ULTRASONIC SEALING TOOL DESIGN FOR THIN FILM PLASTICS Miranda Marcus and Olivia Prior, EWI, 1250 Arthur E. Adams Dr., Columbus OH 43221 Abstract Thin film packaging is used for a wide range of products including packaging of food, medical tools, electronics, and toys. Each of these applications requires a different type of film, from thin and brittle, to composite film including a foil layer, to biodegradable films. These films can be adhesively bonded, heat sealed, impulse welded, and increasingly, ultrasonically welded. Ultrasonic welding offers many benefits to thin film sealing such as faster cycle times, reduction in film usage due to narrower bond widths, elimination of adhesive layers, improved hermeticity for increased shelf life, and less sensitivity to contaminants in the seal area. However, tool design can have a significant effect on weld strength. Optimum tool design depends not just on the thickness of the material to be welded, but also the type of polymer to be joined, and seal requirements (such as hermeticity and peel strength). In this study, we seek to provide starting guidelines with the goal of lowering the cost and duration of the tooling development process by investigating the achievable peel strength of a wide variety of film types with twenty-five horn and anvil design combinations. Tool designs studied include male knurl, female knurl, single ridge, five ridge, and flat, both on horn and anvil, sized for films with a thickness of about 3-6 mil, although some thicker materials were used. Films studied include foil films, biodegradable films, film coated paper, multicolor films, and films for produce packaging. Literature Review Ultrasonic welding can present many advantages over traditional sealing techniques. Compared to heat sealing, ultrasonic sealing offers shorter processing times, especially for thick materials, reduced exposure of the packaging contents to heat, and the ability to cool the welded film under pressure [1]. Compared to induction and infrared sealing, ultrasonic sealing offers consistent seal quality and shorter sealing times [2]. Previous experimentation has shown that weld quality depends significantly on the strength of the film being welded [1,3]. A 2014 study by Ward and Kazakov concluded that polyethylene sealing layers are favorable for maintaining integrity within the weld area due to their broad molecular weight distribution, high toughness, and low zero shear viscosity [4]. Experimentation Introduction Traditionally, bag sealing has been accomplished via thermal welding techniques. However, using ultrasonics offers a cost savings due to the ability to use less film in the package by having a narrower bond width as well as eliminating the need for an adhesive layer. For large-scale manufacturers this can add up to hundreds of thousands of dollars, if not millions, in savings a year. However, identifying the optimum tooling design for an application can be a time consuming and expensive process. Typical film sealing designs include the use of a male or female knurl or a rounded ridge pattern. The sealing pattern can be placed on the horn or anvil, or multiple patterns can be used together, for example, a female knurl can be placed on both the horn and anvil. Additionally, the knurl or rounded ridge can come in a wide variety of dimensions, allowing for thousands of possible tooling variations. Equipment A Branson 2000X 20 kHz ultrasonic welding machine with a 4000 W generator and 7.6-cm diameter pneumatic cylinder was used with the supporting Branson X-Port Program for this investigation, as shown in Figure 1. At maximum shop pressure of 690 kPa, the maximum force that the Branson 2000X welder can apply is 3.15 kN. Carbon paper was used to check the parallelism of the horn to the anvil. This procedure was performed after every tooling change, and was monitored throughout each set of welding trials. The objective of this study is to determine achievable weld strength with a comprehensive sub-set of different combinations of tool design and film material. SPE ANTEC™ Indianapolis 2016 / 1336 Tooling Four common film sealing details were selected for these trials, in addition to a flat face horn and anvil. These details were initially intended to be used for films 36 mil thick and were designed for that size. However, thicker and thinner films were used. EWI designed the sealing details, and the horns and anvils were manufactured by Dukane. The five 50.8-mm long sealing details selected include a 6.35mm wide medium male knurl, a 6.35-mm wide medium female knurl, a single 1.27-mm full round ridge, five 1.27-mm full round ridges, and a 6.35-mm wide flat. All non-flat details are shown in Figures 4-7. These details were placed on five titanium horns and five stainless steel anvils to be used in a variety of combinations. Figure 1: Branson 2000X Welder (20 kHz) A Chatillon Digital Force Gauge was used with the Chatillon TCM 201 motorized force tester to measure the peel strength of each weld. After early peel tests resulted in slipping of the film in the tool with selftightening and mechanical grips, the pneumatic grips shown in Figure 3 were selected for the peel testing trials. Peel tests were run at 50 mm/ min and the peak value (N) was recorded. Figure 4: Female Knurl Horn Schematics Figure 5: Male Knurl Horn Schematics Figure 3: Pneumatic Grips SPE ANTEC™ Indianapolis 2016 / 1337 Figure 9: Flat Anvil Schematic Figure 6: Single Ridge Horn Schematics Materials Twelve unique materials were used in the preliminary trials, welding with every anvil detail and the flat faced horn. A description of each material used and its nominal thickness are described in Table 1. The twelve materials were divided into five groups for comparison. A description of the defining aspect of each group is shown in Table 2. All films are represented just once, with the exception of material 9, which was included in both Group III and IV. Materials 1-10 were provided by Glenroy Inc., while 11-12 were supplied by Bemis Company. Table 1: Summary of Material, Thickness, and Group Figure 7: Five Ridge Horn Schematics Figure 8 shows the basic horn design. The horn design provides an approximate gain of 2.5. When used with a 1.5 booster, the total amplitude was about 75 micrometers. This falls within the recommended amplitude range for most polymers, usually around 40-90 micrometers for amorphous polymer and 50-125 micrometers for semi-crystalline polymers. # Paper/Foil/Coex Paper//PLA (thick) Paper//PLA (thin) PET//LLDPE (white) PET//LLDPE (clear) PET//Foil//LEL Coex PET//Foil/EMAA PET//Foil//LLDPE Thickness (mm) 0.38 0.53 0.21 0.14 0.14 0.10 0.07 0.09 PET//Foil//ACN 0.09 Paper//Foil//ACN OPP/PE Coex PE Coex 0.13 0.05 0.03 Group 1 2 3 4 5 6 7 8 9 10 11 12 I II III III & IV IV V Material Table 2: Material Groups Figure 8: Flat Horn Schematic The anvils were designed to be interchangeable on an aluminum leveling plate, using pins for locating. Each individual anvil has four leveling screws to enable leveling of the anvil to each horn, as shown in Figure 9. The same sealing details that were used on the horns, as shown in Figure 1, were also used on the anvils. In this way every sealing detail could be paired with every other sealing detail, with either one being on the horn or anvil. Group I II III IV V Description: Films with fibreform paper layer Films with Nylon and LDPE (white and clear) interlayers Films with an Aluminum foil interlayer and varying materials on the weld side Films with ACN (Acrylonitrile) sealing layer Films with an ink and anti-fog varnish layer (packaging films) SPE ANTEC™ Indianapolis 2016 / 1338 Prior to welding, all film was cut down into 50x64 mm rectangular pieces. Two identical pieces of film were welded together; care was taken to ensure the correct film orientation for welding (symmetric interfaces, where the same polymer exists on both sides of the interface). All materials are described with the sealing layer noted last. For example, the sealing layer of PET//Foil//LLDPE is LLDPE. For the preliminary trial, all five anvil designs were tested in combination with the flat face horn on each of the twelve types of film material. Afterwards, a down selection was made on the films resulting in three materials for continuation into the in-depth trial where all twenty-five tooling combinations were tested. The three films selected for the in-depth trials were chosen to provide a variety of film types which are widely used. The three films chosen were: Material 1, Paper/Foil/Coex Material 2, Paper//PLA (thick) Material 12, PE Coex. Layer diagrams of each of these selected films are shown in Figures 10-12. Figure 12: Material 12, PE Coex. Figure taken from Bemis Product Data Sheet A214. Preliminary Weld Trials During the preliminary weld trials, the female knurl anvil was used first with the flat horn. Using this initial tooling combination, baseline welding parameters were developed for each film type through varying Weld Energy, Pressure, Trigger Force, Amplitude, and Hold Time. This was done by comparing the weld strength (visually and via peel test) at various welding settings. These initial settings are shown in Table 3. Table 3: Initial Parameter Settings Parameter Weld Energy (J) Pressure (KPa) Trigger Force (N) Amplitude (%) Hold Time (sec) Figure 10: Material 1, Paper/Foil/Coex. Figure taken from Glenroy Product Data Sheet AAFS 001-001. [1mil= 0.025mm] Initial Setting See Table 4 276 222 100 1 It was decided to minimize the variables that would be adjusted during trials in order to ensure comparability between weld strength results on the different materials. Therefore, only weld energy was varied between the film types to optimize strength in the preliminary weld trials. The initial weld energy settings used are show in Table 4. Table 4: Summary of Baseline Weld Energy Settings Figure 11: Material 2, Paper//PLA (thick). Figure taken from Glenroy Product Data Sheet AAO 006-001. # 1 2 3 4 5 6 7 8 9 10 11 12 Material Paper/Foil/Coex Paper//PLA (thick) Paper//PLA (thin) PET//LLDPE (white) PET//LLDPE (clear) PET//Foil//LEL Coex PET//Foil/EMAA PET//Foil//LLDPE PET//Foil//ACN Paper//Foil//ACN OPP/PE Coex PE Coex Weld Energy (J) 100 100 80 100 60 100 200 200 200 350 100 100 SPE ANTEC™ Indianapolis 2016 / 1339 For some of the tooling combinations, however, adjusting energy alone could not result in a good bond. In these cases, the trigger force and/or pressure were adjusted next. Amplitude and hold time were not changed during any of the trials. Weld cycle time is a result of the previously mentioned variables and would generally be between 0.1 and 0.2 seconds. For each material type, three welds were peel tested for each tooling combination set, excepting certain tooling/material combinations that did not generate acceptable welds were not taken for further testing. In all the following tables, the peel strengths shown are the average of three samples welded at the same welding parameters. For the preliminary trials, using just the flat horn with all five anvil types and all twelve materials, three welds at each of the fifty-eight weld material and tooling combinations were made and peel tested, one hundred and seventy-four welds in total. For the welding of three selected materials with all twenty-five tooling combinations, three welds at each of the sixty-one weld material and tooling combinations were made and peel tested, one hundred and eighty-three welds in total. All welding and peel testing was completed by one operator. Results and Discussion Anvil Effect with Flat Horn During the preliminary trials, the flat faced horn was used with all five anvil types. Some trends were noted for all the materials. All the materials welded with the flat horn and flat anvil combinations were weak, even when weld energy was increased. This was expected due to the wide surface area to be bonded. Additionally, slipping of all materials between the flat surfaces was noted. With the small surface area provided by the single ridge anvil, weld settings had to be adjusted to prevent cutting of the materials. For all of the films, some mix of reduced energy input, decreased pressured, and lower trigger force was required. The male knurl anvil required no change in weld parameters from the female knurl anvil. This may be due to both anvils providing the same surface area. Energy input had to be reduced for two materials, PET//Foil/EMAA and Paper//PLA (thick), when the fiveridge anvil was used. Peel Strength Results for Flat Horn Trials Table 5 shows the average peel strength (N) for Group I materials using the flat horn with all five anvil types. The only difference between the two PLA materials is the thickness. Despite this difference in thickness, the peel strength values are very similar for the female and five ridge anvils. The film with the foil layer showed the greatest peel strength with all anvil types. Table 2: Group 1 Average Peel Strength Results (N) Group I Paper//PLA (thin) Paper//PLA (thick) Paper/Foil/C oex Female Five Flat Male Single 57.9 57.9 53.0 41.2 54.9 63.7 59.8 62.8 68.6 31.4 85.3 102.0 81.4 83.4 93.2 Table 6 shows the average peel strength (N) for Group II materials using the flat horn with all five anvil types. These two very similar materials have similar force values when using the single ridge and five ridge anvils, but were unweldable with the flat horn and anvil combination. Interestingly, the clear material required less energy input (60J) than the white material (100J), yet was much stronger when welded with the female and male anvils. Table 3: Group II Average Peel Strength Results (N) Group II PET//LLDPE (clear) PET//LLDPE (white) Female Five 102.0 38.2 Flat Male Single 108.7 87.3 105.9 106.9 45.1 97.1 Table 7 shows the average peel strength (N) for Group III materials using the flat horn with all five anvil types. The material located at the weld interface in this group had a significant effect on which anvil is most suitable. The LLDPE material demonstrated the greatest peel strength, using the male knurl anvil. The LEL Coex showed the second greatest peel strength, using the five ridge anvil. Table 4: Group III Average Peel Strength Results (N) Group III PET//Foil//L EL Coex PET//Foil/ EMAA PET//Foil//L LDPE PET//Foil// ACN Female Five Flat Male Single 60.8 84.3 59.8 53.9 37.3 64.7 51.0 28.4 59.8 60.8 50.0 34.3 92.2 66.7 55.9 40.2 20.6 44.1 3.5 Table 8 shows the average peel strength (N) for Group IV materials using the flat horn with all five anvil types. Both films in this group welded best using the female and male anvils. However, weld strength varied greatly for the other three anvil styles. This may be due to the difference in thickness between the two materials. It is not unexpected that the thicker material performed better SPE ANTEC™ Indianapolis 2016 / 1340 Group IV PET//Foil// ACN Paper//Foil// ACN Female Five Flat Male 60.8 27.5 46.1 55.9 55.9 40.2 20.6 44.1 Single 34.3 Table 9 shows the average peel strength (N) for Group V materials using the flat horn with all five anvil types. The OPP/PE Coex film was designed to peel at a constant value due to the delamination strength of the layers, which it did with three of the four anvil styles. However, using the single ridge anvil provided a significant increase in peel strength. Table 6: Group V Average Peel Strength Results (N) Group V OPP/PE Coex PE Coex Female 24.5 43.1 Five 26.5 Flat Male 18.6 37.3 Single 42.2 36.3 Three Films Welded with All Tool Combinations Table 10 shows the average peel strength (N) for the Paper/Foil/Coex material with all twenty-five tooling combinations. One of the interesting results from welding with all combinations of horn and anvil is the difference in strength when the sealing detail is placed on the horn instead of the anvil. For most of the tooling combinations with this material, the strength was the same regardless of the orientation of the details. However, when welding with the male knurl and flat combination, weld strength was greater when the knurl was on the horn as opposed to the anvil. In fact, the male knurl horn detail with flat anvil detail provided the greatest strength of any combination. There was also a difference in strength when the single ridge and five ridge combination where greater strength was achieved when the five ridge detail was on the horn. However, this difference may be attributed to alignment of the small features. Table 7: Summary for Paper/Foil/Coex Horn Paper/Foil/ Coex Female Five Flat Male Single Female 107.9 103.0 85.3 99.0 96.1 Anvil Five Flat Male 99.0 90.2 99.0 82.4 99.0 91.2 102.0 81.4 83.4 86.3 109.8 103.0 47.1 93.2 103.0 Single 91.2 77.5 93.2 91.2 36.3 Table 8: Summary for Paper//PLA (thick) Paper//PLA (thick) Horn Table 5: Group IV Average Peel Strength Results (N) Table 11 shows the average peel strength (N) for the Paper//Paper (thick) material with all 25 tooling combinations. With this material almost every detail combination showed a difference in strength depending on the placement of the sealing detail on the horn or anvil. The most distinct result is that the lowest peel strengths were achieved with the single ridge detail, whether it was placed on the horn or the anvil. The greatest peel strength was achieved when the male knurl was both on the horn and anvil. Female Five Flat Male Single Female 80.4 83.4 63.7 86.3 31.4 Five 69.6 62.8 59.8 77.5 61.8 Anvil Flat 72.6 79.4 62.8 85.3 40.2 Male 84.3 92.2 68.6 98.1 43.1 Single 49.0 55.9 31.4 50.0 40.2 Table 12 shows the average peel strength (N) for the PE Coex material with all 25 tooling combinations. The male and single ridge horns were not used with this thin material due to easy puncture and cutting despite low weld energy, pressure and trigger force. Additionally, early trials with these horns resulted in some damage to the sealing detail, so their use was discontinued. With this material, peel strength was much greater when the five ridge anvil was used with the female knurl horn than when the female knurl was on the anvil and the five ridge detail was on the horn. In the former case, with the female knurl on the horn, the weld strength was among the highest for all the tooling combinations. However, in the latter case, where the female knurl was on the anvil, the peel strength was the lowest of all tooling combinations, by a significant factor. Table 9: Summary for PE Coex PE Coex Horn with the single and five ridge anvils while the thinner material performed better with the flat anvil. The thicker material would benefit from the smaller surface areas, while the thinner material would be more likely to be damaged when using those anvils. Female Five Flat Female 44.1 26.5 43.1 Five 42.2 37.3 Anvil Flat 35.3 39.2 Male 37.3 Single 45.1 37.3 36.3 Conclusions This fundamental exploration into ultrasonic tooling designs and combinations for thin films has highlighted the importance of proper tooling selection for a given thin film material. Additionally, optimization of welding parameters is essential to achieve maximum bond strength. SPE ANTEC™ Indianapolis 2016 / 1341 These trials have resulted in a number of significant findings. • • • • • Seal layer material plays a significant role in bond strength and tooling selection. The process window is individually dependent on the film composition. Colorant has a definite impact on peel strength. In most cases, the sealing detail can be placed on the horn or anvil. However, when there was a difference, greater strength was generally achieved when the male or female knurl was placed on the horn. Obtaining a wide process window is highly dependent on careful material vs. tooling selection. Acknowledgments A great deal of thanks goes to Glenroy, Inc. and Bemis Company for generous donation of the films used to do this research. References 1. 2. 3. 4. S. Bach, K. Thurling, and J. Majschak, IAPRI Symposium, Berlin, Germany (2011). H. Yeh and A. Benatar, Tappi Journal, 80, 197 (1997). N. Stoehr, B. Baudrit, E. Haberstroh, N. Michael, P. Heidemeyer, and M. Bastian, Journal of Applied Polymer Science, DOI: 10.1002 / APP.41351 (2015). D. Ward and A. Kazakov, PLACE Conference (2014). SPE ANTEC™ Indianapolis 2016 / 1342
© Copyright 2024 Paperzz