Interpreting Asphalt Test Results Danny Gierhart, P.E. Asphalt Institute Regional Engineer Tuttle, Oklahoma [email protected] On almost every roadway project, the component materials are tested. Quality Control - testing that helps the producer ensure that they are providing a quality product Quality Assurance - testing that helps the owner ensure that they are receiving a quality product Regardless of whether you are looking at tests performed for the purpose of Quality Control or Quality Assurance, it’s very important to be able to properly interpret the test results and understand what they are telling you. Stay on top of tests - act sooner rather than later Test results are too often used to simply document the degree out of specification so that a corresponding financial penalty can be assessed. A better use of test results is to track the ongoing quality of a project and make immediate corrections as necessary to ensure a quality pavement. 4 Questions to Ask for Each Test • What is the test designed to tell you? • What are the potential ramifications of a failing test result? • Are the potential ramifications minor or major? • For this test, how much could the degree out of specification affect pavement performance? Over the next 90 minutes, we’ll evaluate the most common QC/QA tests reported for: • Aggregate • Hot Mix (& Warm Mix) Asphalt Aggregate • Gradation • Sand Equivalent Hot (& Warm) Mix Asphalt • Asphalt Binder Content • Lab-Molded Air Voids • Voids in Mineral Aggregate (VMA) • Roadway Density • Moisture Susceptibility Aggregate Gradation or Particle Size Analysis: AASHTO T 30 ASTM D 5444 When you might see this test: This test is typically run on asphalt mix samples after the binder has been extracted or burned off Aggregate Test: Gradation Test Overview: After the binder from the HMA or WMA mixture has been removed by extraction or ignition, the remaining aggregate is dried to a constant weight. The sample is then washed over a No. 200 sieve (0.075 mm) and again dried to a constant weight. Next, the sample is passed through a nest of sieves by a prescribed level of agitation. Particles that are small enough to fall through the openings in the top sieve continue to fall through the nest until they reach a sieve whose openings are too small through which to pass. The contents of each sieve are then weighed, and the cumulative percent passing by mass of each sieve size is then calculated. Aggregate Test: Gradation Example Gradation Results Sieve Size Cumulative Weight (g) % Retained % Passing JMF 1” (25 mm) 0.0 0.0 100 100 3/4” (19 mm) 140.5 8.8 91 96 1/2” (12.5 mm) 256.9 16.2 84 87 3/8” (9.5 mm) 440.9 27.7 72 77 No. 4 (4.75 mm) 791.1 49.8 50 54 No. 8 (2.36 mm) 962.5 60.5 39 40 No. 16 (1.18 mm) 1063.0 66.9 33 30 No. 30 (0.600 mm) 1146.8 72.1 28 23 No. 50 (0.300 mm) 1288.1 81.0 19 14 No. 100 (0.150 mm) 1399.9 88.0 12 10 No. 200 (0.075 mm) 1480.7 93.13 6.9 5.5 Gradation: What to focus on Example Gradation Results Sieve Size Cumulative Weight (g) % Retained % Passing JMF 1” (25 mm) 0.0 0.0 100 100 3/4” (19 mm) 140.5 8.8 91 96 1/2” (12.5 mm) 256.9 16.2 84 87 3/8” (9.5 mm) 440.9 27.7 72 77 No. 4 (4.75 mm) 791.1 49.8 50 54 No. 8 (2.36 mm) 962.5 60.5 39 40 No. 16 (1.18 mm) 1063.0 66.9 33 30 No. 30 (0.600 mm) 1146.8 72.1 28 23 No. 50 (0.300 mm) 1288.1 81.0 19 14 No. 100 (0.150 mm) 1399.9 88.0 12 10 No. 200 (0.075 mm) 1480.7 93.13 6.9 5.5 Sample % Passing vs. Job Mix Formula • What do the test results tell you? How well the plant duplicated the aggregate proportions that were designed in the lab. Failing gradations take the form of a sample % passing ending up outside the allowable tolerance from JMF. • What are the potential ramifications of a failing test result? Potential problems include segregation, harsh/tender mix, and out-of-balance volumetrics. Sample % Passing vs. Job Mix Formula • Are the potential ramifications minor or major? If the mix volumetrics are still in specification, an out-oftolerance gradation shouldn’t affect the mix quality much. • How much does the degree out of spec affect pavement performance? If the gradation strays too far out of tolerance, other mix criteria will be affected, such as binder content, air voids, and VMA. Gradation: What to focus on Example Gradation Results Sieve Size Cumulative Weight (g) % Retained % Passing JMF 1” (25 mm) 0.0 0.0 100 100 3/4” (19 mm) 140.5 8.8 91 96 1/2” (12.5 mm) 256.9 16.2 84 87 3/8” (9.5 mm) 440.9 27.7 72 77 No. 4 (4.75 mm) 791.1 49.8 50 54 No. 8 (2.36 mm) 962.5 60.5 39 40 No. 16 (1.18 mm) 1063.0 66.9 33 30 No. 30 (0.600 mm) 1146.8 72.1 28 23 No. 50 (0.300 mm) 1288.1 81.0 19 14 No. 100 (0.150 mm) 1399.9 88.0 12 10 No. 200 (0.075 mm) 1480.7 93.13 6.9 5.5 Maximum Aggregate Size • What do the test results tell you? The maximum aggregate size influences allowable pavement thickness, susceptibility to segregation, asphalt content, and volumetric requirements. • What are the potential ramifications of a failing test result? A gradation on the maximum sieve size that is less than 100% indicates the presence of over-sized particles. This could result in compaction difficulties, segregation, and asphalt content problems. Maximum Aggregate Size Extra large particles may cause drag marks in the mat Extra coarse aggregate will make the mix easier to segregate Maximum Aggregate Size • Are the potential ramifications minor or major? Gradations results showing less that 100% passing the maximum sieve size are rare and usually only slightly less than 100%. Potential ramifications are minimal. • How much does the degree out of spec affect pavement performance? Results deviating by more than 2 or 3 percentage points on this sieve indicate that a coarser mix category of HMA was sampled than expected. Gradation: What to focus on Example Gradation Results Sieve Size Cumulative Weight (g) % Retained % Passing JMF 1” (25 mm) 0.0 0.0 100 100 3/4” (19 mm) 140.5 8.8 91 96 1/2” (12.5 mm) 256.9 16.2 84 87 3/8” (9.5 mm) 440.9 27.7 72 77 No. 4 (4.75 mm) 791.1 49.8 50 54 No. 8 (2.36 mm) 962.5 60.5 39 40 No. 16 (1.18 mm) 1063.0 66.9 33 30 No. 30 (0.600 mm) 1146.8 72.1 28 23 No. 50 (0.300 mm) 1288.1 81.0 19 14 No. 100 (0.150 mm) 1399.9 88.0 12 10 No. 200 (0.075 mm) 1480.7 93.13 6.9 5.5 Percent Passing the No. 200 Sieve • What do the test results tell you? The % passing the # 200 sieve influences compaction, asphalt content, and volumetric requirements. • What are the potential ramifications of a failing test result? A low % passing the # 200 sieve may result in high air voids, permeability, and a lower AC demand. A high value may result in low air voids and VMA, a higher AC demand, and a tender mix. Check cracking as a result of a high % passing the #200 sieve High % passing the #200 gives the HMA a lighter appearance, indicating a lower film thickness and lower durability. Percent Passing the No. 200 Sieve • Are the potential ramifications minor or major? High dust portions can have major ramifications on the longevity of a roadway. They are typically accompanied by lower than necessary binder contents which reduce pavement durability. • How much does the degree out of spec affect pavement performance? Deviations of less than about 2% typically don’t have too much of an effect. Deviations greater than 2% should be addressed immediately. Gradation: What to focus on Example Gradation Results Sieve Size Cumulative Weight (g) % Retained % Passing JMF 1” (25 mm) 0.0 0.0 100 100 3/4” (19 mm) 140.5 8.8 91 96 1/2” (12.5 mm) 256.9 16.2 84 87 3/8” (9.5 mm) 440.9 27.7 72 77 No. 4 (4.75 mm) 791.1 49.8 50 54 No. 8 (2.36 mm) 962.5 60.5 39 40 No. 16 (1.18 mm) 1063.0 66.9 33 30 No. 30 (0.600 mm) 1146.8 72.1 28 23 No. 50 (0.300 mm) 1288.1 81.0 19 14 No. 100 (0.150 mm) 1399.9 88.0 12 10 No. 200 (0.075 mm) 1480.7 93.13 6.9 5.5 Percent Passing the No. 8 Sieve • What do the test results tell you? The % passing the # 8 sieve has a major influence on voids and permeability. • What are the potential ramifications of a failing test result? A low % passing the # 8 sieve may result in an inherently permeable mix. A high value is not as worrisome as a low value. Low % passing the # 8 indicates a mix that is subject to permeability, which in turn can lead to stripping. Superpave Gradation Requirements - AASHTO M 323 Table 3 - Aggregate Gradation Control Points Nominal Maximum Aggregate Size - Control Points (Percent Passing) 37.5 mm 25.0 mm 19.0 mm 12.5 mm 9.5 mm 4.75 mm Sieve Size Min Max Min Max Min Max Min Max Min Max Min Max 50.0 mm 100 - - - - - - - - - - - 37.5 mm 90 100 100 - - - - - - - - - 25.0 mm - 90 90 100 100 - - - - - - - 19.0 mm - - - 90 90 100 100 - - - - - 12.5 mm - - - - - 90 90 100 100 - 100 - 9.5 mm - - - - - - - 90 90 100 95 100 4.75 mm - - - - - - - - - 90 90 100 2.36 mm 15 41 19 45 23 49 28 58 32 67 - - 30 60 6 12 1.18 mm 0.075mm Be- wary -of JMF- gradations near these lower boundaries - - the mix may6be inherently permeable 0 1 7 2 8 2 10 2 10 Percent Passing the No. 8 Sieve • Are the potential ramifications minor or major? A low % passing the # 8 sieve can have major ramifications on the longevity of a roadway. They are often accompanied by permeability issues which can lead to stripping. • How much does the degree out of spec affect pavement performance? Gradations near the lower broad band are especially of concern when accompanied by a low % passing the # 200 sieve. Aggregate Sand Equivalent Test: AASHTO T 176 ASTM D 2419 When you might see this test: Many agencies specify this test as part of their aggregate quality assurance program. Aggregate Test: Sand Equivalent Flocculating Solution Suspended Clay Clay Reading Sand Reading Sedimented Aggregate Test Overview: This test is an indicator of the amount of detrimental clay or clay-like fines present in the aggregate. A sample of aggregate passing the No. 4 sieve is placed in a flocculating solution, which allows the heavier particles to settle to the bottom of the graduated cylinder, but keeps the fines in suspension. The sand equivalent is the ratio of the sand reading to the clay reading, expressed as a percentage. High amounts of fines result in low SEs. Aggregate Test: Sand Equivalent • What do the test results tell you? The test is intended to show the relative proportions of fine dust or clay-like material in the aggregate. • What are the potential ramifications of a failing test result? A low sand equivalent result indicates a high percentage by volume of clay-like fines. These fines may cause the asphalt binder to debond from the aggregate in the presence of moisture. Low sand equivalents indicate a high percentage of clay-like fines, which can cause a poor bond with the asphalt binder. Aggregate Test: Sand Equivalent • Are the potential ramifications minor or major? A failing sand equivalent test indicates a very poor aggregate quality, which can have major ramifications to the longevity of the pavement. • How much does the degree out of spec affect pavement performance? Sand equivalent results do not have to be much out of spec to be a cause for concern. Hot Mix Asphalt Moisture Susceptibility Test: AASHTO T 283 ASTM D 4867 When you might see this test: Many agencies specify this test as part of their quality assurance program. Moisture Susceptibility A mix that is susceptible to moisture may reveal itself in a number of different ways. It might begin as staining of the surface as in the top picture. It might show up as a rutting problem. It might show up as potholes in the roadway. Each situation can be checked by coring the roadway. Sometimes the core will not come out in one piece. With total stripping, it might not come out at all. Instead you’ll find what looks like loose virgin aggregate in the core hole HMA Test: Moisture Susceptibility • Test Overview – Prepare set of 6 specimens • 6.5 to 7.5% voids – Represents anticipated in-service voids – Use 3 specimens as controls – Remaining 3 specimens are vacuum saturated 70 to 80% – Min. 16 hour freezing at 0oF – 24 Hours in 140oF water bath – Bring all specimens to test temperature (77oF) and determine indirect tensile strength HMA Test: Moisture Susceptibility Saturating Specimens Freezing Specimens Specimens in Hot Water Bath HMA Test: Moisture Susceptibility Determine the indirect tensile strengths of both sets of 3 specimens Calculate the Tensile Strength Ratio (TSR) Avg. wet tensile strength TSR = Avg. dry tensile strength Typical - Minimum of 75% required for field tests HMA Test: Moisture Susceptibility • What do the test results tell you? The test is intended to show the susceptibility of the HMA to moisture damage. • What are the potential ramifications of a failing test result? A failing TSR indicates the mix is inherently susceptible to stripping and raveling. HMA Test: Moisture Susceptibility HMA Test: Moisture Susceptibility • Are the potential ramifications minor or major? The ramifications of a failing TSR can be severe. • How much does the degree out of spec affect pavement performance? Because the test procedure is not one of the most repeatable, results down to around 70% should be confirmed by further testing. TSR results less than 60% would be just cause for immediate work stoppage to investigate and fix the problem. Hot Mix Asphalt Asphalt Binder Content Test (Ignition Oven): AASHTO T 308 ASTM D 6307 When you might see this test: Performed on almost every HMA field sample. HMA Test: Ignition Oven Test Overview: An asphalt mix sample of a specified size is placed in a tared basket. The basket is placed in an ignition oven. The model pictured is equipped with an internal scale, which shows less and less weight as the binder burns off. The sample stays in the oven until the internal scale stabilizes, indicating that all of the binder has burned off. The %binder loss by weight can then be calculated. HMA Test: Ignition Oven • What do the test results tell you? The test shows the percent of asphalt binder by weight of the total mix. • What are the potential ramifications of a failing test result? A low binder content can lead to premature aging of the pavement, stripping, or raveling. A high binder content can lead to flushing or bleeding in the pavement. Low binder contents can lead to raveling, stripping, and premature aging. High binder contents can lead to flushing or bleeding. HMA Test: Ignition Oven • Are the potential ramifications minor or major? The ramifications would likely be different depending on the degree out of spec. Whether any of the potential pavement distresses occur also depend on several other factors. • How much does the degree out of spec affect pavement performance? Binder content is one of several parameters that affect each other. However, binder contents very far out of spec should be a major cause for concern. Hot Mix Asphalt Lab-Molded Air Voids: AASHTO T 166 & T 209 ASTM D 2726 & D 2041 When you might see this test: Performed on almost every HMA field sample. HMA Test: Lab-Molded Air Voids Test Overview: Cylindrical specimens are prepared in a compaction device. They are made up of asphalt binder, aggregate, and air voids. The bulk specific gravity (Gmb) is then calculated for each specimen. The maximum theoretical specific gravity (Gmm) of the mix (where air voids are removed by vacuum) is calculated using uncompacted mix samples. The percent air voids (Va) is calculated: Gmb Va = 100 * Gmm HMA Test: Lab-Molded Air Voids • What do the test results tell you? The test shows the percent air voids in lab-molded specimens. This test indicates a mix property, not inplace air voids. • What are the potential ramifications of a failing test result? With a low air void content, the mix is either has high binder content or the aggregate structure has changed to produce lower inherent voids, which could result in bleeding or rutting. For high air void contents, the mix likely has a low binder content, which could result in low durability, stripping, or raveling. Plastic mix from low air voids & VMA Rutting most likely caused by soft subgrade HMA Test: Lab-Molded Air Voids • Are the potential ramifications minor or major? The ramifications can be severe depending on the degree out of specification. Whether any of the potential pavement distresses occur also depend on other factors. • How much does the degree out of spec affect pavement performance? All failing void contents need some type of action. Mixes that are 1% or more out of spec indicate a need for immediate shutdown for more trials. Hot Mix Asphalt Voids in Mineral Aggregate (VMA): AASHTO T 166 & T 209 ASTM D 2726 & D 2041 When you might see this test: Performed on almost every HMA field sample. HMA Test Result: VMA Va VMA Air Vbe AC AC + Aggregate Vmb Aggregate Test Overview: VMA is a calculated mix volumetric property, consisting of the volume of air voids plus the volume binder not absorbed into the aggregate. The mix needs a minimum VMA to have enough volume to hold the proper amount of air voids and the proper amount of binder. VMA = 100 - Gmb Ps Gsb HMA Test Result: VMA • What do the test results tell you? VMA is calculated from the binder content test and lab-molded specimens. It tells about the total volume of the voids created by aggregates. Most mix specifications require a minimum VMA. • What are the potential ramifications of a failing test result? Samples with low VMA do not have enough void space to provide the proper amount of binder and the proper amount of air. Low VMA, depending on the reason, could result in many distress types. HMA Test Result: VMA • Are the potential ramifications minor or major? The ramifications can be severe depending on the degree out of specification. Whether any of the potential pavement distresses occur also depend on other factors. • How much does the degree out of spec affect pavement performance? Mixes that are 1% or more low indicate a need for immediate shutdown for more trials. Although mixes do not usually have any upper spec limit, problems may occur if VMA is 2% or more high. Hot Mix Asphalt Roadway Density: AASHTO T 166 & T 209 ASTM D 2726 & D 2041 When you might see this test: Performed on almost every HMA project. HMA Test: Roadway Density Test Overview: Cores are cut from the roadway. Like lab specimens, they are made up of asphalt binder, aggregate, and air voids. The bulk specific gravity (Gmb) is then calculated for each specimen. The maximum theoretical specific gravity (Gmm) of the mix (where air voids are removed by vacuum) is calculated using uncompacted mix samples. The percent air voids (Va) is calculated: Gmb Va = 100 * Gmm HMA Test: Roadway Density • What do the test results tell you? The test indicates the in-place density achieved by the compactive effort of the rolling operation. • What are the potential ramifications of a failing test result? Low density may result in permeability, stripping, raveling, cracking, premature aging, and premature failure. High density may result in rutting, flushing, or bleeding. Durability vs Air Voids Stability Cohesion Zone of Highest Durability Flushing Raveling 0 % Air Voids HMA Test Result: VMA • Are the potential ramifications minor or major? The ramifications of failure to achieve proper density are major. Proper density can in part make up for other shortcomings. Improper density can cause failure even if other parameters are good. • How much does the degree out of spec affect pavement performance? Any failing density report should cause the agency to closely examine the rolling operation. The further out of spec, the shorter the anticipated pavement life. How Important is Density? In summary, all failing test results should be followed up on. Some test results may be received after all of the material is already in place. Some test results will be received in time for corrective action, which should be immediate. Remember that a few hours time addressing a problem may prolong the pavement life by several years. QUESTIONS? Good Reference Materials on the Topic: MS-2: Mix Design Methods SP-2: Superpave Mix Design MS-4: The Asphalt Handbook MS-22: HMA Construction http://www.asphaltinstitute.org
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