i.e. (c) « Au. At the same time, it may be noticed that dependencies Au = f(Uimp) and (c) -f(Uimp) have different inclination. Intersection of the curves would happen at the impact velocity of 700 m/s where the pullback velocity is expected to be equal to 250 m/s. The special shot at the impact velocity of 695 m/s has been performed to check that conclusion, which showed the pullback velocity of 247 m/s. Thus, it may be concluded that within impact velocity range of 211-437 m/s this steel does not have optimum spall-strength characteristics. Its thermal treatment corresponds to maximum dynamic strength at the velocity of « 700 m/s. b). Results of shock test for the second set of targets in the form of dependencies W = f (Uimp), (c) =f(Uimp) and Au =f(Uimp) are provided in Fig. 2. Maximum spall-strength (W « 250 m/s) corresponds to the impact velocity of « 490 m/s. Just at that impact velocity the curves (c) -f(Uimp) and Au =f(Uimp) intersect, so that (c) = Au. This is complex alloyed steel, which was studied for two sets of targets of different thermal treatment [5]. u , m/s 50 0 -f—————————I——————————————I- -5 200 250 300 350 400 impact velocity, m/s 500 impact velocity, m/s 40XCHMA steel (HRc 55) m/s 450 450 FIGURE 1. Pull-back velocity (1), diffusion velocity (2) and velocity loss (3) versus impact velocity (40XCHMA steel, 1-set) 268 Microstructure investigations of post-shocked specimens show that in the first set of steel targets spalling looks as a totality of cracks parallel to the free surface of target. This kind of fracture is known to be cleavage. Microstructure mechanisms of dynamic fracture in the second set of 40XCHMA steel turns out to be different at different regions of impact velocity. - Uimp < 500 m/s: (c) > Au. Spall crack has a steplike shape with identical longitudinal and transverse length of step. - Uimp = 500 m/s: (c) = Au. Within the spall zone there is a dense network of short adiabatic shear bands. - Uimp > 500 m/s: (c) < Au. Spall fracture in the form of cleavage. Thus, for both sets of 40XCHMA steel maximum spall-strength corresponds to the strain rate where (c) = Au. On the basis of spall tests of two sets of 40XCHMA steel one can conclude that behavior of diffusion velocity and velocity loss provides information whether the thermal treatment of steel corresponds to the maximum value of dynamic strength. W, u, <c>, m/s 250 200 150 100 180 230 280 330 impact velocity, m/s Figure 3. Fullback velocity (1), velocity loss (2), diffusion velocity (3) versus impact velocity (38XH3M&A st, 2-set) criterion (c) = Au is fulfilled for the entire range of impact velocities under investigation. Accordingly, the pullback velocity is also practically constant. The structural mechanism of dynamic fracture for this steel can be classified as growth of voids within overall range of impact velocities. On comparing two sets of 38XH3M0A steel targets we can conclude that thermal treatment of the second set provides an optimization of dynamic strength properties within more wide range of the impact velocities. However, the value of spallstrength is decreased. 38XH3MOA steel (HRc 39) This is a complex-alloyed Cr-Ni-Mo steel having optimum combination of quasistatic plastic and strength characteristics. To determine its dynamic plasticity and strength characteristics, two sets of targets have been tested under planar conditions. The first set has been prepared from the material as supplied and the second, after thermal treatment, providing a homogenization of structure. a). Results of test for the first set of 38XH3M&A steel targets are provided in Fig. 3. This set of steel targets reveals a non-monotonic behavior of spallstrength on the strain rate. At the impact velocity of ~ 300 m/s, the quantities Au = f(Uimp) and (c) = f(UimP) intersect each other, which corresponds to the criterion (c} = Au. This impact velocity corresponds to the maximum spall-strength of the steel. b). The diffusion velocity (c) =f(Uimp) and velocity loss Au = f(Uimp) lie close to each other, so that, within the limits of scatter of experimental data, the 30XH4M steel (HRc 40) The quantities (c) =f(Uimp)and Au = f (Uimp) lie close to each other within the overall range of impact velocities, so the criterion (c) = Au is fulfilled everywhere while pull-back velocity is invariable (see Fig.4). This means that 30XH4M steel has optimum thermal treatment. Behavior of this steel is similar to that for the second set of 38XH3M0A steel. However this steel has different mechanisms of dynamic plasticity at the mesolevel, mesorotations. As for the mechanism of fracture, 269 W , < c>, a, m/s CONCLUSIONS 250 Together with well-known quasistatic strength characteristics of material an important role in dynamic fracture belongs to kinetic characteristics of microstructure at the mesolevel. The first kinetic characteristic is the velocity dispersion D = c 2 at the mesolevel or diffusion velocity (c), which is a measure of the velocity heterogeneity of dynamic deformation in real time. The second kinetic characteristic is the velocity loss Au. Its value characterizes a quantity of the kinetic energy transferred from macro- to mesolevel. When (c} = Au, the energy exchange is realized under equilibrium conditions. This case corresponds to maximum dynamic strength of material. The mechanism of dynamic fracture corresponding to optimum kinetic characteristics of structure is the step-like cracking at the mesolevel-2 (100-400//w) for ductile steel or network of adiabatic shear bands for brittle steel. For the material where Au »(c) the structural mechanism of the dynamic fracture turns out to be cleavage while the material itself is not in an optimum state from the viewpoint of dynamic strength. 200 150 100 300 350 400 450 500 impact velocity, m/s FIGURE 4. Fullback velocity (1), diffusion velocity (2) and velocity loss (3) versus impact velocity (30XH4M steel) this is step-like cracking at the mesolevel-2 (~ 100 400 fjni) , which is known to be the so-called "horizon" scale of Grady [6]. REFERENCES 28XH3CMBOA steel (HRc 25) 1. Asay, J. R. and Barker, L.M. , J. Appl Phys. 45, 2540-2550 (1974). 2. Mescheryakov, Yu.I. and Divakov, A.K., Dymat J. 1, 271-277(1994). 3. Mescheryakov, Yu.L, "Mesoscopic effects and particle velocity distribution in shock compressed solids". In: "Shock Compression of Condenced Matter-1999"Q&. M.D. Furnish, L.C. Chhabildas, R.S. Nixon. AIP Proceedings 505, Melville, New York. 1999, pp 10651070. 4. Khantuleva, T.A. - Presented to "Shock Compression of Condensed Matter", Atlanta GA, June 24-29, 2001. 5. Mescheryakov, Yu.L, Divakov, A.K., and Zhigacheva, N.I., Material Physics and Mechanics. 3, 63-100, (2001). 6. Grady, D.E. J. of the Mech. and Phys. of Solids, 36, 353- 384, (1988). This steel is commonly used in quenched state. In this study, to provide a high plasticity we use the steel in annealed state. It was expected that this provides the viscous mechanism of fracture. The velocity loss curve for that material lies much higher than the diffusion velocity curve (Au » (c)). Thus, the behavior of kinetic characteristics for this steel is similar to that for the first set of 40XCHMA steel (see Fig.l). Accordingly, the basic mechanism of spall fracture for this steel is cleavage. This result shows that structural mechanisms of dynamic plasticity and fracture are determined by the mutual behavior of kinetic characteristics of mesostructure during the shock loading but not by the quasistatic plasticity and strength of material. 270
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