What´s New
New Line of Sapiens Capillary Columns
• We are pleased to introduce a superb new generation of capillary
columns.
• Columns for today’s demanding applications
• Our columns are able of competing with the best columns in the
market, with ultra-low bleed and high inertness with respect to
active, acid and basic compounds.
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Developed with new integral technology
Molecular Stabilization Process incorporated (MSP)
Highest inertness for polar, acid and basic compounds
Extreme low bleed (improve trace level analysis)
Warranted reproducibility between batches
Perfect for use with Retention Time Locking (RTL)software
Sapiens-1ms
100% Dimethyl polysiloxane, bonded and crosslinked phase,
manufactured with MSP technology
General purpose column,non polar
Ultralow bleed, improved signal to noise ratio for GC-MS
Solvent rinsable
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Sapiens-1ms Equivalent Phase
Agilent: DB1-MS UI, HP-1 MS UI, VF-1MS
Restek: Rxi-1MS
Phenomenex: ZB-1MS
GL Sciences: InertCap 1MS
Sigma-Aldrich: Equity-1
SGE: SOL-GEL-1MS, BPX-1
Macherey-Nagel: OPTIMA-1MS Accent
Structure of Poly(dimethyl)siloxane
Sapiens-1ms: Ultra Inert Test (SAP-1MS)
Good peak shape and response for all active compounds
160
Column: Sapiens-1ms, 30 m x 0,25 mm x 0,25 µm, P/N TR-430232
Oven temperature: 65ºC
Injection: 0,1 µl SAP-1MS Ultra Inert Test
Split: 500:1
Injection temperature: 275ºC
Dertector: FID, 340ºC
Carrier Gas: H2,12psi (82,8 kPa)
Response
2
150
3
140
130
120
110
100
5
90
80
Peak Name
1
2
3
4
5
6
7
8
9
10
11
propionic acid
1-octene
n-octane
1,2-butanediol
4-methylpyridine
trimethylphosphate
n-propylbenxene
1-heptanol
3-octanone
t-butylbenzene
n-decane
7
70
60
10
6
4
50
8
40
9
11
1
30
20
10
0
20
1
2
3
4
5
6
7
Retention time
What´s New
Sapiens-1ms, Ultra Inert Comparative Test (SAP-1MS) vs principal competitors
240
Response
2
3
4
5
7
8
220
9
10
1
2
3
4
5
6
7
8
9
10
11
11
1
200
Peak Name
Column: 30 m x 0,25 mm x 0,25 µm
Oven temperature: 65ºC
Injection: 0,1 µl SAP-1MS Ultra Inert Test
Split: 500:1
Injection temperature: 275ºC
Dertector: FID, 340ºC
Carrier Gas: H2,12psi (82,8 kPa)
Propionic Acid
1-octene
n-octane
1,2-butanediol
4-methylpyridine
Trimethylphosphate
n-propylbenxene
1-heptanol
3-octanone
t-butylbenzene
n-decane
6
Sapiens-1ms
180
160
140
120
Manuf. (G)
100
80
60
40
20
Manuf. (E)
0
1
2
3
4
5
6
7
8
9
Application: Sapiens-1ms, 30m x 0.25mm x 1.0um, P/N TR-431032
Analysis chlorinated solvents and disinfection by-products (EPA 551.1)
Peak Name
Response
Column: Sapiens-1ms, 30 m x 0,25 mm x 1,0 µm, P/N TR-431032
Oven temperature: 33ºC (28 min) to 275ºC (20 min) @ 10ºC/min
Injection: 0,01 µl (50 ppb, Chlorinated Hydrocarbons)
Split: 100:1
8
Injection temperature: 200ºC
Dertector: ECD, 300ºC
Carrier Gas: He, Constant Flow, 0.9 ml/min
240
220
200
1
2
3
4
5
6
7
8
9
10
4
180
160
3
Chloroform
1,1,1-trichloroethane
Carbon tetrachloride
Trichloroacetonitrile
Dichloroacetonitrile
Bromodichloromethane
Trichloroethylene
Chloral hydrate
1,1-dichloro-2-propanone
1,1,2-trichloroethane
11
12
13
14
15
16
17
18
19
Chloropicrin
Bromochloroacetonitrile
1,2-dibromoethane
1,1,1-trichloropropanone
trichloro-2-propanone
Bromoform
Dibromoacetonitrile
1,2,3-trichloropropane
1,2-dibromo-3-chloropropane
140
15
120
5
100
14
6
80
40
9
1
5
10
13
10
15
16
12
7
20
0
19
11
2
60
17
20
25
18
30
35
40
Retention time
21
What´s New
Sapiens-1ms
Internal
Length
(m)
thickness (µm)
Limits (ºC)
Nº (P/N)
0,10
10
0,10
-60 to 325/350
TR-430141
20
0,10
-60 to 325/350
TR-430181
0,18
20
0,18
-60 to 325/350
TR-430984
20
0,36
-60 to 325/350
TR-433484
12
0,33
-60 to 325/350
TR-4333B9
25
0,33
-60 to 325/350
TR-433329
15
0,25
-60 to 325/350
TR-430212
30
0,25
-60 to 325/350
TR-430232
30
0,50
-60 to 325/350
TR-430532
Diam (mm)
0,20
0,25
0,32
22
Film
Temp
Part.
30
1,00
-60 to 325/350
TR-431032
60
0,25
-60 to 325/350
TR-430262
15
0,25
-60 to 325/350
TR-430213
25
0,52
-60 to 325/350
TR-435223
30
0,25
-60 to 325/350
TR-430233
30
1,00
-60 to 325/350
TR-431033