Japanese Journal of Applied Physics Vol. 45, No. 3B, 2006, pp. 2368–2371 #2006 The Japan Society of Applied Physics Measurement of Cantilever Displacement Using a Compact Disk /Digital Versatile Disk Pickup Head En-Te HWU1;2 , Kuang-Yuh H UANG1 , Shao-Kang H UNG2;3 and Ing-Shouh H WANG2 1 Department of Mechanical Engineering, National Taiwan University, Taipei, Taiwan Institute of Physics, Academia Sinica, Taipei, Taiwan 3 Department of Electrical Engineering, National Taiwan University, Taipei, Taiwan 2 (Received July 4, 2005; revised November 13, 2005; accepted December 2, 2005; published online March 27, 2006) We use the optical pickup head of a commercial compact disk (CD)/digital versatile disk (DVD) read only memory (ROM) drive to detect the vertical displacement of micro fabricated cantilever in atomic force microscopy (AFM). Both the contact and AC modes of AFM are demonstrated. The single atomic steps of graphite can be resolved, indicating that atomic resolution in the vertical displacement detection can be achieved with this new setup. The low cost, compact size, and the light weight of CD/DVD optical pickups may offer new advantages in future AFM designs. [DOI: 10.1143/JJAP.45.2368] KEYWORDS: CD, DVD, AFM, cantilever 1. Introduction In atomic force microscopy (AFM),1) the interatomic forces between the tip and the surface induce a vertical displacement of microfabricated cantilever. Currently, two major optical methods, the beam deflection method2–4) and interferometry,5–7) are adopted in the detection of this displacement, because they both have a sensitivity better than 0.1 nm. In this study, we demonstrate for the first time that AFM using a commercial compact disk (CD)/digital versatile disk (DVD) read only memory (ROM) optical pickup is also sufficiently sensitive for detecting single atomic steps of graphite surfaces. This implies that the optical system in the CD/DVD pickup head may have a sensitivity comparable to that of the beam deflection method and interferometry in terms of the displacement measurement of the cantilever. Most of the current AFM designs adopt the beam deflection method, which makes the optical detection system bulky, heavy, and awkward to use. Commercial CD/DVD pickups are small, compact, lightweight, reliable, and economical, and thus may greatly simplify the design of future atomic force microscopes. Inside an optical pickup of a CD/DVD-ROM drive, a laser beam emitted from a laser diode is first diffracted and collimated into three beams, which are then focused onto an optical disk by an objective lens controlled by a voice coil motor (VCM).8) The beams reflected from the disk are then directed back through the pickup and, after passing through an astigmatic element, impinge onto a photo detector integrated chip (PDIC). The PDIC is composed of six split photosensors A–F, with the center having four quadrant photosensors (A–D) similar to the quadrant position-sensitive detectors used in standard atomic force microscopes, and six current preamplifiers for the six photosensors. The detection of the focusing condition of the laser beam on the optical disk adopts the astigmatic method, which uses a cylindrical lens as a beam-shaping device.9) When the laser beams are perfectly focused on the disk surface, the laser spot on the four central quadrant photosensors (A–D) is circular [Fig. 1(b)], but when the disk surface is slightly higher or lower than the focus of the laser beam, the laser spot on the central quadrant sensors appears more elongated, Corresponding author. E-mail address: [email protected] Fig. 1. Shape of laser spot and S-curve of FES. (a) Off focus, FES < 0. (b) On focus, FES ¼ 0. (c) Off focus, FES > 0. (d) Linear region of FES. as illustrated in Figs. 1(a) and 1(c). The shape change of the laser spot on the PDIC can be detected by the focus error signal (FES), which is defined as ðSA þ SC Þ ðSB þ SD Þ, where SA –SD are the preamplifier output voltages of photosensors A–D, respectively. For a circular laser spot, FES ¼ 0. Figure 1(d) shows the well-known S-curve for the relationship of the FES vs the vertical distance of the disk.10) By measuring the FES, the VCM can drive the objective lens to make the laser beam focused on the disk surface (i.e., FES ¼ 0). In this work, we demonstrate that the linear region of FES (6 mm) can also be used to detect the vertical displacement of the AFM cantilever with a high sensitivity. 2. Experimental In our experiments, we modified a commercial scanning probe microscope (SPM; Nanoscope III, Digital Instrument) by replacing its beam deflection module with a slim-type CD/DVD pickup (TOP1100S, Topray Technologies) and a home-made probe clamping module (PCM). The laser module of the pickup emits light at two wavelengths of 655 and 790 nm, used for DVD and CD, respectively. Here, we use only the laser beam of 655 nm, because it is visible and the focus spot is smaller than that of the other beam. The 2368 Jpn. J. Appl. Phys., Vol. 45, No. 3B (2006) E.-T. HWU et al. Fig. 2. (a) Experimental layout of SPM and optical sensor system. (b) Schematic of PCM. experimental layout is shown in Figure 2. The position of the VCM is fixed by gluing it to the frame of the pickup. The pickup laser beam reaches the cantilever through an objective lens (a working distance of 1.28 mm). The axis of the impinging laser beam is perpendicular to the cantilever surface. The PCM is very carefully attached to the pickup, so that the focus spot of the laser beam is right on the back surface of the cantilever. Before gluing our PCM to the pickup, we ensure that the FES, X (defined as SA þ SB SC SD ) and Y (defined as SA þ SD SB SC ) signals are close to zero. The entire pickup-PCM assembly is very compact and rigid, so that it has a very good mechanical stability during the AFM operation. In order to eliminate any need for alignment when the cantilever is changed, an alignment chip from NANOSENSORS is used in our PCM [Fig. 2(b)]. The alignment chip has three ridges that fit right into the corresponding grooves on the back surface of any AFM probe purchased from NANOSENSORS. According to the specification of the alignment chip, the AFM probe can be changed with a repositioning accuracy within 2 mm. We have changed the AFM probe more than 10 times and the vertical deviation is less than 500 nm (calculated from the FES) after a new probe is placed in the alignment chip. For operation in the contact mode, we use the CONTR-50 probe from NANOSENSORS, which has a cantilever with a thickness of 2 mm, a width of 50 mm, a length of 450 mm, and a force constant of 0.07 – 0.4 N/m. For operation in the AC mode, we use the AR5-NCHR-50 probe from NANOSENSORS, which has a cantilever with a thickness of 4 mm, a width of 30 mm, a length of 125 mm, and a resonance frequency of 300 kHz. The focal laser spot is confirmed with a diameter of 5 mm, which is smaller than the width and length of the cantilevers. Since the PDIC already has a preamplifier for each photosensor, we only need to build a simple electronic circuit to obtain the voltages of the FES, X and Y. In the contact mode AFM, the FES voltage is fed into the feedback system of the SPM controller. Topographic images can be obtained by keeping the FES constant through the feedback. In the AC mode, oscillation voltage is applied to the bimorph of the PCM. The AC signals (amplitude and phase) of the FES are connected to the electronics of Nanoscope III through a signal access module. By keeping the oscillation amplitude of the FES constant, topographic images can be obtained; a phase image can also be produced similarly to the conventional tapping mode. Because the electronic circuit is not properly shielded, it results in a noise level of 0:2 nm in the vertical height measurement. All the experiments presented here are carried out on a standard optical table. The room temperature is 22 C and the relative humidity is 50%. 3. Results and Discussion Figures 3(a) and 3(b) show the topographic images of an AFM calibration grating sample taken using the above described new setup in the contact and AC modes, respectively. The sample has a pitch of 463 nm and a height of 31 nm. Many fine structures can be resolved. The quality of the images is comparable to that of images taken using the standard beam deflection module of Nanoscope III [Figs. 3(c) and 3(d)]. The single atomic steps of graphite surfaces can also be 2369 Jpn. J. Appl. Phys., Vol. 45, No. 3B (2006) E.-T. HWU et al. (a) (b) (c) (d) Fig. 3. Topographic images of calibration grating sample, a 607-AFM waffle grating replica purchased from Ted Pella, Inc. The pitch and the grating height are 463 and 31 nm, respectively. (a) Contact mode: scan size = 5 5 mm2 , scan rate = 0.6 Hz. (b) AC mode: scan size = 5 5 mm2 , scan rate = 0.6 Hz, working frequency of cantilever = 296.94 kHz. (c) DI Nanoscope III contact mode: scan size = 5 5 mm2 , scan rate = 0.79 Hz. (d) DI Nanoscope III AC mode: scan size = 5 5 mm2 , scan rate = 0.35 Hz, working frequency of cantilever = 298.85 kHz. resolved with our new setup using the CD/DVD pickup. Figure 4(a) shows a topographic image and a cross-sectional height profile of a graphite surface taken in the contact mode. Markers indicate one step with a height of 0.35 nm and another step with a height of 1.00 nm. Figure 4(b) shows a topographic image and a cross-sectional height profile of a graphite surface taken in the AC mode. Markers indicate one step with a height of 0.36 nm and another step with a height of 0.69 nm. Both modes achieve a resolution of single atomic steps,11) which indicates that the FES voltage is sufficiently sensitive for the detection of the cantilever displacement of one atomic height. We note that our electronics for the FES voltage was not optimally built. No proper electronics shielding was applied. The noise level in our topographic images is 0:2 nm, which is larger than that taken using the beam deflection module of Nanoscope III [Fig. 4(c)]. We believe the electronics noise can be significantly improved if a better electronics is used. Therefore, our experiments successfully demonstrate that the optical system in the CD/DVD pickup may have a sensitivity better than the atomic scale in the displacement measurement of the cantilever. Previously, Quericioli et al.12) used a CD pickup as the cantilever position sensor in an AFM. However their entire mechanical design was very large and induced a mechanical instability. The resolution was only tens of nm. We use a CD/DVD pickup and greatly improve the compactness and rigidity in our pickup-PCM assembly. Therefore, we achieve a much better resolution. There are several advantages in using CD/DVD pickups in the displacement measurement of the AFM cantilever. First, commercial CD/DVD pickups are manufactured in large quantities for the consumer electronics market; consequently, they are of very low cost. Second, some optical pickups (e.g., those of the slim type used for notebook computers) are small, compact, reliable, and of light weight. One can attach the pickup-PCM assembly to a piezo scanner to build a stationary-sample type AFM, which is usually 2370 Jpn. J. Appl. Phys., Vol. 45, No. 3B (2006) E.-T. HWU et al. (a) (b) (c) Fig. 4. Topographic image and cross-sectional profile of graphite surface. (a) Contact mode: scan size = 1 1 mm2 , scan rate = 0.5 Hz. (b) AC mode: scan size = 1 1 mm2 , scan rate = 0.5 Hz, working frequency of cantilever = 297.04 kHz. (c) AC mode taken using the beam deflection module of Nanoscope III: scan size = 1 1 mm2 , scan rate = 0.5 Hz, working frequency of cantilever = 285.97 kHz. The noise level is 0.064 nm. used for large samples. In the beam deflection method, the optical detection system is bulky and heavy. A sophisticated optical design is needed in order to attach the cantilever directly to the scanner, and the resolution usually becomes worse than that of the scanning-sample type AFM. 4. Summary We have demonstrated the capability of the CD/DVD pickup-PCM assembly to detect the vertical cantilever displacement in an AFM. The resolution of single atomic steps of graphite surfaces was achieved in both the contact and AC modes. 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