1/2013 AEROMUCO NEWS Introduction Early September 2012 was a key period for AEROMUCO: mid term meeting and the firs review with EU Officer took place • quality and quantity of available commercial enzymes. Survey and definition of testing methods WP1 has completed its activities within the first 18 months of the program. Work Package 2 in Neuchatel, at CSEM premises. Off course, mid term review is a moment of reflection and revision, when it is time to summarize the work performed and plan forward for the future. And it is also time to publish the first AEROMUCO newsletter, where the mentioned synthesizing effort is reported. Work Package 1 This Work Package ackage had three main objectives: Definition of the general • requirements (environmental, functional, aircraft interfaces.) that shall fulfill the multifunctional coatings to be developed. • Definition of the candidate coatings to be evaluated during the project • Review of the available testing test methods (on ground, in flight). According to the objectives, the specifications have been defined and presented in 3 deliverables. • Aerodynamic requirements (erosion, ice & Dirt) • Definition of candidate coatings / coating systems concept – Specifications ons for multifunctional coatings systems. For anti anticontamination aspects, overview of The main objective of this work package is the development of coatings that are able to reduce the accretion and adhesion of ice on aerodynamic surfaces. To achieve this goal, two main tasks have been performed: • Production of nano/micro-structured nano/ polymeric coatings (by CSEM, CREST and PNP) • Surface functionalization of selected coatings with either hydrophobic or hydrophilic components. • The functionalization of the surface with ‘antifreeze’ agent aims at mimicking the properties of proteins of some arctic fishes or insects inhibiting the blood freezing. EADS is responsible for the testing of the developed coatings in regard to their freezing time delay and ice adhesion properties. Si nano/micro-pillars pillars produced by nanosphere lithography ography A wide selection of functional coatings and structured surfaces has been developed. Preparation of structured surfaces: • Tests of embossing of liquid resins supplied by projects partners (collaboration of CSEM with CREST, 2 • • • EADS): really challenging to achieve, since most of the polymers were thermoset resins. Tests of embossing of thermoset coatings (collaboration with CREST, EADS, CASSIDIAN) Tests of moulding of UV-curable resins (collaboration with CREST, PnP, EADS): positive structuration to obtain pillar arrays. Tests of embossing of thermoplast coatings (collaboration with EADS): tricky demoulding step and samples prepared for further characterisation. low values for the adhesion strength to ice. Furthermore, initial testing are undergoing at EADS IW lab icing wind tunnel. Significant progress has been made in the delay of freezing of supercooled droplets on the coatings and the reduction of ice adhesion. The freezing time delay tests performed at EADS mainly show the influence of the roughness and the hydrophobicity. The freezing time delay of the Methacryloxy based sol-gel coatings (CREST) is slightly longer than that of the highly cross-linked, the Flourinated and the PU type coatings of CREST. The Thermally stable sol-gel coating shows the lowest performance in the tests. Referring to the samples modified by CSEM, the PUR A1+F3 coating is slightly better than the HPUR A1+F3 sample. (a) Test article and reference ice shape Work Package 3 The primary objective of this work package is to develop surface coatings or surface modification processes for aircraft leading edges (e.g. on the wing, empennage or nacelle) that are capable of reducing or eliminating the adhesion of biological contaminants, specifically airborne insects. During the first 18 month following main achievements may be listed: • Lateral view of the clamped ice-aluminum composite beam for ice adhesion testing The ice adhesion tests performed at EADS shows that - in particular – the PnP CF Aero 326 - biphasic coating and the CSEM Sol-Gel Coating A1+F3 yield very Development of two insect impact test systems Pressure Chamber Safety Valve Inlet Quick Acting Valve Muzzle Foam cartridges SPIrIT test rig with main components labelled 3 • • • • • • • Development of a protocol to evaluate and rank anticontamination coatings Development of technology for the purification and recovery of enzymes Procurement, evaluation and selection of suitable commercial enzymes for temporary anticontamination coatings Evaluation and selection of analogues to mimic the adhesion characteristics of the reference insect, Drosophila melanogaster (fruit fly). Purification of novel strains of chitinase and protease enzymes for anti-contamination purposes Selection of mesoporous silane zeolites as possible hosts for encapsulating enzymes • • industrial as well as in service applicability and reparability, compatibility, environmental friendly properties sustainability (e.g. erosion resistance) contribution in diminishing ice accretion and ice adhesion when used with or without a qualified active de-icing system To achieve the aims of WP 4, a broad assessment campaign including lab tests has been performed and flight validation is planned. The general work in this work package includes: • Comparison and assessment of erosion test methods including analysis of the resulting damage patterns for proving sustainability of reference and developed coatings. SAAB rain erosion test facility • SEM image of zeolite particles synthesised (TEOS, CTAB+β-CD, Microwave, Calcined at 500◦C) Work Package 4 The main objective of WP 4 is to evaluate the reciprocal interaction of anti-ice, anticontamination and erosion protection properties of the multifunctional coating developed in WP 2 and WP 3, with respect to their: • • Icing wind tunnel tests for determination of the anti-ice/de-icing performance of coating/de-icing system combinations Definition of anti-ice and anti-dirt solution in functionalised coating systems for demonstrator Assessment of interdependency of the functionalities anti-ice, -dirt, erosion when tested altogether 4 The main achievements in this work package include: • Finalisation of an erosion test campaign including facilities at UL, EADS and SAAB. It has been the first time that different kinds of rain erosion methods have been systematically compared. • Definition of demonstrators for IWT/T /T campaign at CIRA Images of samples tested with PJET. • Definition of test parameters for full scale Icing Wind Tunnel tests at CIRA in M30. Work Package 5 The objectives of the WP5 are related to the management and the valorisation of the knowledge created within the project, with the final aim of achieving a wide impact of the project results. WP5, in particular, is aimed at three main objectives: • Allowing easy communication and maximum transparency for all involved partners and increasing the synergy of the cooperation during the project • Undertaking and monitoring actions that will pave the way for broad dissemination of the project results • Setting-up up an Exploitation plan that will define the exploitation path and rules related to the results generated by the project, both internally within the project consortium and extern externally (protection of knowledge) In the first 18 months a web-based portal has been created and published at www.aeromuco.eu by month 6. CIRA IWT test facility • It has been defined that the test articles from SAAB and AAEM (picture beside) need to be tested separately for the sake of more realistic test results. AEROMUCO partners obtained users-ID users and password to access a private section of the portal. WP Leaders possess special rights in order to manage the content of their specific sections, while other members can read, download and pre-upload upload (waiting for WP Leader L approval) documentation. The same internet address also links to the public web page, where everyone can access general information related to AEROMUCO Project including project contents, partners and structure. In addition to this, several dissemination dissem activities already took place, including the 5 publication of scientific articles and the participation to International Conferences. Work Package 6 The main objectives of WP6 are: • To identify and confirm deliverables, milestones, staff levels, materials, external costs, travel and setup of meeting schedules for the partnership • To coordinate and conduct the project according to the work plan • To ensure efficient and high-quality communication between the partners • To ensure a smooth transfer of information (e.g. reports) to and from the Commission • To distribute the financial support paid by the Commission among the partners Conclusion Within the first 18 months of the project, all major tasks regarding coating and test method development have been successfully established. The next phase covers the final assessment of the coating candidates by means of the lab experimental setups. A proposal of the most promising coatings will be prepared and the final down selection for the flight tests and Icing Wind Tunnel testing at CIRA will be carried out in agreement with the industrial advisory board. The IWT/T campaign and the flight test at the Dassault flight test centre at Istres will be performed during the summer 2013. Further major project goals in WP6 are: • Training and exchange of young researchers • Implementing the gender action plan The main achievements have been: • Signature of GPFs • Signature of CA • Signature of Grant Agreement • Templates for reporting created (in collaboration with WP5) • Procedures for reporting and publication established • Homepage created (in collaboration with WP5) • Advanced payment to all the partners • Completed Kick-off meeting, 6M, 12M and 18M technical meetings • Finalised respective deliverables that were sent to the Commission • Completed 18M mid term review • Exchange of researches between several partners 6
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