Bull Eng Geol Environ (2015) 74:775–788 DOI 10.1007/s10064-014-0673-x ORIGINAL PAPER Experimental study on cracking damage characteristics of a soil and rock mixture by UPV testing Y. Wang • X. Li Received: 24 January 2014 / Accepted: 4 September 2014 / Published online: 30 September 2014 Ó Springer-Verlag Berlin Heidelberg 2014 Abstract This paper investigates the ultrasonic pulse velocity (UPV), mechanical properties and cracking characteristics of a soil and rock mixture (SRM) with varying rock percentages under uniaxial compression. Cylindrical SRM specimens (50 mm diameter and 100 mm height) with rock percentages of 20, 30, 40 and 50 % were produced to perform a series of uniaxial compressive strength (UCS) tests. A P-wave transducer (500 kHz) and associated equipment were employed for all the testing to record the ultrasonic parameters during the whole deformation process. Test results indicates the UCS and UPV decreased with increasing rock percentages for all specimens. The failure mechanism of all specimens showed a splittingsliding mixed pattern; macro-cracks have a direction of 0°– 10° parallel or sub-parallel to the normal stress. In addition, an equation was proposed for the relationship between UPV and crack width. Crack initiation stress was lower for specimens with a high rock percentage. The crack initiation stress level was about 0.2–0.5 times of peak-strength, and the total width of cracks was about 2–5 mm at peakstrength. Based on the width of cracks and UPV, the total stress–strain curve was divided into three stages: the linearelastic stage; the damage initiation and stable development stage; and the damage acceleration stage. Moreover, a three-stage damage evolution equation and constitutive model were established and compared with the testing data. These results confirm that the UPV and mechanical Y. Wang X. Li (&) Key Laboratory of Shale Gas and Geoengineering, Institute of Geology and Geophysics, Chinese Academy of Science, Beijing 100029, China e-mail: [email protected] Y. Wang e-mail: [email protected] properties of SRMs are closely related to the rock percentage. In this regard, the UPV test can be suitably exploited for determing the cracking evolution characteristics for SRM. Keywords Soil and rock mixture (SRM) UPV testing Mechanical properties Cracking characteristics Introduction Soil and rock mixture (SRM) is a unique type of complicated inhomogeneous geomaterial and widely encountered in geotechnical engineering projects (Medley and Lindquist 1995; Goodman and Ahlgren 2000; Lindquist and Goodman 1994). Ancient landslides, debris-flow and rock-filling dams are usually comprised of SRM (Li et al. 2004; Chen et al. 2003; Zhang et al. 2004). Also, with the development of many kinds of large-scale engineering projects, the stability of an engineering geological body (such as a slope, a foundation and adjoining rock in tunnels, etc.) are controlled mostly by the mechanical properties of the SRM. SRMs, as a special engineering geological body, consist of many components such as stiff rock blocks, comparatively soft soils or particles, mixed blocks ranging in shape and size. The individual components of SRMs usually have different mechanical and physical properties and different responses under internal and external loadings. Furthermore, complicated relationship exists among those individual components. Thus, different mechanical behaviors (such as cracking characteristics, translation of stress, stress propagation, carrying capacity and fracture mode, etc.) exist between SRMs and other homogeneous geomaterials. The physical and mechanical properties of SRMs are more complicated than those of general soil and rock mechanics 123 776 due to a complicated composition and interior structure. To study the physical and mechanical properties of SRMs, many scholars have conducted significant studies from various points of view. For example, Lindquist (1994), Lindquist and Goodman (1994) and Medley (2001) studied the strength and deformation characteristics of SRMs via multistage triaxial tests and field investigations; results show that block percentages influence the mechanical behavior of SRMs to a large extent. Also, block size distributions based on chords was proposed for studying the field distribution characteristics of SRMs. You and Tang (2002) and Xu and Hu (2007) studied the physical and mechanical properties of SRMs and the influential factors via in situ tests. Chen et al. (2005) studied spatial factors such as the configuration, structure, environment and evolution of SRMs in the context of the spatial effect of an SRM slope on a large scale. Vallejo and Mawby (2000) studied the influence of porosity on the shear strength of granular material/clay mixtures. Xu et al. (2008) studied the mesostructure and meso-mechanical properties of SRMs using a digital image processing-based finite element method. Unfortunately, one of the challenges in investigating the mechanical properties and meso-structure is inspection in real-time, which includes the detection of damage zones, cracks and defects. Ultrasonic techniques, known as being non-destructive and easy to apply for in situ and laboratory conditions, are commonly used for establishing the strength of concrete or rock via UPV measurement (Kahraman 2001; Yasar and Erdogan 2004). These techniques have been used for measuring various concrete properties. The UPV method has also been suggested as a being useful for estimating elastic and strength properties of rock; some empirical correlations between the UPV and compressive strength and modulus of elasticity have been established (Saka and Uchikawa 1995). UPV can also be used to evaluate the cracks or defects in a material (Akkaya et al. 2003) or to analyze the concrete microstructure development and strength (Ercikdi et al. 2014; Zhang et al. 2010; Su et al. 2012). When associated to tomography, UPV can give good qualitative information on the changes in a material properties as well as on its microcracking state (Grinzato et al. 2004; Meglis et al. 2005). Kahraman (2004) also studied the influence of the fracture roughness of granites on UPV and provided a correlation between both parameters. Although acoustic emission seems to be more appropriate in the evaluation of the crack damage in concrete, and especially in rocks under uniaxial compression (Farmer 1983; Eberhardt et al. 1999), UPV appears also to provide some indication about the damage in concrete (Selleck et al. 1998; Mirmiram and Wei 2001). The basic objective of the present work is to analyze and develop the usefulness of UPV testing for exploring the mechanical properties and crack evolution in an SRM 123 Y. Wang, X. Li specimen, and also to establish a damage evolution equation and constitutive model. To the authors’ knowledge, so far no experimental results have been published using UPV testing to research the mechanical and deformation characteristics of SRMs. The SRM specimens are cylindershaped with a 50 mm diameter and a height of 100 mm with varying rock percentage (20, 30, 40, and 50 %, mass proportion). All three produced specimens were tested. Correlation between UPV and UCS and width of cracks are established. Based on the width of cracks and UPV, the total stress–strain curve of SRMs was divided into three stages. Moreover, the three-phase damage evolution equation and constitutive model were established, and also compared with the testing data. Experimental procedure The testing material Remolded SRM specimens were used for the experiments. The soil was obtained from a pit in the Chinese Academy of Sciences Institute of Atmospheric Physics at a depth of 15 m. According to the geotechnical testing standard for soil test method (GB/T 50123-1999), some physical and mechanical parameters are shown in Table 1. The soil contained a notable amount of strongly hydrophilic clay minerals. The liquid limit of the hard clay can reach 40 % and the plastic limit can reach 36 %; the plasticity index was about 48 and the liquidity index was about 0.05–0.127. These indices indicated this soil is a typical hard plastic and high plastic clay. To identify the mineral composition and mineral contentwe conducted Scanning Electron Microscope (SEM) and X-Ray diffraction (XRD) tests on the soil. By XRD analysis, the main clay minerals can be identified. The clay minerals were identified from their basal reflections determined from the XRD pattern (Moore and Reynolds 1997) after: (1) air drying (normal); (2) glycolation for 48 h; and (3) heating to 550°. The net peak areas of the basal reflection of the clay minerals were calculated above the background and considered as a Table 1 Basic properties of soil material and rock blocks from geotechnical testing Property Soil Rock blocks Natural density (g/cm3) 1.66 Dry density (g/cm3) 2.03 – Water content ( %) 9.5 – Relative density (GS) 2.72 – 2.67 Compressive strength wet (MPa) 0.56 2.727 Compressive strength dry (MPa) 50.65 100.74 Cracking damage characteristics of soil and rock 777 Fig. 1 SEM images of: a soil sample #1; b soil sample #2 Table 2 Main mineralogical composition of a soil specimen obtained from XRD Mineral Soil specimen #1 (%) Soil specimen #2 (%) Montmorillonite 61.52 60.28 Kaolinite 26.73 24.86 Illite 6.25 9.58 chlorite 3.5 3.28 proporation of each mineral in the mixture. The total association was taken to by equal to 100 %. Then the relative properties were deduced semi-quantitatively. SEM tests, as shown in Fig. 1, revealed rodlike and irregular quartz grains with a grain size of about 0.01–0.03 mm and probably surrounded by clay minerals. The XRD tests revealed the main clay mineralogical composition, as shown in Table 2. According to Table 2, it is clear that the soil has a higher percentage of clay mineral, similar to kaolinite, montmorillonite, and illite. As stated above, the mechanics of SRMs are restricted by the shape, distribution, size and percentage of rock blocks. The rock percentage is the most important index influencing the mechanical properties of SRMs (Lindquist and Goodman 1994; Xu et al. 2008). As such, we ignored the other factors influencing the mechanical properties. The rock blocks used corundum balls with 8-mm diameters; properties of the corundum material are listed in Table 1. Specimen preparation A total of 60 SRM specimens were prepared for UPV testing. A compact test was used to produce the specimen (Donaghe and Torrey 1994). According to the relationship between the density and the compaction number, the optimal hammer count was determined to be 20. During the preparation of SRM specimens, an extra amount of free water was added to the mixture; the optimal water content was determined by compaction test to be 9.5 %. The rock blocks used for specimen preparation and SRM specimens with different percentages after air-drying are shown in Fig. 2. The required amount of rock blocks and soil material for each specimen (Table 3) were mixed and homogenized in a mixer. Then, the mixtures were poured into cast iron cylinders 50 mm in diameter by 100 mm in height. The compaction apparatus was used to compact the mixture with 20 counts with three layers. The specimens were then sealed with plastic warp and allowed to air-dry. Experimental system The testing system utilized for the UPV tests includes a rigid loading device, an ultrasonic detector and an ultrasonic transducer (500 kHz) specially designed for this test. The overall setup of the test system is shown in Fig. 3. During the test, axial load is applied by the hydraulic jack, which can provide a maximum axial force of 100 kN. The axial force is measured by stress sensors. The load controller can record the axial force at every stress level. The precision of the load controller is 0.01 kN. The axial deformation is measured by a micrometer installed on the platform; its precision is to 0.001 mm. The ultrasonic detector is a common detector utilized in concrete detection (Model ZBL-520) which can provide a 1,000 V spike for a duration of 20 ls to 20 ms for the transducer and also can accurately record wave signals with good precision. In the UPV testing, the sampling interval was 0.1 ls and the arrival time of each pulse could be read to 0.05 ls; sampling length is 1,024. Before the measurements, the middle-lateral surfaces of SRM specimens were made smooth and flat. A thin film of Vaseline was applied to the surface of the transducers (transmitter and receiver) in order to 123 778 Y. Wang, X. Li Fig. 2 Specimens with UPV testing. a Rock blocks in the specimens; b specimens after air-drying Table 3 The required amount of blocks and soil for each specimen Rock percentage (%) Dry soil (g) Dry soil and water (g) Block mass (g) Ball no. 20 337.4751 371.2226 364.4731 110 30 303.5799 333.9379 327.8663 170 40 267.7268 294.4995 289.1449 240 50 229.7410 252.7151 248.1203 300 ensure ful contact and to eliminate the air pocket between transducers and the specimen. The specially designed transducer is the core component determining the success of the test. The transducer (500 kHz) is cylindrical and one end can be connected with the plane at the middle part of specimens. The piezoelectric ceramic disk is equipped in the cylindrical bore (as shown in the top left corner of Fig. 3) and one end connects with a tungsten powder mixture filler and spring, the other end connects with a boss button. The tungsten powder mixture filler can make the piezoelectric ceramic disk move forward and emit signals. A thread cover and a shim are used to constrain the boss button and the spring makes the head of the boss button extend 1 mm from the center bore of the shim once no pressure is applied. When the transducer is subjected to pressure, the boss button moves backward by compressing the spring and the pressure can be afforded by the shim. During the tests, the transducer was fixed using a rubber strip, enabling the piezoelectric ceramic disk can to be in close contact with the specimen during the tests. Testing procedure All devices were installed as shown in Fig. 3 and were checked to ensure that they were working normally. The UPV testing method employed was the ultrasonic transmission method (through-transmission method). Uniaxial compressive strength tests for the specimens were carried out at the speed of 0.1 kN/step. Complete information 123 regarding the stress value, displacement value and ultrasonic parameters were recorded. Every three specimens of varying rock percentages were tested. As is known, the first cycle wave is stable and renewable under the same transducer and same contact between transducers and specimens. The first cycle wave is scarcely contaminated by other waves arriving late and is easy to identify. Therefore, the first cycle wave was selected as the initial wave. The waveforms collected by the receiving transducer consist of an initial transmitted pulse, followed by later reflections at various interfaces, such as the rock– soil interfaces, and the transducers and the specimen. Due to absorption attenuation, scattering attenuation and diffusion attenuation into an ultrasonic wave, the received ultrasonic frequency was reduced to some extent. Figure 4a shows the received waveform of sample SRM20-1 before loading by ultrasonic detector. The initial wave was selected to obtain the travel time t at each loading step (Fig. 4b). After measuring the path length L the velocities were calculated as UPV = L/t. Research idea SRMs are characterized by complex ingredients and an anomalistic structure distribution. Failure characteristics of SRMs are complicated under internal or external loadings. Different mechanical properties exist among soils and rocks. Determining the level of failure may be difficult and unreliable without using complicated methods and procedures, such as in situ experiments, indoor experiments, numerical simulation and so on (Lindquist and Goodman 1994; Goodman and Ahlgren 2000; You and Tang 2002; Li et al. 2004; Xu and Hu 2007). Sometimes special procedures and methods have to be designed, tried and then applied to the element under consideration. Such methods are usually slow and costly. However, UPV testing as a useful and reliable nondestructive tool for assessing the mechanical characteristics of rock and concrete material demonstrates a strong advantage (Su et al. 2012; Grinzato et al. 2004). The Cracking damage characteristics of soil and rock Fig. 3 Testing system (1. Upper cross beam; 2. Rigid column; 3. Platform; 4. Guide bar; 5. Pedestal; 6. Transmission line; 7. Force sensor; 8. Load controller; 9. Hydraulic jack; 10. Micrometer gauge; 779 11. Rigid cushion; 12. SRM specimen; 13. Rubber strip; 14. Transmitter; 15. Receiver; 16. Ultrasonic detector) Fig. 4 Received wave form for sample SRM20-1 in its initial state (a) and the principle to obtain UPV (b) method present here is a technique that can be applied to structurally cracked elements in order to explore the cracking characteristics of SRMs using UPV testing. Due to the elastic mismatch between a soil matrix and rock blocks, soil and blocks are considerd to be in a weak cementation state. Under loading, differential deformation occurs at the interface between the rock blocks and soil, which causes differential sliding, moving and rotation of the rock blocks. As such, the local concentration of stress causes tensile damage around the rock/soil interface. Afterwards, a series of non-linear behavior appears, including crack initiation, propagation and coalescence and movement of blocks. The research idea is to measure the velocity through the SRM specimens under uniaxial compressive test in realtime. When cracks appear in the specimen, it is obvious 123 780 Y. Wang, X. Li Fig. 5 Test procedure in non-cracked and cracked specimens that the velocity is reduced (see Fig. 5). The velocity through an SRM is higher than the velocity through air or water; the crack is either filled with air or water. Hence, a reduction in the measured velocity can be noticed when the specimen cracks. However, when the cracks are wide, the sound waves are wholly reflected and no signal is received. Furthermore, a relation between the UPV and total crack width was deduced. The basic idea was that the reduction in the velocity through an SRM is basically due to the formation of cracks, as shown in Fig. 5. According to the principle that states when in the state of weak deformation, travel time in the medium is almost constant, the final relationship was as follows: 1 1 1 1 w¼ L ð1Þ V V0 Va V0 , where w is the total crack width, V is the velocity in the SRM at any stress level, V0 is the velocity in the SRM at zero stress level, Va is the wave velocity in air, taken as 340 m/s and L is the side length of the specimen. In terms of physical interpretation of Eq. (1), during compressive loading the travel time increment of the ultrasonic wave through a specimen is equal to the time increment when the cracks are filled with air. (Note: Eq. (1) is deduced when cracks appear in the specimen. So, if ‘‘w’’ is positive, it indicates that the SRM specimens are cracking and if the ‘‘w’’ is negative, it implies that the SRM specimens are in a consolidation stage.) Results and discussion Peak strength variation against rock percentage Axial stress–strain curves for typical specimens (SRM20-1, SRM30-4, SRM40-7 and SRM50-10) are shown in Fig. 6. 123 Fig. 6 Stress-strain curve for typical SRM specimens Table 4 Peak strength value and peak strain value for specimens with different rock percentages Rock percentage ( %) Peak strength (MPa) Peak strain ( %) Mean Standard deviation Mean Standard deviation 20 5.897 0.449 1.081 0.014 30 4.676 0.385 1.037 0.033 40 4.549 0.087 0.885 0.027 50 3.212 0.185 0.798 0.081 Upon reaching peak strength, the specimens remained complete, but cracks parallel or sub-parallel to axial direction appeared (Fig. 8). The average peak strengths with different rock percentages are shown in Table 4. As Fig. 7 depicts, increasing the rock percentage results in a reduction in peak strength. Also, peak strains decease Cracking damage characteristics of soil and rock Fig. 7 Peak strength and peak strain versus rock percentage for tested specimens with an increasing rock percentage. Our data is in aggrement with the results of Medley (2001) and some of the results of Xu and Hu (2007). According to Table 4, peak strength and strain are not uniform for the specimens with the same rock percentage. This is due to the difference of block distribution in the specimen. Failure mechanism Because the rock–soil interface was in the state of weak cementation, differential deformation occurred at the interface, causing differential sliding between the soil and rock blocks under axial loading androck block movement and rotation. As such, locally concentrated stress causes tensile damage around the rock/soil interface. Figure 8 is the failure 781 morphology of SRM specimens with different rock percentages. As shown in Fig. 8, the cracks are almost parallel to the axial direction. The observed failure patterns for specimens with different rock percentage revealed that all specimen failures followed the same mechanism. Figure 8 shows typical failure patterns observed for tested specimens under uniaxial compressive loading. The combination of splitting and sliding failire patterns lead to the formation of two kinds of cracks, the rock/soil main cracks and secondary cracks surrounding the rock blocks. With an increasing rock percentage, the number of cracks increased. Splitting failure occurred in the soil matrix with crack propagation and coalescence and the main cracks formed in the soil. Sliding occurred along the interfaces between blocks and soil and this caused formation of secondary cracks. The sliding failure is simply a result of the relative movement and rotation of the blocks in the SRM. These failure mechanisms at different rock percentage were consistent with previously reported results (Xu et al. 2008) (Fig. 9). Ultrasonic pulse velocity As in the analysis above, the failure mode of SRM specimens are a mixed pattern (a combination of splitting and sliding). Cracks in specimens propagated and coalesced with an increasing axial loading. Cracks are filled with air and when ultrasonic waves pass through the specimens, the UPV deceases gradually. Figure 10 is the relationship between the UPV and axial stress of typical specimens SRM20-1, SRM30-4, SRM40-7 and SRM50-10. As is shown, rock percentage is the main factor influencing the UPV; at the same stress level the UPV is lower in specimens with more rock blocks than those with less blocks. Fig. 8 Failure morphology for SRM specimens under uniaxial compressive test Fig. 9 Sketch maps of the failure morphology for SRM specimens with different rock percentages 123 782 Y. Wang, X. Li 2. 3. Fig. 10 Relationship between the UPV and axial stress of typical specimens Table 5 UPV of initial specimens and of failure with different rock percentages Rock percentage (%) Initial UPV value Failure UPV value Mean (m/s) Standard deviation (m/s) Mean (m/s) Standard deviation (m/s) 20 4859.946 26.380 3536.056 26.258 30 4563.342 35.957 1795.870 9.921 40 4332.505 39.399 1678.357 20.694 50 3769.232 44.642 1533.664 17.408 Table 5 is the UPV of specimen unloading and failure. We can see that the UPV decreased with an increasing rock percentage. Also, the UPV of the same rock percentage is different, due to the different distribution of rock blocks in the specimens. Cracking evolution analysis The total crack width is calculated according to Eq. (1); they are caused by micro cracking and plastic deformation during compressive processes. The width of cracks was plotted against relative stress (i.e., the ratio of axial stress to the maximum axial stress) for typical specimens SRM20-1, SRM30-4, SRM40-7 and SRM50-10. Figure 11 depicts a clear crack evolution pattern and the cracking evolution can be divided into three stages: 1. Linear-elastic deformation: in this stage, the SRM specimen was consolidated, pores and opening cracks were closed by being subjected to axial loading, little elastic energy was released, although some elements were damaged; 123 Rock/soil jointed crack initiation and stable crack growth: These actives can be attributed to local degradation such as interconnection of the large pores, rock–soil jointed interfaces cracking and multiple branching cracks. It is clear that in fact the cracking processes operate at this stage, which seems to control the lifetime of the SRM; Crack acceleration and coalescence: when the specimen approaches its ultimate strength it is assumed that unstable cracking occurs by interconnection between the defects created in the second stage. The compressive cracking process up to peak load is well described by the stress markers rci and rcd (see Fig. 12) where the typical stress–strain curve up to peak strength is discussed. The onset of microcracking is associated with the stress level rci and is followed by a nonlinear increase of the lateral strain. Unstable microcracking occurs for the crack damage stress level rcd and is associated with the reverse point in the total volumetric strain curve (Vr). This point is connected to the maximum compaction of the specimen and to the onset of dilation, since the increase in volume generated by the cracking process is larger than the standard volumetric decrease due to the axial load. The relations between the width and relative velocity (i.e., the ratio of velocity to the maximum velocity) is illustrated in Fig. 13. We can see that the sum of crack widths is closely related to the UPV. It is also clear from Fig. 14 that the relative velocity stays almost constant in the first stage until the relative velocity reaches a certain level, and then a slower and severe reduction in the relative velocity is obtained. Also, from Fig. 9, a clear pattern of crack evolution can be obtained. The point corresponding to crack initiation and crack acceleration is associated to rci and rcd. Like rock material, this is the first that we obtain the rci and rcd for SRM specimens using UPV tests. Results of rci and rcd related to the corresponding stress level are shown in Table 6. With an increasing rock percentage, the relative stress for rci and rcd is reduced. Damage constitutive model In recent years, continuum damage mechanics was applied to study the initiation and growth of cracks in rock and soil. Great achievements were made (Chaboche 1981; Kachanov 1986; Lemaitre and Chaboche 1990), but no experimental results about damage characteristics of SRMs under loading were republished. Under loading conditions, internal structure, strength, and deformation characteristics would change accordingly for SRMs. The UPV testing is a reliable and non-destructive tool, having been used in concrete and rock widely; some mechanical properties related to damage characteristics have been conducted. In Cracking damage characteristics of soil and rock 783 Fig. 11 Typical plots of total crack width against relative stress for specimens SRM20-1, SRM30-4, SRM40-7 and SRM50-10 Fig. 12 Typical stress–strain curve for rocks under uniaxial compressive loading up to peak stress Fig. 13 A typical plot showing the relationship between crack width and relative velocity 123 784 Y. Wang, X. Li Fig. 14 Relationship between relative velocity and relative stress during loading Fig. 15 Typical plots of the damage factor against relative stress for typical specimens SRM20-1, SRM30-4, SRM40-7 and SRM50-10 Table 6 The relative stress for rci, rcd and the total crack widths at peak strength V2 ¼ E 1m q ð1 þ mÞð1 2mÞ ð3Þ Specimen No. Crack initiation stress level (%) Crack damage stress level (%) Crack width at peak strength (mm) SRM20-1 0.463 0.768 3.054 SRM20-3 0.481 0.794 2.756 SRM20-4 0.443 0.773 2.934 SRM30-1 0.427 0.736 3.728 SRM30-2 0.403 0.772 4.651 Combining with Eqs. (2) and (3), the damage factor defined using UPV, is as follows: SRM30-4 0.435 0.865 4.897 D ¼ 1 V~2 =V 2 SRM40-5 0.337 0.653 4.327 SRM40-6 0.332 0.711 4.003 SRM40-7 0.261 0.763 4.605 SRM50-8 0.231 0.682 4.751 SRM50-9 0.226 0.645 4.855 SRM50-10 0.208 0.717 4.343 _ ~ 1m E V ¼ q ð1 þ mÞð1 2mÞ ~2 this paper we try to establish a damage evolution equation and a constitutive model for SRM specimens by UPV testing. According to classic damage mechanics, the damage factor can be defined as follows: ~ D ¼ 1 E=E ð2Þ where D is the damage factor, E~ and E are the undamaged and damaged Elastic modulus. When the longitudinal ultrasonic wave with a certain frequency goes through the SRM specimens, the velocity v, bulk density q, modulus of elastic E and Poisson’s ratio m exist in the following relationship: 123 If the change of the Poisson’s ratio and density are ignored during loading for damage specimens, ð4Þ ð5Þ where V and V~ are the velocity of undamaged and damaged material. This definition is based on the assumption that the initial damage factor of SRM is 0, and the damage factor is 1 when the specimen has failed. Because the changes in ultrasonic wave velocity can comprehensively reflect changes in the internal structure of SRM specimens, phenomenon such as crack initiation, propagation and coalescence can be reflected by UPV. So the damage factor definition based on UPV could completely reflect the macro mechanics of micro cracks for SRM specimens. There will be a problem when the damage factor obtained by Eq. (5); in linear-elastic stage the UPV can increase due to the compaction effect. In this case, D \ 0; however, this is impossible, so we specify it as D = 0. Figure 15 is the relationship between relative stress and the damage factor for typical specimens SRM20-1, SRM304, SRM40-7 and SRM50-10. As shown in the figure, during uniaxial compression, the damage factors for the specimens are not uniform. The damage factor changed suddenly at some stress level and this phenomenon is consistent with the relationship of crack width and relative stress. Cracking damage characteristics of soil and rock 785 Fig. 16 Three-stage damage evolution equation and constitutive model for SRM30-4 Research of the damage mechanics of rock and soil is a fundamental and frontier issue in geotechnical engineering. Experimental research of damage evolution characteristics and constitutive relations are reliable and practical conditions to ensure numerical simulation results in geotechnical engineering. The pre-existing damage constitutive model can be divided into two major categories. One is the continuous function and the other is the piecewise describing function. Because information regarding crack evolution can be reflected via UPV, the damage evolution of an SRM is a nonlinear process; it is difficult to describe the cracking evolution with a continuous function. So, the piecewise describing function is a good choice. Based on results of the stress–strain curve and the crack evolution characteristics above, the pre-peak stress–strain curve can be divided into a quasi linear stage, a stable damage evolution stage and a damage acceleration stage. Taking SRM30-4 as an example, the three-phase damage constitutive model is shown in Fig. 16. According to the damage factor defined by the UPV, the damage factors during the uniaxial compressive test were calculated. Firstly, the relationship of D and e1 was analyzed using the method of least squares regression. Linear (y = ax ? b), logarithmic (y = a ? lnx), exponential (y = aex) and power (y = axb) curve fitting approximations were executed and the approximation equations that have the highest correlation coefficient were determined for the damage evolution equations. Then, based on the equivalent strain principle, the relevant constitutive model is expressed as r1 ¼ Eð1 DÞe1 ð6Þ 1. Quasi linear phase The constitutive model is linear. The constitutive model in this stage by linear curve fitting approximation is expressed as: r1 ¼ 0:0808 þ 5:59408e1 0\r1 \2:44076 MPa ð7Þ The corresponding damage evolution equation is: D¼0 ð8Þ 123 786 Y. Wang, X. Li Table 7 Damage evolution equation and constitutive model for SRM specimens Specimen no. SRM20-1 SRM30-4 SRM40-7 SRM50-10 Evolution stage Damage evolution equation Damage constitutive model Correlation coefficient (r) (1) D=0 r1 = -0.14121 ? 8.97584e1 0.9994 (2) D = 2.27713exp (-1.62444/e1) r1 = E(1-2.27713exp (-1.62444/e1)) e1 0.8865 (3) D = 0.57467e1.57493 1 r1 = E(1-0.57467e1.57493 )e1 1 0.9394 (1) D=0 r1 = 0.0808 ? 5.59408e1 0.9994 (2) D = 2.4852exp (-1.43659/e1) r1 = E(1-2.4852exp (-1.43659/e1))e1 0.9452 (3) D = 0.7895e1.57493 1 r1 = E(1-0.7895e1.57493 )e1 1 0.9913 (1) D=0 r1 = 0.0291 ? 4.45117e1 0.9855 (2) D = 1.00844exp (-0.40446/e1) r1 = E(1-1.00844exp (-0.40446/e1))e1 0.9265 (3) D = 1.15365exp (-0.38258/e1) r1 = E(1-1.15365exp (-0.38258/e1))e1 0.8928 (1) (2) D=0 D = 1.50392exp (-1.26212/e1) r1 = 0.04665 ? 2.81125e1 r1 = E(1-1.50392exp (-1.26212/e1))e1 0.9731 0.9853 (3) D = 1.05582e1.78802 1 r1 = E(1-1.05582e1.78802 )e1 1 0.9175 2. Damage initiation and stable development stage: r1 ¼ Eð1 DÞe1 ð9Þ According to the damage factor defined by UPV, the damage factor during uniaxial compressive tests is calculated, and the relationship between D and e1 is analyzed using least squares regression. Linear (y = ax ? b), logarithmic (y = a ? lnx), exponential (y = aex) and power (y = axb) curve fitting approximations were executed and the approximation equations that have the highest correlation coefficient were determined for the damage evolution equation: D ¼ 2:4852expð1:43659=e1 Þ ð10Þ Combination with equations (9) and (10), the constitutive model of SRM30-4 in this stage is expressed as: r1 ¼ Eð1 2:4852 expð1:43695=e1 ÞÞ e1 2:44076\r1 \4:13248 MPa ð11Þ 3. Damage acceleration stage: In this stage, the relationship of D and e1 was analyzed using least squares regression. The damage evolution equation was as follows: D¼ 0:7895e0:4639 1 ð12Þ Combination with Eqs. (5) and (6), the constitutive model of SRM30-4 in this stage is expressed as: e1 4:13248\r1 \4:77452MPa r1 ¼ E 1 0:7895e0:4639 1 ð13Þ Correlation coefficients (r) were 0.9994, 0.94524 and 0.9913 for SRM30-4, respectively. The damage evolution 123 equation and constitutive model for SRM20-1, SRM40-7 and SRM50-10 were obtained using the same method (Table 7). As shown in Table 7, the correlation coefficient of all equations are very good, but they do not necessarily indicate the goodness-of-fit of the equations. Thus, validation of the equations was checked by a t and F test. The significance of the r values can be determined by the t test, which compares the computed t value with the tabulated t value using a null hypothesis. The significance of the regressions was determined by analysis of variance (F test). In these tests, a 95 % condidence interval (p B 0.05) was chosen. It is well known that if the computed t and F values are greater than the tabulated t and F values, the null hypothesis is rejected (Levine et al. 2011). In this regard, computed t and F values are greater than the tabulated t and F values, indicating the validity of these equations (Table 7). Figure 17 illustrate the stress–strain curve using measured and estimated data. As is shown, the estimated curve was in agreement with the measured curve. Conclusions The present work encompassed a series of UPV tests on SRM specimens with different rock percentages (i.e., 20, 30, 40 and 50 %), in an effort to contribute to the field of UPV, a non-destructive technique for researching mechanical properties and cracking evolution in real-time. An experimental system was developed to match the UPV tests. A technique that can be applied to structurally cracked elements in order to explore the cracking Cracking damage characteristics of soil and rock Fig. 17 Stress–strain curves for measured and estimated data characteristics of SRMs using UPV testing has been conducted. Because deformation of the middle part is most evident under uniaxial compressive tests, the ultrasonic transducer (500 kHz) was installed in the middle part of specimens. Test results revealed that UCS and UPV deceased with an increasing rock percentage for all specimens. Specimens with a different rock percentage failed by a combination of splitting and sliding failures; the macrocracks were 0–10° parallel to the axial of specimen. A relationship between crack widths and UPV was established. Crack evolution is reflected by the change in UPV, and the non-linear failure process of SRMs was divided into three stages. 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