Friction and wear of carbonate rocks under high velocity sliding BONEH1, 3, Yuval, SAGY2, Amir, and RECHES3, Ze'ev 1 Earth and Planetary Sciences, Washington University, One Brooking Drive, MO 63130. 2 Geological Survey of Israel, 30 Melkhe Israel St., Jerusalem, Israel. 3 School of Geology & Geophysics, University of Oklahoma, Norman, OK 73019. Under High velocity: 1. Wear-rates are low 2. Wear-rates do NOT depend on normal stress (in contradiction with Archard equation, below) We experimentally analyze the wear and friction of experimental faults made of three carbonate rocks: Kasota dolomite (KD), Dover limestone (DL), and dolomite-quartzite pair (KDBQ), and tested a wide range of normal stress (up to 7 MPa) and up to seismic slip-velocity (1 m/s). B DC G – wear volume; K – material constant H – hardness; x – slip distance ; σn – normal stress R Friction coefficient and Power - density Rotary Shear Apparatus TC UB The friction coefficient depends on BOTH slip velocity normal stress (fig. below, left). It correlates best with the power-density (Fig. below, right). Power Density = Shear stress * Velocity [Work per unit square], namely 𝑚 𝑀𝑊 Three friction regimes are apparent: 𝜏 ∗ 𝑉 = 𝑀𝑃𝑎 ∗ = 2 𝑠 𝑚2 1. High friction coefficient (μ ~ 0.9) under low power-density of < 0.05 MW/m . 2. Low friction coefficient (μ ~ 0.3) under high power-density > 0.4 MW/m2. 3. Transition zone for intermediate power density of 0.05 – 0.4 MW/m2. B 1.5 mm Predicted dynamic friction for various velocities LB Synthesis: Fault surface evolution Brittle regime: Low velocity and high normal stress = High wear-rate, high friction, and gouge covered surface. We analyze here the wear-rate and friction coefficient during the steady-state state. Queener et al. 1965 Transient stage V = total wear β, n = constants x = slip distance K = steady-state Steady-state stage Wear map Ductile Brittle Ductile regime: High velocity and high normal stress = Low wear-rate, low friction, and shiny, hard surface. Transition Friction map Conclusions Experimental faults Lower blocks of Kasota dolomite and Dover limestone samples after low-velocity experiments. The ring areas that are covered with light colored, gouge powder are the sliding fault slip surfaces. They are surrounded by inner and outer rings of ejected gouge. Dover limestone Combined: Wear and Friction maps Wear and Friction Maps We found above that the wear-rate and friction depends on both slip velocity and normal stress. An effective way to present these relations is by Wear map and Friction map (below) that are frequently used in the engineering literature to depict frictional resistance and wear-rate behavior of materials under a wide range of loading conditions. The wear and friction maps for carbonate rocks (below) can be used for predicting fault behavior. Kasota dolomite A Thermally decomposed carbonate slip surfaces: A below displays a transition from gouge powder (bright yellow, P) to patches of decomposed crust (light brown, DC) on the slip surface. Dark gray area (R) are exposed rock surfaces. Dolomite on quartzite sample under V = 0.14 m/s. B below displays continuous coverage by the decomposed shining surfaces in limestone, formed under V = 0.36 m/s. P Experimental settings Thermal Correction - The displacement normal to the slip direction (FND) is first corrected for the thermal expansion of the sample due to frictional heating. Fitting and differentiate – The FND signal is fitted and differentiate to determined the wear-rate in units of: [μm/m] - (micron of fault wear/ meter of fault slip) Under low slip–velocity (namely: high friction and low temperature), the slip surfaces are covered with powder (A below). Under high slip–velocity (namely: low friction and high temperature), the slip surfaces are covered with hard, dark and shinny crust (Siman-Tov et al., in pre). These surfaces were probably created by thermal decomposition (Han et al, 2007). A Archard’s wear equation - Archard (1953) wear equation states that total wear is linearly related to slip distance and normal stress. The main objectives: A. Determine the effects of normal stress and slip velocity on wear-rate; B. Investigate the relations between wear-rate and frictional strength. Wear-rate calculations Wear-rate [mm/m] Under Low velocity : Wear-rates depend on normal stress Wear-rate [mm/m] The two graphs on the right display wear-rates as function of slip velocity. They indicate: Slip along faults is always associated with frictional resistance and surface wear. The dominant factors that control friction and wear are: rock composition (lithology, grain size, mineral hardness), environmental conditions (fluids chemistry/pressure, humidity, temperature), fault-zone conditions (roughness, hardness, gouge thickness, gouge grain size), and mechanical loading (normal stress, slip velocity, pore pressure). Rotary shear apparatus at Oklahoma University (Reches & Lockner (2010). The experiment configuration (left) includes: an Upper block (UB) with a ring-shaped contact sliding on a flat, lower block (LB). Two metal disks, which are fixed on each block, host eddy currents sensors (in green) that measure the fault normal displacement (FND). Thermocouples (TC) are embedded in the upper block ~ 3 mm from the slip surface. We continuously monitored: shear and normal stress, velocity and FND Observations: Fault slip surfaces Observations: Wear–rates and Friction coefficients Motivation: Friction and wear relations Non-linear Coulomb friction In an ideal Coulomb material, the shear stress is a linear function of the normal stress. We observed however (left), that = 𝒂𝒏 𝒃 where a and b are constants, and where b is a function of slip velocity (right). These relations indicate more ductile behavior at high velocities. • Two regimes of wear-friction-fault morphology in experimental carbonate faults: • Brittle regime • Conditions: Low velocity and high normal stress • Fault properties: High wear-rate, high friction (m > 0.7) , gouge covered surface • Deformation mechanism: asperity fracture, three-body shear • Ductile regime • Conditions: High velocity (seismic) and high normal stress • Fault properties: Low wear-rate, low friction ( m < 0.5), shining-hard surface • Deformation mechanism: plastic flow, thermal decomposition - Arachard, J. F., 1953. Contact rubbing of flat surfaces. Journal of Applied Physics, v. 24, 8, p. 981-988. - Boneh, Y., 2012. Wear and gouge along faults: Experimental and mechanical analysis. MS Thesis, U of Oklahoma. - Han, R. et al., 2007, Ultralow friction of carbonate faults caused by thermal decomposition: Science, v. 316. - Queener, C.A., et al., 1965, Transient wear of machine parts: Wear, v. 8, p. 391-400. - Siman-Tov et al., in prep.
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