Electronic Supplementary Information for Dalton Transactions
This journal is © The Royal Society of Chemistry 2008
Electronic Supplementary Information (ESI) for:
Synthesis, structure, and characterization of a new thorium-organic
framework material, Th3F5[(C10H14)(CH2CO2)2]3(NO3)
Kang Min Oka and Dermot O’Hareb,*
a
Department of Chemistry, Chung-Ang University, Seoul, 155-756, Republic of Korea.
b
Chemistry Research Laboratory, University of Oxford, Oxford, OX1 3TA, UK.
*Corresponding Author
Professor Dermot O’Hare
Fax: 44 1865 285131; Tel: 44 1865 285130; E-mail: [email protected]
S1.
Experimental
and
calculated
powder
X-ray
diffraction
patterns
for
Th3F5[(C10H14)(CH2CO2)2]3(NO3)
S2. Thermogravimetric analysis diagram for Th3F5[(C10H14)(CH2CO2)2]3(NO3)
S3. IR spectrum for Th3F5[(C10H14)(CH2CO2)2]3(NO3)
1
S1.
Experimental
and
calculated
powder
X-ray
diffraction
patterns
for
Th3F5[(C10H14)(CH2CO2)2]3(NO3)
2
S2. Thermogravimetric analysis diagram for Th3F5[(C10H14)(CH2CO2)2]3(NO3)
100
95
Weight (%)
90
85
80
75
70
65
60
55
0
100
200
300
400
500
600
700
800
o
Temperature ( C)
S3. IR spectrum of Th3F5[(C10H14)(CH2CO2)2]3(NO3)
Transmittance
100
90
80
4000
3500
3000
2500
2000
1500
1000
500
-1
Wavenumbers (cm )
3