Enthalpies of Sublimation of Organic and Organometallic Compounds.
1910–2001
James S. Chickosa…
Department of Chemistry, University of Missouri-St. Louis, Saint Louis, Missouri 63121
William E. Acree, Jr.b…
Department of Chemistry, University of North Texas, Denton, Texas 76203
共Received 22 October 2001; accepted 11 February 2002; published 7 June 2002兲
A compendium of sublimation enthalpies, published within the period 1910–2001
共over 1200 references兲, is reported. A brief review of the temperature adjustments for the
sublimation enthalpies from the temperature of measurement to the standard reference
temperature, 298.15 K, is included, as are recently suggested values for several reference
materials. Sublimation enthalpies are included for organic, organometallic, and a few
inorganic compounds. © 2002 American Institute of Physics.
Key words: compendium; enthalpies of condensation; evaporation; organic compounds; organometallic
compounds; sublimation; sublimation enthalpy.
enthalpies to 298.15 K. . . . . . . . . . . . . . . . . . . . . . .
2. A hypothetical molecule illustrating the different
hydrocarbon groups in estimating Cp. . . . . . . . . . .
Contents
1. Introduction. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
2. Heat Capacity Adjustments. . . . . . . . . . . . . . . . . . .
3. Group Additivity Values for C p c (298.15 K)
Estimations. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
4. Reference Materials for Sublimation Enthalpy
Measurements. . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
5. Sublimation Enthalpy Compendium. . . . . . . . . . . .
6. References for Tables 6 and 7. . . . . . . . . . . . . . . . .
7. Acknowledgments. . . . . . . . . . . . . . . . . . . . . . . . . .
8. References. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
List of Tables
1. Equations for the temperature adjustments of
sublimation enthalpies. . . . . . . . . . . . . . . . . . . . . . .
2. Group values for estimating the C p c (298.15 K)...
3. Some estimations of C p c (298.15 K) using the
group values of Tables 2共A兲 and 2共B兲. . . . . . . . . .
4. Recommended reference standards for
sublimation enthalpy measurements. . . . . . . . . . . .
5. A list of acronyms used in Tables 6 and 7. . . . . . .
6. Reported enthalpies of sublimation of organic
compounds, 1910–2001. . . . . . . . . . . . . . . . . . . . . .
7. Enthalpies of sublimation of some organometallic
and inorganic compounds, 1910–2001. . . . . . . . . .
537
538
541
1. Introduction
539
Sublimation enthalpies are important thermodynamic
properties of the condensed phase. Frequently they are used
in correcting enthalpies of formation to the gas phase and in
evaluating environmental transport properties.1,2 Sublimation
enthalpy measurements are also useful to studies of polymorphism and predictions of molecular packing. The measurements provide benchmark numbers that can be used to validate the calculations.3 Examination of the data in this
compendium will reveal some large discrepancies in reported
enthalpies of sublimation. It is likely that some of the discrepancies reported by different laboratories are due to measurements made on different polymorphic modifications.4
Sublimation enthalpy measurements also can reveal differences in interactions in chiral solids and their racemic modifications. Very little experimental work has been reported in
this respect.5,6
Our interests in sublimation enthalpies goes back nearly 3
decades.5 Initially interested in using sublimation enthalpies
to correct enthalpies of formation data to a standard state, we
have since focused our attention on their measurement,7
estimation,8 and assessment.9 In a parallel study, a compilation of available sublimation enthalpies was initiated in the
1980s.5 A reasonably exhaustive version of this database
covering the literature up to the mid 1990s is available on
line at http://webbook.nist.gov/chemistry/. The present version updates this compilation to the year 2001. Although our
intent has been to provide an exhaustive coverage of the
literature from 1910 to 2001, this listing is probably still far
from complete.
539
539
667
697
697
538
540
542
543
544
545
633
List of Figures
1. A thermodynamic cycle for adjusting sublimation
a兲
Author to whom correspondence should be addressed; electronic mail:
[email protected]
b兲
Electronic mail: [email protected]
© 2002 American Institute of Physics.
0047-2689Õ2002Õ31„2…Õ537Õ162Õ$35.00
538
537
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
538
J. S. CHICKOS AND W. E. ACREE, JR.
⌬ subH m共 298.15 K兲
⫽⌬ subH m共 Tm兲 ⫹
冕
Tm
298.15
共 C p c ⫺Cp g 兲 dT,
共1兲
⌬ subH m共 298.15 K兲
⬇⌬ subH m共 Tm兲 ⫹ 共 C p c ⫺Cp g 兲关 Tm⫺298.15兴 .
FIG. 1. A thermodynamic cycle for adjusting sublimation enthalpies to
298.15 K.
2. Heat Capacity Adjustments
Sublimation enthalpies are measurements based on mass
transport and as such are directly or indirectly dependent
upon vapor pressure. The vapor pressure of different solids at
the same temperature can vary by many orders of magnitude.
In order to obtain a reasonable amount of mass transport, it is
frequently necessary to conduct these measurements at temperatures that differ substantially from the standard reference
temperature, 298.15 K. The actual temperature of measurement depends on the sensitivity of the instrument or apparatus and the properties of the substance. In addition, these
measurements are often conducted as a function of temperature.
The magnitude of the sublimation enthalpy is dependent
on temperature. Figure 1 and Eqs. 共1兲 and 共2兲 illustrate the
origin of this temperature dependence in terms of a thermodynamic cycle. If the heat capacities of the solid and gas
phase are known, C p c and C p g , respectively, then the sublimation enthalpy at 298.15 K can be related to the experimental measurements by using Eq. 共1兲. This equation, generally
referred to as Kirchhoff’s equation, can be used to adjust
sublimation enthalpy measurements to any reference temperature. Tm represents either the temperature of measurement for calorimetric measurements or the mean temperature
of measurement for experiments conducted over narrow
ranges of temperature. Treating the heat capacities of the two
phases as independent of temperature and integrating Eq. 共1兲
results in Eq. 共2兲. Since the magnitude of the heat capacity of
the gas phase is usually smaller than that of the solid phase
共c兲, sublimation enthalpies increase with decreasing temperature
Experimental heat capacities for many solids at 298.15 K
are available.10 Experimental gas phase heat capacities for
compound that are solids at 298.15 K are unavailable and
generally need to be estimated. Gas phase heat capacities can
be calculated from statistical mechanics or estimated by
group additivity methods.11 A number of group additivity
methods have been developed to estimate gas phase heat
capacities.11–13 However, group values for some functional
groups are not available. This has encouraged the development of other estimation methods. Table 1 briefly summarizes the various equations that have been used in place of
the second term in Eq. 共2兲.
Equation 共3兲 can easily be derived by assuming that the
gas is ideal and that the Dulong–Petit value of 3RN holds for
the solid, where the term R represents the gas constant and N
is the number of atoms/molecule.5 A similar relationship but
characterized by a temperature coefficient of 6R 关Eq. 共4兲兴 has
been suggested by Pedley.14 Temperature coefficients of 40
J mol⫺1 have been used by Melia and Merrifield,15 and a
value of 60 J mol⫺1 has been used by de Kruif et al.16 for a
series of amino acids and peptides.
A major limitation of most of the equations listed in Table
1 is that the heat capacity adjustments are treated as universal
constants independent of molecular structure. Only Eq. 共7兲 is
sensitive to differences in molecular structure. This equation
was derived from a correlation using estimated heat capacities of the solid at 298.15 K.17 This correlation was developed from the observed dependence of the temperature adjustment on both molecular structure and size.17
Experimental or estimated values of C p c (298.15 K) can be
used in this equation.
Previous work has demonstrated that Eq. 共7兲 gives results
that are generally as good as or better than the use of the
other equations in Table 1.7,8共b兲,18 The use of Eq. 共7兲 should
be limited to the temperature range 200–500 K. A standard
deviation of ⫾33 J mol⫺1 has been associated with the term:
关 0.75⫹0.15C p c (298.15 K) 兴 . The total uncertainty of the
temperature adjustment depends on both the magnitude of
C p c and Tm . In applications, an uncertainty of one-third of
TABLE 1. Equations for the temperature adjustments of sublimation enthalpies
Corrections for the sublimation enthalpies 共J mol⫺1兲
(C p c ⫺Cp g ) 关 Tm⫺298.15兴 ⫽2R关 Tm⫺298.15兴
(C p c ⫺Cp g ) 关 Tm⫺298.15兴 ⫽6R关 Tm⫺298.15兴
(C p c ⫺Cp g ) 关 Tm⫺298.15兴 ⫽40关 Tm⫺298.15兴
(C p c ⫺Cp g ) 关 Tm⫺298.15兴 ⫽60关 Tm⫺298.15兴
(C p c ⫺Cp g ) 关 Tm⫺298.15兴 ⫽ 关 0.75⫹0.15C p c (298.15 K) 兴关 Tm⫺2.98兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
共2兲
Equation
Reference
共3兲
共4兲
共5兲
共6兲
共7兲
5
14
15
16
17
ENTHALPY OF SUBLIMATION
the total temperature adjustment has been arbitrarily chosen
as the uncertainty 共⫾2 ␴兲.9
Equations 共3兲–共6兲 do not require C p c values; their use can
be an advantage if an appropriate group value or experimental heat capacity is unavailable for a particular substance.
Temperature adjustments to 298.15 K are often small and
frequently of the same order of magnitude as the uncertainty
associated with the measurement. This is the rationale some
authors give for not adjusting the measurements for temperature. It should be emphasized that the magnitude of the sublimation enthalpy will increase with decreasing temperature
and even though the temperature adjustment may be small,
failure to adjust for temperature incorporates a systematic
error that can easily be minimized by using of one of the
equations in Table 1.
The sublimation enthalpies reported in this paper, have not
been adjusted to 298.15 K unless done so by the reporting
authors. Different authors have used different methods. In
some cases experimental data have been used for C p c and
only Cp g has been estimated. The reader is encouraged to
refer to the original literature for details. In an effort to provide some assistance to the reader in this regard, a brief
discussion of one of the few group additivity methods that
are available for estimating the heat capacity of solids is
included below.12,19 This is followed by an illustration of
how this value can be used in conjunction with Eq. 共7兲 to
provide temperature adjustments.
3. Group Additivity Values
for C p c „298.15 K… Estimations
Table 2 parts 共A兲 and 共B兲 lists a set of group values that
can be used in estimations of C p c (298.15 K). The groups
and their corresponding values are identified by the italics. A
hypothetical molecule is given in Fig. 2 that identifies each
hydrocarbon group. The functional groups are selfexplanatory. The R terms in Table 2 represent unidentified
groups and are not included in the value. The use of these
group values is illustrated with examples of C p c (298.15 K)
estimations in Table 3. Values in brackets should be considered as tentative assignments. Further details are available in
the literature.19
4. Reference Materials for Sublimation
Enthalpy Measurements
Calibration is a fundamental requirement for every sublimation enthalpy measurement. Unlike other thermochemical
measurements, uncertainties in sublimation enthalpies can be
large, often several kJ mol⫺1 or more, particularly for com-
539
pounds exhibiting low vapor pressures. While some of the
observed differences in reported enthalpies may be due to
polymorphism, others are probably due to the lack of a sufficient number of reference compounds that vary in their
range of volatility. The ability of an experimental technique
to measure vapor pressure in one pressure or temperature
region does not in itself guarantee the same accuracy in another. Substantial variations in sublimation values are revealed in the tables that follow. This variance clearly establishes the importance of documenting the accuracy of the
measurements through the use of appropriate reference materials that approximate the temperature and pressure regimes of the measurements.
A series of compounds have recently been proposed as
reference materials.9 These have been classified as primary,
secondary, or tertiary reference materials, on the basis of
various criteria. The materials classified as primary and secondary reference materials are listed in Table 4. The temperature range, the corresponding vapor pressures, and the
recommended values are also included in the table.
5. Sublimation Enthalpy Compendium
The sublimation enthalpies, reported during the time period 1910–2001, are included in Tables 6 and 7. Table 5
contains a listing of the acronyms that are used in these two
tables. Table 6 contains sublimation enthalpy data for organic
compounds and Table 7 contains data for organometallic and
a few inorganic compounds. Information in Table 6 is organized as shown below. Compounds are arranged according to
molecular formula. The name of the compound, occasionally
a synonym, and the CAS registry number are included on the
first line. If the information was available, the first entry on
the second line contains information regarding the polymorphic form studied. However, in most cases this information
was not available. The range of temperatures studied is the
next entry in the table. For measurements performed at a
constant temperature or when not specified, this entry is left
blank. The sublimation enthalpy at the mean temperature of
measurement ⌬ subH m(T m) is the next entry followed by the
mean temperature 共K兲, an acronym briefly describing the
type of measurement, and the reference to the original work.
In some cases the type of measurement was not available, or
recorded. In these instances this entry was left blank. If the
authors of the work have adjusted their results to 298.15 K,
then this information along with the reference is entered on
the third line. This information is repeated for multiple measurements. The measurements are arranged in reverse chronological order. A similar format is followed in Table 7 with
the major exception that each organometallic compound is
arranged alphabetically by element and then according to the
Hill system.
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
540
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 2. Group values for estimating the C p c (298.15 K)
共A兲 Group values for estimating the C p c (298.15 K) of hydrocarbons.a
Hydrocarbon Groups
Aliphatic groups
Description of group
Formula
primary sp 3 C
secondary sp 3 C
tertiary sp 3 C
quaternary sp 3 C
– CH3
– CH2 –
–CHR–
– CR3
Cyclic aliphatic and olefinic groups
⫺1
JK
mol
⫺1
36.6
26.9
9
⫺5
Description of group
Formula
J K⫺1 mol⫺1
secondary sp 3 C
tertiary sp 3 C
quaternary sp 3 C
tertiary sp 2 C
quaternary sp 2 C
– Cc H2 –
– Cc HR–
– Cc R2 –
– Cc HR–
– Cc R2 –
24.6
11.7
6.1
15.9
关4.7兴
cyclic
cyclic
cyclic
cyclic
cyclic
Olefinic and Acetylenic Groups
Aromatic Groups
Description of group
Formula
J K⫺1 mol⫺1
secondary sp 2 C
tertiary sp 2 C
quaternary sp 2 C
vCH2
vCH–
vC–
46
21.4
6.9
tertiary sp C
quaternary sp C
wC–H
wC–
37.1
15.5
Description of group
Formula
J K⫺1 mol⫺1
tertiary aromatic sp 2 C
quaternary aromatic sp 2 C
internal quaternary
aromatic C
vCa H–
vCa R–
vCa R–
17.5
8.5
关9.1兴
共B兲 Group values for estimating the C p c (298.15 K) contribution of various functional groups.
Monodentate functional groups
Description of group
Alcohols, phenols
Fluorine
Chlorine
Bromine
Iodines
Nitrile
Carboxylic acid
Acid chloride
Aldehyde
Isocyanate
Nitro group
Secondary sp 3
Nitrogen
Primary amides
Thiols
Sulfonamide
Substituted urea
Formula
Tridentate functional groups
⫺1
JK
mol
–OH
–F
–Cl
–Br
–I
–CN
– CO2 H
–COCl
– (CvO)H
–NCO
– NO2
– NH2
23.5
关24.8兴
28.7
32.4
关27.9兴
42.3
53.1
关60.2兴
关84.5兴
关52.7兴
56.1
21.6
– CONH2
–SH
– SO2 NH2
– NHCONH2
54.4
关51.9兴
104
82.8
⫺1
Description of group
Formula
J K⫺1 mol⫺1
tertiary sp 3 N
tertiary sp 2 N
cyclic tertiary sp 2 N
cyclic tertiary sp 3 N
cyclic tertiary amide
cyclic imide
phosphine oxide
– NR2
vN–
vNc –
– Nc R–
–CONR–
–CONHCO–
–共PO兲R–
关31.5兴
Bidentate functional groups
Description of group
Ketones
Cyclic ketones
Ester
Lactones
Cyclic carbonates
Cyclic anhydrides
Ether
Cyclic ether
Secondary sp 3 N
Cyclic secondary
sp 3 N
Tertiary sp 2 N
Secondary amide
Formula
Tetradentate function groups
⫺1
JK
mol
–CO–
– (CO) c –
– CO2 R
– CO2 –
– OCO2 –
– CO2 CO–
–O–
–Oc–
–NH–
– Nc H–
28
34.3
40.3
45.2
关68.2兴
80.3
49.8
9.7
⫺0.3
23.9
vNH
–CONH–
10.7
44.4
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
13.9
1.2
52.7
74.1
28.5
⫺1
Description of group
Formula
J K⫺1 mol⫺1
quaternary silicon
quaternary tin
quaternary germanium
– SiR2 –
– SnR2 –
Ge
32.4
77.2
18.9
ENTHALPY OF SUBLIMATION
541
TABLE 2. Group values for estimating the C p c (298.15 K)—Continued
Bidentate functional groups
Tetradentate function groups
⫺1
Description of group
Formula
Cyclic secondary
amide
Tertiary sp 3 N
Cyclic urea
Carbamates
Sulfides
Cyclic sulfides
Disulfides
Sulfoxides
Sulfones
–CONH–
46.4
– NR2
–NHCONH–
–OCONH–
–S–
– Sc –
–S–S–
–SO–
– SO2 –
31.5
63.6
76.1
116
20.3
41
47.7
88.7
a
JK
mol
⫺1
Description of group
Formula
J K⫺1 mol⫺1
See Ref. 19.
FIG. 2. A hypothetical molecule illustrating the different hydrocarbon
groups in estimating Cp.
The authors have made an effort to present the data accurately and without error. However some of the information
has been obtained from non-English journals with translations occasionally provided by the author’s students. These
tables have been complied over a period of 25 years and
have gone through numerous revisions. Some errors have
been corrected; however it is unlikely that all the errors
have been detected and corrected. The reader is encouraged
to consult the original literature when using this compendium.
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
542
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 3. Some estimations of C p c (298.15 K) using the group values of Tables 2共A兲 and 2共B兲
*Domalski and Hearing.10
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
ENTHALPY OF SUBLIMATION
543
TABLE 4. Recommended reference standards for sublimation enthalpy measurementsa
Formula
Substance
Temperature
range
共K兲
C7 H6 O2
C10H8
C10H10Fe
C14H10
C16H10
I2
Benzoic acid
Naphthalene
Ferrocene
Authracene
Pyrene
Iodine
298 –383
250–353
277–360
338 –360
350– 420
273–387
a
Vapor pressure
共Pa兲
⌬ subH m(298.15 K)
共kJ mol⫺1兲
Classification
0.1–360
0.1–995
0.1–166
0.1–1.0
0.2–50
4 –12 600
(89 700⫾1000)
(72 600⫾600)
(73 420⫾1080)
(103 360⫾2670)
(100 200⫾3590)
(62 440⫾82)
Primary
Primary
Primary
Secondary
Secondary
Secondary
See Ref. 9.
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
544
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 5. A list of acronyms used in Tables 6 and 7
A
B
BE
BG
C
CATH
GC
CGC–DSC
DBM
DM
DSC
E
EB
EM
EV
GS
GSM
HSA
I
IPM
KG
LE
MCV
ME
MEM
MG
MM
MS
NA
OM
PG
QF
QR
RG
SG
SMZG
T
TC
TB
TE
TGA
TPTD
TRM
TSGC
U
UV
V
VG
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
calculated from the vapor pressure data reported by the method of least squares
calculated from the sum of the enthalpy of vaporization at temperature T and the
enthalpy of fusion at the melting point
experimental value closest to the results obtained by adding the experimental
fusion and vaporization enthalpies
Bourdon gauge
calorimetric determination
cathetometer
gas chromatography
combined correlation gas chromatography–differential scanning calorimetry
dibutyl phthalate manometer
diaphram manometer
differential scanning calorimeter
estimated
ebulliometer
effusion manometer
evaporation
gas saturation, transpiration
glass spring manometer
head space analysis
isoteniscope
inclined piston manometry
Knudsen gauge
Langmuir evaporation
method of calibrated volume
Mass effusion–Knudsen effusion
modified entrainment method
McLeod gauge
mercury manometer
mass spectrometry
not available at the time of publication
oil manometer
Penning gauge
quartz fiber
quartz resonator
Rodebush gauge
spoon gauge
silica membrane zero gauge
tensimeter
thermal conductivity manometer
thermobalance
torsion effusion
thermal gravimetric analysis
temperature programmed thermal desorption particle beam mass spectrometry
thermoradiometric method
temperature scanning gas chromatography
unreliable
ultraviolet absorption
viscosity gauge
MKS baratron vacuum gauge
ENTHALPY OF SUBLIMATION
545
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001
Molecular formula
Polymorph
CBrN
CBr4
共monoclinic兲
共monoclinic兲
共cubic兲
共cubic兲
CCl4
CFN
CF2 N2
CF2 O
关␣兴
关␤兴
CF5 N
CIN
CN4 O8
CO
CO2
CHF3
CHI3
CHN
CHN3 O6
CH2 N2
Temperature range 共K兲
cyanogen bromide
共273–308兲
共256 –308兲
carbon tetrabromide
CClN
CF4
Compound
共295–319兲
共321–329兲
共277–363兲
cyanogen chloride
共196 –259兲
carbon tetrachloride
共209–225兲
共227–248兲
cyanogen fluoride
共147–191兲
共139–192兲
共133–203兲
difluorocyanamide
共179–198兲
carbonyl fluoride
共130–159兲
tetrafluoromethane
共76 –90兲
共70–76兲
共86 – 89兲
共80– 86兲
pentafluoromethyl amine
共128 –141兲
cyanogen iodide
共337– 426兲
共298 – 414兲
共337– 426兲
共278 –374兲
tetranitromethane
共255–286兲
carbon monoxide
共54 – 61兲
共51– 68兲
共57– 68兲
carbon dioxide
共198 –216兲
共70–102兲
共139–195兲
共154 –196兲
trifluoromethane
共89–118兲
iodoform
共308 –365兲
hydrogen cyanide
共244 –258兲
共202–254兲
trinitromethane
cyanamide
共227–289兲
⌬ subH m /kJ mol⫺1
CAS registry number
(Tm /K)
45.2⫾4.2
47
Method
MM
GS
54.5⫾0.7
54.4⫾1.3
49.4⫾1.3
48.3
51.9
共298兲
共307兲
共325兲
共320兲
共320兲
C
BG
BG
35.7
共228兲
A
43.3
38.8
37.9
共226兲
共217兲
B
28.9
24.4
29.3
共176兲
共166兲
共168兲
20.6 共liq兲
共189兲
23.2
共145兲
14.7
16.8
14.7
17.0
14.0
共83兲
共73兲
共88兲
共76兲
共83兲
18.6
共135兲
59.9
58.6
59.8⫾0.4
58.3
共352兲
共356兲
47.4
共271兲
7.6
8.1
7.9
共58兲
共60兲
共62兲
26.1
27.2⫾0.4
26.3
26.2
共207兲
25.6
共103兲
69.9
共323兲
35.6
37.6
共251兲
共228兲
45.2⫾2.1
54.8⫾4.2
46.7⫾0.4
共298兲
75.9
75.2
共290兲
共298兲
A
A
GSM
A
GSM
共326兲
共167兲
共173兲
A
A
LE
A
A
MM
A
TE,ME
Reference
关506-68-3兴
关54/7兴关70/1兴
关20/1兴
关558-13-4兴
关84/3兴
关59/5兴
关59/5兴
关55/8兴
关41/4兴
关506-77-4兴
关47/2兴
关56-23-5兴
关63/6兴
关60/1兴关48/1兴
关48/1兴
关1495-50-7兴
关87/4兴关64/17兴
关47/2兴
关31/1兴
关7127-18-6兴
关87/4兴关66/10兴
关353-50-4兴
关87/4兴关68/3兴
关75-73-0兴
关87/4兴关70/25兴
关87/4兴关70/25兴
关67/19兴
关63/6兴
关33/5兴
关335-01-3兴
关87/4兴关51/18兴
关506-78-5兴
关87/4兴关43/2兴
关47/2兴
关43/2兴关70/1兴
关33/2兴
关509-14-8兴
关87/4兴关41/6兴
关630-08-0兴
关87/4兴
关47/2兴
关31/3兴
关124-38-9兴
关87/4兴
关74/13兴
关47/2兴
关37/5兴
关75-46-7兴
关87/4兴
关75-47-8兴
关43/1兴
关74-90-8兴
关87/4兴关26/4兴
关47/2兴
关517-25-9兴
关99/35兴
关70/7兴
关67/4兴关70/1兴
关77/1兴
关420-04-2兴
关83/7兴
关83/7兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
546
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
CH2 N4
tetrazole
CH2 O2
(CH2 O2 ) 2
CH3 Cl
共333– 404兲
共333–363兲
formic acid
共268 –281兲
共203–218兲
共265–268兲
共253–275兲
formic acid dimer
共203–218兲
methyl chloride
共130–172兲
CH3 Cl2 OP
methylphosphonic dichloride
CH3 I
methyl iodide
共176 –227兲
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
88.16
87.8⫾1.4
88.0⫾1.6
97.5⫾4.2
共353兲
共369兲
60.5
62.1⫾1
60.7
60.1
共275兲
共213兲
共266兲
共264兲
64.1⫾1
共213兲
31.6⫾0.1
28.0
共151兲
共348兲
Method
C
ME
ME
ME
TE,ME
A
TE,ME
B
62.3
CH3 NO
CH3 N5
CH4
CH4 N2 O
formamide
共251–273兲
5-aminotetrazole
共383– 443兲
methane
共53–91兲
共54 –90兲
共79– 89兲
共48 –78兲
共67– 88兲
urea
共338 –362兲
共345–368兲
CH4 N2 S
CH5 N3 O
nitroguanidine
共402– 473兲
N-methylhydroxylamine
共273–308兲
1-methyl-1-nitrosohydrazine
CH5 N3 S
thiosemicarbazide
CH5 O3 P
methylphosphonic acid
CH6 N4 S
thiocarbohydrazide
C2 BrCl5
bromopentachloroethane
共383– 433兲
1,2-dibromotetrachloroethane
CH5 NO
共191兲
VG
72.4
71.7
71.7
共264兲
共298兲
共276兲
TE,ME
112.6⫾1.2
ME
9.7
9.2
10.0
9.7
9.62
共72兲
共72兲
共84兲
共63兲
共77兲
90.9
96.9
98.6
95.4
87.9⫾2.1
共381兲
共351兲
共298兲
共361兲
共356兲
88.2
共357兲
112.0⫾2
109⫾2.0
111⫾3.0
106.6
107.6
112⫾1.5
93.7⫾10
共298兲
共408兲
共298兲
共384兲
共298兲
共298兲
ME
TE
142.7⫾2.0
共298兲
ME
56.6
共288兲
I
79.5⫾0.4
共298兲
125.8⫾1.5
共298兲
C
152.1⫾3.0
共298兲
C
44.4
共398兲
A,MS
A
TE,ME
thiourea
共368 –395兲
CH4 N4 O2
40.2⫾0.4
U 69.9
TE,ME
C
48.1⫾4.2
C2 Br2 Cl4
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
Reference
关288-94-8兴
关93/8兴
关93/8兴
关90/31兴
关51/3兴关70/1兴
关64-18-6兴
关87/4兴
关78/16兴
关30/1兴关60/1兴
关47/2兴
关14523-98-9兴
关78/16兴
关74-87-3兴
关95/23兴
关40/3兴
关676-97-1兴
关70/1兴关55/4兴
关74-88-4兴
关82/6兴
关43/1兴关60/1兴
关75-12-7兴
关83/7兴
关83/7兴
关79/11兴
关4418-61-5兴
关90/31兴
关74-82-8兴
关87/4兴
关63/6兴关55/2兴
关60/1兴
关51/15兴
关47/2兴
关57-13-6兴
关87/5兴
关83/7兴
关83/7兴
关78/19兴
关56/6兴关60/1兴
关70/1兴关87/4兴
关53/1兴
关62-56-5兴
关00/23兴
关94/20兴
关94/20兴
关83/7兴
关83/7兴
关82/8兴
关70/11兴
关556-88-7兴
关78/15兴
关593-77-1兴
关87/4兴关57/11兴
关758-19-0兴
关98/36兴
关79-19-6兴
关82/8兴
关993-13-5兴
关55/4兴关70/1兴
关2231-57-4兴
关82/8兴
关79504-02-2兴
关87/4兴关49/11兴
关630-25-1兴
ENTHALPY OF SUBLIMATION
547
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
C2 Br4
C2 Cl3 F3
C2 Cl4 F2
C2 Cl6
共melting point
186.6兲
triclinic form
cubic form
C2 F2 O2
C2 F6
C2 N2
C2 N6 O12
C2 H2
Compound
(Tm /K)
52.5
56.7
共398兲
共373兲
44.2
共236兲
32.9
共219兲
A
36.4
38.2
共278兲
共265兲
A
58.9
48.8
共331兲
共382兲
A
共286 – 447兲
59.1⫾0.7
共367兲
共286 – 447兲
51
共367兲
共335– 453兲
共288 –333兲
oxalyl fluoride
共234 –260兲
hexafluoroethane
50.5
59.0
共310兲
16.7
共247兲
26
共103兲
33
33.6
34.4
32.4
共224兲
共204兲
共223兲
共224兲
NA
70.7
30.4
70.7⫾1.7
70.7⫾1.7
共298兲
共308兲
共303兲
23.5
21.9
21.8
20.2
25.2
22.7
21.1
22.1
共130兲
共298兲
共162兲
共298兲
共193兲
共160兲
共298兲
共129兲
81
77.7⫾1.4
共302兲
共298兲
I
I
40.7
共258兲
ME
93.4
93.3
98.5
92.5
93.7⫾1.3
97.9⫾2.2
93.3
61.8
90.6
共316兲
共318兲
Temperature range 共K兲
共383– 453兲
共323– 423兲
tetrabromoethylene
共221–310兲
1,1,2-trichloro-1,2,2-trifluoroethane
共205–233兲
1,1,2,2-tetrachloro-1,2-difluoroethane
共235–293兲
共237–293兲
hexachloroethane
共317–345兲
共306 – 459兲
cyanogen
共202–239兲
共177–230兲
共202–245兲
共198 –240兲
共293–343兲
共293–313兲
共293–343兲
acetylene
共98 –145兲
共151–193兲
共130–189兲
C2 H2 I2
C2 H2 O4
␣
␤
␣
␤
␣
共orthorhombic兲
共monoclinic兲
C2 H3 ClO2
共89–169兲
trifluoroacetamide
共288 –329兲
共288 –329兲
trans-diiodoethylene
共253–265兲
oxalic acid 共anhydrous兲
共303–328兲
共310–325兲
共303–328兲
共311–325兲
共311–323兲
共292–320兲
共333–378兲
chloroacetic acid
75.3⫾4.2
C2 H3 Cl3 O2
Method
A
GS,A
A
MM
hexanitroethane
共133–191兲
C2 H2 F3 NO
CAS registry number
⌬ subH m /kJ mol⫺1
trichloroacetaldehyde hydrate
共298兲
共318兲
共317兲
共306兲
ME
Reference
关87/4兴关49/11兴
关35/4兴
关79-28-7兴
关87/4兴
关76-13-1兴
关47/2兴
关76-12-0兴
关87/4兴关47/2兴
关47/2兴
关67-72-1兴
关87/4兴
关47/2兴
关47/3兴关60/1兴
关70/1兴关41/1兴
关47/3兴关60/1兴
关41/1兴
关35/3兴
关30/6兴
关359-40-0兴
关87/4兴
关76-16-4兴
关63/6兴关48/4兴
关460-19-5兴
关87/4兴
关47/2兴
关39/2兴
关25/2兴关75/10兴
关16/1兴
关918-37-6兴
关99/35兴
关87/4兴关63/10兴
关69/10兴关77/1兴
关68/5兴
关74-86-2兴
关87/4兴
H
关60/1兴
H
A
H
A
TE
A
GS
关56/18兴
关47/2兴
关43/4兴
关354-38-1兴
关87/4兴关78/6兴
关78/6兴
关590-27-2兴
关33/1兴关60/1兴
关87/4兴
关144-62-7兴
关87/4兴
关87/4兴
关83/23兴
关83/23兴
关75/5兴
关53/4兴关60/1兴
关53/4兴关60/1兴
关47/6兴
关26/3兴
关79-11-8兴
关28/1兴关49/4兴
关70/1兴
关302-17-0兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
548
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C2 H3 FN2 O5
共263–319兲
2-fluoro-2,2-dinitroethanol
C2 H3 NO3
oxalic acid, monoamide
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
50.9
Method
Reference
共291兲
A
108.9⫾2.1
107.9
共298兲
共359兲
ME
ME
31.5
共266兲
A
80.7⫾0.5
84.1
84.0⫾0.7
80.6⫾0.5
84.1
共298兲
共288兲
共298兲
C
ME
ME
72.0⫾8.8
共298兲
18.4
15.3
44.5 共liq兲
44.2
15.0
44.3 共liq兲
43.7
共91.5兲
共298兲
共274兲
共298兲
A,MS
H
关47/2兴
关17003-75-7兴
关77/1兴关68/7兴
关471-47-6兴
关88/18兴
关53/1兴关60/1兴
关87/4兴
关556-61-6兴
关47/2兴
关288-88-0兴
关99/8兴
关89/8兴
关89/8兴
关85/6兴
关61/3兴
关595-86-8兴
关99/35兴
关74-85-1兴
关87/4兴关51/15兴
共260兲
共298兲
A
H
54.8
49.8
共239兲
共258兲
A
205.1⫾0.7
100.8
共356兲
ME
117.3⫾1.2
115.8
113.0
共298兲
共387兲
共361兲
TE,ME
TE,ME
ME
103.8
105.1
105.4
共298兲
共361兲
共369兲
TE,ME
TE,ME
ME
128.7
共436兲
TE,ME
55.6⫾2.1
共355–363兲
C2 H3 NS
C2 H3 N3
methyl isothiocyanate
共238 –293兲
1,2,4-triazole
共281–296兲
共281–296兲
C2 H3 N3 O6
1,1,1-trinitroethane
C2 H4
ethylene
共79–104兲
共237–289兲
共77–103兲
共237–283兲
C2 H4 Br2
1,2-dibromoethane
共229–248兲
共251–281兲
C2 H4 I2
1,2-diiodoethane
C2 H4 N2 O2
diformylhydrazine
共340–373兲
共370– 403兲
oxamide
ME
关87/4兴
H
65.7⫾4.1
C2 H4 N2 O2
共370–398兲
共353–369兲
C2 H4 N2 S2
dithiooxamide
共345–372兲
共360–378兲
C2 H4 N4
C2 H4 N4
C2 H4 N4
C2 H4 O2
(C2 H4 O2 ) 2
C2 H4 O3
C2 H5 NO
dicyandiamide
共420– 450兲
1-methyltetrazole
共282–311兲
5-methyltetrazole
共323– 418兲
acetic acid
共243–289兲
共213–230兲
共213–230兲
acetic acid dimer
共213–230兲
共213–230兲
methyl hydrogen carbonate
共204 –237兲
acetamide
共273–293兲
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
86.7⫾1.9
ME
93.8⫾0.5
ME
54.5 共liq兲
67.3⫾1
70⫾1
共274兲
共223兲
共213兲
TE,ME
TE,ME
70.2⫾1
68.9⫾1
共213兲
共213兲
TE
ME
18.2⫾1.6
共220兲
78.5⫾0.3
77.8
77.2
共284兲
共298兲
TE,ME
关82/19兴
关47/2兴
关106-93-4兴
关48/1兴
关48/1兴关47/2兴
关87/4兴
关624-73-7兴
关54/6兴关70/1兴
关628-36-4兴
关80/11兴
关56/6兴关60/1兴
关471-46-5兴
关88/18兴
关83/7兴
关53/1兴
关60/1兴关70/1兴
关79-40-3兴
关88/18兴
关83/7兴
关53/1兴关60/1兴
关87/4兴
关461-58-5兴
关83/7兴
关16681-77-9兴
关90/31兴
关4076-36-2兴
关90/31兴
关64-19-7兴
关87/4兴
关78/16兴
关78/16兴
关78/16兴
关78/16兴
关7456-87-3兴
关73/9兴
关60-35-5兴
关98/38兴
关83/7兴
关83/7兴
ENTHALPY OF SUBLIMATION
549
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
C2 H5 NO2
C2 H5 NO2
C2 H5 NS
C2 H5 N5
C2 H5 N5
C2 H6
C2 H6 N2 O
C2 H6 N2 O2
C2 H6 N2 S
Compound
Temperature range 共K兲
共298 –349兲
共293–306兲
methyl carbamate
共287–305兲
glycine
共408 – 431兲
共325– 425兲
共413– 450兲
共453– 471兲
共412– 417兲
thioacetamide
1-methyl-5-aminotetrazole
共379– 438兲
2-methyl-5-aminotetrazole
共310–373兲
ethane
共80–90兲
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
78.7⫾0.3
80.3⫾1
80.3⫾1.3
77.4⫾0.4
U57.2
共298兲
共298兲
共323兲
共300兲
C
GS
74.5⫾0.8
共296兲
GS
136.5⫾2
U 96.2⫾4
138.1⫾4.6
136.4⫾4.0
共419兲
共375兲
共298兲
共462兲
TE,ME
LE
C
ME
130.5⫾2
共414兲
ME
83.3⫾0.3
82.8⫾0.3
共298兲
共298兲
C
C
Method
116.4⫾1.7
ME
90.6⫾1.1
ME
22.6
20.5
共85兲
共90兲
94.4⫾0.84
97.1⫾0.4
94.9⫾0.6
93.3⫾1.2
87.3
99.3⫾0.7
78.2
共343兲
共298兲
共337兲
共355兲
共348兲
69.9
共319兲
DBM
112.9⫾3
111⫾3.0
共298兲
共381兲
ME
TE
B
N-methylurea
N-methyl-N-nitromethanamine
共315–324兲
N-methylthiourea
C2 H6 O2 S
dimethyl sulfone
C2 H6 O4
bis-hydroxymethyl peroxide
C
C
TE
E
77.0⫾2.9
C2 H8 N2
C2 H8 N6 O2
C3 HN
C3 H2 N2
C3 H2 OS2
C3 H2 OS3
C3 H3 N3
CH2 N4
C3 H3 N3 O2
C3 H3 N3 O3
94.1⫾4.2
ethylenediamine
共242–278兲
65.6
1,1⬘ -共1,2-ethanediyl兲bis共1-nitrosohydrazine兲
172.4⫾1.3
cyanoacetylene
共247–279兲
42.3
malononitrile
共278 –299兲
78.2⫾1.0
79.1⫾8
1,3-dithiol-2-one
73.6⫾0.8
1,3-dithiole-2-thione
75.4⫾0.4
1,3,5-triazine
共212–229兲
58.2
54.2⫾0.2
共283–313兲
56.5⫾2.1
tetrazole
共242–264兲
U 43.1
6-azauracil
141
cyanuric acid
ME
共263兲
IPM
共298兲
共264兲
共298兲
ME
共298兲
共298兲
共222兲
共298兲
TE,ME
共253兲
ME
LE
Reference
关75/18兴关77/1兴
关71/16兴
关65/8兴
关59/3兴关87/4兴
关52/4兴
关598-55-0兴
关59/4兴
关56-40-6兴
关79/1兴
关77/2兴
关77/3兴
关65/1兴关70/1兴
关64/16兴
关59/1兴
关62-55-5兴
关82/7兴关85/5兴
关82/17兴
关5422-44-6兴
关90/31兴
关6154-04-7兴
关90/31兴
关74-84-0兴
关72/26兴
关63/6兴
关598-50-5兴
关93/17兴
关93/17兴
关90/25兴
关90/5兴关87/5兴
关87/5兴
关86/6兴
关82/13兴
关4164-28-7兴
关52/2兴关77/1兴
关598-52-7兴
关00/23兴
关94/20兴
关67-71-0兴
关70/1兴关U/3兴
关17088-73-2兴
关53/3兴关70/1兴
关107-15-3兴
关87/4兴关75/32兴
关216489-95-1兴
关98/36兴
关1070-71-9兴
关87/4兴
关109-77-3兴
关90/18兴
关67/3兴关70/1兴
关2314-40-1兴
关73/16兴关77/1兴
关930-35-8兴
关73/16兴关77/1兴
关290-87-9兴
关83/7兴
关82/16兴
关82/9兴
关288-94-8兴
关68/8兴
关461-89-2兴
关74/8兴
关108-80-5兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
550
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
Compound
Temperature range 共K兲
共440– 473兲
C3 H3 N5 O10
1,1,1,2,2-pentanitropropane
C3 H4 N2
imidazole
共292–309兲
共288 –310兲
C3 H4 N2
pyrazole
共268 –287兲
共253–273兲
C3 H4 N2 O
C3 H4 N2 O4
2-cyanoacetamide
共325–348兲
3-nitro-2-isoxazoline-2-oxide
C3 H4 OS2
1,3-dithiolan-2-one
C3 H4 O2 S
thiete sulfone 共2H-thiete-1,1-dioxide兲
C3 H4 O3
ethylene carbonate
共273–297兲
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
131
133
共458兲
共298兲
77.4⫾1.3
共298兲
83.1⫾0.2
83.1⫾0.2
80.8
74.5⫾0.4
85.3
共300兲
共298兲
共301兲
共298兲
共298兲
ME
ME
ME,TE
C
74.3⫾0.4
74.0⫾0.4
72.7
69.2⫾3
71.8
67.7
共275兲
共298兲
共265兲
共298兲
ME
99.7
共336兲
TE,ME
Method
Reference
ME,TE
关83/7兴
关83/7兴
关62626-83-9兴
关99/35兴
关288-32-4兴
关87/9兴
关86/15兴
关83/7兴
关80/5兴
关61/3兴
关288-13-1兴
关87/9兴
关87/9兴关86/15兴
关83/7兴
关80/5兴
关79/11兴
关61/3兴
关107-91-5兴
关83/7兴
关4122-45-6兴
关77/1兴关69/10兴
关2080-58-2兴
关73/16兴关77/1兴
关7285-32-7兴
关69/11兴关77/1兴
关96-49-1兴
关87/4兴关71/12兴
关77/1兴
关70/1兴关58/1兴
关141-82-2兴
关99/10兴
关99/10兴
关87/4兴关47/6兴
关83/26兴
关80-69-3兴
关83/26兴
关822-38-8兴
关67/5兴关70/1兴
关79-06-1兴
关57/6兴
关930-21-2兴
关96/21兴
关75-19-4兴
关63/6兴
TE,ME
C
71.1⫾8.4
80.3⫾0.4
83.7⫾2.5
78.5⫾4.2
B
共285兲
ME
共348兲
共298兲
共306兲
ME
73.2⫾2.5
C3 H4 O4
malonic acid
共339–357兲
共291–320兲
C3 H4 O5
tartronic acid
C3 H4 S3
C3 H5 NO
1,3-dithiolan-2-thione
共294 –303兲
acrylamide
共303–358兲
2-azetidinone
C3 H6
cyclopropane
108.9⫾0.7
111.4⫾0.7
72.7
105.1⫾0.8
116.4⫾0.3
C3 H5 NO
C3 H6 N2 O
C3 H6 N2 O2
C3 H6 N2 O2
C3 H6 N4
C3 H6 N6
C3 H6 N6 O3
共115–141兲
2-imadazolidinone
acetylurea
共360– 407兲
malonamide
共397– 403兲
1,5-dimethyltetrazole
共303–343兲
2,4,6-triamino-s-triazine 共melamine兲
共417–531兲
共417– 447兲
N,N⬘ ,N⬙ -trinitrosohexahydrotriazine
共343– 447兲
共383– 411兲
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
A
C
C
81.8⫾0.8
共298兲
81.8
共330兲
77.4⫾0.3
共298兲
ME
29.2
27.4
28.2
共145兲
共298兲
共128兲
B
H
A,MS
83.7
共298兲
102.4⫾0.7
103.1⫾0.7
103.1⫾0.7
共383兲
共298兲
共298兲
C
126.4⫾0.5
共298兲
C
86.2⫾1.0
C
ME
121.3⫾4.2
123.3
共474兲
共432兲
GS
134.3⫾0.7
112.1
112.1
共298兲
ME
ME
关51/15兴
关120-93-4兴
关99/32兴
关591-07-1兴
关88/12兴
关88/12兴
关85/5兴
关108-13-4兴
关89/17兴
关5144-11-6兴
关90/31兴
关108-78-1兴
关60/6兴关70/1兴
关87/4兴
关13980-04-6兴
关78/15兴
关74/11兴
关53/6兴关60/1兴
ENTHALPY OF SUBLIMATION
551
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
(Tm /K)
134.3
112.5⫾0.8
130.1
共298兲
74.1⫾1
73.2⫾1
共233兲
共233兲
TE
ME
81.3⫾1
79.4⫾1
共233兲
共233兲
TE
ME
57.9
55.6
56.5
56.2⫾0.2
共223兲
共298兲
共298兲
共298兲
TE,ME
共320–339兲
93.2⫾0.2
91.5
93.9
共298兲
共331兲
共298兲
ME
TE,ME
acetone oxime
共313–333兲
N-methyl acetamide
59.6
共323兲
I
70.8⫾2.0
54.0
共298兲
75⫾4.0
79.2⫾0.3
73.3
79.1⫾0.4
共298兲
132.8⫾1
132.4⫾1.3
144.8⫾4.2
共414兲
共433兲
共298兲
TE,ME
C
U 105⫾8
138.3⫾8
共392兲
共461兲
LE
ME
133.1⫾0.7
134⫾2
U 105⫾4
共393兲
共298兲
共368兲
C
C
LE
77.7
76.3
71.9
89.1⫾0.8
共265兲
共298兲
共322兲
共299兲
TE,ME
146⫾1
共298兲
C
U 83.7⫾4
共404兲
LE
U 96.2⫾4.2
共387兲
LE
28.5
共86兲
B
91.8⫾1.2
100.3⫾0.2
共354兲
共343兲
TE
92.5⫾1.3
99.1⫾0.4
共357兲
共348兲
TE
87.2⫾0.6
共353兲
TE
Polymorph
Temperature range 共K兲
C3 H6 N6 O6
N,N⬘ ,N⬙ -trinitrohexahydrotriazine
C3 H6 O2
(C3 H6 O2 ) 2
C3 H6 O3
C3 H6 S3
C3 H7 NO
C3 H7 NO
C3 H7 NO
C3 H7 NO2
C3 H7 NO2
C3 H7 NO2
C3 H7 NO2
C3 H7 NO2
C3 H7 NO3
C3 H7 NO2 S
C3 H8
C3 H8 N2 O
C3 H8 N2 O
C3 H8 N2 O
C3 H8 N2 S
CAS registry number
⌬ subH m /kJ mol⫺1
共325–360兲
共329–371兲
propionic acid
共225–238兲
propionic acid dimer
共225–238兲
1,3,5-trioxane
共212–231兲
Method
ME
共350兲
C
C
1,3,5-trithiane
共288 –303兲
propanamide
共283–343兲
共318 –346兲
L-共d兲-alanine
共407– 426兲
共413– 450兲
D-共l兲-alanine
共342– 442兲
共453– 469兲
␤-alanine
共384 – 402兲
共318 – 418兲
ethyl carbamate
共256 –273兲
共292–307兲
sarcosine 共N-methylglycine兲
共380– 413兲
DL-serine
共354 – 454兲
L-cysteine
共337– 437兲
propane
N-ethylurea
共333–365兲
1,1-dimethylurea
共326 –369兲
1,3-dimethylurea
共316 –373兲
1,3-dimethylthiourea
TE
GS
GS
Reference
关121-82-4兴
关78/15兴
关74/11兴
关69/12兴
关79-09-4兴
关78/16兴
关78/16兴
关32574-16-6兴
关78/16兴
关78/16兴
关110-88-3兴
关83/7兴
关83/7兴
关75/17兴
关69/8兴关77/1兴
关291-21-4兴
关01/14兴
关83/7兴
关83/7兴
关127-06-0兴
关87/4兴关75/33兴
关79-16-3兴
关96/21兴
关52/4兴关60/1兴
关79-05-0兴
关00/1兴
关75/18兴关77/1兴
关60/13兴
关59/3兴
关56-41-7兴
关79/1兴关87/4兴
关77/3兴
关77/3兴
关338-69-2兴
关77/2兴
关65/1兴关70/1兴
关64/16兴
关107-95-9兴
关83/24兴
关83/24兴
关77/2兴
关51-79-6兴
关83/7兴
关83/7兴
关76/10兴
关59/4兴
关107-97-1兴
关78/4兴
关302-84-1兴
关77/2兴
关52-90-4兴
关77/2兴
关74-98-6兴
关63/6兴
关625-52-5兴
关90/5兴关87/5兴
关86/6兴关90/5兴
关598-94-7兴
关90/5兴关87/5兴
关86/6兴
关96-31-1兴
关90/5兴关87/5兴
关534-13-4兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
552
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
Compound
Temperature range 共K兲
C3 H8 N2 S
1-ethylthiourea
C3 H8 O2 S
ethyl methyl sulfone
C3 H9 NO2 S
C4 F6 NS2
C4 F12P4
C4 N2
C4 HF6 N3
C4 H2
C4 H2 N2
C4 H2 N2 S
C4 H2 O3
C4 H2 O4
C4 H2 O4
C4 H3 BrN2 O2
C4 H3 FN2 O2
C4 H3 NO3
C4 H4 BrN3 O
C4 H4 Cl4 O2 S
C4 H4 F3 NO3
C4 H4 IN3 O
C4 H4 N2
C4 H4 N2
C4 H4 N2 OS
C4 H4 N2 OS
CH2 N4
(Tm /K)
111.8⫾3
107.3⫾4.0
108⫾3.0
118.8⫾5
77.8⫾2.9
trimethyl amine • sulfur dioxide complex
共292–349兲
60.6
bis共trifluoromethyl兲-1,3,2-dithiazol-2-yl
共253–283兲
49.0⫾1.5
1,2,3,4-tetrakis共trifluoromethyl兲tetraphosphetane
共292–339兲
65.3
dicyanoacetylene
共263–273兲
44.3
3,5-bis共trifluoromethyl兲-1,2,4-triazole
共271–283兲
butadiyne
共190–232兲
共188 –234兲
fumaronitrile
共250–269兲
共245–281兲
4-cyanothiazole
maleic anhydride
共308 –326兲
共308 –325兲
butyndioic acid
Method
Reference
共298兲
共298兲
共361兲
B,HA
B
B
共298兲
ME
关00/23兴
关94/17兴
关94/20兴
关625-53-6兴
关00/23兴
关594-43-4兴
关U/3兴关70/1兴
关177634-55-8兴
关87/4兴关43/3兴
共307兲
共268兲
PG
共307兲
共268兲
I
75.6⫾0.8
74.7⫾0.8
共277兲
共298兲
ME
36.2
36.3
共211兲
A
69.6
68.6
72⫾0.8
共260兲
共298兲
共263兲
TE,ME
73.9⫾0.4
共298兲
C
85.4
68.8
70.0
71.5⫾5
共317兲
共258兲
共298兲
TE,ME
NA
3,4-dihydroxy-3-cyclobutene-1,2-dione
共469– 499兲
152.5
154.3
83.7⫾16.7
5-bromouracil
128.4
5-fluorouracil
NA
2-nitrofuran
75.3⫾2.1
5-bromocytosine
共403– 468兲
148.4⫾1.5
3,3,5,5-tetrachlorotetrahydrothiophene 1,1-dioxide
共303–348兲
88.7
N-共trifluoroacetyl兲aminoacetic acid
共273–393兲
98.8
5-iodocytosine 共4-amino-5-iodopyrimidinone兲
共413– 463兲
144⫾1.5
pyrazine
共288 –317兲
56.2
56.3⫾0.5
succinonitrile
共279–298兲
70⫾0.3
2-thiouracil
129.3
4-thiouracil
tetrazole
125.5
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
CAS registry number
⌬ subH m /kJ mol⫺1
共486兲
共298兲
共298兲
ME
ME,TE
E
LE
共435兲
共325兲
ME
共288兲
共438兲
共303兲
C
共289兲
LE
LE
关00/41兴
关393-02-2兴
关87/4兴关58/20兴
关1071-98-3兴
关57/4兴关75/10兴
关87/4兴
关709-62-6兴
关94/22兴
关94/22兴
关460-12-8兴
关47/2兴
关33/3兴
关764-42-1兴
关83/7兴
关83/7兴
关67/3兴关70/1兴
关1452-15-9兴
关66/5兴关70/1兴
关108-31-6兴
关87/4兴
关83/7兴
关78/10兴
关49/2兴关70/1兴
关110-16-7兴
关72/7兴
关2892-51-5兴
关83/7兴
关83/7兴
关71/5兴关77/1兴
关51-20-7兴
关74/8兴
关51-21-8兴
关02/1兴
关609-39-2兴
关80/28兴关86/5兴
关2240-25-7兴
关75/14兴
关3737-41-5兴
关78/31兴
关383-70-0兴
关87/4兴关60/20兴
关1122-44-7兴
关75/14兴
关290-37-9兴
关95/5兴
关62/4兴关70/1兴
关110-61-2兴
关60/7兴关77/1兴
关141-90-2兴
关74/8兴
关591-28-6兴
关288-94-8兴
关74/8兴
ENTHALPY OF SUBLIMATION
553
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C4 H4 N2 O2
pyrazine 1,4-dioxide
C4 H4 N2 O2
uracil
共394 – 494兲
共452–587兲
共452–587兲
共378 – 428兲
共500–545兲
共393– 458兲
C4 H4 N2 O2 S
C4 H4 N2 O3
C4 H4 N2 S2
C4 H4 N6
C4 H4 N8 O13
C4 H4 N8 O14
C4 H4 O
C4 H4 O2
C4 H4 O2
C4 H4 O3
C4 H4 O4
C4 H4 O4
C4 H4 O4
C4 H4 S
C4 H5 N
thiobarbituric acid
共400– 461兲
barbituric acid
共294 – 438兲
共392– 493兲
共404 – 479兲
2,4-dithiouracil
共393– 443兲
8-azaadenine
共418 – 463兲
bis-共2,2,2-trinitroethyl兲-N-nitrosoamine
共333–354兲
bis-共2,2,2-trinitroethyl兲-N-nitroamine
共340–356兲
furan
共173–187兲
cyclobutane-1,2-dione
共251–289兲
共295–335兲
cyclobutane-1,3-dione
共274 –322兲
succinic anhydride
共298 –320兲
共290–311兲
cis-butenedioic acid
共348 –389兲
共357–367兲
共356 –371兲
trans-butenedioic acid
共371–391兲
共358 –371兲
diglycolic anhydride
共382–303兲
thiophene
共195–228兲
共192–213兲
pyrrole
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
116.9⫾0.8
共298兲
C
127.0⫾2.0
130.6⫾4.0
131⫾5
120.5⫾1.3
121.7
133.9⫾8
126.5⫾2.2
120.5⫾5.2
115.5⫾2.1
U 83.7
共439兲
共519兲
共298兲
共403兲
共425兲
共523兲
共440兲
共426兲
共485兲
TE
ME,TE
TE,GS
QR
MS
HSA
C
LE
ME
MS
110⫾4.0
共430兲
TE
111.3⫾0.3
113⫾4.0
123.3⫾1.7
共442兲
共440兲
GS
TE
ME
119.7⫾2.4
共418兲
128.4⫾1.3
共440兲
97.9⫾0.8
共343兲
ME
117.6⫾0.8
共348兲
ME
39.2
共180兲
69.1⫾3.5
54.8
共270兲
共315兲
HSA
73.6⫾3.7
共298兲
HSA
80.5⫾1.6
80.7⫾1.6
82.2
共309兲
共298兲
共302兲
ME
C
ME,TE
105.4⫾1.7
110⫾2.5
共368兲
ME
共381兲
共365兲
TE,ME
QF
84.2⫾1.1
共294兲
ME,TE
46.8
49.0
共213兲
共203兲
Method
109⫾4.2
123.6⫾2.0
136⫾6.3
134.3⫾4.2
NA
C4 H5 NO2
C4 H5 N3 O
succinimide
共317–340兲
cytosine
共505–525兲
共423– 483兲
83.1⫾1.5
83.6⫾1.5
88.0
151.7⫾0.7
147.2⫾2.6
155.0⫾3.0
共329兲
共298兲
ME
B
共453兲
共298兲
GS
ME
Reference
关2423-84-9兴
关97/25兴
关66-22-8兴
关00/2兴
关80/18兴
关80/18兴
关80/19兴
关79/28兴
关78/17兴
关77/13兴
关75/16兴关74/8兴
关72/32兴关00/2兴
关65/2兴
关504-17-6兴
关99/6兴
关67-52-7兴
关99/42兴
关99/6兴
关90/32兴
关2001-93-6兴
关75/14兴
关1123-54-2兴
关75/14兴
关34882-73-0兴
关73/1兴
关19836-28-3兴
关73/1兴
关110-00-9兴
关53/15兴
关33689-28-0兴
关U/5兴
关85/2兴
关15506-53-3兴
关78/14兴
关108-30-5兴
关90/4兴
关90/4兴
关83/7兴
关110-16-7兴
关74/5兴
关38/1兴关60/1兴
关70/1兴
关34/1兴
关110-17-8兴
关77/4兴
关38/1兴关35/1兴
关60/1兴
关34/1兴
关4480-83-5兴
关83/7兴
关110-02-1兴
关87/4兴关56/8兴
关44/1兴
关109-97-7兴
关41/3兴
关123-56-8兴
关90/4兴
关90/4兴
关89/27兴
关71-30-7兴
关98/37兴
关84/12兴
关84/12兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
554
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
Compound
Temperature range 共K兲
共450– 470兲
C4 H5 N3 O2
5-aminouracil
C4 H5 N3 O2
6-azathymine
共358 – 403兲
2-thiocytosine
共408 – 458兲
bis-共2,2,2-trinitroethyl兲amine
共338 –349兲
2-butyne
共200–239兲
2-methylimidazole
共301–318兲
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
167⫾10
176⫾10
NA
150.6
共298兲
共298兲
C4 H5 N7 O12
C4 H6
C4 H6 N2
C4 H6 N2 O
3-amino-5-methylisoxazole
C4 H6 N2 O2
C4 H6 N4 O8
2,5-piperazinedione
共413– 450兲
2,4-diamino-6-hydroxypyrimidine
共423– 471兲
1,1,3,3-tetranitrobutane
C4 H6 N4 O8
2,2,3,3-tetranitrobutane
C4 H6 N4 O8
1,1,1,3-tetranitro-2-methylpropane
C4 H6 N4 O8
1,1,1,4-tetranitrobutane
C4 H6 O4
dimethyl oxalate
Reference
TE
C
关80/9兴
关80/21兴
关77/15兴
关74/8兴关75/16兴
关932-52-5兴
关74/8兴
关932-53-6兴
关74/14兴
关333-49-3兴
关75/14兴
关34880-53-0兴
关73/1兴关77/1兴
关503-17-3兴
关47/2兴
关693-98-1兴
关92/25兴
关92/25兴
关1072-67-9兴
关73/20兴关77/1兴
关106-57-0兴
关87/4兴关56/7兴
关56-06-4兴
关99/42兴
关3759-60-2兴
关99/35兴
关20919-97-5兴
关99/35兴
关42216-58-0兴
关99/35兴
关20919-96-4兴
关99/35兴
关553-90-2兴
关96/10兴
关96/10兴
关96/10兴
关96/10兴
关76/5兴关75/13兴
关110-15-6兴
关83/7兴
关83/7兴
关70/1兴关60/4兴
关70/1兴关60/4兴
关60/4兴关99/10兴
关47/6兴
关147-73-9兴
关83/23兴
关516-05-2兴
关00/22兴
关00/22兴
关83/26兴
关1748-15-8兴
关67/5兴
关67/5兴关70/1兴
关31110-30-2兴
关87/4兴
关625-37-6兴
关87/4兴
关625-77-4兴
关65/8兴关71/23兴
关543-24-8兴
关79/1兴
关56-84-8兴
关77/2兴
ME
145.6
C4 H5 N3 S
Method
LE
112.5⫾2.3
共380兲
158⫾1.6
共433兲
80.8⫾0.4
ME
37.4
共220兲
A
88.2⫾0.7
88.4⫾0.7
共309兲
共298兲
ME
共428兲
ME
81.6⫾2.5
C4 H6 N4 O
共268 –298兲
C4 H6 O4
共289–306兲
succinic acid
共356 –376兲
共372– 401兲
C4 H6 O6
共292–320兲
meso tartaric acid
103.8⫾2.1
147.6⫾0.2
GS
87.9⫾0.8
共298兲
78.2⫾0.8
共298兲
91.2
共298兲
99.6
共298兲
74.6⫾0.7
75.6⫾1.6
75.3⫾1.6
74.9⫾0.6
47.4⫾0.5
共298兲
共283兲
共298兲
120.5
123.1
118.1⫾3.3
120.3⫾4.4
121.8⫾3.3
73.6
共368兲
共298兲
共386兲
共298兲
共298兲
共306兲
TE,ME
116.2⫾0.9
117.4⫾1.9
113.2⫾0.4
共348兲
共298兲
ME
ME
C
88.6
91.4⫾2.5
共335兲
共298兲
68
共368兲
80
共378兲
73.2⫾0.8
共298兲
C
127.0⫾1.0
共389兲
TE,ME
U 96⫾4.2
共420兲
LE
C
HSA
B
BG
ME
A
156.9
C4 H6 O4
C4 H6 S3
C4 H7 NO
C4 H7 NO
C4 H7 NO2
C4 H7 NO3
C4 H7 NO4
methylmalonic acid
共341–354兲
1,3-dithian-2-thione
共321–348兲
cis 2-butenoic acid amide
共353–387兲
trans 2-butenoic acid amide
共363– 413兲
diacetamide
N-acetylglycine
共383– 400兲
L-aspartic acid
共370– 470兲
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
ENTHALPY OF SUBLIMATION
555
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C4 H8
cyclobutane
C4 H8 Cl2 S
C4 H8 Cl3 O4 P
C4 H8 N2 O
C4 H8 N2 O2
C4 H8 N2 O2
C4 H8 N2 O2
C4 H8 N2 O2
C4 H8 N4 O2
C4 H8 N4 O4
C4 H8 N8 O8
␦ form
␤ form
C4 H8 O2
(C4 H8 O2 ) 2
C4 H8 O2
C4 H8 O4
C4 H8 S2
C4 H8 S2
C4 H9 I
C4 H9 Li
C4 H9 ONa
C4 H9 NO
C4 H9 NO
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
36.4
共145兲
bis 共2-chloroethyl兲sulfide
共263–287兲
77.2
84.5
共1-hydroxy-2,2,2-trichloroethyl兲phosphonic acid dimethyl ester
共293–357兲
107
tetrahydro-2-pyrimidone
89.3
1,2-diacetylhydrazine
共347–358兲
103.1⫾1.7
dimethylglyoxime
共331–352兲
96.8⫾1.3
共331–352兲
97.1⫾1.3
Method
B
关505-60-2兴
共275兲
B
共308兲
共298兲
共352.5兲
共341.5兲
ME
ME
共376兲
C
共298兲
共392兲
C
TE
N-acetylglycine amide
共378 – 406兲
N-nitrosomorpholine
123.5⫾1.7
126.3⫾2.3
140.2⫾2.3
135⫾3
81.6
1,4-dinitrosopiperazine
共325–360兲
101.3⫾8
1,4-dinitropiperazine
共325–360兲
111.3⫾8
1,3,5,7-tetranitro-1,3,5,7-tetrazacyclooctane ␦-form
共461– 487兲
161.9
共415– 479兲
161⫾0.3
共371– 403兲
175.2
butanoic acid
共238 –255兲
76.0⫾1.5
butanoic acid dimer
共238 –255兲
85⫾1.5
1,4-dioxane
共237–272兲
35.6
1,3,5,7-tetroxane
79.6⫾0.2
79.5
1,3-dithiane
共266 –279兲
62.9⫾0.7
69.9⫾0.4
共250–271兲
72.6
52.3⫾0.8
1,4-dithiane
63.0
68.9
共253–276兲
72.4
2-iodo-2-methylpropane
共202–223兲
49.8
butyl lithium
共333–368兲
109.7
sodium tert-butoxide
NA
butanamide
共298 –347兲
82⫾4.0
86.4⫾0.4
共292–304兲
85.4⫾1.7
共353–373兲
87
共336 –382兲
86.4⫾0.4
共298 –341兲
87.0⫾0.8
79.9
2-methylpropanamide
共343兲
共343兲
共474兲
共447兲
共385兲
共248兲
TE,ME
共248兲
TE,ME
共255兲
A
共298兲
C
C
共298兲
共298兲
共263兲
共298兲
ME
GC
TE,ME
C
共298兲
共298兲
共268兲
E
共212.5兲
MG
共350.5兲
共298兲
TE
共298兲
共363兲
共359兲
共320兲
ME
GS
ME
Reference
关287-23-0兴
关63/6兴
关87/4兴
关63/6兴关47/4兴
关52-68-6兴
关87/4兴
关1852-17-1兴
关99/32兴
关3148-73-0兴
关87/4兴关59/12兴
关95-45-4兴
关87/4兴关56/7兴
关56/7兴关70/1兴
关60/1兴
关2620-63-5兴
关99/12兴
关99/12兴
关95/33兴
关88/6兴关86/16兴
关59-82-2兴
关88/20兴
关140-79-4兴
关74/11兴关77/1兴
关4164-37-8兴
关74/11兴关77/1兴
关2691-41-0兴
关76/8兴
关78/15兴
关69/12兴
关107-92-6兴
关78/16兴
关19496-06-1兴
关78/16兴
关123-91-1兴
关47/2兴
关293-30-1兴
关77/1兴关69/8兴
关75/17兴
关505-23-7兴
关99/3兴
关89/30兴
关83/7兴
关71/23兴
关505-29-3兴
关99/15兴
关89/30兴
关83/7兴
关558-17-8兴
关87/4兴关44/2兴
关109-72-8兴
关87/4兴关62/12兴
关865-48-5兴
关90/22兴
关541-35-5兴
关00/1兴
关75/18兴关77/1兴
关73/19兴关77/1兴
关60/1兴
关59/3兴
关59/3兴
关60/13兴
关563-83-7兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
556
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
Compound
Temperature range 共K兲
共288 –354兲
共285–302兲
C4 H9 NO2
C4 H9 NO2
C4 H9 NO2
C4 H9 NO2
C4 H9 NO3
C4 H9 NO3
C4 H9 NO4
C4 H9 NO5
C4 H9 N3 O2
C4 H10
C4 H10N2
C4 H10N2
C4 H10N2 O
C4 H10N2 O
C4 H10N2 S
C4 H10O
C4 H10O2 S
C4 H10O4
C4 H11NO
2-aminoisobutyric acid
共439– 462兲
共403– 424兲
共439– 469兲
DL-2-aminobutanoic acid
共400– 418兲
L-2-aminobutanoic acid
4-aminobutanoic acid
共384 – 407兲
C4 H11NO2
C5 Cl6
hexachlorocyclopentadiene
C5 F10
decafluorocyclopentane
共229–281兲
C5 F12
(Tm /K)
82⫾4
86.1⫾0.2
86.0⫾0.2
共298兲
共294兲
共298兲
125.8
134.2⫾1.0
125.9⫾0.4
共450.5兲
共413.5兲
共455兲
TE,ME
ME
132⫾2
共409兲
TE,ME
162.8⫾0.8
共455兲
ME
138.9⫾0.6
140⫾2
共395兲
共298兲
C
C
共391兲
LE
共319兲
共311兲
C
C
共368兲
共339兲
C
C
共368兲
C
DL-threonine
共341– 441兲
U 96⫾8
2-methyl-2-nitro-1-propanol
plastic phase
59.5⫾3.0
crystalline phase
73.2⫾3.7
2-methyl-2-nitro-1,3-propanediol
plastic phase
79.3⫾4.0
crystalline phase
102.0⫾5.1
2-hydroxymethyl-2-nitro-1,3-propanediol
plastic phase
77.3⫾3.9
1-关2-共ethenyloxy兲ethyl兴-1-nitrosohydrazine
112.1⫾1.9
n-butane
35.9
piperazine
72.1
65.2
共279–321兲
73.1
trimethylammonium cyanide
共219–236兲
45
N-propylurea
共332–373兲
90.7⫾1.0
N-isopropylurea
共368 – 411兲
100.6⫾1.3
99.7⫾0.4
trimethylthiourea
83⫾3.0
tert-butyl alcohol
共253–298兲
51.3
diethyl sulfone
86.2⫾2.5
meso-erythritol
157
135.1⫾2.2
2-methyl-2-amino-1-propanol
plastic phase
crystalline phase
diethanolamine
CAS registry number
⌬ subH m /kJ mol⫺1
Reference
TE
ME
关00/01兴
关89/6兴
关89/6兴
关62-57-7兴
关87/4兴关65/1兴
关87/4兴关79/1兴
关65/1兴关64/16兴
关2835-81-6兴
关79/1兴
关1492-24-6兴
关65/1兴关64/16兴
关65-12-2兴
关83/24兴
关83/24兴
关80-68-2兴
关77/2兴
关76-39-1兴
关94/27兴
关94/27兴
关77-49-6兴
关94/27兴
关94/27兴
关126-11-4兴
关94/27兴
关216489-98-4兴
关98/36兴
关106-97-8兴
关66/3兴
关110-85-0兴
关98/18兴
关97/39兴
关87/4兴
共298兲
共107兲
B
共298兲
共385兲
共294兲
B
共227.5兲
共366兲
共389兲
共352兲
共333兲
TE
共275兲
A
共298兲
B
86.5⫾4.3
114.5⫾5.7
共368兲
共339兲
C
C
105.9⫾2.
共298兲
C
73.6
共283兲
B
32.1
38.2
共266兲
共115兲
43.7
共145兲
n-dodecafluoropentane
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
Method
关87/4兴
关927-67-3兴
关90/5兴关87/5兴
关691-60-1兴
关90/5兴
关90/5兴关86/6兴
关2489-77-2兴
关94/20兴
关75-65-0兴
关47/2兴
关597-35-3兴
关U/3兴关70/1兴
关149-32-6兴
关90/7兴
关50/1兴关60/1兴
关70/1兴
关124-68-5兴
关94/27兴
关94/27兴
关111-42-2兴
关82/5兴
关77-47-4兴
关63/6兴关58/5兴
关376-77-2兴
关87/4兴关67/21兴
关63/6兴关51/8兴
关56/9兴
关678-26-2兴
关63/6兴关51/8兴
关56/9兴
ENTHALPY OF SUBLIMATION
557
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C5 N4
tetracyanomethane
C5 H2 F6 N2
3,5-bis共trifluoromethyl兲pyrazole
C5 H2 N4 O6
C5 H3 Br2 N
2,4,6-trinitropyridine
共335–357兲
2,4,6-trinitropyridine N-oxide
共377– 403兲
2,5-dibromopyridine
C5 H3 Br2 N
2,6-dibromopyridine
C5 H3 Cl2 N
2,3-dichloropyridine
C5 H3 Cl2 N
2,5-dichloropyridine
C5 H3 Cl2 N
2,6-dichloropyridine
C5 H3 Cl2 N
3,5-dichloropyridine
C5 H3 NO3
5-nitro-2-furancarboxaldehyde
C5 H3 N3
C5 H4 N2 O3
2,2-dicyanopropionitrile
共293–333兲
4-nitropyridine-N-oxide
C5 H4 N4
共311–335兲
purine
C5 H4 N4
1,2,4-triazolo关1,5a兴pyrimidine
C5 H4 N4 O
hypoxanthine
共423– 473兲
6-mercaptopurine
共413– 458兲
2-thenoic acid
共315–323兲
2-furoic acid
共317–328兲
C5 H2 N4 O7
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
61.1⫾8.8
共298兲
DSC
69.0⫾0.6
共266兲
ME
82.1⫾2.2
共298兲
C
85.6⫾3.0
共298兲
C
73.5⫾3.1
共298兲
C
67.1⫾2.0
共298兲
C
72.0⫾1.6
共298兲
C
67.3⫾1.9
共298兲
C
73.9⫾0.5
共313兲
T
108.9⫾0.3
89.1⫾2.5
共298兲
C
Method
101.7⫾2.9
106.3⫾2.9
75.3⫾2.1
NA
C5 H4 N4 S
C5 H4 O2 S
C5 H4 O3
C5 H5 ClN2 O2
C5 H5 ClN2 O2
C5 H5 FN2 O2
C5 H5 FN2 O2
C5 H5 F3 N2
C5 H5 NO
C5 H5 NO
C5 H5 NO
C5 H5 NO
C5 H5 NO2
C5 H5 NO2
86.9
共419兲
158.1⫾1.6
共448兲
148.5⫾1.5
共435兲
97.1
共319兲
108.4⫾2.2
1-methyl-6-chlorouracil
共417– 465兲
108.8⫾8
3-methyl-6-chlorouracil
共444 – 493兲
104.6⫾6
1-methyl-5-fluorouracil
共381– 423兲
116.5⫾1.9
共480–515兲
125.5⫾8
3-methyl-5-fluorouracil
共465– 487兲
79.5⫾17
3共5兲-trifluoromethyl-5共3兲-methylpyrazole
78.2⫾0.8
2-hydroxypyridine
86.6⫾1.3
3-hydroxypyridine
88.3⫾1.3
4-hydroxypyridine
118.6⫾5.2
103.8⫾1.7
pyridine N-oxide
79.3⫾1.0
3-hydroxypyridine N-oxide
共345–392兲
121.8⫾4.4
pyrrole-2-carboxylic acid
E
ME
HSA
HSA
共402兲
TE
HSA
HSA
共297兲
ME
共298兲
C
共298兲
C
共298兲
共298兲
C
C
共298兲
共298兲
ME
Reference
关24331-09-7兴
关73/3兴
关14704-41-7兴
关91/21兴
关78013-51-1兴
关95/31兴
关25242-76-6兴
关95/31兴
关624-28-2兴
关97/16兴
关626-05-1兴
关97/16兴
关2402-77-9兴
关97/17兴
关16110-09-1兴
关97/17兴
关2402-78-0兴
关97/17兴
关2457-47-8兴
关97/17兴
关698-63-5兴
关80/28兴关86/5兴
关10359-20-3兴
关94/19兴
关1124-33-0兴
关95/3兴
关95/31兴
关120-73-0兴
关74/7兴
关275-02-5兴
关97/39兴
关68-94-0兴
关75/14兴
关6112-76-1兴
关75/14兴
关527-72-0兴
关53/12兴关60/1兴
关88-14-2兴
关53/1兴关60/1兴
关70/1兴
关31737-09-4兴
关78/17兴
关4318-56-3兴
关78/17兴
关155-16-8兴
关02/1兴
关78/17兴
关4840-69-1兴
关78/17兴
关10010-93-2兴
关91/21兴
关142-08-5兴
关82/15兴关86/5兴
关109-00-2兴
关82/15兴关86/5兴
关626-64-2兴
关92/3兴
关82/15兴关86/5兴
关694-59-7兴
关88/19兴
关6602-28-4兴
关98/12兴
关634-97-9兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
558
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C5 H5 NO2
共350–354兲
N-methylmaleimide
共276 –289兲
C5 H5 N3 O
C5 H5 N5
pyrazine carboxamide
共353–383兲
adenine
共400– 438兲
共448 – 473兲
C5 H5 N5 O
guanine
C5 H5 N7 O14
1,1,1,3,5,5,5-heptanitropentane
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
126.8
Method
Reference
共352兲
ME
75.3⫾0.5
73.3⫾0.5
共282兲
共298兲
ME
87.9
共368兲
ME
关53/12兴关60/1兴
关930-88-1兴
关97/12兴
关97/12兴
关98-96-4兴
关87/4兴关60/16兴
关59/13兴
关73-24-5兴
关00/17兴
关87/4兴
关75/16兴关74/8兴
关84/38兴关00/17兴
关65/2兴关70/1兴
关73-40-5兴
关75/16兴关74/8兴
关20919-99-7兴
关99/35兴
关383-72-2兴
关87/4兴关60/20兴
关7321-55-3兴
关90/28兴
关504-29-0兴
关98/17兴
关85/13兴
关84/6兴
关462-08-8兴
关98/17兴
关84/6兴
关504-24-5兴
关98/17兴
关85/13兴
关84/6兴
关615-77-0兴
关00/2兴
关80/19兴
关78/17兴
关608-34-4兴
关00/2兴
关78/17兴
关72/32兴关00/2兴
关65-71-4兴
关84/12兴
关84/12兴
关80/19兴
关80/9兴
关77/13兴
关75/16兴关74/8兴
关626-48-2兴
关80/13兴
关108-55-4兴
关90/4兴
关90/4兴
关96-54-8兴
关41/3兴
关1121-89-7兴
关90/4兴
关90/4兴
关1121-07-9兴
关97/12兴
关97/12兴
关149-87-1兴
关79/1兴
关1122-47-0兴
140.4
109.2
126.3
127.2
108.7⫾8
ME
共460.5兲
LE
QR
ME
186.2
C5 H6 F3 NO3
C5 H6 N2
C5 H6 N2
C5 H6 N2
C5 H6 N2
C5 H6 N2 O2
C5 H6 N2 O2
C5 H6 N2 O2
C5 H6 N2 O2
C5 H6 O3
C5 H7 N
C5 H7 NO2
C5 H7 NO2
C5 H7 NO3
C5 H7 N3 O
111.7
glycine, N-共trifluoroacetyl兲 methyl ester
共293– 463兲
57.3
dimethylmalonodinitrile
62.0⫾0.7
2-aminopyridine
76.5⫾0.4
38.6⫾1.9
78.7⫾0.8
3-aminopyridine
80.7⫾0.3
84.0⫾1.4
4-aminopyridine
87.1⫾0.4
53.8⫾0.8
88.1⫾1.1
1-methyluracil
共343– 428兲
121.7⫾4.0
共378 – 418兲
112.5⫾2.6
共435– 480兲
104.6⫾8
3-methyluracil
共344 – 419兲
118.8⫾3.0
共438 – 498兲
75.3⫾8
69.5⫾1.2
5-methyluracil 共thymine兲
共383– 438兲
125.7⫾3.6
131.3⫾4.0
共378 – 428兲
124.4⫾1.3
138⫾10
134.1⫾4.2
124.3
6-methyluracil
共426 –503兲
131
glutaric anhydride
共298 –320兲
85.9⫾1.6
86.1⫾1.6
N-methylpyrrole
NA
glutarimide
共317–340兲
93.6⫾1.6
94.1⫾1.6
N-methylsuccinimide
共280–298兲
80.6⫾0.3
80.1⫾0.3
共dl兲-5-oxoproline
共394 – 416兲
133.2⫾1
1-methylcytosine
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
LE
共298兲
共308兲
共298兲
共298兲
共298兲
C
DSC
C
共298兲
共298兲
C
C
共298兲
共298兲
C
DSC
C
共439兲
共398兲
共457兲
TE
QR
HSA
共382兲
共463兲
TE
HSA
ME
共411兲
共298兲
共403兲
共298兲
共298兲
ME
QR
TE
C
LE
共298兲
共309兲
共298兲
ME
共329兲
共298兲
ME
共289兲
共298兲
ME
共405兲
TE,ME
ENTHALPY OF SUBLIMATION
559
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
Compound
Temperature range 共K兲
共455– 487兲
共423– 443兲
C5 H7 N3 O
C5 H7 N3 O
3-methylcytosine
共487–526兲
3,5-dimethyl-4-nitrosopyrazole
C5 H7 N3 O2
1-methyl-N-hydroxycytosine
C5 H8 Br4
C5 H8 NO2
pentaerythrityl tetrabromide
共384 – 434兲
5-amino-3,4-dimethylisoxazole
C5 H8 N2
2,3-diazabicyclo关2.2.1兴hept-2-ene
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
141.2⫾0.6
141.8⫾8.8
149.1⫾9.0
共433兲
共298兲
150.6
102.9⫾3.0
Method
Reference
GS
ME
关98/37兴
关84/12兴
关84/12兴
关4776-08-3兴
关65/2兴
关1122-04-9兴
关01/4兴
关20541-50-8兴
关98/37兴
关3229-00-3兴
关87/4兴关41/1兴
关19947-75-2兴
关73/21兴关77/1兴
关2721-32-6兴
关74/17兴关77/1兴
关76/12兴
关67-51-6兴
关01/4兴
关91/21兴
关1072-62-4兴
关92/25兴
关92/25兴
关78-11-5兴
关78/15兴
关71/34兴关78/15兴
关69/3兴
关53/6兴关60/1兴
关70/1兴
关1072-72-6兴
关72/15兴
关72/15兴关77/1兴
关80-62-6兴
关52/5兴关60/1兴
关6007-71-2兴
关69/11兴关77/1兴
关1193-10-8兴
关69/11兴关77/1兴
关110-94-1兴
关99/10兴
关99/10兴
关47/6兴
关595-46-0兴
关00/22兴
关00/22兴
关601-75-2兴
关00/22兴
关00/22兴
关83/26兴
关15856-96-9兴
关87/4兴
关15856-96-9兴
关87/4兴
关675-20-7兴
关53/5兴关60/1兴
关60/21兴
关147-85-3兴
关79/1兴
关78/4兴
关77/2兴
关51-35-4兴
关79/1兴
关56-86-0兴
关77/2兴
HSA
共298兲
C
共399兲
GSM
126.7⫾1.5
84
87.9⫾2.5
C5 H8 N2
C5 H8 N2
C5 H8 N4 O12
C5 H8 O2
C5 H8 O2 S
C5 H8 O2 S
C5 H8 O4
C5 H8 O4
C5 H8 O4
C5 H9 NO
C5 H9 NO
C5 H9 NO
C5 H9 NO2
C5 H9 NO3
C5 H9 NO4
共298兲
83.4⫾2.4
83.3⫾0.2
共298兲
共301兲
C
ME
89.2⫾0.4
89.6⫾0.4
共312兲
共298兲
ME
150.4⫾1.3
146⫾12
U121.3
151.9⫾2.1
共298兲
ME
71.7⫾1.7
72.6⫾1.7
共317兲
共298兲
3,5-dimethylpyrazole
2-ethylimidazole
共303–321兲
pentaerythritol tetranitrate
共328 – 405兲
共370– 411兲
C5 H8 OS
43.9⫾2.1
55.3⫾0.6
ME
tetrahydro-4H-thiopyran-4-one
methyl methacrylate
共194 –223兲
60.7
2,5-dihydro-2-methyl-thiophene-1,1-dioxide
60.7⫾2.5
2,5-dihydro-3-methyl-thiophene-1,1-dioxide
64.0⫾2.5
1,5-pentanedioic acid 共glutaric acid兲
共348 –363兲
117.0⫾1.2
119.8⫾1.2
共292–320兲
U52.6
dimethylmalonic acid
共347–363兲
110.2⫾1.0
111.7⫾2.1
ethylmalonic acid
共347–362兲
111.2⫾1.2
112.8⫾2.2
105.5⫾0.5
cis 2-pentenoic acid amide
共323–333兲
106.5
trans 2-pentenoic acid amide
共353–383兲
57.9
␦-valerolactam
共293–312兲
74.5
L-共l兲-proline
共396 – 416兲
共380– 420兲
共323– 423兲
trans 4-hydroxy-L-proline
共461– 481兲
L-glutamic acid
共353– 453兲
I
共205兲
共356兲
共298兲
共306兲
ME
共355兲
共298兲
ME
ME
共355兲
共298兲
ME
ME
C
A
共328兲
共368兲
共303兲
127.4⫾1
149⫾4
U 50⫾8
共406兲
共400兲
共373兲
TE,ME
C
LE
162.6⫾2
共471兲
TE,ME
U 121⫾34
共403兲
LE
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
560
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C5 H10
cyclopentane
C5 H10N2 O2
C5 H10N2 O2
C5 H10O2
C5 H10O5
C5 H10O5
C5 H11NO
C5 H11NO
C5 H11NO2
C5 H11NO2
C5 H11NO2
C5 H11NO2
C5 H11NO2
C5 H11NO2 S
C5 H11NO2 S
C5 H12
N-acetylglycine, N-methylamide
共348 –363兲
N-acetyl-L-alanine amide
共366 – 410兲
2,2-dimethylpropanoic acid
共278 –303兲
C5 H12N2 O
C5 H12N2 O
C5 H12N2 O
C5 H12N2 O
C5 H12N2 S
C5 H12N2 S
(Tm /K)
42.6
共122兲
97.8
共355.5兲
115.0⫾1.2
118.1⫾1.6
115⫾3
共376兲
共298兲
共388兲
C
62.3⫾0.6
62.1⫾0.6
共291兲
共298兲
GS
GS
共298兲
C
共382兲
ME
Method
B
TE
1,3,5,7,9-pentoxecane
87.9⫾0.5
D-xylose
共370–395兲
158.0⫾3.1
pentanamide
共333–374兲
89.3⫾0.4
共353–373兲
89.1
2,2-dimethylpropanamide
共298 –359兲
89⫾2.0
共288 –306兲
86.6⫾0.4
共dl兲 2-aminopentanoic acid 共DL-norvaline兲
共439– 461兲
120
121.1⫾0.4
butyl carbamate
共292–316兲
94.1⫾8
DL-valine
共320– 420兲
U 79.5⫾8
L-valine
162.8⫾8
5-aminopentanoic acid
共384 –394兲
141.8⫾0.5
144⫾3
DL-methionine
共363– 463兲
U 134⫾8
L-共d兲-methionine
共463– 485兲
125⫾0.8
2,2-dimethylpropane
共223–256兲
共171–249兲
C5 H12
CAS registry number
⌬ subH m /kJ mol⫺1
共230–252兲
n-pentane
1,3-diethylurea
共321–379兲
共384 –590兲
N-butylurea
GS
共298兲
共298兲
TE
ME
共450兲
共455兲
ME
ME
GS
共370兲
LE
共455兲
ME
共389兲
共289兲
C
C
共413兲
LE
共474兲
ME
164⫾4
共298兲
C
28.2
33.2
23.9
22.0
22.8
共241兲
共210兲
共298兲
共241兲
A
H
A
42.0
共143兲
B
96.8⫾0.9
NA
共361兲
TE
ME
99⫾4
103.2⫾0.8
共352兲
101.1⫾1.1
106.0⫾0.5
共377兲
共355兲
TE
101.6⫾0.7
100.7⫾0.3
共379兲
共352兲
TE
121.7⫾3
120.2⫾3.0
共298兲
共298兲
B,HA
B
N-isobutylurea
N-tert-butylurea
diethylthiourea
tetramethylthiourea
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
Reference
关287-92-3兴
关63/6兴
关7606-79-3兴
关87/4兴关55/7兴
关15962-47-7兴
关99/12兴
关99/12兴
关88/6兴关86/16兴
关75-98-9兴
关00/20兴
关00/20兴
关16528-92-0兴
关74/16兴
关58-86-6兴
关99/1兴
关626-97-1兴
关59/3兴关70/1兴
关60/1兴
关759-10-9兴
关00/1兴
关89/6兴
关760-78-1兴
关87/4兴关65/1兴
关65/1兴关64/16兴
关592-35-8兴
关59/4兴
关516-06-3兴
关77/2兴
关72-18-4兴
关65/1兴关64/16兴
关660-88-8兴
关83/24兴
关83/24兴
关59-51-8兴
关77/2兴
关63-68-3兴
关87/4兴关65/1兴
关64/16兴
关81/5兴
关463-82-1兴
关87/4兴
关63/6兴关36/1兴
关47/2兴
关33/6兴
关109-66-0兴
关63/6兴
关623-76-7兴
关90/5兴关87/5兴
关86/19兴
关592-31-4兴
关87/6兴
关86/6兴关90/5兴
关592-17-6兴
关90/5兴
关90/5兴关86/6兴
关1118-12-3兴
关90/5兴
关90/7兴关86/6兴
关26914-14-7兴
关00/23兴
关94/17兴
关2782-91-4兴
ENTHALPY OF SUBLIMATION
561
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
C5 H12O2
Compound
Temperature range 共K兲
C5 H12O2 S
neopentyl glycol
plastic phase
crystalline phase
1,1,1-tris共hydroxymethyl兲ethane
plastic phase
crystalline phase
tert-butyl methyl sulfone
C5 H12O4
pentaerythritol
C5 H12O3
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
84.5⫾3
84.0
83.0⫾0.5
83.0⫾0.2
Method
Reference
共298兲
共298兲
共298兲
共298兲
ME
75.5⫾3.8
87.6⫾4.4
共368兲
共350兲
C
C
84.2⫾4.2
109.2⫾5.5
共319兲
共311兲
C
C
131.3⫾6.6
161⫾1.0
163
131.4
143.9⫾0.8
共403兲
共437兲
共298兲
C
TE
161
共298兲
B
160
共298兲
B
161
共298兲
B
关00/23兴
关94/20兴
关85/5兴
关82/7兴
关126-30-7兴
关94/3兴关94/27兴
关94/3兴关94/27兴
关77-85-0兴
关94/27兴
关94/27兴
关14094-12-3兴
关U/3兴关70/1兴
关115-77-5兴
关94/27兴
关90/7兴
关90/7兴
关51/3兴关60/1兴
关53/4兴关60/1兴
关488-81-3兴
关90/7兴
关488-82-4兴
关90/7兴
关87-99-0兴
关90/7兴
关118-75-2兴
关27/2兴关60/1兴
关70/1兴
关118-74-1兴
关94/39兴
关94/1兴
关91/2兴
关91/2兴
关89/32兴
关87/4兴
关86/18兴关97/40兴
关80/36兴
关77/10兴
关49/3兴关70/1兴
关392-56-3兴
关87/4兴关65/22兴
关79/33兴
关65/10兴
关355-68-0兴
关87/4兴关67/21兴
关57/5兴
关16419-78-6兴
关87/4兴
关57/4兴
关670-54-2兴
关83/7兴
关63/4兴关70/1兴
关87/4兴
关58/14兴
C
C
82.4⫾2.5
共418 – 455兲
共tetragonal兲
C5 H12O5
共397– 410兲
共379– 408兲
adonitol
C5 H12O5
D-arabitol
C5 H12O5
xylitol
C6 Cl4 O2
tetrachloro-1,4-benzoquinone
共333–356兲
C6 Cl6
C6 F6
C6 F12
C6 N2
C6 N4
hexachlorobenzene
共258 –313兲
共253–303兲
共461–506兲
共387–502兲
共314 –373兲
共288 –318兲
共312–337兲
共369–397兲
hexafluorobenzene
共215–278兲
共238 –268兲
dodecafluorocyclohexane
共252–326兲
共293–333兲
dicyanodiacetylene
共294 –335兲
共295–335兲
tetracyanoethylene
共290–312兲
共333–371兲
ME
ME
98.7⫾8.3
105
77.4⫾0.8
89.6⫾0.2
90.5⫾0.2
85.5
62.7
94.7
101.3
79.5⫾12
92⫾8.2
QF
共278兲
共337兲
共298兲
GS
C
C
共402兲
共344兲
共303兲
GS
GS
RG
49.2
49.8
46.0
共263兲
共253兲
共316兲
36.4
36.2
共dicyanobutadiyne兲
34.4
35.9
共267兲
共313兲
84.3
81.2⫾5.9
共302兲
共352兲
共309兲
共315兲
78.0
C6 N6 O3
C6 N6 O6
C6 HCl3 O2
benzotrifurazan
共303–333兲
benzotrifuroxan
共363– 433兲
trichloro-1,4-benzoquinone
共301–327兲
C6 HCl5
pentachlorobenzene
C6 HCl5 O
pentachlorophenol
IPM,A
B
TE,ME
MG
GS
95.8⫾3.8
关99/44兴
172.0⫾2.5
关99/44兴
关634-85-5兴
关27/2兴关60/1兴
关70/1兴
关608-93-5兴
关91/2兴
关87-86-5兴
88.7⫾8.3
87.1⫾0.4
QF
共298兲
C
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
562
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C6 HF5 O
pentafluorophenol
共273–299兲
1,3,5-trinitrochlorobenzene
共341–363兲
2,6-dichloro-1,4-benzoquinone
共274 –315兲
⌬ subH m /kJ mol⫺1
CAS registry number
(Tm /K)
Method
67.4⫾2.1
C6 H2 ClN3 O6
C6 H2 Cl2 O2
C6 H2 Cl4
1,2,3,4-tetrachlorobenzene
C6 H2 Cl4
1,2,4,5-tetrachlorobenzene
C6 H2 Cl4
1,2,3,5-tetrachlorobenzene
C6 H2 Cl4 O2
C6 H3 Br3 O
tetrachlorohydroquinone
共298 –359兲
共333–356兲
2,4,6-tribromophenol
C6 H3 ClN2 O2
5-chlorobenzofurazan-1-oxide
C6 H3 ClO2
chlorobenzoquinone
共264 –289兲
67.4⫾1.7
103.0
GS
共352兲
69.9⫾8.3
ME
QF
78.8⫾0.2
共298兲
C
83.2⫾0.3
共298兲
C
79.6⫾0.3
共298兲
C
89
88.7
共313兲
QF
97.6⫾1.1
C6 H3 Cl3
C6 H3 Cl3
C6 H3 Cl3
C6 H3 Cl3 O2
C6 H3 N3 O4
C6 H3 N3 O6
1,2,3-trichlorobenzene
共258 –313兲
共289–303兲
1,2,4-trichlorobenzene
共279–298兲
1,3,5-trichlorobenzene
共282–301兲
trichlorohydroquinone
共298 –336兲
共314 –335兲
4-nitrobenzofurazan-1-oxide
C6 H4 BrCl
1,3,5-trinitrobenzene
共313–395兲
共353–395兲
picric acid
共314 – 406兲
2,4,6-trinitroresorcinol
共325– 436兲
1,4-bromochlorobenzene
C6 H4 BrI
共279–355兲
共294 –337兲
1,4-bromoiodobenzene
C6 H3 N3 O7
C6 H3 N3 O8
C6 H4 Br2
共279–355兲
4-bromo-1-nitrobenzene
共293–303兲
1,4-dibromobenzene
C6 H4 Br3 N
共298 –354兲
共278 –353兲
共228 –347兲
共248 –303兲
2,4,6-tribromoaniline
C6 H4 ClI
1,4-chloroiodobenzene
C6 H4 BrNO2
81.2⫾1.8
共298兲
C
69.0⫾8.3
共276兲
QF
72.7
75.1⫾0.75
65.7
共298兲
共296兲
RG
62.3
共289兲
RG
72.7⫾0.5
56.5
共298兲
共291兲
RG
101.5
101.3
共313兲
共324兲
QF
97.3⫾1.6
共298兲
C
107.3⫾0.6
99.6⫾2.1
共298兲
共374兲
ME
ME
105.1⫾1.6
共298兲
ME
120.8⫾1.1
共298兲
ME
69.3⫾0.1
69.3⫾0.4
67.9⫾0.8
共298兲
共298兲
共316兲
DM
ME,TE,DM
78.5⫾0.2
78.5⫾0.4
共298兲
共298兲
DM
ME,TE,DM
88.3
共303兲
ME
74.2⫾0.1
73.2
73.3⫾0.4
73.8
59.8
共298兲
共313兲
共326兲
共288兲
共298兲
ME
101.1⫾1.1
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
ME,GS
Reference
关U/4兴关70/1兴
关771-61-9兴
关69/5兴关70/1兴
关88-88-0兴
关50/2兴
关697-91-6兴
关27/2兴关60/1兴
关70/1兴
关634-66-2兴
关91/2兴
关95-94-3兴
关91/2兴
关634-90-2兴
关91/2兴
关87-87-6兴
关87/4兴
关27/2兴关60/1兴
关118-79-6兴
关87/3兴
关17348-69-5兴
关96/6兴
关695-99-8兴
关27/2兴关60/1兴
关70/1兴
关87-61-6兴
关94/39兴
关85/8兴
关49/7兴关60/1兴
关120-82-1兴
关49/7兴关60/1兴
关108-70-3兴
关85/8兴
关49/7兴关60/1兴
关608-94-6兴
关87/4兴
关27/2兴关60/1兴
关18771-85-2兴
关96/6兴
关99-35-4兴
关78/15兴
关50/2兴关70/1兴
关88-89-1兴
关78/15兴
关82-71-3兴
关78/15兴
关106-39-8兴
关00/31兴
关98/13兴
关61/2兴
关589-87-7兴
关00/31兴
关98/13兴
关586-78-7兴
关87/4兴关25/3兴
关106-37-6兴
关00/31兴
关87/4兴
关61/2兴
关59/5兴
关40/1兴关60/1兴
关147-82-0兴
关87/3兴
关637-87-6兴
ENTHALPY OF SUBLIMATION
563
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
C6 H4 ClNO2
C6 H4 ClNO2
C6 H4 Cl2
Compound
Temperature range 共K兲
共259–320兲
共303–323兲
3-chloro-1-nitrobenzene
共275–286兲
4-chloro-1-nitrobenzene
共283–303兲
1,4-dichlorobenzene
共258 –313兲
共303– 423兲
C6 H4 Cl2 O
共293–311兲
共311–325兲
共248 –303兲
2,3-dichlorophenol
C6 H4 Cl2 O
2,4-dichlorophenol
C6 H4 Cl2 O
2,5-dichlorophenol
C6 H4 Cl2 O
2,6-dichlorophenol
C6 H4 Cl2 O
3,4-dichlorophenol
C6 H4 Cl2 O
3,5-dichlorophenol
C6 H4 Cl2 O2
共273–295兲
2,6-dichlorohydroquinone
共324 –345兲
C6 H4 INO2
C6 H4 I2
3-iodo-1-nitrobenzene
共295–306兲
C6 H4 N2
1,4-diiodobenzene
共372– 401兲
2-cyanopyridine
C6 H4 N2
3-cyanopyridine
C6 H4 N2
C6 H4 N2 O
C6 H4 N2 O
C6 H4 N2 O
(Tm /K)
71.9⫾0.2
71.9⫾0.4
61.1⫾0.6
Method
Reference
共298兲
共298兲
DM
ME, TE, DM
83.2
共293兲
ME
64.8⫾0.2
53.1
65.2⫾2.0
65.4
65.7
64.8⫾0.8
63⫾0.4
56.9
共298兲
DM
共298兲
共313兲
C
GS
共303兲
共318兲
共275兲
ME
71.7⫾2.2
共298兲
C
70.1⫾1.1
共298兲
C
73.6⫾2.1
共298兲
C
75.8⫾1.1
共298兲
C
81.3⫾2.3
共298兲
C
82.8⫾1.1
71.8
共298兲
共284兲
C
关00/31兴
关98/13兴
关53/8兴关60/1兴
关121-73-3兴
关35/1兴关38/1兴
关60/1兴
关100-00-5兴
关87/4兴关25/3兴
关106-46-7兴
关00/31兴
关94/39兴
关89/25兴
关85/4兴
关81/12兴
关61/2兴关70/1兴
关61/2兴
关40/1兴关60/1兴
关576-24-9兴
关94/5兴
关120-83-2兴
关94/5兴
关583-78-8兴
关94/5兴
关87-65-0兴
关94/5兴
关95-77-2兴
关94/5兴
关591-35-5兴
关94/5兴
关87/4兴
关20103-10-0兴
关27/2兴关60/1兴
关70/1兴
关645-00-1兴
关35/1兴关38/1兴
关60/1兴
关624-38-4兴
关87/4兴
关100-70-9兴
关84/6兴
关100-54-9兴
关84/6兴
关89/22兴
关100-48-1兴
关84/6兴
关89/22兴
关14906-64-0兴
关98/12兴
关14906-59-3兴
关98/12兴
关273-09-6兴
关90/29兴
关80/6兴
关480-96-6兴
关90/29兴
关612-29-3兴
关87/4兴关74/34兴
关528-29-0兴
关97/30兴
关87/4兴关76/1兴
关76/1兴
关76/1兴
关35/1兴关38/1兴
74.7⫾1.7
92.0⫾8.3
QF
83.2⫾1.2
共300兲
63.4
共386.5兲
70.7⫾1.2
共298兲
C
72.1⫾1.8
79.0
共298兲
C
DSC
73.2⫾0.6
75.6
共298兲
C
DSC
101.9⫾2.0
共298兲
ME
104.4⫾4.3
共298兲
ME
64.4⫾1.6
64.9
共298兲
共298兲
C
79.6⫾1.7
共298兲
C
95.5
共333兲
95.5⫾0.9
82.9
81.8⫾2.3
87.9⫾2.1
86.6⫾1.2
共298兲
共358兲
共370兲
共298兲
共333兲
4-cyanopyridine
3-cyanopyridine N-oxide
共345–392兲
4-cyanopyridine N-oxide
共345–392兲
benzofurazan
C6 H4 N2 O2
benzofurazan N-oxide
C6 H4 N2 O3
1-nitro-2-nitrosobenzene 共dimer兲
共323–343兲
1,2-dinitrobenzene
C6 H4 N2 O4
CAS registry number
⌬ subH m /kJ mol⫺1
共343–377兲
共343–397兲
共343–397兲
共328 –338兲
TE
TE
TE
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
564
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C6 H4 N2 O4
1,3-dinitrobenzene
共335–356兲
共332–383兲
共332–383兲
共315–329兲
C6 H4 N2 O4
C6 H4 N2 O5
C6 H4 N2 O5
C6 H4 N2 O5
C6 H4 N2 O5
C6 H4 N2 S
C6 H4 N4 O6
C6 H4 O2
(C6 H4 O2 ) –
(C6 H6 O2 )
C6 H4 O5
C6 H4 S4
(C6 H4 S4 ) –
(C12H4 N4 )
C6 H5 BrCl
C6 H5 BrO
C6 H5 ClO
C6 H5 ClO
C6 H5 ClO2
CAS registry number
(Tm /K)
Method
76.1
84.2⫾1.9
87.0⫾0.8
81.1⫾1.7
共345.5兲
共357兲
共298兲
共323兲
TE
TE
94.3⫾0.7
93.1⫾2.3
96.2⫾2.5
89.1⫾1.7
共298兲
共368兲
共298兲
共357兲
TE
TE
96.6
共323兲
104.6⫾4.2
共313兲
93.4
共306兲
112.1⫾4.2
共313兲
123.5
共355兲
70.73⫾0.2
共298兲
C
115.9
125.3⫾0.8
共343兲
共298兲
LE
ME
68.0⫾0.5
62.8⫾3.3
68.5⫾0.6
62.8
共262兲
ME,TE
共269兲
QF
89.1
88.6⫾1
U 181.2
NA
共325.5兲
共313兲
ME,TE
121.3
共391兲
TE,ME
共345兲
共351兲
TGA
TE,ME
HSA
共410兲
TE,ME
共298兲
共298兲
TE,ME,DM
共298兲
ME
1,4-dinitrobenzene
共339–398兲
共339–398兲
共345–368兲
C6 H4 N2 O5
⌬ subH m /kJ mol⫺1
2,3-dinitrophenol
共303–343兲
2,4-dinitrophenol
共293–333兲
2,5-dinitrophenol
共278 –333兲
2,6-dinitrophenol
共293–333兲
3,4-dinitrophenol
共328 –383兲
2,1,3-benzothiadiazole
2,4,6-trinitroaniline
共328 –371兲
共326 – 449兲
1,4-benzoquinone
共260–278兲
quinhydrone 共quinone-hydroquinone兲
共317–334兲
共300–325兲
furan-2,5-dicarboxylic acid
共378 – 402兲
tetrathiofulvalene
61.0
95.3⫾1
共341–361兲
92⫾6.3
共tetrathiofulvalene兲-共7,7,8,8-tetracyanoquinodimethane兲
共TTF–TCNQ兲
130⫾2
1-bromo-4-chlorobenzene
共250–335兲
69.3⫾0.4
69.1⫾0.2
4-bromophenol
共260–302兲
87.3⫾0.4
3-chlorophenol
53.1
4-chlorophenol
共252–293兲
chlorohydroquinone
共306 –334兲
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
60.8
51.9
共278兲
102.9⫾8.3
共320兲
QF
Reference
关60/1兴
关99-65-0兴
关87/4兴
关76/1兴
关76/1兴
关35/1兴关38/1兴
关60/1兴关70/1兴
关100-25-4兴
关97/30兴
关76/1兴
关76/1兴
关35/1兴关38/1兴
关60/1兴
关66-56-8兴
关58/1兴
关51-28-5兴
关58/1兴关70/1兴
关329-71-5兴
关58/1兴
关573-56-8兴
关58/1兴关70/1兴
关577-71-9兴
关58/1兴
关273-13-2兴
关98/2兴
关489-98-5兴
关87/4兴关69/12兴
关78/15兴
关106-51-4兴
关81/4兴
关56/5兴关77/1兴
关53/10兴
关27/2兴
关106-34-3兴
关87/4兴
关81/4兴
关53/10兴关60/1兴
关51/6兴
关3238-40-2兴
关83/5兴
关31366-25-3兴
关95/35兴
关80/22兴
关79/7兴
关40210-84-2兴
关80/22兴
关106-39-8兴
关98/13兴
关98/13兴
关106-41-2兴
关71/8兴
关108-43-0兴
关38/1兴关60/1兴
关70/1兴
关106-48-9兴
关87/4兴
关38/1兴关60/1兴
关70/1兴
关615-67-8兴
关27/2兴关60/1兴
关70/1兴
ENTHALPY OF SUBLIMATION
565
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C6 H5 I
iodobenzene
共243–255兲
共248 –303兲
nitrosobenzene 共dimer兲
共297–339兲
C6 H5 NO
C6 H5 NO2
C6 H5 NO2
C6 H5 NO2
C6 H5 NO3
共345–392兲
3-pyridinecarboxylic acid
共352–360兲
共345–392兲
2-nitrophenol
C6 H5 NO3
C6 H5 NO3
85.1
80.8
共312兲
91.0⫾0.5
92.7⫾0.5
98.0⫾2.3
共329兲
共298兲
共298兲
C
123.9⫾3.7
101.1⫾0.6
105.2⫾0.6
123.4⫾1.2
共298兲
共362兲
共298兲
共298兲
ME
C
107.7⫾0.7
111.3⫾0.6
113.9⫾4.7
共362兲
共298兲
共298兲
C
73.3
54.8
73.2⫾1.3
共298兲
共282.5兲
C
91.2⫾0.5
98.5⫾0.6
100.2⫾0.6
76.2
91.6⫾1.7
共298兲
共321兲
共298兲
共319.5兲
C
ME
92.4
98.8⫾1
91.2⫾1.7
共298兲
共298兲
C
ME
94.4⫾4.0
共298兲
ME
152.3⫾1.9
共298兲
ME
136.1⫾1.2
共298兲
ME
74.5
共273兲
ME
C
ME
4-nitrophenol
pyridine-2-carboxylic acid N-oxide
共345–392兲
pyridine-3-carboxylic acid N-oxide
C6 H5 NO4
pyridine-4-carboxylic acid N-oxide
共345–392兲
2-nitro-1,3-dihydroxybenzene
共253–293兲
4-nitrocatechol
C6 H5 NO5
methyl 5-nitro-2-furancarboxylate
C6 H5 N3
1-H-benzotriazole
C6 H5 NO4
ME
3-nitrophenol
共305–352兲
共339–351兲
C6 H5 NO3
共275兲
Method
4-pyridinecarboxylic acid
共305–334兲
共325–336兲
C6 H5 NO3
43.1
40.0
CAS registry number
(Tm /K)
2-pyridinecarboxylic acid
共273–292兲
共298 –310兲
C6 H5 NO3
⌬ subH m /kJ mol⫺1
121.1⫾1.4
C
104.2⫾2.1
共327–345兲
共327–345兲
C6 H5 N5 O6
C6 H6
1,3-diamino-2,4,6-trinitrobenzene
共335–382兲
benzene
共258 –273兲
共223–279兲
共183–197兲
98.2⫾0.7
98.8
99.0⫾0.5
97.9
共298兲
共336兲
共298兲
C
ME
ME
ME
140
143.5
共350兲
共298兲
LE
41.7
45.2
44.6
45.1
44.8
44.4
共264兲
共298兲
共278兲
共298兲
共298兲
BG
H
Reference
关591-50-4兴
关60/1兴
关40/1兴
关586-96-9兴
关87/4兴关74/34兴
关30/3兴
关98-98-6兴
关99/9兴
关99/9兴
关98/12兴
关59-67-6兴
关00/3兴
关99/9兴
关99/9兴
关84/6兴
关55-22-1兴
关99/9兴
关99/9兴
关98/12兴
关88-75-5兴
关94/28兴
关87/4兴
关35/1兴关38/1兴
关60/1兴
关554-84-7兴
关94/28兴
关92/13兴
关92/13兴
关87/4兴
关35/1兴关38/1兴
关60/1兴
关100-02-7兴
关94/28兴
关71/8兴
关35/1兴关38/1兴
关60/1兴
关824-40-8兴
关98/12兴
关2398-81-4兴
关95/3兴关95/11兴
关13602-12-5兴
关98/12兴
关601-89-8兴
关58/1兴
关3316-09-4兴
关86/3兴
关1874-23-3兴
关80/28兴关86/5兴
关95-14-7兴
关99/8兴
关89/8兴
关89/8兴
关61/3兴
关28930-29-2兴
关87/4兴关69/12兴
关78/15兴
关71-43-2兴
关94/39兴
关87/4兴关76/23兴
关84/21兴
H
TE,ME
关80/1兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
566
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
Compound
Temperature range 共K兲
共221–268兲
共263–270兲
C6 H6
C6 H6 ClN
C6 H6 Cl6
C6 H6 Cl6
C6 H6 Cl6
C6 H6 Cl6
C6 H6 F8 O2
C6 H6 N2 O
C6 H6 N2 O
C6 H6 N2 O2
C6 H6 N2 O2
共193兲
共193兲
共279兲
共261兲
共229兲
共279兲
共282兲
共273兲
共192兲
共226兲
MM
A
A
共307兲
共118兲
MM
共293兲
ME
共328兲
共334兲
TE
共328兲
共379兲
TE
共298兲
共308兲
共273兲
共338兲
共298兲
共335兲
共328兲
共303兲
共303兲
共328兲
ME,TE
ME
GS
C
C
GS
TE
共328兲
共298兲
共338兲
C
ME
121.2⫾3.3
111.8
共298兲
共378兲
C
ME
116.1⫾1.5
99.9
共298兲
共397.5兲
C
ME
119.2⫾2.3
共298兲
ME
125.3⫾1.8
共298兲
ME
90⫾3.0
82.4⫾2
共313兲
90⫾4.2
79.9⫾1.7
89.0⫾0.7
共298兲
4-pyridinecarboxamide
3-pyridinecarboxamide N-oxide
共413– 430兲
4-pyridinecarboxamide N-oxide
共409– 430兲
2-nitroaniline
共310–319兲
C6 H6 N2 O2
53.9⫾0.8
49.4⫾0.4
45.6
44.1
43.1
44.6
46.6
44.6
U33.2
43.3
Method
3-pyridinecarboxamide
共383– 412兲
C6 H6 N2 O2
(Tm /K)
共184 –200兲
共214 –238兲
2,4-hexadiyne
共282–333兲
47⫾2
solid phase transition
1.0
4-chloroaniline
共283–303兲
90.7
␣-hexachlorocyclohexane 共melting point 160 °C兲
共313–363兲
95.7
共324 –344兲
92.9
␤-hexachlorocyclohexane 共melting point 314 °C兲
共506 –551兲
103.7
共313–363兲
107
共368 –390兲
102.9
␥-hexachlorocyclohexane 共melting point 114 °C兲
共310–384兲
92.4⫾4.0
共292–326兲
97.7⫾0.6
共243–303兲
106.6⫾0.9
90.1⫾0.7
90.8⫾0.7
共313–358兲
70.5
共313–363兲
99.2
共293–313兲
88.9
共293–313兲
101.2
共313–343兲
89.7
共333–365兲
115.5
␦ -hexachlorocyclohexane 共melting point 142 °C兲
共313–363兲
97.3
共328 –358兲
97.5
2,2,3,3,4,4,5,5-octafluoro-1,6-hexanediol
89.2⫾8.4
2-pyridinecarboxamide
93.1⫾3.3
共323–373兲
93.1
共363–393兲
C6 H6 N2 O
CAS registry number
⌬ subH m /kJ mol⫺1
2-methyl-5-pyrazine carboxylic acid
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
ME,TE
Reference
关77/4兴
关77/4兴
关74/22兴
关60/1兴
关60/1兴
关56/8兴
关47/2兴
关36/3兴关74/22兴
关33/4兴
关13/1兴
关2809-69-0兴
关82/11兴
关82/11兴
关106-47-8兴
关87/4兴关25/3兴
关319-84-6兴
关87/4兴关60/1兴
关47/1兴
关319-85-7兴
关89/32兴
关87/4兴关60/1兴
关47/1兴
关58-89-9兴
关98/15兴
关96/12兴
关94/1兴
关91/5兴
关91/5兴
关90/26兴
关87/4兴关60/1兴
关83/5兴关70/8兴
关70/8兴
关60/12兴
关47/1兴
关319-86-8兴
关87/4兴关60/1兴
关47/1兴
关355-74-8兴
关74/18兴关77/1兴
关1452-77-3兴
关01/1兴
关87/4兴关60/16兴
关59/13兴
关98-92-0兴
关01/1兴
关87/4兴关60/16兴
关59/13兴
关1453-82-3兴
关01/1兴
关87/4兴关60/16兴
关59/13兴
关1986-81-8兴
关01/1兴
关38557-82-3兴
关01/1兴
关88-74-4兴
关85/7兴
关38/1兴关60/1兴
关35/1兴
关58/1兴关70/1兴
关34/1兴
关97/30兴
关5521-55-1兴
ENTHALPY OF SUBLIMATION
567
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C6 H6 N2 O2
3-nitroaniline
共320–384兲
共320–384兲
共288 –343兲
共332–341兲
共332–341兲
C6 H6 N2 O2
共346 –366兲
C6 H6 N4 O
(Tm /K)
100.9⫾1.5
108.3⫾3
93.6⫾0.7
94.6⫾0.3
96.5⫾0.3
97.6
88.3⫾1.7
88.7⫾2.5
Method
Reference
共298兲
C
共351兲
共351兲
共298兲
共316兲
ME,TE
ME
C
C
ME
TE
关97/25兴
关99-09-2兴
关85/7兴
关73/5兴
关73/5兴
关73/5兴
关58/1兴关70/1兴
关34/1兴
关38/1兴关60/1兴
关35/1兴
关100-01-6兴
关90/2兴
关90/2兴
关87/19兴关91/18兴
关85/7兴
关77/28兴关90/2兴
关73/5兴
关58/1兴关70/1兴
关56/2兴
关56/2兴
关38/1兴
关38/1兴关60/1兴
关34/1兴
关1074-98-2兴
关98/12兴
关1006-08-02兴
关78/17兴
关875-31-0兴
关65/2兴
关3058-38-6兴
关87/4兴关69/12兴
关108-95-2兴
关75/3兴
关71/8兴
关60/3兴关70/1兴
关58/18兴
关48/5兴
关47/1兴关60/1兴
关120-80-9兴
关91/7兴
关84/20兴
关38/1兴关60/1兴
关35/1兴
关108-46-3兴
关91/7兴
关91/7兴
关83/3兴
关68/4兴
关58/1兴
关38/1兴关60/1兴
关35/1兴
关123-31-9兴
关91/7兴
关91/7兴
关83/3兴
关81/4兴
关56/5兴
关53/10兴
关27/2兴
关60706-28-7兴
4-nitroaniline
共351– 417兲
共303–363兲
C6 H6 N2 O3
CAS registry number
⌬ subH m /kJ mol⫺1
共357–367兲
3-methyl-4-nitropyridine N-oxide
共345–392兲
7-methylhypoxanthine
101.4⫾1.3
101.5⫾1.7
94.6
107⫾3
100.4⫾2.1
100.9⫾0.6
109.3
99.3⫾1.7
97.5⫾1.7
100.7⫾2.5
98.7⫾2.5
103.3⫾1.7
共298兲
共298兲
106.7⫾2.0
共298兲
共298兲
共298兲
共333兲
共298兲
共356兲
共298兲
共361兲
共362兲
ME
TE
GS
ME,TE
ME
ME
ME
ME
ME
TE
TE
ME
100.4⫾13
C6 H6 N4 O
C6 H6 N6 O6
C6 H6 O
C6 H6 O2
C6 H6 O2
9-methylhypoxanthine
共500–552兲
2,4,6-trinitro-1,3,5-benzenetriamine
共402– 451兲
phenol
共263–298兲
共230–273兲
共282–313兲
共283–303兲
共270–313兲
共278 –305兲
1,2-dihydroxybenzene
共298 –346兲
C6 H6 O3
168.2
共417兲
LE
65.3⫾3.3
69.7⫾0.9
68.7⫾0.5
68.2
68.1
67.8
共280兲
共298兲
HSA
ME
GS
ME
87.5⫾0.3
86.6⫾1.6
80.8
共298兲
共298兲
C
C
85.3⫾0.5
87.5⫾0.5
92.7
93.3⫾2.1
93.4
95.4⫾1.7
共334兲
共298兲
共353兲
C
C
GS
94.1⫾0.5
93.7⫾0.5
101.7
103.9⫾1
103.8
90.1⫾0.8
103.8
共298兲
共334兲
共370兲
共342兲
共313兲
98.7⫾1
共324兲
共293兲
共292兲
TE
共303兲
1,4-dihydroxybenzene
共341– 400兲
(C6 H6 O2 ) –
(C10H8 O2 )
HSA
1,3-dihydroxybenzene
共328 –379兲
共324 –335兲
共283–323兲
C6 H6 O2
84
共326 –345兲
1,4-hydroquinone-1,4-naphthoquinone
1,2,3-trihydroxybenzene
C
C
GS
ME,TE
QF
TE,ME
关81/4兴
关87-66-1兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
568
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C6 H6 O3
共377–398兲
1,2,4-trihydroxybenzene
C6 H6 O3
1,3,5-trihydroxybenzene
C6 H7 Cl2 N
C6 H7 Cl2 N
C6 H7 Cl2 N
C6 H7 FN2 O2
C6 H7 F3 N2 O4
C6 H7 N
C6 H7 N
(C6 H7 N) – (SO2 )
C6 H7 NO
C6 H7 NO
C6 H7 NO
共383– 406兲
2-chloroaniline hydrochloride
共373– 473兲
3-chloroaniline hydrochloride
共383– 473兲
4-chloroaniline hydrochloride
共373– 483兲
1,3-dimethyl-5-fluorouracil
共338 –373兲
N-关N-共trifluoroacetyl兲glycyl兴glycine
共273– 423兲
3-methylpyridine
共225–255兲
4-methylpyridine
共230–257兲
aniline–sulfur dioxide complex
共277–323兲
2-aminophenol
C6 H7 NO
C6 H7 NO
2-methyl-4-hydroxypyridine
C6 H7 NO
2-methyl-5-hydroxypyridine
C6 H7 NO
2-methyl-6-hydroxypyridine
C6 H7 NO
2-methylpyridine N-oxide
C6 H7 NO
3-methylpyridine N-oxide
C6 H7 NS
C6 H7 NS
C6 H7 N5
C6 H7 N5
116.9⫾0.6
89.1
Method
Reference
共298兲
共387兲
C
119.8⫾1.6
共298兲
C
131.7⫾1.0
127.9
共298兲
C
TE,ME
77.6
共388兲
71.3
共398兲
77.8
共388兲
关86/3兴
关34/2兴
关533-73-3兴
关86/3兴
关108-73-6兴
关86/3兴
关83/23兴
关137-04-2兴
关87/4兴关75/31兴
关141-85-5兴
关87/4兴关75/31兴
关20265-96-7兴
关87/4兴关75/31兴
120.4⫾3.8
共356兲
67
共288兲
62.2
共240兲
RG,ME
62.7
共243兲
RG,ME
82.1
共300兲
93.5⫾0.8
95.3⫾0.7
96.9⫾0.6
103.9⫾0.9
共332兲
共337兲
共298兲
共298兲
C
C
C
C
98.8⫾0.9
101.6⫾0.9
104.7⫾1.2
共335兲
共298兲
共298兲
C
C
C
101.1⫾0.7
103.6⫾0.7
111
109.1⫾1.4
92.1
共335兲
共298兲
共438兲
共298兲
共417兲
C
C
89.3⫾1.3
共298兲
C
113.0⫾1.3
共298兲
C
96.2⫾2.1
共298兲
C
92.0⫾1.3
共298兲
C
78.2⫾2.2
共298兲
C
共298兲
C
共298兲
ME
共365兲
B
共452兲
B
TE
4-aminophenol
共403– 430兲
2-methyl-3-hydroxypyridine
C6 H7 NO3 S
(Tm /K)
3-aminophenol
共423– 459兲
C6 H7 NO
CAS registry number
⌬ subH m /kJ mol⫺1
82.2⫾2.4
4-methylpyridine N-oxide
共345–392兲
85.3⫾2.6
共316 –341兲
79.1⫾1.3
sulfanilic acid 共4-aminobenzene sulfonic acid兲
66.9
4-methylthiopyridine
共347–383兲
75.3⫾3.8
1-methyl-4-thiopyridone
共440– 465兲
188.3⫾9.2
1-methyladenine
138.2
2-methyladenine
121.7
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
C
I
ME
ME
关02/1兴
关400-58-8兴
关87/4兴关60/20兴
关108-99-6兴
关87/4兴关51/5兴
关108-89-4兴
关87/4兴关51/5兴
关31/2兴
关95-55-6兴
关96/18兴
关96/18兴
关96/18兴
关86/11兴
关591-27-5兴
关96/18兴
关96/18兴
关86/11兴
关123-30-8兴
关96/18兴
关96/18兴
关87/4兴
关86/11兴
关54/8兴关60/1兴
关1121-25-1兴
关82/15兴关86/5兴
关18617-86-6兴
关82/15兴关86/5兴
关1121-78-4兴
关82/15兴关86/5兴
关3279-76-3兴
关82/15兴关86/5兴
关931-19-1兴
关95/3兴
关1003-73-2兴
关95/3兴
关1003-67-4兴
关98/12兴
关95/31兴
关121-57-3兴
关38/1兴关60/1兴
关22581-72-2兴
关74/21兴
关6887-59-8兴
关74/21兴
关5142-22-3兴
关00/17兴
关1445-08-5兴
关00/17兴
ENTHALPY OF SUBLIMATION
569
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C6 H7 N5
3-methyladenine
C6 H7 N5
8-methyladenine
C6 H7 N5
9-methyladenine
共413– 458兲
C6 H8 ClN
C6 H8 N2
aniline hydrochloride
共383– 471兲
1,2-diaminobenzene
C6 H8 N2
1,3-diaminobenzene
C6 H8 N2
1,4-diaminobenzene
C6 H8 N2 O2
1,3-dimethyluracil
共311–367兲
共340–369兲
共313–363兲
共400– 454兲
C6 H8 O2
共344 –370兲
1-methylthymine
共378 – 428兲
1,3-cyclohexanedione
C6 H8 O2
1,4-cyclohexanedione
C6 H8 N2 O2
C6 H8 O4
⌬ subH m /kJ mol⫺1
CAS registry number
(Tm /K)
Method
117.5
83.7⫾9
ME
HSA
103.2
ME
121.7
92⫾8
共428兲
87.5
共398兲
85.5⫾0.3
共298兲
C
90.4⫾0.4
共298兲
C
92.2⫾0.2
共298兲
C
115.8⫾3.0
96.9⫾1.2
96.4⫾1.4
101.7⫾2.1
46⫾4.2
77.0⫾1.2
92
共338兲
共298兲
共298兲
共338兲
共426兲
共352兲
TE
C
C
QR
HSA
ME
HSA
124.4⫾1.3
共398兲
QR
89.8⫾1.1
共298兲
C
75.0⫾1.0
84.4
84.2
共298兲
共289兲
共298兲
C
TE,ME
HSA
HSA
dimethyl fumarate
NA
84.5⫾1.7
C6 H8 O4
dimethyl maleate
44.8
C6 H8 O4
共317–341兲
cyclobutane-1,1-dicarboxylic acid
C6 H8 O4
cyclobutane-1,2-dicarboxylic acid
C6 H9 N3 O
1,3,5-trimethyl-4-nitrosopyrazole
C6 H9 N3 O
1,5-dimethylcytosine
共390– 437兲
1,N-dimethylcytosine
共401– 426兲
L-histidine
共392– 492兲
1-methyl-4N-methoxycytosine
共316 –325兲
共320–357兲
41.8⫾4.2
112.2⫾0.7
C
120.0⫾0.9
C
88.0⫾2.0
C6 H9 N3 O
C6 H9 N3 O2
C6 H9 N3 O2
C6 H9 N3 O2
C6 H9 N3 O3
C6 H9 N3 O3
1,5-dimethyl-N-hydroxycytosine
共357–394兲
trimethyl isocyanurate
共330–346兲
trimethyl cyanurate
共331–360兲
共298兲
C
132.8⫾0.6
GS
122.2⫾0.3
GS
142⫾8
共442兲
LE
107.6⫾0.3
106.9⫾0.4
106.4⫾0.8
ME
GS
115.2⫾0.6
GS
86.6⫾1.3
88.2⫾1.3
88.2⫾1.3
共338兲
共298兲
共298兲
C
C
C
90.3⫾1.0
共298兲
C
Reference
关5142-23-4兴
关00/17兴
关78/17兴
关22387-37-7兴
关00/17兴
关700-00-5兴
关87/4兴关65/2兴
关78/17兴
关142-04-1兴
关87/4兴关75/31兴
关95-54-5兴
关97/26兴
关108-45-2兴
关97/26兴
关106-50-3兴
关97/26兴
关874-14-6兴
关00/2兴
关89/17兴
关85/5兴
关80/19兴
关78/17兴
关72/32兴关00/2兴
关65/2兴
关4160-72-9兴
关80/19兴
关504-02-9兴
关93/23兴
关637-88-7兴
关93/23兴
关83/7兴
关83/7兴
关624-49-7兴
关72/7兴
关34/1兴
关624-48-6兴
关38/1兴关60/1兴
关35/1兴
关34/1兴
关5445-51-2兴
关83/26兴
关3396-14-3兴
关83/26兴
关7171-70-2兴
关01/4兴
关17634-60-5兴
关98/37兴
关6220-49-1兴
关98/37兴
关71-00-1兴
关77/2兴
关99/42兴
关99/42兴
关98/37兴
关6220-53-7兴
关98/37兴
关827-16-7兴
关88/12兴
关88/12兴
关89/17兴关85/5兴
关877-89-4兴
关89/17兴关85/5兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
570
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
⌬ subH m /kJ mol⫺1
Polymorph
Temperature range 共K兲
C6 H10N6 O9
N-共2,2-dinitropropyl兲-2,2-dinitro-N-nitroso-1-propanamine
共323–336兲
110.9⫾8
N-共2,2-dinitropropyl兲-2,2-dinitro-N-nitro-1-propanamine
共398 – 423兲
99.2⫾0.8
1-methylcyclopentanol
共253–281兲
73.7⫾0.4
67.0⫾0.2
67.4⫾0.2
cyclohexanone
共243–265兲
49.3
4-methyl-2,6,7-trioxabicyclo关2.2.2兴octane
67.4
1,6-hexanedioic acid 共adipic acid兲
NA
共295–318兲
140
133.6⫾1.3
共359– 406兲
129.3⫾2.5
C6 H10N6 O10
C6 H10O
crystal III
crystal III
crystal II
C6 H10O
C6 H10O3
C6 H10O4
C6 H10O4
共292–320兲
cis-1,3,5,7-tetraoxadecalin
C6 H10O4
trans-1,3,5,7-tetraoxadecalin
C6 H10O5
1,6-anhydro-␤-D-glucose
共344 –386兲
共386 – 405兲
共dl兲-dimethyl tartrate
共314 –339兲
共315–358兲
C6 H10O6
C6 H10O6
C6 H10O6
共d兲-dimethyl tartrate
共310–320兲
共308 –317兲
CAS registry number
(Tm /K)
Method
关28464-26-8兴
关73/12兴关77/1兴
关28464-24-6兴
ME
关73/12兴
关1462-03-9兴
ME
关97/4兴
关97/4兴
C
关97/4兴
关108-94-1兴
关48/5兴
关766-32-5兴
关95/28兴
关124-04-9兴
关01/19兴
TPTD
关01/15兴
ME
关99/10兴关60/4兴
ME
关50/4兴关60/1兴
关70/1兴
A
关47/6兴
关75096-35-4兴 or 关54933-94-7兴
关98/19兴
关75096-35-4兴 or 关54933-94-7兴
关98/19兴
关498-07-7兴
ME
关99/1兴
ME
关99/1兴
关608-69-5兴
HSA
关81/8兴
ME
关54/5兴关77/1兴
关38/1兴关60/1兴
关37/6兴
关5057-96-5兴
HSA
关81/8兴
关54/5兴关77/1兴
关38/1兴关60/1兴
关37/6兴
ME
共267兲
共298兲
共291兲
共254兲
共298兲
共298兲
共383兲
U37.2
共306兲
94.9
共298兲
81.5
共298兲
125.1⫾1.0
100.3⫾5.9
共365兲
共395兲
112⫾5.6
113.8
U 95.0
U 92.5
共326兲
共336兲
77.4⫾8
U 113
88.3
85.8
共315兲
共312兲
meso-dimethyl tartrate
98.3
95.8
C6 H11NO
⑀-caprolactam
共330–340兲
共258 –308兲
共294 –314兲
C6 H11NO
C6 H11NO
C6 H11NO
C6 H11NO2
C6 H11N3 O6
C6 H11N5 O8
C6 H11NS
C6 H12
Reference
89.3⫾0.8
86.3⫾0.2
87.3⫾0.2
77.5
83.3⫾0.8
共335兲
共338兲
共298兲
共273兲
ME
C
共354兲
共317兲
C
ME
cyclohexanone oxime
74.0⫾0.3
共288 –348兲
79.9⫾0.7
cis 2-hexenoic acid amide
共323–333兲
80
trans 2-hexenoic acid amide
共353–393兲
55.8
1-amino-1-cyclopentanecarboxylic acid
123.4⫾4
2,3,3-trinitro-2-methylpentane
90.8
N-共2,2-dinitropropyl兲-2,2-dinitro-1-propanamine
105.4⫾4.2
1-methyl-2-thiopiperidone
共363–370兲
81.2⫾2.9
cyclohexane
共223–280兲
37.6
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
共328兲
共368兲
共455兲
ME
共298兲
共366兲
共265兲
B
关38/1兴关60/1兴
关37/6兴
关502-44-3兴
关92/12兴
关92/12兴
关92/12兴
关87/4兴
关53/5兴关60/1兴
关70/1兴关60/21兴
关100-64-1兴
关92/6兴
关92/6兴
关820-99-5兴
关87/4兴
关820-99-5兴
关87/4兴
关52-52-8兴
关65/1兴关64/16兴
关62154-78-3兴
关99/35兴
关1924-47-6兴
关73/1兴关77/1兴
关13070-07-0兴
关74/21兴
关110-82-7兴
关87/4兴关76/23兴
ENTHALPY OF SUBLIMATION
571
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
Compound
Temperature range 共K兲
C6 H12N2
共268 –278兲
共228 –268兲
共269–279兲
solid phase transition
1,4-diazabicyclo关2.2.2兴octane
共324 –351兲
共353–369兲
共323–373兲
3,3,4,4-tetramethyl-⌬ 1 -1,2-diazetine
C6 H12N2 O4
2,3-dinitro-2,3-dimethylbutane
C6 H12N2
C6 H12N2 O6
C6 H12N4
C6 H12O
C6 H12O2
crystal I
crystal III
C6 H12O2
C6 H12O6
C6 H13ClO2 S
C6 H13NO
C6 H13NO
C6 H13NO2
C6 H13NO2
C6 H13NO2
C6 H13NO2
C6 H13NO2
C6 H14
(Tm /K)
36.4⫾0.7
46.6
37.2
37.7
36.5
6.73
共279.9兲
共186兲
共273兲
共248兲
共274兲
共186兲
61.9⫾3.3
52.3⫾3.3
54.4
共338兲
共361兲
共348兲
62.3⫾1.0
共298兲
79.5⫾0.8
2,5-hexanediol dinitrate
共293–313兲
119
1,3,5,7-tetraazatricyclo关 3.3.1.13,7兴 -decane
共298 – 453兲
76.8
共302–328兲
78.8
74.9⫾2.9
共281–298兲
74.1⫾0.8
75.3
cyclohexanol
共272–298兲
60.7
cis 1,2-cyclohexanediol
89.0
70⫾3.0
88.0⫾1.9
共289–320兲
43.7
trans 1,2-cyclohexanediol
85.9⫾1.4
共289–320兲
42.5
myo-inositol
181
154.7⫾1.4
161
178
168
1-hexanesulfonyl chloride
共273–303兲
60.7 共liq兲
tert-butylacetamide
共278 –295兲
78.3⫾0.3
77.9⫾0.4
hexanamide
共301–371兲
85⫾4.0
共293–303兲
98.7⫾1.7
共338 –368兲
95.1⫾4
共dl兲-2-aminohexanoic acid
共435– 469兲
CAS registry number
⌬ subH m /kJ mol⫺1
Method
Reference
B
B
关74/22兴
关63/6兴
关60/1兴
关47/2兴
关34/4兴
关84/25兴
关280-57-9兴
关60/5兴关70/1兴
关60/5兴关70/1兴
关63/6兴
A
A
C
共298兲
共303兲
共313兲
共316兲
共298兲
共289兲
TE,ME
TE
共285兲
共366兲
共343兲
共304兲
C
C
ME
共343兲
共304兲
C
ME
共477兲
共298兲
共298兲
TE
B
共288兲
共287兲
共298兲
ME
共298兲
共298兲
共353兲
TE
共450兲
ME
共455兲
ME
共373兲
LE
共455兲
ME
153.3⫾0.8
155⫾3
共398兲
共298兲
C
C
50.8
共178兲
B
114.5⫾0.4
GS
2-amino-3-methylpentanoic acid
120.1⫾0.8
L-共d兲-2-amino-4-methylpentanoic acid 共L-共d兲-leucine兲
共323– 423兲
U 83.7⫾4
D-共l兲-leucine
共446 – 464兲
150.6⫾0.8
6-aminohexanoic acid
共388 – 407兲
n-hexane
关78/34兴
关3964-18-9兴
关99/35兴
关42730-17-6兴
关87/4兴关57/7兴
关100-97-0兴
关87/4兴
关83/7兴
关60/5兴关70/2兴
关60/2兴
关58/6兴
关108-93-0兴
关87/4兴关48/5兴
关1792-81-0兴
关99/30兴
关95/17兴
关95/17兴
关87/4兴关40/1兴
关1460-57-7兴
关95/17兴
关87/4兴关40/1兴
关87-89-8兴
关99/30兴
关90/7兴
关90/7兴
关90/7兴
关83/23兴
关14532-24-2兴
关87/4兴关63/11兴
关762-84-5兴
关83/13兴
关83/13兴
关628-02-4兴
关00/1兴
关73/19兴关77/1兴
关59/3兴关70/1兴
关87/4兴
关616-06-8兴
关65/1兴关64/16兴
关87/4兴
关3107-04-8兴
关65/1兴关64/16兴
关328-38-1兴
关77/2兴
关61-90-5兴
关65/1兴关70/1兴
关64/16兴
关60-32-2兴
关83/24兴
关83/24兴
关110-54-3兴
关63/6兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
572
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C6 H14N2 O2
L-lysine
共397– 497兲
L-arginine
共441–541兲
1,6-hexanediol
C6 H14N4 O2
C6 H14O2
C6 H14O2 S
tert-butyl ethyl sulfone
C6 H14O6
D-mannitol
C6 H14O6
D-sorbitol
C6 H14O6
D-galactitol
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
U 88⫾8
共447兲
LE
U 134⫾8
共491兲
LE
112.0⫾0.4
83.3⫾1.7
共298兲
C
202
共298兲
B
186
共298兲
B
共298兲
B
共373兲
B
Method
86.6⫾2.5
C6 H16N2 O2
C6 H16N2 O2
C7 F14
C7 F16
C7 HF5 O2
C7 H4 S3
C7 H4 S3
C7 H5 BrO2
C7 H5 BrO2
C7 H5 BrO2
C7 H5 ClO2
C7 H5 ClO2
C7 H5 ClO2
C7 H5 FO2
C7 H5 FO2
205
N,N⬘ -bis共2-hydroxyethyl兲ethylenediamine
142.7
diisopropyl ammonium nitrite
共288 –299兲
39
perfluoromethylcyclohexane
51.6
n-hexadecafluoroheptane
57.7
pentafluorobenzoic acid
共335–359兲
91.6⫾4.2
4,5-benzo-1,2-dithiole-3-thione
共350–361兲
102.6⫾0.4
107⫾0.4
4,5-benzo-1,3-dithiole-2-thione
118.8⫾0.4
2-bromobenzoic acid
95.9⫾0.4
110.9⫾1.1
83.3⫾0.4
3-bromobenzoic acid
99.2⫾0.2
105.0⫾1.1
4-bromobenzoic acid
103.1⫾0.6
107.6⫾1.1
2-chlorobenzoic acid
100.9⫾0.5
116.2⫾0.6
79.5⫾3.3
共293.5兲
共234兲
B
B
GS
共355兲
共298兲
共298兲
共298兲
共298兲
C
C
DSC
共298兲
共298兲
C
C
共298兲
共298兲
C
C
共298兲
C
DSC
101.4⫾0.4
99.6
105.8
80.8⫾3.3
共298兲
共413兲
共298兲
C
C
C
102.5⫾0.4
101.9
107.9
87.9⫾3.3
共298兲
共413兲
共298兲
C
C
C
93.9⫾0.5
94.4⫾0.8
共316兲
共298兲
ME
93.3⫾0.5
93.6⫾0.6
共310兲
共298兲
ME
3-chlorobenzoic acid
4-chlorobenzoic acid
2-fluorobenzoic acid
共309–323兲
3-fluorobenzoic acid
共303–317兲
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
Reference
关56-87-1兴
关77/2兴
关74-79-3兴
关77/2兴
关629-11-8兴
关90/14兴
关72/12兴关77/1兴
关34008-94-1兴
关U/3兴关70/1兴
关69-65-8兴
关90/7兴
关3615-56-3兴
关90/7兴
关608-66-2兴
关90/7兴
关4439-20-7兴
关97/39兴
关3129-93-9兴
关87/4兴关65/19兴
关355-02-2兴
关63/6兴关57/5兴
关335-57-9兴
关63/6兴关51/7兴
关602-94-8兴
关69/5兴关70/1兴
关3354-42-5兴
关72/16兴
关72/16兴
关934-36-1兴
关73/16兴关77/1兴
关88-65-3兴
关94/4兴
关87/8兴
关83/8兴
关585-76-2兴
关94/4兴
关87/8兴
关586-76-5兴
关94/4兴
关87/8兴
关118-91-2兴
关95/24兴
关83/8兴
关38/1兴关60/1兴
关70/1兴
关535-80-8兴
关95/24兴
关75/20兴
关75/20兴
关38/1兴关60/1兴
关70/1兴
关74-11-3兴
关95/24兴
关75/20兴
关75/20兴
关38/1兴关60/1兴
关70/1兴
关445-29-4兴
关00/5兴
关00/5兴
关455-38-9兴
关00/5兴
关00/5兴
ENTHALPY OF SUBLIMATION
573
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
(Tm /K)
91.2⫾1.3
共370兲
93.1⫾3.8
共298兲
111.4⫾0.8
112.8⫾2.0
92.6⫾0.2
103.0⫾0.4
共352兲
共298兲
共298兲
共298兲
ME
109.6⫾0.5
111.1⫾1.9
96.4⫾0.3
共355兲
共298兲
共298兲
ME
111.0⫾0.4
112.9⫾2.5
99.3⫾0.4
共372兲
共298兲
共298兲
ME
69.5⫾0.4
共298兲
C
72.9⫾0.6
共298兲
B
115.8⫾0.5
118.7⫾0.5
共356兲
共298兲
ME
ME
107.2⫾0.4
110.0⫾0.4
共354兲
共298兲
ME
ME
115.4⫾0.6
119.7⫾0.6
共374兲
共298兲
ME
ME
112.4
113.2⫾1.5
99.2⫾2
104.6⫾1.7
103.3⫾2.5
U122-132
118.4⫾4.2
共308兲
共298兲
102.2
共346兲
ME
132.4⫾2.1
共338兲
ME
111.2⫾2.1
103.3
104.6
共298兲
共337兲
共298兲
2,4,6-N-tetranitro-N-methylaniline
共335– 416兲
benzimidazole
133.8⫾1.6
共298兲
ME
共363兲
共298兲
共350兲
共298兲
共298兲
C
共340–359兲
90.2⫾0.6
94.3⫾0.6
101.8⫾0.4
102.2⫾0.4
98.9⫾0.4
90.9⫾0.2
91.1⫾0.2
87.7⫾0.9
97.1
共318兲
共298兲
ME
Polymorph
Temperature range 共K兲
C7 H5 FO2
4-fluorobenzoic acid
共358 –382兲
C7 H5 IO2
C7 H5 IO2
C7 H5 IO2
CAS registry number
⌬ subH m /kJ mol⫺1
2-iodobenzoic acid
共345–359兲
3-iodobenzoic acid
共347–363兲
4-iodobenzoic acid
共363–379兲
C7 H5 NO
benzoxazole
C7 H5 NS
benzothiazole
C7 H5 NO4
3-共5-nitro-2-furyl兲-2-propenal
C7 H5 NO4
2-nitrobenzoic acid
共346 –356兲
Method
GS
C
DSC
C
C
97.9⫾2.1
C7 H5 NO4
C7 H5 NO4
C7 H5 N3 O6
3-nitrobenzoic acid
共347–361兲
4-nitrobenzoic acid
共367–381兲
2,4,6-trinitrotoluene
共293–353兲
共301–349兲
共297–330兲
共327–349兲
共323–353兲
C7 H5 N3 O7
C7 H5 N3 O7
C7 H5 N5 O8
C7 H6 N2
C7 H6 N2
C7 H6 N2 O2
共340–353兲
2,4,6-trinitroanisole
共334 –342兲
3-hydroxy-2,4,6-trinitrotoluene
共310–365兲
共325–350兲
indazole
共308 –317兲
5-methoxybenzofurazan
共298兲
共338兲
ME
GS
ME
TGA
ME
ME
ME
Reference
关456-22-4兴
关69/5兴关70/1兴
关87/4兴
关69/5兴关00/5兴
关88-67-5兴
关00/5兴
关00/5兴
关94/30兴关95/24兴
关83/8兴
关618-51-9兴
关00/5兴
关00/5兴
关94/30兴关95/24兴
关619-58-9兴
关00/5兴
关00/5兴
关94/30兴关95/24兴
关273-53-0兴
关98/20兴
关95-16-9兴
关98/20兴
关1874-22-2兴
关80/28兴关86/5兴
关552-16-9兴
关99/31兴
关99/31兴
关121-92-6兴
关99/31兴
关99/31兴
关62-23-7兴
关99/31兴
关99/31兴
关118-96-7兴
关87/4兴
关78/15兴
关76/3兴关77/5兴
关71/4兴
关70/3兴
关70/26兴关78/15兴
关50/1兴关60/1兴
关70/1兴
关50/2兴
关606-35-9兴
关87/4兴关70/1兴
关50/2兴
关602-99-3兴
关78/15兴
关70/3兴
关70/3兴
关479-45-8兴
关78/15兴
关51-17-2兴
关98/6兴
关98/6兴
关87/9兴
关87/9兴
关86/15兴
关271-44-3兴
关87/9兴
关87/9兴关86/15兴
关85/6兴
关61/3兴
关4413-48-3兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
574
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C7 H6 N2 O2
5-methylbenzofurazan-1-oxide
C7 H6 N2 O3
5-methoxybenzofurazan-1-oxide
C7 H6 N2 O3
anti
syn
C7 H6 N2 O3
anti
syn
C7 H6 N2 O3
anti
C7 H6 N2 O4
2-nitrobenzaldoxime
C7 H6 N2 O4
C7 H6 N2 O4
C7 H6 N2 O5
C7 H6 O2
(Tm /K)
89.2⫾0.7
Method
Reference
共298兲
C
92.2⫾1.2
共298兲
C
96.0⫾1.6
共298兲
C
关96/6兴
关19164-41-1兴
关96/6兴
关7791-49-3兴
关96/6兴
关6635-41-2兴
关83/9兴
关83/9兴
关3431-62-7兴
关83/9兴
关83/9兴
关1129-37-9兴
关83/9兴
关25321-14-6兴
关72/6兴
关121-14-2兴
关77/1兴关70/3兴
关77/1兴关70/3兴
关76/3兴关77/5兴
关70/1兴关71/4兴
关606-20-2兴
关76/3兴关77/5兴
关611-38-1兴
关87/4兴
关534-52-1兴
关47/1兴关60/1兴
关65-85-0兴
关01/5兴
关99/42兴
关99/36兴
关98/38兴
关97/36兴
关90/3兴
关90/3兴
关88/4兴
关88/4兴
关85/9兴
关85/10兴
关83/8兴
关82/3兴
关82/12兴
关82/1兴
关81/3兴
关80/20兴
关80/30兴
关78/17兴
关76/7兴
关75/6兴
关75/5兴
关74/5兴
关73/1兴
关73/2兴
关73/2兴
关72/9兴
关72/3兴
关72/1兴关71/6兴
关71/17兴
关70/19兴关99/42兴
关70/9兴
关69/2兴
关68/9兴
关65/6兴
关54/1兴关70/1兴
U 26.4⫾1.7
U 40.2⫾1.7
MS
MS
U 41.0⫾1.7
U 42.7⫾1.7
MS
MS
U 56.4⫾1.7
MS
76.1⫾0.8
ME
3-nitrobenzaldoxime
4-nitrobenzaldoxime
1,1-dinitrophenylmethane
共312–323兲
2,4-dinitrotoluene
共332–342兲
共277–344兲
C7 H6 N2 O4
CAS registry number
⌬ subH m /kJ mol⫺1
2,6-dinitrotoluene
共277–323兲
共dinitromethyl兲benzene
共312–323兲
3,5-dinitro-o-cresol
共290–324兲
benzoic acid
共323–394兲
共313–343兲
共307–314兲
共293–319兲
共320–370兲
共316 –391兲
共293–313兲
共328 –398兲
共344 –395兲
共281–323兲
共294 –331兲
共293–318兲
共273–318兲
共293–311兲
共338 –383兲
共338 –383兲
共290–315兲
共293–308兲
共299–329兲
共290–315兲
共324 –392兲
共348 –378兲
共291–307兲
共243–387兲
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
98.3⫾2.5
99.6⫾2.5
95.8⫾1.25
99.6⫾1.3
共337兲
共298兲
共310兲
98.3⫾.8
共300兲
76.1
共317.5兲
103.3
88.3⫾0.5
90.5⫾0.3
89⫾6
87.5⫾0.4
86.7
88.7⫾0.9
89.3⫾0.9
87.5⫾0.3
89.2⫾1.0
95.1⫾1.8
90.8⫾0.6
89.5⫾0.4
89.1⫾0.2
89.5⫾0.5
90.6⫾2
93.45⫾1
U 133.5⫾4.5
85⫾2
88.3⫾2.9
88.5⫾0.8
92.5⫾4
88.5⫾1.6
92.9⫾0.2
88.1⫾0.2
89.0⫾0.4
89.3⫾0.4
86.6⫾1.3
90.⫾0.3
89.5⫾0.2
89.1
86.6⫾1.7
90.4⫾0.8
89.7⫾0.6
88.9⫾0.5
90.9
91.5⫾0.5
ME
GS
ME
GS
TE
共298兲
共311兲
共298兲
共335兲
共298兲
共294兲
共306兲
共353兲
共369兲
共296兲
共298兲
共314兲
共303兲
共367兲
共298兲
共363兲
共299兲
共298兲
C
GS
TGA
TGA
ME
C
QR
DSC
C
DM
ME
GS
C
SG
LE
C
ME
TE
ME
TCM
ME
C
ME,C
ME
C
ME
HSA
C
GS
ME
GS
ENTHALPY OF SUBLIMATION
575
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
C7 H6 O2
C7 H6 O2
Compound
Temperature range 共K兲
共333–389兲
共377–394兲
4-hydroxybenzaldehyde
共303–336兲
共312–336兲
tropolone
共273–333兲
C7 H6 O2
3-共2-furyl兲-2-propenal
C7 H6 O3
2-hydroxybenzoic acid
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
84.2⫾0.8
85.8
84.5⫾0.5
共318兲
共383兲
共364兲
98.2⫾1.3
91.2
共298兲
共324兲
84.1⫾0.4
83.7⫾0.8
共298兲
Method
TE
T
I
ME
76.1⫾2.1
共307–324兲
共312–332兲
共312–332兲
共298 –328兲
共368 – 408兲
共368 – 408兲
C7 H6 O3
C7 H6 O3
C7 H6 O4
2,4-dihydroxybenzoic acid
C7 H6 O4
2,5-dihydroxybenzoic acid
C7 H6 O4
2,6-dihydroxybenzoic acid
C7 H6 O4
3,4-dihydroxybenzoic acid
C7 H6 O4
3,5-dihydroxybenzoic acid
C7 H6 O5
3,4,5-trihydroxybenzoic acid
共391– 421兲
2-aminotropone
共273–333兲
benzamide
共325–342兲
共323–349兲
formanilide
共298 –318兲
2-aminobenzoic acid 共I兲
C7 H7 NO
C7 H7 NO2
C7 H7 NO2
C7 H7 NO2
C7 H7 NO2
123.5⫾0.74
125.0⫾0.74
共363兲
共298兲
C
112.4⫾0.7
114.1⫾0.7
116.3
共363兲
共298兲
C
C
ME
TE
ME
ME
GS
4-hydroxybenzoic acid
共398 – 433兲
2,3-dihydroxybenzoic acid
C7 H7 NO
共333兲
共298兲
共315兲
共322兲
共322兲
共313兲
3-hydroxybenzoic acid
C7 H6 O4
C7 H7 NO
95.1⫾0.5
96.3⫾0.5
95.7⫾0.8
94.9⫾0.4
93.22⫾0.8
99.2⫾2
94.8⫾0.4
95.1⫾0.4
2-aminobenzoic acid 共II兲
共331–349兲
3-aminobenzoic acid
共366 –385兲
共367–389兲
4-aminobenzoic acid
共364 –384兲
共367–389兲
GS
116⫾4
TGA
126⫾6
TGA
109⫾3
TGA
111⫾7
TGA
153⫾9
TGA
135⫾6
TGA
75.1
共406兲
71.13⫾0.4
ME
96.9
101.7⫾1
共333.5兲
共298兲
77.8
共308兲
111.6⫾1.7
共298兲
100⫾1
99.6⫾0.5
104.9⫾1
共338兲
共378兲
共298兲
TE,ME
C
C
122⫾1
122.3⫾3
128⫾3.2
共375兲
TE,ME
C
C
112.3⫾1
114⫾3.5
共373兲
共298兲
C
TE,ME
C
Reference
关60/1兴
关38/1兴
关34/2兴
关27/3兴
关123-08-0兴
关87/4兴关71/8兴
关60/14兴
关533-75-5兴
关71/3兴
关51/4兴关70/1兴
关623-30-3兴
关80/28兴关86/5兴
关69-72-7兴
关93/22兴
关93/22兴
关80/2兴关81/11兴
关77/4兴
关77/4兴
关74/5兴
关73/2兴
关54/1兴关70/1兴
关60/1兴
关99-06-9兴
关93/22兴
关93/22兴
关99-96-7兴
关93/22兴
关93/22兴
关54/1兴关60/1兴
关303-38-8兴
关99/36兴
关89-86-1兴
关99/36兴
关490-79-9兴
关99/36兴
关303-07-1兴
关99/36兴
关99-50-3兴
关99/36兴
关99-10-5兴
关99/36兴
关149-91-7兴
关34/2兴
关6264-93-3兴
关71/3兴
关55-21-0兴
关87/4兴关60/21兴
关82/2兴
关103-70-8兴
关87/4兴关60/21兴
关118-92-3兴
关72/4兴
关79/1兴
关74/1兴
关74/1兴
关99-05-8兴
关79/1兴
关74/1兴
关74/1兴关77/13兴
关150-13-0兴
关79/1兴
关74/1兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
576
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
C7 H7 NO2
共melting point 330 K兲
anti
syn
C7 H7 NO2
anti
syn
C7 H7 NO2
anti
C7 H7 NO2
C7 H7 NO3
anti
syn
C7 H7 NS
Compound
Temperature range 共K兲
2-hydroxybenzaldoxime
共423–513兲
共298 –310兲
2,4-dihydroxybenzaldoxime
C7 H8 N4 O2
form I
form I
form II
form II
C7 H8 O
C7 H8 O
C7 H8 O
C7 H8 O2
C7 H8 O2
C7 H8 O2
C7 H8 O2
C7 H8 O2 S
共298兲
C
共468兲
共298兲
DSC
关74/1兴关77/13兴
关38/1兴关60/1兴
关94-67-7兴
关84/12兴
关84/12兴
关83/9兴
关83/9兴
关22241-18-5兴
关83/9兴
关83/9兴
关699-06-9兴
关83/9兴
关99-99-0兴
关71/4兴
关70/3兴
关5399-68-8兴
关83/9兴
关83/9兴
关2227-79-4兴
关89/11兴
关82/17兴
关108-88-3兴
关70/3兴
关64-10-8兴
关87/2兴
关3398-07-0兴
关83/9兴
关83/9兴
关5231-96-9兴
关79/12兴
关33496-46-7兴
关71/3兴
关31010-51-2兴
关78/17兴
关65/2兴
关20535-82-4兴
关78/17兴
关58-55-9兴
关99/40兴
关99/40兴
关99/40兴
关99/40兴
关83/17兴
关83/17兴关99/40兴
关95-48-7兴
关87/4兴
关60/3兴关70/1兴
关108-39-4兴
关87/4兴
关60/3兴
关106-44-5兴
关60/3兴关70/1兴
关150-76-5兴
关87/4兴关60/14兴
关488-17-5兴
关84/20兴
关452-86-8兴
关84/20兴
关95-71-6兴
关99/28兴
关99/28兴
关52911-98-5兴
关74/21兴
MS
MS
U 52.7⫾1.7
U 57.3⫾1.7
MS
MS
U 54.4⫾1.7
MS
79.1⫾2.5
79.1
共298兲
共298兲
U 76.2⫾1.7
U 93.7⫾1.7
ME
MS
MS
thiobenzamide
monophenylurea
共392– 412兲
2-aminobenzaldoxime
C7 H8 N4 O
96.7⫾9.4
105.2⫾10
U 51⫾1.7
U 65.3⫾1.7
Reference
4-nitrotoluene
C7 H8 N2 O
C7 H8 N4 O
116⫾3.7
U 142
Method
4-hydroxybenzaldoxime
toluene
C7 H8 N2
(Tm /K)
3-hydroxybenzaldoxime
C7 H8
C7 H8 N2 O
anti
syn
C7 H8 N2 O
CAS registry number
⌬ subH m /kJ mol⫺1
103.4⫾2.2
97.2⫾0.6
共298兲
共298兲
C
C
43.1
共298兲
B
136⫾6
共406兲
TE
U 33.9⫾1.7
U 63.6⫾1.7
共2-pyridyl兲acetamide
103.8
1-amino-7-imino-1,3,5-cycloheptatriene
共273–333兲
49.4⫾0.4
9-ethylhypoxanthine
108.8⫾13
U 83.7
1,9-dimethylhypoxanthine
75.3⫾13
1,3-dimethylxanthine 共theophylline兲
共413– 453兲
132.0⫾0.3
142
共413– 453兲
134.2⫾0.3
144
126
135
2-methylphenol
共273–303兲
74.8
共273–303兲
76.0⫾0.8
3-methylphenol
共273–285兲
56.1
共284 –313兲
61.7⫾1.0 共liq兲
4-methylphenol
共273–307兲
73.9⫾1.5
4-methoxyphenol
共278 –300兲
88.7
3-methyl-1,2-dihydroxybenzene
93.2⫾1.0
4-methyl-1,2-dihydroxybenzene
94.9⫾1.0
2-methyl-1,4-dihydroxybenzene
共333–368兲
97.2⫾1.4
100.4⫾1.4
4-methoxy-6-methyl-2-thiopyrone
共402– 415兲
130.5⫾5.9
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
MS
MS
共298兲
B,E
ME
HSA
HSA
HSA
共433兲
共298兲
共433兲
共298兲
共421兲
共298兲
T
T
ME,TE
共288兲
共288兲
共279兲
GS
共290兲
共289兲
共298兲
C
共298兲
C
共351兲
共298兲
GS
共408兲
B
ENTHALPY OF SUBLIMATION
577
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C7 H8 O2 S
C7 H8 O2 S
6-methyl-2-methylthio-4-pyrone
共388 – 433兲
methyl phenyl sulfone
C7 H8 O3
3-methoxycatechol
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
87.4⫾3.8
共410兲
Method
B
92⫾2.9
C7 H8 S3
C7 H8 S3
C7 H9 F3 N2 O4
C7 H9 N
C7 H9 N5
C7 H9 N5
C7 H10
C7 H10
C7 H10N2
C7 H10N2 O2
C7 H10N2 O2
C7 H10N2 O2
C7 H10O
C7 H10O
C7 H10O2
C7 H10O3
C7 H10O3
C7 H10S3
C7 H11N3 O
C7 H11N3 O
C7 H11N3 O2
C7 H11N5 O10
C7 H12
91.7⫾0.8
4,5-tetramethylene-1,3-dithiole-2-thione
共340–352兲
98.3
102.1⫾2.9
4,5-tetramethylene-1,2-dithiole-3-thione
共335–350兲
101.6
105.3
N-关N-共trifluoroacetyl兲glycyl兴glycine methyl ester
共323– 419兲
127.9
p-toluidine
78.8⫾0.5
8,9-dimethyladenine
共369–374兲
105.8⫾0.8
2,9-dimethyladenine
共359–364兲
123.5
norbornene
37.8⫾0.14
37.7⫾0.9
38.7⫾0.5
33.6⫾0.08
solid phase transition
4.37
nortricyclene
38.7⫾0.7
39.2⫾1.1
␣-tert-butylmalononitrile
共293–323兲
59.8⫾0.7
1,3-dimethylthymine
共313–363兲
109.2⫾2.1
1,3,5-trimethyluracil
共321–331兲
103.5⫾1.5
1,3,6-trimethyluracil
共300–340兲
106.7⫾2.5
bicyclo关2.2.1兴heptan-2-one
共300–340兲
49.0⫾1.7
bicyclo关2.2.1兴heptan-7-one
共300–340兲
47.3⫾2.2
2-oxabicyclo关2.2.2兴octan-3-one
69.6⫾2.1
2,4,10-trioxaadamantane
74.4⫾0.4
tetramethylsuccinic anhydride
74.1⫾4.2
4,5-tetramethylene-1,3-dithiolan-2-thione
共353–369兲
99.0
103.9⫾2.9
1,N,N-trimethylcytosine
110.9⫾1.7
1,5,N-trimethylcytosine
共396 – 431兲
108.0⫾2.0
1,5-dimethyl-N-methoxycytosine
共327–365兲
95.6⫾0.7
1,1,1,4,4-pentanitro-2,2-dimethylpentane
103.8
bicyclo关2.2.1兴heptane
40.0⫾0.1
40.3⫾0.32
40.4⫾0.8
39.33⫾0.13
共298兲
共346兲
共342兲
共298兲
共338兲
共298兲
共361兲
ME
共371兲
共298兲
共298兲
共298兲
C
BG
C
共130兲
共298兲
共298兲
BG
C
共298兲
共338兲
QR
共326兲
ME
共320兲
QR
共298兲
BG
共298兲
BG
共298兲
C
共360兲
共298兲
GS
GS
共298兲
共298兲
共298兲
C
C
Reference
关52911-99-6兴
关74/21兴
关3112-85-4兴
关U/3兴关70/1兴
关934-00-9兴
关86/3兴
关698-42-0兴
关67/5兴关70/1兴
关67/5兴关70/1兴
关14085-34-8兴
关72/16兴
关72/16兴
关433-33-0兴
关87/4兴关60/20兴
关106-49-0兴
关90/24兴
关87578-82-3兴
关87/7兴
关76470-20-7兴
关92/5兴
关498-66-8兴
关82/4兴
关78/5兴
关76/4兴
关73/27兴
关92/17兴
关279-19-6兴
关78/5兴
关76/4兴
关4210-60-0兴
关90/18兴
关4401-71-2兴
关80/19兴
关4401-71-2兴
关96/5兴
关13509-52-9兴
关80/19兴
关497-38-1兴
关78/1兴
关10218-02-7兴
关78/1兴
关4350-84-9兴
关80/17兴
关281-32-3兴
关74/16兴
关281-32-3兴
关54/3兴关70/1兴
关2164-87-6兴
关67/5兴关70/1兴
关67/5兴关70/1兴
关2228-27-5兴
关98/37兴
关25307-94-2兴
关98/37兴
关98/37兴
关242800-94-8兴
关99/35兴
关279-23-2兴
关87/1兴
关82/4兴
关78/5兴
关73/27兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
578
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
C7 H12ClN5
C7 H12O3
C7 H12O4
C7 H12O4
C7 H13N
C7 H13NO
Compound
Temperature range 共K兲
40.1⫾0.8
共284 –326兲
40.0⫾0.8
2-chloro-4,6-bis共ethylamino兲-s-triazine 共Simazin兲
共323– 403兲
130.8
1,4-dimethyl-2,6,7-trioxabicyclo关2.2.2兴octane
74.9
1,7-heptanedioic acid 共pimelic acid兲
共288 –308兲
178
共358 –371兲
136.6⫾1.0
139.9⫾1.0
butylmalonic acid
共348 –362兲
122.5⫾1.4
124.6⫾2.3
1-azabicyclooctane
50.8⫾0.4
共273–362兲
50.8⫾0.2
C7 H14
trans-6-heptenoic acid amide
共362–393兲
cycloheptane
C7 H14N2
3,3,5,5-tetramethyl-1-pyrazoline
C7 H14N2 O2
N-acetyl L-valinamide
C7 H14N2 O2 S
C7 H14O
C7 H15NO
C7 H15NO2
⌬ subH m /kJ mol⫺1
C7 H16
C7 H16N2 S
1,3-di-n-propylthiourea
C8 H2 Cl4 N2
C8 H4 Cl2 N2
C8 H4 N2
C8 H4 N2
C8 H4 N2
C8 H4 N2 O2
C8 H4 O2
C8 H4 O3
共305兲
BG
TSGC
共338兲
GS-GC
关71/1兴关77/1兴
关75/2兴
关122-34-9兴
关87/4兴关64/14兴
关27761-61-1兴
关95/28兴
关111-16-0兴
关01/15兴
关99/10兴
关99/10兴
关534-59-8兴
关00/22兴
关00/22兴
关100-76-5兴
关71/10兴关77/1兴
关48/3兴关70/1兴
关60/1兴
共298兲
共365兲
共298兲
共355兲
共298兲
TPTD
ME
ME
ME
共298兲
53.5
共134兲
61.6⫾0.2
共298兲
共376兲
共298兲
共418兲
C
共310兲
ME
共291兲
C
96.2⫾0.8
134.9⫾3
132.5⫾3.0
2,4,5,6-tetrachloro-1,3-benzenedicarbonitrile
共363– 418兲
109.1
2,3,6,7-tetrachloroquinoxaline
共347–361兲
106.2⫾0.3
108.2⫾1.9
2,3-dichloroquinoxaline
共313–329兲
92.4⫾0.4
93.1⫾0.9
1,2-dicyanobenzene
86.9⫾1.5
1,3-dicyanobenzene
90.1⫾1.5
1,4-dicyanobenzene
89.7⫾1.8
88.8⫾1.5
1,4-dicyanobenzene di-N-oxide
73.0⫾2.0
benzocyclobutenedione
共304 –367兲
U 89.5
phthalic anhydride
共313–383兲
87.9
共333– 403兲
84.4⫾1.2
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
Reference
共377兲
57.9
C8 Cl4 N2
Method
97.2
129.8⫾1.9
133.1⫾2.2
共391– 425兲
126⫾2.0
2-methyl-2共methylthio兲propanal, O-关共methylamino兲carbonyl兴oxime
共298 –323兲
80
1-methylcyclohexanol
75.9⫾0.4
heptanamide 共enanthamide兲
共345–365兲
99.6
hexyl carbamate
共291–314兲
n-heptane
CAS registry number
(Tm /K)
GS
共183兲
B
共298兲
共298兲
B,HA
C
共378兲
ME, GS
共354兲
共298兲
ME
ME
共321兲
共298兲
ME
ME
共298兲
GS
共298兲
GS
共298兲
共298兲
ME
GS
共298兲
ME
共336兲
共348兲
共388兲
GS
关87/4兴
关291-64-5兴
关63/6兴
关2721-31-5兴
关76/12兴
关37933-88-3兴
关99/12兴
关99/12兴
关90/13兴
关116-06-3兴
关87/4兴关76/11兴
关590-67-0兴
关98/34兴
关628-62-6兴
关59/3兴关60/1兴
关87/4兴
关2114-20-7兴
关59/4兴
关142-82-5兴
关63/6兴
关26536-60-7兴
关00/23兴
关94/17兴
关1897-45-6兴
关87/4兴关80/37兴
关25983-14-6兴
关00/26兴
关00/26兴
关2213-63-0兴
关00/26兴
关00/26兴
关91-15-6兴
关80/10兴
关626-17-5兴
关80/10兴
关623-26-7兴
关92/24兴
关80/10兴
关3729-34-8兴
关92/24兴
关6383-11-5兴
关89/9兴
关85-44-9兴
关87/4兴关72/25兴
关79/6兴
ENTHALPY OF SUBLIMATION
579
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
Compound
Temperature range 共K兲
共303–333兲
C8 H5 F3 OS2
C8 H5 F3 O2 S
C8 H5 F3 O3
C8 H5 NO
C8 H5 NO2
C8 H5 N3
C8 H6 ClNO3
C8 H6 ClNO3
C8 H6 N2
C8 H6 N2
C8 H6 N2
C8 H6 N2 O
C8 H6 O3
共459兲
关71/6兴
关46/2兴关70/1兴
关60/1兴
关4552-64-1兴
关97/19兴
关15788-02-0兴
关97/19兴
关92/28兴
关326-90-9兴
关97/33兴
关613-90-1兴
关69/9兴关77/1兴
关87/4兴
关85-41-6兴
关87/4兴关56/13兴
关27032-01-5兴
关87/4兴
关67/3兴关70/1兴
关22751-23-1兴
关87/4兴关47/1兴
关60/1兴
关99-47-8兴
关87/4兴关47/1兴
关60/1兴
关253-52-1兴
关95/25兴
关98/7兴关93/19兴
关72/10兴
关91-19-0兴
关95/25兴
关93/19兴
关253-82-7兴
关98/7兴关93/19兴
关95/25兴
关1196-57-2兴
关00/26兴
关00/26兴
关00/15兴
关15804-19-0兴
关00/15兴
关2433-66-7兴
关97/25兴
关2518-24-3兴
关87/4兴关56/13兴
关3676-85-5兴
关87/4兴
共348兲
关67/6兴
共350兲
关67/6兴
关120-57-0兴
关53/7兴关60/1兴
关87/4兴
关88-99-3兴
关99/16兴
关121-91-5兴
关99/16兴
关87/4兴关62/2兴
关62/2兴关70/1兴
关100-21-0兴
关99/16兴
关87/4兴关62/2兴
关62/2兴
共298兲
C
共298兲
共298兲
C
ME
共298兲
共298兲
共418兲
103.6
共311兲
TE
109.1
共314兲
TE
82.3⫾2.3
81.1⫾0.4
96.7
共298兲
共298兲
C
C
ME
66.6⫾2.0
69.4⫾0.6
共298兲
共298兲
C
C
77.6⫾0.5
76.6⫾1.4
共298兲
共298兲
C
C
116.1⫾0.6
118.5⫾3.1
125.8⫾4.0
共391兲
共298兲
共298兲
ME
ME
C
156.3⫾5.5
共298兲
C
112.0⫾1.9
3-aminophthalimide
共386 – 459兲
108.3
4-aminophthalimide
共444 – 498兲
135.3
monobenzo-1,3␣,4,6␣-tetraazapentalene
共323–373兲
74.9⫾2.9
monobenzo-1,3␣,6,6␣-tetraazapentalene
共323–383兲
63.6⫾2.9
piperonal
共293–353兲
90.8
共298兲
C
共401兲
RG
3-nitrobenzeneacetyl chloride
共299–343兲
RG
ME
phthalazine
quinoxaline
quinazoline
2-hydroxyquinoxaline
共383–399兲
quinoxaline-1,4-dioxide
C8 H6 N4
C
125.4
125.5⫾1.3
C8 H6 N2 O2
C8 H6 N4
共318兲
Reference
共393兲
2,3-dihydroxyquinoxaline
C8 H6 N2 O2
81⫾1
88.4⫾1.2
Method
82.8
C8 H6 N2 O2
C8 H6 N2 O2
(Tm /K)
1,1,1-trifluoro-4-共2-thienyl兲-4-mercapto-3-buten-2-one
95.1⫾3.7
1,1,1-trifluoro-4-共2-thienyl兲-4-hydroxy-3-buten-2-one
86.2⫾0.6
86.2⫾0.6
4,4,4-trifluoro-1-共2-furanyl兲-butane-1,3-dione
70⫾10
␣-oxo-benzeneacetonitrile
共292–304兲
78.7⫾4.2
phthalimide
共378 – 418兲
pyridinium dicyanomethylide
共403– 433兲
共403– 433兲
2-nitrobenzeneacetyl chloride
共296 –327兲
CAS registry number
⌬ subH m /kJ mol⫺1
C8 H6 O4
phthalic acid
C8 H6 O4
isophthalic acid
C8 H6 O4
共493–563兲
共493–563兲
terephthalic acid
共523– 633兲
共523– 633兲
共323兲
129.8⫾0.6
共298兲
C
142.0⫾0.7
114.2
106.7⫾2.2
共298兲
共508兲
共523兲
C
146.6⫾0.5
139.2
131.
共298兲
共538兲
共573兲
C
GS
GS
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
580
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C8 H6 S
共392– 425兲
2,3-benzothiophene
共273– 403兲
C8 H7 ClO
C8 H7 N
C8 H7 NO3
C8 H7 NO4
C8 H7 NO4
C8 H7 NO4
C8 H7 NO4
C8 H7 NO4
C8 H7 NO4
C8 H7 NO5
C8 H7 NO5
C8 H7 NO5
C8 H7 N3 O2
C8 H7 N3 O6
C8 H7 N3 O6
C8 H7 N3 O7
C8 H8
2-chloroacetophenone
共278 –323兲
indole
共291–319兲
共275–303兲
共283–301兲
共283–328兲
3-nitroacetophenone
共293–343兲
2-methyl-3-nitrobenzoic acid
共357–371兲
2-methyl-6-nitrobenzoic acid
共355–369兲
3-methyl-2-nitrobenzoic acid
共371–385兲
3-methyl-4-nitrobenzoic acid
共363–379兲
4-methyl-3-nitrobenzoic acid
共363–377兲
5-methyl-2-nitrobenzoic acid
共355–371兲
3-methoxy-2-nitrobenzoic acid
共398 – 410兲
4-methoxy-3-nitrobenzoic acid
共387– 401兲
3-methoxy-4-nitrobenzoic acid
共388 – 402兲
3,6-diaminophthalimide
共461–508兲
2,2,2-trinitro-1-phenylethane
共293–308兲
3-methyl-2,4,6-trinitrotoluene
共319– 411兲
2,4,6-trinitrophenetole
共352–364兲
共342–352兲
cubane
共239–262兲
C8 H8
cyclooctatetraene
C8 H8 N2 O2
1,3-benzenedicarboxamide
C8 H8 N2 O2
1,4-benzenedicarboxamide
共373– 498兲
2-phenylacetic acid
共305–321兲
C8 H8 O
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
98.24⫾2.5
共408兲
61.1
65.7⫾0.2
共288兲
共298兲
GS
C
90.7
共293兲
TE
75
77.8⫾1.6
70.0
74.9
共305兲
共289兲
共292兲
共305兲
110
共308兲
117.3⫾0.6
119.5⫾2.3
共364兲
共298兲
ME
ME
117.8⫾0.6
120.0⫾2.2
共362兲
共298兲
ME
ME
121.7⫾0.5
124.4⫾2.7
共378兲
共298兲
ME
ME
116.8⫾0.6
119.3⫾2.5
共371兲
共298兲
ME
ME
116.1⫾0.6
118.6⫾2.5
共370兲
共298兲
ME
ME
116.5⫾0.5
118.7⫾2.2
共363兲
共298兲
ME
ME
136.6⫾1.3
141.9⫾1.3
共404兲
共298兲
ME
ME
126.5⫾0.8
131.2⫾0.8
共394兲
共298兲
ME
ME
126.1⫾1.1
131.0⫾1.1
共395兲
共298兲
ME
ME
98.5
共476兲
RG
84.1⫾0.4
共301兲
ME
129.8⫾1.1
共365兲
ME
79 共liq兲
120.5⫾2.1
共358兲
共347兲
ME
ME
80.3⫾1.6
共298兲
ME
Method
ME
54.4
B
54.4⫾4.2
ME
57.3⫾4.2
98.6⫾0.4
共313兲
ME
Reference
关34/2兴关70/1兴
关95-15-8兴
关81/14兴
关79/2兴
关532-27-4兴
关87/4兴关47/1兴
关60/1兴
关120-72-9兴
关87/4兴
关74/5兴
关55/10兴
关54/4兴关60/1兴
关121-89-1兴
关87/4兴
关1975-50-4兴
关01/7兴
关01/7兴
关13506-76-8兴
关01/7兴
关01/7兴
关5437-38-7兴
关01/7兴
关01/7兴
关3113-71-1兴
关01/7兴
关01/7兴
关96-98-0兴
关01/7兴
关01/7兴
关3113-72-2兴
关01/7兴
关01/7兴
关4920-80-3兴
关99/31兴
关99/31兴
关89-41-8兴
关99/31兴
关99/31兴
关5081-36-7兴
关99/31兴
关99/31兴
关1660-15-7兴
关87/4兴关56/13兴
关38677-56-4兴
关72/6兴关77/1兴
关87/4兴
关632-92-8兴
关87/4兴关78/15兴
关4732-14-3兴
关87/4兴关50/2兴
关50/5兴关70/1兴
关50/2兴
关277-10-1兴
关66/2兴关70/1兴
关87/4兴
关629-20-9兴
关49/9兴
关1740-57-4兴
关71/15兴关77/1兴
关3010-82-0兴
关72/14兴关77/1兴
关103-82-2兴
关01/10兴
ENTHALPY OF SUBLIMATION
581
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C8 H8 O2
2-methylbenzoic acid
共297–337兲
C8 H8 O2
C8 H8 O2
C8 H8 O2
C8 H8 O2
C8 H8 O2 S
C8 H8 O3
C8 H8 O3
C8 H8 O3
C8 H8 O3
C8 H8 O3
C8 H9 NO
C8 H9 NO
anti
C8 H9 NO
anti
C8 H9 NO
C8 H9 NO
C8 H9 NO
C8 H9 NO2
C8 H9 NO2
C8 H9 NO2
C8 H9 NO2
C8 H9 NO2
C8 H9 NO2
C8 H9 NO2
3-methylbenzoic acid
共303–323兲
4-methylbenzoic acid
共318 –337兲
2,5-dimethyl-1,4-benzoquinone
共273–293兲
4-hydroxyacetophenone
共320–349兲
phenyl vinyl sulfone
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
99.0⫾0.6
Method
Reference
共298兲
ME
95.9⫾0.1
137.7⫾0.5
共298兲
ME
DSC
97.0⫾0.3
共298兲
ME
98.8⫾0.3
共298兲
ME
77.0
共283兲
QF
95.7
共335兲
关01/10兴
关118-90-1兴
关86/4兴
关83/8兴
关99-04-7兴
关86/4兴
关99-94-5兴
关86/4兴
关137-18-8兴
关27/2兴关60/1兴
关87/4兴
关99-93-4兴
关87/4兴关60/14兴
关5535-48-8兴
关69/11兴关77/1兴
关579-75-9兴
关87/4兴
关78/7兴
关73/2兴关87/4兴
关54/1兴关60/1兴
关586-38-9兴
关87/4兴关78/7兴
关100-09-4兴
关87/4兴关78/7兴
关148-53-8兴
关87/4兴
关121-33-5兴
关53/7兴关60/1兴
关103-84-4兴
关87/4兴关55/3兴
关87/4兴关60/21兴
关41977-54-2兴
关83/9兴
关3235-02-7兴
关83/9兴
关103-81-1兴
关87/4兴关60/21兴
关99-92-3兴
关87/4兴关60/21兴
关613-93-4兴
关87/4兴关55/3兴
关87/4兴关60/21兴
关4389-45-1兴
关01/20兴
关01/20兴
关2941-78-8兴
关01/20兴
关01/20兴
关4389-50-8兴
关01/20兴
关01/20兴
关52130-17-3兴
关01/20兴
关01/20兴
关2458-12-0兴
关01/20兴
关01/20兴
关2486-70-6兴
关01/20兴
关01/20兴
关103-01-5兴
关80/29兴
关80/29兴
82⫾2.5
2-methoxybenzoic acid
共318 –353兲
101.2
共319–324兲
104.7⫾0.3
共353–368兲
90.8⫾0.4
共353–368兲
90.9
3-methoxybenzoic acid
共318 –326兲
107.5⫾0.4
4-methoxybenzoic acid
共334 –344兲
109.8⫾0.6
2-hydroxy-3-methoxybenzaldehyde
共282–303兲
54.1
4-hydroxy-3-methoxybenzaldehyde 共vanillin兲
共293–353兲
88.7
acetanilide
共303–324兲
80.6
共317–336兲
87.2
3-methylbenzaldoxime
U 31⫾1.7
4-methylbenzaldoxime
U 36⫾1.7
2-phenylacetamide
共329–352兲
96.4
4-aminoacetophenone
共314 –338兲
92.7
N-methylbenzamide
共297–321兲
75
共307–329兲
85.7
2-amino-3-methylbenzoic acid
共343–357兲
105.8⫾0.6
107.3⫾1.8
2-amino-5-methylbenzoic acid
共345–361兲
108.9⫾0.5
110.6⫾1.9
2-amino-6-methylbenzoic acid
共339–355兲
114.7⫾1.2
116.1⫾2.0
3-amino-2-methylbenzoic acid
共367–381兲
125.6⫾0.8
127.8⫾2.6
3-amino-4-methylbenzoic acid
共363–377兲
117.3⫾0.9
119.4⫾2.5
4-amino-3-methylbenzoic acid
共367–383兲
119.8⫾0.7
122.0⫾2.6
N-phenylglycine
114.1⫾1.0
128.0⫾2.0
B
共333兲
共322兲
共360兲
共360兲
ME
GS
GS
共322兲
ME
共339兲
ME
共292.5兲
共323兲
共313.5兲
共326.5兲
MS
MS
共340.5兲
共326兲
共309兲
共318兲
共350兲
共298兲
ME
ME
共353兲
共298兲
ME
ME
共347兲
共298兲
ME
ME
共374兲
共298兲
ME
ME
共370兲
共298兲
ME
ME
共375兲
共298兲
ME
ME
共365.4兲
共298兲
C
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
582
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C8 H9 NO2
D ␣-phenylglycine
C8 H9 NO2
anti
syn
C8 H9 NO2
anti
C8 H9 NO2
C8 H9 NO7
C8 H10
C8 H10
C8 H10NO5 PS
C8 H10N2 O
C8 H10N2 O2
C8 H10N2 O2
C8 H10N4 O2
form I
form I
form II
form II
form I
form I
form II
form II
C8 H10O
C8 H10O
C8 H10O
C8 H10O
C8 H10O
C8 H10O
C8 H10O
C8 H10O2
C8 H10O2
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
148.9⫾2.2
165.0⫾6.0
共443兲
共298兲
Method
C
C
2-methoxybenzaldoxime
U 20.1⫾1.7
U 32.6⫾1.7
MS
MS
U 67.3⫾1.7
MS
4-methoxybenzaldoxime
methyl 2-aminobenzoate
共287–298兲
78.4
methyl 5-nitro-2-acetoxy-2,5-dihydro-2-furancarboxylate
89.1⫾2.1
1,2-dimethylbenzene
60.1
1,4-dimethylbenzene
共247–286兲
59.4
60.8
methyl parathion 共O,O-dimethyl-O-4-nitro-phenylthiophosphate兲
共298 –308兲
125.1
共278 –288兲
108.7
4-N,N-dimethylaminonitrosobenzene
共323–334兲
82.0⫾1.7
N,N-dimethyl-3-nitroaniline
92.7⫾0.3
N,N-dimethyl-4-nitroaniline
102.7⫾1.1
共344 –366兲
98.7⫾1.7
共372–393兲
101.3⫾2.0
caffeine 共1,3,7-trimethylxanthine兲
共413– 463兲
104.8⫾0.2
115
共413– 463兲
113.6⫾0.2
119
105.1⫾0.7
共373– 473兲
103.6
共446 –509兲
100.0⫾0.6
110
共446 –509兲
110.7⫾0.7
114
4-ethylphenol
共278 –317兲
80.3⫾0.5
2,3-dimethylphenol
共283–323兲
共292.5兲
ME
共248兲
B
共271兲
共286兲
B
共303兲
共283兲
GS,A
GS
共298兲
ME
共298兲
C
共298兲
共355兲
共298兲
C
ME
ME
共438兲
共298兲
共369兲
共298兲
T
共423兲
共478兲
共298兲
共362兲
共298兲
T
ME
UV
MM
MM
GS
84.⫾1.0
GS
65.9⫾0.2
GS
85.0⫾0.25
GS
2,6-dimethylphenol
共277–313兲
75.6⫾0.17
GS
3,4-dimethylphenol
共282–323兲
85.7⫾0.1
GS
3,5-dimethylphenol
共282–323兲
82.8⫾0.3
GS
100.8
QF
2,4-dimethylphenol
共282–318兲
2,5-dimethylphenol
共282–323兲
2,5-dimethylhydroquinone
共332–361兲
1,4-dimethoxybenzene
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
Reference
关875-74-1兴
关80/29兴
关80/29兴
关29577-53-5兴
关83/9兴
关83/9兴
关5235-04-9兴
关83/9兴
关134-20-3兴
关87/4兴关54/4兴
关60/1兴
关22401-53-2兴
关80/28兴关86/5兴
关95-47-6兴
关86/12兴
关106-42-3兴
关87/4兴关74/32兴
关86/12兴
关298-00-0兴
关84/33兴
关83/5兴关79/10兴
关138-89-6兴
关94/29兴
关619-31-8兴
关85/5兴
关100-23-2兴
关85/5兴
关87/4兴关56/2兴
关94/29兴
关58-08-2兴
关99/40兴
关99/40兴
关99/40兴
关99/40兴
关85/22兴
关84/37兴
关79/17兴
关79/17兴关99/40兴
关79/17兴
关79/17兴关99/40兴
关123-07-9兴
关63/3兴关70/1兴
关87/4兴
关526-75-0兴
关60/3兴关70/1兴
关87/4兴
关105-67-9兴
关60/3兴关70/1兴
关95-87-4兴
关60/3兴关70/1兴
关87/4兴
关576-26-1兴
关60/3兴关70/1兴
关87/4兴
关95-65-8兴
关60/3兴关70/1兴
关87/4兴
关108-68-9兴
关60/3兴关70/3兴
关87/4兴
关615-90-7兴
关27/2兴关60/1兴
关150-78-7兴
ENTHALPY OF SUBLIMATION
583
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C8 H10O2 S
methyl-p-tolyl sulfone
C8 H10O2 S
methyl benzyl sulfone
C8 H11N
1-norbornylisocyanide
C8 H11N5
8-ethyl-9-methyladenine
C8 H11N5
共365–370兲
6,8,9-trimethyladenine
共334 –342兲
bicyclo关2.2.2兴octene
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
84.1⫾2.3
共298兲
Method
100⫾3.3
99.2⫾3
C8 H12
60.6⫾0.5
共298兲
127.1⫾0.7
115.2⫾1.0
共368兲
ME
98.6⫾0.2
共338兲
ME
43.8⫾0.4
C8 H12N2
tetramethylsuccinonitrile
C8 H12N2
tetramethylpyrazine
C8 H12N2 O2
C8 H12O2
1,3-dimethyl-5-ethyluracil
共312–321兲
共300–316兲
共319–340兲
4,4-dimethyl-1,3-cyclohexanedione
C8 H12O2
5,5-dimethyl-1,3-cyclohexanedione
C
81.2⫾1.7
C8 H12O2
C8 H14
C8 H14
C8 H14ClN5
C8 H14N2
C8 H14N2 O2
C8 H14N2 O2
C8 H14O
C8 H14O4
C8 H14O6
C8 H14O6
C8 H14O6
C8 H15N
94.6⫾4.0
共298兲
C
98.7⫾1.7
99.3⫾0.2
110⫾1.2
共316兲
共308兲
共330兲
ME
ME
QR
99.2⫾2.1
共298兲
ME
99.8⫾1.1
2,2,4,4-tetramethyl-1,3-cyclobutanedione
70.3⫾3.5
72.2⫾0.6
72.4⫾0.6
bicyclo关2.2.2兴octane
共323–363兲
46.3⫾0.8
共298兲
ME
47.7⫾0.8
48.0⫾2
共298兲
4.6
共164兲
solid phase transition
3,4-dimethyl-2,4-hexadiene
53.1
2-chloro-4-ethylamino-6-isopropylamino-1,3,5-triazine 共atrazine兲
共324 –354兲
114.6
共323– 403兲
113.8
1,4-dimethyl-2,3-diazabicyclo关2.2.2兴octane
72.0⫾0.5
␣-acetylproline N-methylamide
共308 –318兲
69.1
␤-acetylproline N-methylamide
共319–335兲
60.7
3-oxabicyclo关3.2.2兴nonane
53.1⫾0.5
1,8-octanedioic acid 共suberic acid兲
共310–320兲
148
147.8⫾3.8
共379– 407兲
143.1⫾3.8
共d兲-dimethoxysuccinic acid dimethyl ester
53.1
共dl兲-dimethoxysuccinic acid dimethyl ester
57.7
meso dimethoxysuccinic acid dimethyl ester
74.1
3-azabicyclo关3.2.2兴nonane
HSA
C
BG
HA
C
共339兲
共338兲
GS
GS–GC
共298兲
C
共313兲
共327兲
TPTD
共298兲
共393兲
M
Reference
关00/24兴
关3185-99-7兴
关U/3兴关70/1兴
关3112-90-1兴
关U/3兴关70/1兴
关103434-09-9兴
关87/17兴
关116988-56-8兴
关94/6兴
关87/7兴
关139909-51-6兴
关94/6兴
关931-64-6兴
关70/5兴关77/1兴
关71/10兴
关3333-52-6兴
关73/8兴关77/1兴
关1124-11-4兴
关96/28兴
关31703-08-9兴
关96/5兴
关83/14兴
关83/14兴
关562-46-9兴
关93/23兴
关126-81-8兴
关93/23兴
关933-52-8兴
关75/3兴
关71/5兴
关71/23兴
关280-33-1兴
关71/1兴关77/1兴
关87/4兴
关71/1兴关77/1兴
关70/5兴关71/1兴
关77/1兴
关84/25兴
关56/7兴关60/1兴
关1912-24-9兴
关82/23兴
关64/14兴关87/4兴
关49570-30-1兴
关76/12兴
关19701-85-0兴
关87/4兴关55/7兴
关87/4兴关55/7兴
关283-27-2兴
关71/10兴关77/1兴
关505-8-6兴
关01/15兴
关99/10兴关60/4兴
关60/4兴关70/1兴
关87/4兴
关37/6兴
关37/6兴
关37/6兴
关283-24-9兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
584
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
C8 H15NO
C8 H15N5 O
C8 H15N5 S
C8 H15N5 S
C8 H15N7 O2 S3
C8 H16
C8 H16N2 O2
C8 H16N2 O2
C8 H16N2 O2
C8 H17NO
C8 H17NO2
C8 H18
C8 H18
C8 H18N2 O2
C8 H18O
C8 H18O2
C8 H18O2 S
C8 H18O2 S
C9 H5 BrClNO
C9 H5 Br2 NO
C9 H5 ClINO
C9 H5 ClINO
C9 H5 Cl2 NO
Compound
Temperature range 共K兲
⌬ subH m /kJ mol⫺1
CAS registry number
(Tm /K)
Method
57.8⫾1.3
共298兲
C
trans 2-octenoic acid amide
共373–393兲
73.5
共383兲
2-methoxy-4,6-bis共ethylamino兲-1,3,5-triazine
共323– 403兲
98.2
共338兲
GS–GC
2-methylthio-4,6-bis共ethylamino兲-1,3,5-triazine
GS–GC
共323–355兲
101.3
共338兲
2-methylthio-4-methylamino-6-isopropyl-1,3,5-triazine
GS–GC
共323–357兲
101.5
共338兲
3-关关关2-关共aminoiminomethyl兲aminol兴-4-thiazolyl兴methyl兴thio兴-N-共aminosulfonyl兲propanimidamide
共famotidine兲
207.0
TGA
cyclooctane
58.7
共166兲
B
N-acetyl L-leucine amide
115.6⫾1.4
共376兲
C
119.8⫾1.5
共298兲
N-acetyl D-leucine amide
114.8⫾0.3
共393兲
C
120.4⫾0.4
共298兲
共374 – 401兲
101⫾3
共388兲
TE
N-acetyl L-isoleucine amide
142.7⫾0.2
共390兲
C
147.4⫾0.3
共298兲
octanamide
共325–374兲
110.5⫾2.9
GS,ME
8-aminooctanoic acid
共391– 402兲
166.2⫾0.9
共397兲
C
170⫾4
共298兲
C
n-octane
68.1
共216兲
B
2,2,3,3-tetramethylbutane
共286 –377兲
43.6
共301兲
共273–338兲
43.4⫾0.2
共298兲
42.9⫾0.9
共298兲
共263–279兲
56.2
A,MG
solid phase transition
2.0
共153兲
1,4-bis-共2-hydroxyethyl兲piperazine
共334 –356兲
104.1
1-octanol
105.4⫾2.5
共244兲
1,8-octanediol
139.3⫾0.9
共298兲
C
di-n-butyl sulfone
100.4⫾2.5
di-tert-butyl sulfone
94.1⫾2.9
7-bromo-5-chloro-8-hydroxyquinoline
共353–368兲
110.1⫾0.8
共361兲
ME
113.2⫾0.8
共298兲
5,7-dibromo-8-hydroxyquinoline
共365–380兲
113.6⫾1.3
共372兲
ME
117.3⫾1.3
共298兲
共363–393兲
94.1
5-chloro-7-iodo-8-hydroxyquinoline
共359–378兲
111.3⫾0.4
共368兲
ME
114.8⫾0.4
共298兲
5-iodo-7-chloro-8-hydroxyquinoline
共383– 414兲
131.0
5,7-dichloro-8-hydroxyquinoline
共351–366兲
106.3⫾0.7
共358兲
ME
109.3⫾0.7
共298兲
共363–393兲
92.9
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
Reference
关70/5兴
关87/4兴
关673-04-1兴
关87/4兴关64/14兴
关1014-70-6兴
关87/4兴关64/14兴
关1014-69-3兴
关87/4兴关64/14兴
关76824-35-6兴
关97/36兴
关292-64-8兴
关63/6兴
关28529-34-2兴
关99/12兴
关99/12兴
关16624-68-3兴
关99/12兴
关99/12兴
关88/6兴关86/16兴
关56711-06-9兴
关99/12兴
关99/12兴
关629-01-6兴
关59/3兴关87/4兴
关1002-57-9兴
关83/24兴
关83/24兴
关111-65-9兴
关63/6兴
关594-82-1兴
关87/4兴
关52/1兴关70/1兴
关47/8兴
关31/4兴
关84/25兴
关122-96-3兴
关84/30兴
关111-87-5兴
关65/6兴
关629-41-4兴
关90/14兴
关598-04-9兴
关U/3兴关70/1兴
关1886-75-7兴
关U/3兴关70/1兴
关7640-33-7兴
关92/20兴
关92/20兴
关521-74-4兴
关92/20兴
关92/20兴
关63/5兴
关130-26-7兴
关92/20兴
关92/20兴
关35048-13-6兴
关63/5兴
关773-76-2兴
关92/20兴
关92/20兴
关63/5兴
ENTHALPY OF SUBLIMATION
585
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C9 H5 I2 NO
5,7-diiodo-8-hydroxyquinoline
共389– 404兲
C9 H6 ClNO
C9 H6 INO
C9 H6 N2 O2
C9 H6 N2 O2
C9 H6 N2 O2
C9 H6 N2 O3
C9 H6 O2
共403– 423兲
5-chloro-8-hydroxyquinoline
共317–327兲
5-iodo-8-hydroxyquinoline
共363–393兲
5-nitroquinoline
共310–324兲
6-nitroquinoline
共336 –350兲
8-nitroquinoline
共338 –352兲
5-nitro-8-hydroxyquinoline
共352–362兲
C9 H6 O2
chromone
C9 H6 O6
1,3,5-benzenetricarboxylic acid
共553–593兲
5-phenyl-1,2-dithiole-3-thione
共363–373兲
C9 H7 NO
C9 H7 NO
C9 H7 NO
2-hydroxyquinoline
共375–390兲
4-hydroxyquinoline
共415– 433兲
8-hydroxyquinoline
共293–303兲
共308 –328兲
C9 H7 N3 O2
C9 H7 NO
C9 H7 NO2
C9 H8 N2
C9 H8 N2
C9 H8 N2
(Tm /K)
121.9⫾0.8
126.8⫾0.8
110.9
共396兲
共298兲
ME
97.5⫾0.9
98.7⫾0.9
共322兲
共298兲
ME
118.8
Method
ME
93.2⫾0.7
94.2⫾0.7
共317兲
共298兲
ME
101.5⫾1.0
103.8⫾1.0
共343兲
共298兲
ME
104.3⫾0.9
106.7⫾0.9
共345兲
共298兲
ME
114.1⫾2.2
111.2⫾3.0
共298兲
共298兲
ME
C
83.1
86.2
共298兲
共323兲
C
ME
81.3⫾0.2
共298兲
C
159.4
共573兲
GS
117.4⫾0.4
123.3⫾0.4
共368兲
共298兲
115.2⫾0.6
119.4⫾0.6
共383兲
共298兲
ME
128.8⫾1.1
135.1⫾1.1
共424兲
共298兲
ME
89.5⫾0.9
89.0⫾1.4
108.8⫾1.7
共298兲
共298兲
ME
C
ME
130.7⫾0.8
136.4⫾0.8
共412兲
共298兲
ME
99.8
92.5⫾4.2
共325.5兲
91.1⫾0.5
91.1⫾0.5
共307兲
共298兲
ME
101.1⫾0.9
103.1⫾0.9
104.8⫾4.8
共337兲
共298兲
共298兲
ME
102.9⫾0.7
105.0⫾0.7
103.3⫾3.4
共339兲
共298兲
共298兲
ME
103.6⫾1.0
105.7⫾1.0
共341兲
共298兲
ME
coumarin
共293–353兲
C9 H6 S3
CAS registry number
⌬ subH m /kJ mol⫺1
5-amino-6-nitroquinoline
共400– 424兲
⍀-cyanoacetophenone
共318 –333兲
N-methylphthalimide
共298 –316兲
3-aminoquinoline
共329–345兲
5-aminoquinoline
共329–349兲
6-aminoquinoline
共333–349兲
ME
C
C
Reference
关83-73-8兴
关92/20兴
关92/20兴
关63/5兴
关130-16-5兴
关92/20兴
关92/20兴
关13207-63-1兴
关63/5兴
关607-34-1兴
关97/2兴
关97/2兴
关613-50-3兴
关97/2兴
关97/2兴
关607-35-2兴
关97/2兴
关97/2兴
关4008-48-4兴
关89/2兴
关89/2兴
关91-64-5兴
关91/12兴
关53/7兴关60/1兴
关87/4兴
关491-38-3兴
关88/13兴
关554-95-0兴
关87/4兴关62/2兴
关3445-76-9兴
关72/16兴
关72/16兴
关59-31-4兴
关90/1兴
关90/1兴
关611-36-9兴
关90/1兴
关90/1兴
关148-24-3兴
关89/2兴
关89/2兴
关63/5兴关70/1兴
关87/4兴
关35975-00-9兴
关98/11兴
关98/11兴
关614-16-4兴
关87/4兴
关69/9兴关77/1兴
关550-44-7兴
关97/12兴
关97/12兴
关580-17-6兴
关93/10兴
关93/10兴
关93/10兴
关611-34-7兴
关93/10兴
关93/10兴
关93/10兴
关580-15-4兴
关93/10兴
关93/10兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
586
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C9 H8 N2
8-aminoquinoline
共329–314兲
C9 H8 N2 O
2-methyl-3-hydroxyquinoxaline
共375–391兲
C9 H8 N2 O2
2-methylquinoxaline-1,4-dioxide
C9 H8 N2 O2
C9 H8 O2 S
3-methylaminophthalimide
共402– 450兲
1-indanone
共288 –308兲
trans-cinnamic acid
共333–347兲
共333–347兲
phenyl propadienyl sulfone
C9 H8 O2 S
phenyl prop-1-ynyl sulfone
C9 H8 O2 S
phenyl prop-2-ynyl sulfone
C9 H8 O
C9 H8 O2
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
93.0
93.3⫾0.5
共305兲
共298兲
ME
117.2⫾0.4
119.7⫾2.8
123.0⫾4.4
共383兲
共298兲
共298兲
ME
ME
C
107.0⫾6.2
共298兲
C
104.9
共417兲
RG
83.5⫾0.7
共298兲
GS
105.0⫾0.8
107.1⫾0.8
共340兲
共298兲
ME
ME
Method
105.4⫾2.5
95.4⫾2.5
C9 H8 O3
C9 H8 O4
C9 H9 N
C9 H9 N
C9 H9 NO2
C9 H9 N3 O6
C9 H10Cl2 N2 O
C9 H10N2 O
C9 H10O
C9 H10O2
C9 H10O2
C9 H10O2
C9 H10O2
C9 H10O2
105.⫾2.5
endo-5-norbornene-2,3-dicarboxylic anhydride
97⫾4.2
monomethyl terephthalate
共433– 493兲
72.1
共433– 493兲
82.8
130.4
2,6-dimethylbenzonitrile
83.9⫾2.8
3-methylindole
共288 –333兲
83.3
4-acetomidobenzaldehyde
共328 –346兲
99
2,4,6-trinitromesitylene
共319–397兲
103.6⫾1.2
3-共3,4-dichlorophenyl兲-1,1-dimethylurea 共diuron兲
119⫾0.6
133.9⫾0.7
1-phenyl-3-pyrazolidinone
共327–348兲
84.3
trans 3-phenyl-2-propen-1-o1
共288 –307兲
109.6
69.5
2-ethylbenzoic acid
共298 –313兲
100.5
101.1⫾0.4
共298 –313兲
100.7⫾2.5
3-ethylbenzoic acid
共300–318兲
99.1
99.7⫾0.4
共300–318兲
99.1⫾2.5
4-ethylbenzoic acid
共310–329兲
98.2
98.9⫾0.2
共311–330兲
97.6⫾0.2
共320–329兲
97.5⫾2.5
4-acetylanisole
共276 –300兲
77.7
共283–333兲
93.7
2,3-dimethylbenzoic acid
共316 –337兲
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
102.3⫾0.4
B
B
共298兲
MG
共448兲
共473兲
GS
共298兲
C
共303兲
共337兲
ME
共393兲
共298兲
C
共337.5兲
共297.5兲
ME
共305.5兲
共298兲
共298兲
ME
ME
ME
共309兲
共298兲
共298兲
ME
ME
ME
共319.5兲
共298兲
共321兲
共298兲
ME
ME
ME
ME
V
共308兲
共326兲
ME
Reference
关578-66-5兴
关93/10兴
关93/10兴
关14003-34-0兴
关00/26兴
关00/26兴
关00/15兴
关6639-86-7兴
关97/25兴
关5972-09-8兴
关87/4兴关56/13兴
关83-33-0兴
关98/21兴
关140-10-3兴
关99/27兴
关99/27兴
关2525-42-0兴
关69/13兴关70/1兴
关2525-41-9兴
关69/13兴关70/1兴
关2525-40-8兴
关69/13兴关70/1兴
关129-64-6兴
关73/17兴关77/1兴
关1679-64-7兴
关87/4兴
关62/2兴
关98/28兴
关21789-36-6兴
关91/3兴
关83-34-1兴
关87/4兴
关122-85-0兴
关87/4兴关60/21兴
关602-96-0兴
关87/4兴关78/15兴
关330-54-1兴
关97/17兴
关97/17兴
关92-43-3兴
关87/4兴关60/21兴
关4407-36-7兴
关87/4兴
关54/4兴
关612-19-1兴
关87/4兴关76/6兴
关84/1兴
关76/6兴
关619-20-5兴
关87/4兴关76/6兴
关84/1兴
关76/6兴
关619-64-7兴
关87/4兴关76/6兴
关84/1兴
关84/1兴
关76/6兴
关100-06-1兴
关59/2兴
关54/4兴关60/1兴
关87/4兴
关603-79-2兴
关84/9兴
ENTHALPY OF SUBLIMATION
587
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C9 H10O2
2,4-dimethylbenzoic acid
共312–331兲
C9 H10O2
C9 H10O2
C9 H10O2
C9 H10O2
C9 H10O2
C9 H10O2 S
2,5-dimethylbenzoic acid
共315–334兲
2,6-dimethylbenzoic acid
共309–324兲
3,4-dimethylbenzoic acid
共325–347兲
3,5-dimethylbenzoic acid
共322–341兲
3-methylphenyl acetate
共274 –317兲
p-tolyl vinyl sulfone
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
104.6⫾0.4
Method
Reference
共298兲
ME
102.7⫾0.3
103.5⫾0.3
共321兲
共298兲
ME
ME
103.6⫾0.6
105.0⫾0.6
共324兲
共298兲
ME
ME
98.2⫾0.2
99.1⫾0.2
共317兲
共298兲
ME
ME
104.5⫾0.3
106.4⫾0.3
共336兲
共298兲
ME
ME
100.8⫾0.3
102.3⫾0.3
共332兲
共298兲
ME
ME
60.7
共295兲
TE
关84/9兴
关611-01-8兴
关84/9兴
关84/9兴
关610-72-0兴
关84/9兴
关84/9兴
关632-46-2兴
关84/9兴
关84/9兴
关619-04-5兴
关84/9兴
关84/9兴
关499-06-9兴
关84/9兴
关84/9兴
关122-46-3兴
关47/1兴关60/1兴
关5535-52-4兴
关69/11兴关77/1兴
关121-32-4兴
关87/4兴关57/3兴
关60/1兴
关1521-38-6兴
关85/1兴
关85/1兴
关91-52-1兴
关85/1兴
关85/1兴
关1466-76-8兴
关85/1兴
关85/1兴
关93-07-2兴
关85/1兴
关85/1兴
关2785-98-0兴
关96/15兴
关96/15兴
关1132-21-4兴
关85/1兴
关85/1兴
关613-75-2兴
关80/28兴关86/5兴
关150-68-5兴
关87/4兴关72/9兴
关120-66-1兴
关87/4兴关60/21兴
关103-89-9兴
关60/21兴
关611-74-5兴
关95/11兴
关603-71-4兴
关93/3兴关93/21兴
关63-91-2兴
关77/2兴
关65/1兴关70/1兴
关87/4兴关64/16兴
关60-18-4兴
关77/2兴
关15482-60-7兴
关89/11兴
82.4⫾2.5
C9 H10O3
C9 H10O4
C9 H10O4
C9 H10O4
C9 H10O4
C9 H10O4
C9 H10O4
3-ethoxy-4-hydroxybenzadehyde
共296 –338兲
2,3-dimethoxybenzoic acid
共336 –356兲
2,4-dimethoxybenzoic acid
共346 –367兲
2,6-dimethoxybenzoic acid
共335–378兲
3,4-dimethoxybenzoic acid
共359–378兲
2,5-dimethoxybenzoic acid
共324 –342兲
3,5-dimethoxybenzoic acid
共356 –376兲
C9 H10O5
2-共diacetoxymethyl兲furan
C9 H11ClN2 O
3-共4-chlorophenyl兲-1,1-dimethylurea
共303–379兲
N-共2-methylphenyl兲acetamide
共315–340兲
N-共4-methylphenyl兲acetamide
共331–350兲
N,N-dimethylbenzamide
共289–305兲
2,4,6-trimethylnitrobenzene
B
101.5
共311兲
115.1⫾0.3
116.6⫾0.3
共346兲
共298兲
ME
ME
120.5⫾0.4
123.4⫾0.4
共357兲
共298兲
ME
ME
118.4⫾0.4
121.7⫾0.4
共367兲
共298兲
ME
ME
126.1⫾0.6
129.8⫾0.6
共369兲
共298兲
ME
ME
113.3⫾0.7
116.1⫾0.7
共333兲
共298兲
ME
124.5⫾0.6
127.1⫾0.6
共369兲
共298兲
ME
ME
114.6⫾4.9
共341兲
ME,C
96.8
共327.5兲
99.0
共341兲
89.7⫾0.3
共298兲
78.6⫾1.0
共298兲
C
U 90⫾6.3
154⫾8
共392兲
共455兲
LE
ME
101⫾8
共462兲
LE
109.6⫾2.5
C9 H11NO
C9 H11NO
C9 H11NO
C9 H11NO2
C9 H11NO2
C9 H11NO3
C9 H11NS
C9 H13ClN6
L-共l兲-phenylalanine
共342– 442兲
L-tyrosine
共412–512兲
N,N-dimethylthiobenzamide
94.8⫾2.0
共298兲
2-关共4-chloro-6-ethylamino-s-triazin-2-yl兲amino兴-2-methylpropionitrile
共cyanazine兲
C
关21725-46-2兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
588
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
C9 H12F3 N3 O5
C9 H12N2
C9 H12N2 O2
C9 H12N2 O2
C9 H12O
C9 H12O
C9 H12O
C9 H12O2
C9 H12O2
C9 H12O2
C9 H13N5
C9 H13N5
C9 H14
C9 H14
C9 H14
C9 H14N2 O2
C9 H14N2 O2
C9 H14N2 O2
C9 H16
C9 H16ClN5
C9 H16NO2
Compound
Temperature range 共K兲
共339–365兲
90.7
N-关N-共N-关trifluoroacetyl兴glycyl兲glycyl兴glycine methyl ester
共343– 433兲
133.4
N-methyl-7-共methylimino兲-1,3,5-cycloheptatrienylamine
49.4⫾4
3-ethoxyphenylurea
75.3⫾8.3
4-ethoxyphenylurea
83.7⫾8.3
2,3,6-trimethylphenol
86.7⫾0.6
2,4,6-trimethylphenol
82.8⫾0.3
95.0
␣,␣-dimethylbenzyl alcohol
共276 –302兲
82.8⫾0.7
82.3⫾0.7
3-isopropyl-1,2-dihydroxybenzene
97.8⫾1.7
1,2,3-trimethoxybenzene
共375兲
98.0⫾0.3
1,3,5-trimethoxybenzene
共375兲
100.6⫾1.9
6,9-dimethyl-8-ethyladenine
共345–351兲
94.1⫾0.1
8-propyl-9-methyladenine
共364 –370兲
124.2⫾0.8
bicyclo关3.2.2兴non-6-ene
48⫾1.0
bicyclo关3.3.1兴non-2-ene
48.2⫾0.4
bicyclo关4.2.1兴non-3-ene
49.7⫾0.8
1,3-dimethyl-5-propyluracil
共317–327兲
111.0⫾1.6
1,3-dimethyl-5-isopropyluracil
共316 –328兲
102.9⫾1.6
1,3-diethylthymine
89.8⫾0.4
共307–325兲
95.0⫾2.1
bicyclo关3.3.1兴nonane
50.6⫾2
2-chloro-4,6-bis共isopropylamino兲-1,3,5-triazine
共323– 403兲
125.1
2,2,6,6-tetramethyl-4-oxopiperidine-1-oxyl
83.3⫾1.7
C9 H16N2
2-methyl-2-piperidinopropionitrile
C9 H16O4
nonanedioic acid
共367–377兲
C9 H17NO
C9 H17NO
C9 H17NO2
C9 H17N5 O
C9 H17N5 S
⌬ subH m /kJ mol⫺1
CAS registry number
(Tm /K)
共352兲
Method
Reference
GS
关82/23兴
关651-18-3兴
关87/4兴关60/20兴
关1502-10-9兴
关71/3兴关77/1兴
关13142-86-4兴
关54/12兴关70/1兴
关150-69-6兴
关54/12兴关70/1兴
关2416-94-6兴
关99/17兴
关527-60-6兴
关99/17兴
关71/24兴关99/17兴
关617-94-7兴
关99/18兴
关99/18兴
关2138-48-9兴
关84/10兴
关634-36-6兴
关00/24兴
关621-23-8兴
关00/24兴
关139909-52-7兴
关94/6兴
关117954-97-9兴
关87/7兴
关7124-86-9兴
关82/4兴
关6671-66-5兴
关82/4兴
关1456-33-0兴
关82/4兴
关82413-39-6兴
关96/5兴
关175412-48-3兴
关96/5兴
关21472-93-5兴
关80/7兴
关80/19兴
关260-65-9兴
关77/9兴
关139-40-2兴
关87/4兴关64/14兴
关2896-70-0兴
关65/7兴关70/1兴
关87/4兴
关2273-41-8兴
关97/28兴
关123-99-9兴
关99/10兴
关99/10兴
关2896-70-0兴
关66/4兴关70/1兴
关14952-05-7兴
关87/4兴
关3637-11-4兴
关87/4兴
关65/7兴关70/1兴
关1610-17-9兴
关87/4兴关64/14兴
关834-12-8兴
关87/4兴关64/14兴
共358兲
E
E
共298兲
GS
共298兲
共298兲
GS
C
共289兲
共298兲
GS
共298兲
C
共298兲
C
共298兲
C
共348兲
ME
共367兲
ME
共298兲
C
共298兲
C
共298兲
C
共322兲
ME
共322兲
ME
共298兲
共317兲
C
QR
共298兲
TSGC
共338兲
GS–GC
ME
80.3⫾0.5
共298兲
156.2⫾0.5
159.9⫾1.0
共372兲
共298兲
ME
2,2,6,6-tetramethyl-4-oxopiperidine
60.8⫾2.7
trans 2-nonenoic acid amide
共383–393兲
111.9
2,2,6,6-tetramethyl-1-hydroxy-4-oxopiperidine
共288 –328兲
80
80.1⫾4.6
2-methoxy-4-ethylamino-6-isopropylamino-1,3,5-triazine
共323– 403兲
94.4
2-methylthio-4-ethylamino-6-isopropylamino-1,3,5-triazine
共323– 403兲
100.9
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
ME
共388兲
共303兲
ME
共338兲
GS–GC
共338兲
GS–GC
ENTHALPY OF SUBLIMATION
589
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
⌬ subH m /kJ mol⫺1
CAS registry number
(Tm /K)
Polymorph
Temperature range 共K兲
C9 H18NO2
2,2,6,6-tetramethyl-4-hydroxypiperidine-1-oxyl
共293–318兲
101.5⫾5.2
共306兲
N,N-diethyl-N⬘ -isobutanoylthiourea
共363兲
120.8⫾2.5
共298兲
3,3-dimethyl-1-共methylthio兲-2-butanone O-共共methylamino兲carboxyl兲-oxime
共298 –328兲
93.5⫾6
共308兲
di-tert-butylcarbonate
65.4⫾0.2
共298兲
nonamide
共353–370兲
114.6⫾3.3
2,2,6,6-tetramethyl-1,4-dihydroxypiperidine
共318 –348兲
100.4⫾0.6
共328兲
n-nonane
74.6
共219兲
71.4
共298兲
1,3-dibutylthiourea
141.0⫾2
共298兲
137⫾3.0
共298兲
diethylammonium diethyldithiocarbamate
111.8⫾3.0
di-tert-butylmethanol
62.7⫾0.9
共298兲
1,9-nonanediol
148.7
octafluoronaphthalene
共293–323兲
79.4⫾2.5
共308兲
1,2,4,5-benzenetetracarboxylic dianhydride 共pyromellitic dianhydride兲
100.4
共559兲
88.4
1-共4-bromophenyl兲-1H-pyrrole-2,5-dione
共350–370兲
105.9⫾0.7
dimethyltetrachloroterephthalane 共chlorthal兲
共348 – 433兲
104.9⫾1.4
共390兲
2-cyanoquinoline
89.3⫾3.3
共298兲
共312–326兲
93.4⫾0.7
共319兲
94.4⫾0.7
共298兲
3-cyanoquinoline
91.3⫾1.8
共298兲
共312–326兲
93.4⫾0.7
共319兲
93.2⫾0.8
共298兲
1-共3-nitrophenyl兲-1H-pyrrole-2,5-dione
共350–370兲
115.7⫾0.9
1-共4-nitrophenyl兲-1H-pyrrole-2,5-dione
共350–370兲
117.3⫾1.2
1,4-naphthoquinone
91.0⫾0.8
共298兲
共301–325兲
90.7⫾2
共313兲
72.4⫾3.8
共1,4-naphthoquinone兲-共1,4-naphthohydroquinone兲
C9 H18N2 OS
C9 H18N2 O2 S
C9 H18O3
C9 H19NO
C9 H19NO2
C9 H20
C9 H20N2 S
C9 H20N2 S2
C9 H20O
C9 H20O2
C10F8
C10H2 O6
C10H6 BrNO2
C10H6 Cl4 O4
C10H6 N2
C10H6 N2
C10H6 N2 O4
C10H6 N2 O4
C10H6 O2
(C10H6 O2 ) –
(C10H8 O2 )
2(C10H6 O2 ) –
(C10H8 O2 )
C10H7 Br
Reference
ME
关2226-96-2兴
关66/4兴关70/1兴
C
ME
C
ME
ME
B
H
B,HA
C
ME
C
ME,GS
C
ME
C
ME
C
C
C
TE,ME
关01/9兴
关39196-18-4兴
关87/4兴关76/11兴
关34619-03-9兴
关85/17兴
关1120-07-6兴
关59/3兴
关3637-10-3兴
关66/4兴关70/1兴
关111-84-2兴
关63/6兴
关63/6兴关93/16兴
关109-46-6兴
关00/23兴
关94/17兴
关1518-58-7兴
关79/14兴
关14609-79-1兴
关98/22兴
关3937-56-2兴
关90/14兴
关313-72-4兴
关87/4兴关74/9兴
关89-32-7兴
关75/11兴
关67/15兴
关13380-67-1兴
关98/25兴
关1861-32-1兴
关81/20兴
关1436-43-7兴
关95/14兴
关95/14兴
关95/14兴
关34846-64-5兴
关95/14兴
关95/14兴
关95/14兴
关7300-93-8兴
关98/25兴
关4338-06-1兴
关98/25兴
关130-15-4兴
关89/21兴
关81/4兴
关56/5兴关70/1兴
关21414-85-7兴
共330–351兲
102.3⫾2
2共1,4-naphthoquinine兲-共1,4-naphthohydroquinone兲
共342.4兲
ME,TE
关81/4兴
关66653-77-8兴
共315–340兲
2-bromonaphthalene
88.7⫾3
共328.5兲
ME,TE
81.2⫾1.0
64⫾5
共298兲
共298兲
TE,ME
83.8
共343兲
ME
87.1⫾0.9
共298兲
ME
关81/4兴
关580-13-2兴
关93/13兴
关81/6兴
关2589-15-3兴
关87/4兴关74/36兴
关326-06-7兴
关92/28兴
关612-55-5兴
C10H7 F3 O2
共275–378兲
dihydroheptachlor
共333–353兲
benzoyltrifluoracetone
C10H7 I
2-iodonaphthalene
C10H7 Cl7
Method
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
590
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C10H7 NO2
1-nitronaphthalene
共309–326兲
共325–332兲
⌬ subH m /kJ mol⫺1
CAS registry number
(Tm /K)
Method
90.8
C10H7 NO2
1-nitroso-2-naphthol
C10H7 NO2
2-nitroso-1-naphthol
C10H7 NO2
4-nitroso-1-naphthol
C10H7 NO2
1-phenyl-1H-pyrrole-2,5-dione
共350–370兲
azulene
共283–326兲
C10H8
共290–372兲
共253–293兲
共293–323兲
C10H8
68.5⫾1.9
106.9⫾2.1
共318兲
共328.5兲
ME
ME
86.6⫾4.2
ME
56.5⫾4.2
ME
87.4⫾4.2
ME
98.1⫾1
C
78.4⫾1.3
72.7
82.8
82.9
75.8
75.3
76.8⫾0.2
95.4⫾0.4
67.6
共303兲
共298兲
共305兲
共298兲
共273兲
共298兲
70.4
71.7
73.7⫾1.0
78.2⫾1
70.9⫾0.4
72.3⫾0.4
75.8⫾1.1
72.6⫾0.4
72.6⫾0.1
72.8
72.8⫾0.3
72.4⫾0.7
72.5⫾0.1
72.6⫾0.6
71.3
74.77⫾0.4
73.9⫾0.2
74.35⫾1.7
72.3⫾0.4
72.5⫾0.3
67.8⫾3.5
72.5
72.7⫾1.7
64⫾.5
72.1⫾0.25
73.0⫾0.3
72.7
66.5
72.7⫾0.3
66.3
65.8
69.2
72.1
72.4
共298兲
共333兲
共258兲
64.0
65.7
66.5⫾1.7
76.6
共298兲
共297兲
共298兲
共298兲
HSA
CGC–DSC
C
ME
naphthalene
共313–353兲
共243–273兲
共337–352兲
共283–323兲
共302–352兲
共271–285兲
共274 –353兲
共253–273兲
共280–305兲
共253–273兲
共253–273兲
共303–329兲
共263–343兲
共263–298兲
共281–297兲
共281–290兲
共283–323兲
共230–260兲
共276 –283兲
共283–303兲
共253–283兲
共273–311兲
共279–294兲
共288 –306兲
共237–276兲
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
共323兲
共298兲
共303兲
共298兲
共327兲
共298兲
共293兲
共280兲
共298兲
共289兲
共298兲
共298兲
共293兲
共268兲
共292兲
CGC–DSC
GS
GS
GC
DSC
DSC
GS
DSC
TE,ME,DM
GS
ME
C
DM
TE
GS
TE
ME
TSGC
C
DM
HSA
GS
ME
LE
C
C
ME
KG
V
ME
ME
ME
QF
Reference
关56/10兴
关86-57-7兴
关87/4兴关74/9兴
关87/4兴关50/2兴
关70/1兴
关131-91-9兴
关68/6兴关77/1兴
关132-53-6兴
关68/6兴关77/1兴
关605-60-7兴
关68/6兴关77/1兴
关941-69-5兴
关98/25兴
关275-51-4兴
关98/5兴
关98/5兴
关87/4兴
关87/4兴关93/16兴
关58/1兴
关58/1兴关93/16兴
关72/1兴
关62/1兴关70/1兴
关47/7兴
关91-20-3兴
关98/5兴
关95/7兴
关94/1兴
关88/29兴
关88/4兴
关88/4兴
关83/11兴
关83/8兴
关83/1兴关81/1兴
关82/23兴
关82/1兴
关82/3兴
关81/1兴
关80/1兴
关79/27兴
关77/4兴
关77/4兴
关75/1兴
关76/1兴
关75/4兴
关75/3兴
关74/19兴
关74/9兴
关73/15兴
关72/1兴
关72/2兴
关71/31兴
关68/1兴
关63/1兴关70/1兴
关59/2兴
关58/18兴
关58/1兴
关57/9兴
关53/1兴关60/1兴
关54/10兴
关51/12兴
关40/1兴
关38/1兴
关26/2兴
ENTHALPY OF SUBLIMATION
591
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
C10D8
C10H8 Br2 N2
C10H8 NO2
C10H8 N2
Compound
Temperature range 共K兲
共283–303兲
naphthalene-d8
共282–323兲
2,3-bis共bromomethyl兲quinoxaline
共351–365兲
indole-3-acetic acid
共313– 423兲
2,2⬘ -bipyridine
C10H8 N2
2,4⬘ -bipyridine
C10H8 N2
4,4⬘ -bipyridine
C10H8 N2 O2
8-nitroquinaldine
共346 –360兲
C10H8 N2 O3
C10H8 O
C10H8 O
C10H8 O
C10H8 O
3-acetamidophthalimide
共428 – 468兲
1-naphthol
共296 –313兲
共279–328兲
1-naphthol 共␣ form兲
共298 –312兲
1-naphthol 共␤ form兲
共314 –324兲
2-naphthol
共305–323兲
共277–324兲
共283–323兲
C10H8 O
2-naphthol 共␣ form兲
共298 –312兲
2-naphthol 共␤ form兲
共314 –332兲
1,6-oxido关10兴annulene
C10H8 O2
1,4-naphthohydroquinone
C10H8 O2
1,2-dihydroxynaphthalene
C10H8 O2
1,3-dihydroxynaphthalene
C10H8 O2
2,3-dihydroxynaphthalene
C10H9 N
共341–359兲
1-naphthylamine
C10H8 O
C10H8 O
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
82.0
Method
Reference
共293兲
ME
70.6⫾0.5
共303兲
GS
111.7⫾0.5
114.0⫾2.0
共358兲
共298兲
ME
ME
64.0⫾1.5
共368兲
ME
81.8⫾2.3
75.0⫾5.0
81.9⫾0.3
共298兲
共298兲
C
B
87.9⫾1.7
共298兲
C
106.3⫾2.8
共298兲
C
108.3⫾0.8
111.0⫾0.8
共353兲
共298兲
ME
108.5
共443兲
RG
91.2⫾0.4
89.1⫾1.7
91.5⫾3.8
共304兲
共298兲
ME
ME
B
关25/3兴
关1146-65-2兴
关83/11兴
关3138-86-1兴
关00/26兴
关00/26兴
关87-51-4兴
关88/4兴
关366-18-7兴
关95/26兴
关96/24兴
关85/6兴
关581-47-5兴
关95/26兴
关553-26-4兴
关95/26兴
关881-07-2兴
关97/2兴
关97/2兴
关6118-65-6兴
关87/4兴关56/13兴
关90-15-3兴
关74/3兴
关74/5兴
关26/1兴关70/1兴
关27/1兴
93.3
共305兲
关87/4兴关60/14兴
84.3
共319兲
94.2⫾0.5
87.4⫾2.5
78.7⫾0.8
共300兲
共298兲
83.0⫾3.8
共298兲
关87/4兴关60/14兴
关135-19-3兴
关74/3兴
关74/5兴
关68/1兴关77/1兴
关87/4兴
关26/1兴关27/1兴
关70/1兴
97.8
共305兲
关87/4兴关60/14兴
87.8
共323兲
关87/4兴关60/14兴
关4759-11-9兴
关69/7兴关77/1兴
关571-60-8兴
关81/4兴
关574-00-5兴
关88/9兴
关132-86-5兴
关88/9兴
关92-44-4兴
关88/9兴
关79/5兴
关134-32-7兴
关47/1兴关70/1兴
关91-59-8兴
关87/4兴
关68/1兴关77/1兴
关47/2兴关70/1兴
关5343-98-6兴
关69/9兴关77/1兴
关87/4兴
关826-81-3兴
关90/1兴
ME
ME
B
80.4⫾8.4
B
119⫾1
共381兲
ME,TE
109.3⫾0.9
共298兲
C
116.0⫾1.1
共298兲
C
109.6⫾1.0
109.4⫾0.5
共298兲
共350兲
C
ME
90.0⫾4.2
C10H9 N
2-naphthylamine
共283–323兲
C10H9 NO
␤-cyanopropiophenone
C10H9 NO
共318 –333兲
2-methyl-8-hydroxyquinoline
共424 – 442兲
73.9
74.1⫾1.7
88.3⫾4.2
TE
共298兲
101.7⫾4.2
108.5
共325.5兲
ME
132.2⫾1.0
共433兲
ME
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
592
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
Compound
Temperature range 共K兲
共296 –307兲
C10H9 NO
C10H9 NO2
共308 –333兲
4-methyl-2-hydroxyquinoline
共391– 405兲
C10H10
indole-3-acetic acid
共313– 423兲
bullvalene
C10H10
1,4-dihydronaphthalene
C10H10N2
2,3-dimethylquinoxaline
共294 –308兲
C10H10N2
4-aminoquinaldine
共352–373兲
C10H10N2
1-benzylimidazole
C10H10N2 O2
C10H10O2
3-dimethylaminophthalimide
共392– 431兲
1-phenyl-1,3-butanedione
C10H10O2 S
共278 –300兲
p-tolyl propadienyl sulfone
C10H10O2 S
p-tolyl prop-1-ynyl sulfone
C10H10O2 S
p-tolyl prop-2-ynyl sulfone
C10H10O3
cis-2-methoxycinnamic acid
共339–352兲
共339–352兲
trans-2-methoxycinnamic acid
共368 –382兲
共368 –382兲
trans-3-methoxycinnamic acid
共353–367兲
共353–367兲
trans-4-methoxycinnamic acid
共369–383兲
共369–383兲
dimethyl isophthalate
共295–309兲
C10H10O3
C10H10O3
C10H10O3
C10H10O4
C10H10O4
dimethyl terephthalate
共311–330兲
共373– 413兲
共373– 413兲
C10H11N
2,4,6-trimethylbenzonitrile
C10H11NO
2,4,6-trimethylbenzonitrile N-oxide
共300–338兲
C10H11NO
3-amino-1-phenyl-but-2-enone
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
139.0⫾1.0
90.4⫾0.7
87.2⫾1.9
87.9
共298兲
123.1⫾1.6
128.1⫾1.6
共398兲
共298兲
ME
64.0⫾1.4 U
共368兲
ME
71.8
共298兲
C
63.6⫾1.6
共298兲
87.7⫾0.4
87.8⫾0.4
85.8⫾1.8
共301兲
共298兲
共298兲
ME
ME
C
112.1⫾0.8
115.3⫾0.8
共363兲
共298兲
ME
102.1⫾0.4
共298兲
ME
90.9
共407兲
RG
91.0⫾0.6
83.7
共298兲
共289兲
ME
V
Method
ME
C
ME
113⫾2.5
B
103.3⫾2.5
B
107.5⫾2.5
B
119.3⫾0.6
121.7⫾0.6
共346兲
共298兲
ME
ME
124.9⫾0.6
128.8⫾0.6
共375兲
共298兲
ME
ME
120.9⫾0.9
124.0⫾0.9
共360兲
共298兲
ME
ME
130.2⫾1.0
134.0⫾1.0
共376兲
共298兲
ME
ME
100.7⫾0.2
100.9⫾0.2
100.7
共302兲
共298兲
共298兲
ME
103.8⫾0.3
104.6⫾0.3
94.4
88.3
105.3
共321兲
共298兲
共388兲
共393兲
ME
82.9⫾1.6
共298兲
C
87.5⫾0.5
87.9⫾1.9
84.7⫾1.8
77.5⫾3.7
共314兲
共298兲
共319兲
共298兲
C
GS
ME
C
Reference
关90/1兴
关89/2兴
关89/2兴
关87/4兴关63/5兴
关607-66-9兴
关90/1兴
关90/1兴
关87-51-4兴
关88/14兴
关1005-51-2兴
关81/2兴
关612-17-9兴
关99/19兴
关2379-55-7兴
关00/26兴
关00/26兴
关96/28兴
关6628-04-2兴
关98/11兴
关98/11兴
关4238-71-5兴
关99/20兴
关87/4兴关56/13兴
关93-91-4兴
关92/28兴
关87/4兴关59/2兴
关16192-08-8兴
关69/13兴关70/1兴
关14027-53-3兴
关69/13兴关70/1兴
关16192-07-7兴
关69/13兴关70/1兴
关14737-91-8兴
关99/27兴
关99/27兴
关6099-03-2兴
关99/27兴
关99/27兴
关6099-04-3兴
关99/27兴
关99/27兴
关830-09-1兴
关99/27兴
关99/27兴
关120-61-6兴
关98/1兴
关98/1兴
关98/28兴
关120-61-6兴
关98/1兴
关98/1兴
关87/4兴
关62/2兴
关98/28兴
关2571-52-0兴
关91/3兴
关2904-59-8兴
关93/12兴
关93/12兴
关92/14兴
关91/3兴
关1128-85-4兴
ENTHALPY OF SUBLIMATION
593
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
Compound
Temperature range 共K兲
共298兲
共298兲
C
C
90.⫾0.8
共298兲
C
112.6⫾2.0
共298兲
C
100.4⫾2.2
3-dimethylamino-6-aminophthalimide
共434 – 459兲
108.8
cyclodeca-1,2,6,7-tetraene
73.0⫾0.4
acetylglycine anilide
共362–365兲
122.1
4-phenylburytric acid
共309–323兲
112.4⫾0.8
113.0⫾1.0
4-methoxy-␣-methylstyrene
81.2⫾0.4
2-phenyl-2-methyl-1,3-dioxolane
共293–324兲
81.9⫾0.5
2,3,6-trimethylbenzoic acid
104.4⫾0.2
共314 –336兲
103.6⫾0.2
2,4,6-trimethylbenzoic acid
103.6⫾0.3
共316 –340兲
102.5⫾0.3
2,3,4-trimethylbenzoic acid
109.3⫾0.3
共329–351兲
108.2⫾0.3
2,3,5-trimethylbenzoic acid
106.7⫾0.3
共320–338兲
105.7⫾0.3
2,4,5-trimethylbenzoic acid
109.6⫾0.5
共324 –346兲
108.3⫾0.5
3,4,5-trimethylbenzoic acid
111.0⫾0.5
共340–359兲
109.3⫾0.5
2-isopropylbenzoic acid
共300–320兲
100.2⫾0.4
101.0⫾0.4
3-isopropylbenzoic acid
共300–316兲
103.3⫾0.3
104.1⫾0.3
4-isopropylbenzoic acid
共316 –334兲
99.0⫾0.3
101.1⫾0.3
p-tolyl trans-prop-1-enyl sulfone
83.7⫾2.1
p-tolyl prop-2-enyl sulfone
95.8⫾2.9
p-tolyl isopropenyl sulfone
88.7⫾2.5
3,4,5-trimethoxybenzoic acid
共354 –372兲
127.9⫾0.8
131.2⫾0.8
N,N-dimethyl-3-toluamide
共373– 405兲
29.9
p-phenacetin 共4-ethoxyphenylacetamide兲
共312–387兲
115.5⫾2.4
1,2,4,5-tetramethylbenzene
71.7⫾0.3
共298兲
C
共446兲
RG
共298兲
C
关93/24兴
关91/3兴
关1563-87-7兴
关65/8兴关70/1兴
关2571-54-2兴
关91/3兴
关2904-59-8兴
关01/4兴
关10495-38-2兴
关87/4兴关56/13兴
关2451-55-6兴
关91/20兴
C10H11NO3
2,4,6-trimethoxybenzonitrile
C10H11NO4
2,4,6-trimethoxybenzonitrile N-oxide
C10H12N2 O2
C10H12O
C10H12O
C10H12O2
C10H12O2
C10H12O2
C10H12O2
C10H12O2
C10H12O2
C10H12O2
C10H12O2
C10H12O2
C10H12O2
C10H12O2 S
C10H12O2 S
C10H12O2 S
C10H12O5
C10H13NO
C10H13NO2
C10H14
109.4⫾2.1
91.9⫾1.9
Reference
N-phenyldiacetamide
C10H12
(Tm /K)
Method
C10H11NO2
C10H11N3 O2
CAS registry number
⌬ subH m /kJ mol⫺1
共363.5兲
共316兲
共298兲
ME
ME
共298兲
共308兲
T
共298兲
共325兲
ME
ME
共298兲
共328兲
ME
ME
共298兲
共340兲
ME
ME
共298兲
共329兲
ME
ME
共298兲
共335兲
ME
ME
共298兲
共350兲
ME
ME
共310兲
共298兲
ME
共308兲
共298兲
ME
共324兲
共298兲
ME
B
B
B
共363兲
共298兲
ME
ME
共388兲
I
C,ME
共298兲
C
关87/4兴关55/7兴
关1821-12-1兴
关01/10兴
关01/10兴
关1712-69-2兴
关99/19兴
关3674-77-9兴
关95/13兴
关2529-36-4兴
关87/15兴
关87/15兴
关480-63-7兴
关87/15兴
关87/15兴
关1076-47-7兴
关87/15兴
关87/15兴
关2437-66-3兴
关87/15兴
关87/15兴
关528-90-5兴
关87/15兴
关87/15兴
关1076-88-6兴
关87/15兴
关87/15兴
关2438-04-2兴
关87/11兴
关87/11兴
关5651-47-8兴
关87/11兴
关87/11兴
关536-66-3兴
关87/11兴
关87/11兴
关32228-15-2兴
关69/13兴关70/1兴
关3112-87-6兴
关69/13兴关70/1兴
关67605-02-1兴
关69/11兴关77/1兴
关118-41-2兴
关01/16兴
关01/16兴
关6935-65-5兴
关87/4兴关69/25兴
关62-44-2兴
关72/9兴关87/4兴
关95-93-2兴
关94/13兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
594
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
Compound
Temperature range 共K兲
共263–277兲
共318 –348兲
C10H14
C10H14
C10H14NO5 PS
C10H14N2 O
C10H14N2 O4
C10H14O
C10H14O
C10H14O
C10H14O
C10H14O2
C10H14O2
C10H14O2
C10H14O2
C10H15NO
C10H15NO
C10H15NO2
C10H15NO2
C10H15N5
C10H15N5
C10H16
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
74.6⫾0.3
71.3
72.4
52.6⫾0.2 共vap兲
55.6
Method
Reference
共298兲
共333兲
共298兲
ME
A
H
共298兲
共298兲
C
共298兲
共298兲
C
关89/18兴
关47/4兴
关47/4兴关93/16兴
关488-23-3兴
关94/13兴
关94/13兴关90/23兴
关527-53-7兴
关94/13兴
关94/13兴关90/23兴
关56-38-2兴
关79/10兴关83/5兴
关120-22-9兴
关98/23兴
关88381-75-3兴
关90/10兴
关585-34-2兴
关99/21兴
关99/13兴
关87/4兴
关98-54-4兴
关99/21兴
关99/13兴
关99/13兴
关87/4兴关60/14兴
关89-83-8兴
关87/4兴关60/14兴
关75/3兴
关71/17兴
关70/1兴关60/1兴
关47/1兴
关57/9兴关87/4兴
关700-58-3兴
关78/8兴
关78/8兴
关98-29-3兴
关00/21兴
关00/21兴
关84/20兴
关1948-33-0兴
关99/28兴
关99/28兴
关4026-05-5兴
关00/21兴
关00/21兴
关490-06-2兴
关84/20兴
关55658-55-4兴
关81/8兴
关80124-30-7兴
关81/8兴
关7575-82-8兴
关90/10兴
关54654-31-7兴
关90/10兴
关153495-35-3兴
关94/6兴
关117954-98-0兴
关87/7兴
关281-23-2兴
关00/10兴
关00/4兴
关98/5兴
关87/4兴
1,2,3,4-tetramethylbenzene
1,2,3,5-tetramethylbenzene
52.0⫾0.2 共vap兲
55.2
ethyl parathion 共O,O-diethyl-O-4-nitrophenylthiophosphate兲
共298 –318兲
100.6
4-diethylaminonitrosobenzene
107.9⫾3.7
2,2-dinitroadamantane
共278 –317兲
96.4⫾1.4
3-tert-butylphenol
88.9⫾0.5
共278 –319兲
86.0⫾0.5
共266 –299兲
70.7
4-tert-butylphenol
89.4⫾2.5
共293–334兲
85.0⫾0.5
85.9⫾0.5
共280–304兲
84.3
thymol
共273–295兲
75.1
共293–323兲
89.1⫾4.5
共229–312兲
U 69.0
共273–313兲
91.2⫾4.1
共283–323兲
adamantan-2-one
共320–370兲
4-tert-butyl-1,2-dihydroxybenzene
共303–323兲
2-tert-butyl-1,4-dihydroxybenzene
共333–368兲
3-tert-butyl-1,2-dihydroxybenzene
共334 –384兲
共298兲
C
共298兲
T
共298兲
共298兲
共281兲
C
GS
共298兲
共313兲
共298兲
共292兲
C
GS
共284兲
共303兲
共270兲
HSA
TGA
TE
91.5
共298兲
79.7⫾2.1
80.3⫾2.5
共345兲
共298兲
BG
BG
98.7⫾0.9
99.2⫾0.9
99.3⫾1.4
共313兲
共298兲
共298兲
GS
GS
C
101.2⫾1.3
104.4⫾1.3
共351兲
共298兲
GS
共359兲
共298兲
GS
GS
共298兲
C
共334兲
HSA
共334兲
HSA
共339兲
T
共350兲
T
共347兲
ME
共366兲
ME
70.1⫾0.8 共liq兲
73.5⫾0.8 共liq兲
6-methyl-3-isopropyl-1,2-dihydroxybenzene
96.6⫾0.9
共dl兲-carvoxime
共324 –343兲
101.6⫾5
共d兲-carvoxime
共324 –343兲
90.8⫾4.5
1-nitroadamantane
共321–357兲
63.6⫾1.0
2-nitroadamantane
共331–368兲
58.0⫾2.3
6,9-dimethyl-8-propyladenine
共345–349兲
129.0⫾0.1
8-butyl-9-methyladenine
共363–368兲
135.1⫾1.2
adamantane (tricyclo关 3.3.1.12,6兴 decane)
59.1
58.3
52.6
共278 –368兲
59.7
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
共308兲
共298兲
共308兲
共298兲
共293兲
CGC–DSC
ENTHALPY OF SUBLIMATION
595
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
Compound
Temperature range 共K兲
⌬ subH m /kJ mol⫺1
CAS registry number
(Tm /K)
共328 –373兲
共343– 483兲
C10H16
C10H16
C10H16
C10H16
C10H16NOS
C10H16N2
C10H16N2
C10H16N2 O2
C10H16O
C10H16O
C10H16O
C10H16O
C10H16O
C10H16S
C10H16S4
C10H17NOS
C10H17NOS
C10H17NOS
C10H18
55.3
共343兲
54.3
共358兲
58.45
共298兲
共278 – 443兲
59.5
共300兲
共310–336兲
59.7⫾0.8
共326兲
58.6
共298兲
共310–336兲
59.3⫾0.2
共326兲
60.5⫾1.3
共298兲
共312–366兲
53.6
共332兲
54.8
共298兲
59.3⫾0.16
共298兲
59.5
共298兲
共313–353兲
58.6⫾0.6
共333兲
59.6
共298兲
62.3
共298兲
2,2-dimethyl-3-methylenebicyclo关2.2.1兴heptane 共camphene兲
46.8
tricyclo关 4.3.1.03,8兴 decane
共310–335兲
64.9⫾1.8
共323兲
65.6
共298兲
tricyclo关 5.2.1.02,6兴 decane
共359– 443兲
52.9⫾1.3
共298兲
tricyclo关 5.2.1.04,10兴 decane hexahydrotriquinacene
56.6⫾1.3
共307兲
S-2,3,3-trichloroallyl N,N-diisopropylthiocarbonate 共triallate兲
共293–318兲
84
methyl共1,1,1-trimethylpropyl兲propanedinitrile
62.0⫾0.7
共298兲
共1,1-dimethylpropyl兲ethylpropanedinitrile
76.2⫾0.8
共298兲
1,3-dimethyl-5-butyluracil
共306 –311兲
106.3⫾1.3
共309兲
共dl兲-camphor
51.8⫾0.8
共273–293兲
51.5⫾2.6
共283兲
共273–298兲
U 65.8
50.7
共273– 453兲
53.6
共363兲
共285–318兲
54.7
共301兲
共d兲-3-bornanone
共273– 408兲
54.2
共288兲
共323–339兲
55
共331兲
共408 – 451兲
49.8
共423兲
cis-8-methyl-2-hydrindanone
60.9⫾0.2
共298兲
adamantan-1-ol
共320–370兲
86.6⫾2.5
共298兲
adamantan-2-ol
共320–370兲
87.9⫾2.1
共345兲
88.7⫾2.5
共298兲
1,7,7-trimethylbicyclo关2.2.1兴heptan-2-thione
共262–282兲
62.2⫾0.9
共272兲
61.7⫾0.9
共298兲
1,3,5,7-tetramethyl-2,4,6,8-tetrathiaadamantane
117.1⫾4.1
共298兲
carbamothioic acid, N-butyl-N-共2-propynyl兲, S-ethyl ester
共298 –313兲
82.1
共305.5兲
carbamothioic acid, N,N-dipropyl S-共2-propynyl兲 ester
共298 –313兲
92.4
共305.5兲
carbamothioic acid, N-2-methylpropyl-N-共2-propynyl兲, S-ethyl ester
共298 –313兲
74
共305.5兲
bicyclo关3.3.2兴decane
58.2⫾2
共298兲
Method
C
TSGC
BG
I
C
DBM
C
TSGC
BG
TSGC
ME
HSA
C
BG
BG
BG
ME
TE
ME
ME
ME
Reference
关87/4兴
关87/4兴关68/18兴
关82/4兴
关75/30兴
关75/2兴
关75/2兴关93/16兴
关71/1兴
关71/1兴关93/16兴
关71/7兴
关71/7兴关93/16兴
关70/2兴
关70/16兴
关67/1兴
关67/1兴关93/16兴
关67/1兴
关79-92-5兴
关77/12兴
关53130-19-1兴
关75/2兴
关75/2兴关93/16兴
关6004-38-2兴
关71/1兴关77/1兴
关17760-91-7兴
关79/13兴
关2303-17-5兴
关83/5兴关78/18兴
关85688-96-6兴
关90/28兴
关85688-95-5兴
关90/28兴
关82413-40-9兴
关96/5兴
关21368-68-3兴
关77/6兴
关75/3兴
关60/1兴关40/1兴
关60/1兴关37/2兴
关60/1兴关10/1兴
关57/9兴
关13854-85-8兴
关87/4兴
关87/4兴
关87/4兴
关13351-29-6兴
关70/6兴关77/1兴
关768-95-6兴
关78/8兴
关700-57-2兴
关78/8兴
关78/8兴
关53402-10-1兴
关99/26兴
关99/26兴
关7000-79-5兴
关78/3兴
关59300-35-5兴
关87/4兴关76/11兴
关59300-36-6兴
关87/4兴关76/11兴
关59300-34-4兴
关87/4兴关76/11兴
关283-50-1兴
关77/9兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
596
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C10H18
cis-decahydronaphthalene
C10H18
C10H18O
C10H18O
C10H18O
C10H18O
C10H18O4
C10H19N5 S
C10H20N2 OS
C10H20N2 OS
C10H20O
C10H20O
C10H20O
C10H20O
C10H20O2
C10H20O3
C10H21NO
C10H22
C10H22O
C10H22O2
C10H24N4
C11H6 N4
C11H7 N2
C11H8 N4
C11H8 O2
(Tm /K)
64.8
62.5
共230兲
共298兲
B
66.2
64.3
共241兲
共298兲
B
80.3
共305兲
ME
80.1
共297兲
69.3
共365兲
41.1
共388兲
165.3⫾2.9
160.7⫾2.5
共389兲
ME
共338兲
GS–GC
共338兲
GS–GC
关493-01-6兴
关63/6兴
关63/6兴关93/16兴
关493-02-7兴
关63/6兴
关63/6兴关93/16兴
关10482-56-1兴
关54/4兴关60/1兴
关98-55-5兴
关87/4兴
关6627-72-1兴
关87/4兴
关124-76-5兴
关87/4兴关36/4兴
关111-20-6兴
关99/10兴关60/4兴
关60/4兴关70/1兴
关87/4兴
关1610-18-0兴
关87/4兴关64/14兴
关7287-19-6兴
关87/4兴关64/14兴
共298兲
C
关01/9兴
共298兲
C
关01/9兴
关106-22-9兴
关54/4兴关60/1兴
关1502-05-2兴
关55/5兴
关89-78-1兴
关81/8兴
关2216-51-5兴
关81/8兴
关334-48-5兴
关68/2兴关70/1兴
关87/4兴
关61/1兴
关14156-10-6兴
关80/23兴
关2319-29-1兴
关59/3兴
关124-18-5兴
关80/23兴
关63/6兴
关63/6兴关93/16兴
关112-30-1兴
关65/5兴关87/4兴
关65/5兴
关112-47-0兴
关90/14兴
关295-37-4兴
关83/4兴
关6343-21-1兴
关72/13兴关77/1兴
关6023-46-7兴
关94/44兴
关13358-02-6兴
关71/14兴关77/1兴
关86-55-5兴
关83/8兴
关74/2兴关77/1兴
关87/4兴
Method
trans-decahydronaphthalene
␣-terpineol
共283–328兲
共dl兲-␣-terpineol
共287–308兲
共dl兲-borneol
共350– 475兲
共dl兲-isoborneol
共373– 457兲
sebacic acid
共375– 403兲
C10H19N5 O
CAS registry number
⌬ subH m /kJ mol⫺1
2-methoxy-4,6-bis共isopropylamino兲-1,3,5-triazine
共323–365兲
92.2
2-methylthio-4,6-bis共isopropylamino兲-1,3,5-triazine
共323–393兲
100
N,N-diethyl-N⬘ -isovaleroylthiourea
共363兲
121.5⫾3.2
N,N-diethyl-N⬘ -pivaloylthiourea
共366兲
114.9⫾2.7
citronellol
共283–333兲
66.1
cyclodecanol
共287–292兲
100.5⫾0.5
共dl兲-menthol
共279–299兲
78.6⫾4
共l兲-menthol
共279–299兲
95.8⫾4.8
decanoic acid
共293–303兲
118.8⫾2.2
共308兲
共288兲
TM
共289兲
HSA
共289兲
HSA
共298兲
ME
117.1⫾1.7
共295兲
ME
117.1⫾0.8
共298兲
ME
125.9⫾1.3
共361.5兲
ME
80.3
84.8
82.4
共298兲
共243兲
共298兲
B
B
115.5⫾6.3
112.5⫾6.3
共268兲
共298兲
ME
155.8⫾0.9
1,4,8,11-tetraazacyclotetradecane
共352–372兲
133.9⫾2.5
bicyclo关2.2.1兴hept-5-ene-2,2,3,3-tetracarbonitrile
117.2⫾5.4
2,2-dicyano-3-phenylpropionitrile
共318 –388兲
96.2⫾0.4
3-methyl-1,1,2,2-tetracyanocyclohex-4-ene
82⫾2.1
1-naphthoic acid
117.6⫾0.4
共340–360兲
110.4⫾0.2
共298兲
C
共362兲
TE
共408兲
MG
共353兲
T
共350兲
MG
共355兲
DSC
ME
共290–301兲
peroxydecanoic acid
共293–303兲
decanamide
共353–370兲
decane
decanol
共264 –273兲
1,10-decanediol
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
Reference
ENTHALPY OF SUBLIMATION
597
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C11H8 O2
2-naphthoic acid
共347–363兲
C11H9 N
C11H9 NO2
C11H9 NO3
C11H10
C11H10N2 O3
C11H10N2 O3
C11H10O2
C11H11N
C11H11N
C11H11N3 O
C11H12N2 O3
C11H12O2
C11H12O4
C11H12O4
C11H12O4
C11H12O4
C11H12O4
C11H12N2 O2
C11H13NO
C11H13NO
C11H14
C11H14N2 O2
C11H14N2 O2
C11H14N2 O3
C11H14O
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
113.6
Method
Reference
共298兲
C
119.5⫾0.6
113.6⫾0.8
共365兲
DSC
ME
117.2
共298兲
C
共298兲
BE
关74/28兴
关93-09-4兴
关83/8兴
关74/2兴关77/1兴
关87/4兴
关74/28兴
关939-23-1兴
关00/7兴
关1631-28-3兴
关98/25兴
关1081-17-0兴
关98/25兴
关91-57-6兴
关74/10兴
关68/1兴关77/1兴
关13297-17-1兴
关97/25兴
关40016-70-4兴
关97/25兴
关2985-72-7兴
关99/4兴
关877-43-0兴
关95/27兴
关93-37-8兴
关95/27兴
关5809-38-1兴
关01/4兴
关20771-72-6兴
关93/24兴
关39522-76-4兴
关98/26兴
关7345-82-6兴
关99/27兴
关99/27兴
关16909-09-4兴
关99/27兴
关99/27兴
关10538-51-9兴
关99/27兴
关99/27兴
关2316-26-9兴
关99/27兴
关99/27兴
关16909-11-8兴
关99/27兴
关99/27兴
关73-22-3兴
关77/2兴
关14091-93-1兴
关93/24兴
关7294-89-5兴
关93/24兴
关4421-32-3兴
关95/10兴
关95/10兴
关718-36-5兴
关89/15兴
关128478-71-7兴
关90/10兴
关3585-88-4兴
关89/15兴
关2270-20-4兴
关01/10兴
4-phenylpyridine
81.4⫾1.6
1-共4-methylphenyl兲-1H-pyrrole-2,5-dione
共350–370兲
104.6⫾0.8
1-共4-methoxyphenyl兲-1H-pyrrole-2,5-dione
共350–370兲
121.1⫾0.8
2-methylnaphthalene
65.7⫾0.85
61.7⫾1.7
2-methyl-3-acetylquinoxaline-1,4-dioxide
117.0⫾2.4
2-methyl-3-carboxymethoxyquinoxaline-1,4-dioxide
118.3⫾2.6
pentacyclo关 5.4.0 2,60 3,100 5,9兴 undecane-8,11-dione
92.6⫾1.0
2,6-dimethylquinoline
84.5⫾1.5
2,7-dimethylquinoline
87.5⫾1.5
3,5-dimethyl-1-phenyl-4-nitrosopyrazole
100.4⫾2.2
4-关共4-nitrophenyl兲amino兴pent-3-ene-2-one
121.9⫾3.9
1-phenyl-4,7-dioxaspiro关2.4兴heptane
91.8⫾0.8
trans-2,3-dimethoxycinnamic acid
共380–392兲
136.6⫾0.9
共380–392兲
141.0⫾0.9
trans-2,4-dimethoxycinnamic acid
共391– 404兲
144.2⫾1.3
共391– 404兲
149.2⫾1.3
trans-2,5-dimethoxycinnamic acid
共376 –391兲
134.5⫾1.1
共376 –391兲
138.8⫾1.1
trans-3,4-dimethoxycinnamic acid
共390– 404兲
144.9⫾0.8
共390– 404兲
149.9⫾0.8
trans-3,5-dimethoxycinnamic acid
共385–397兲
136.7⫾0.5
共385–397兲
141.4⫾0.5
L-tryptophane
共340– 440兲
87.9⫾8 U
共E兲-3-共methylamino兲-1-phenyl-but-2-en-1-one
99.2⫾4.2
4-phenylaminopent-3-ene-2-one
89.9⫾3.8
pentacyclo关 5.4.0 2,60 3,100 5,9兴 undecane
54.7⫾0.9
共273–323兲
54.9⫾1.1
4-nitrobenzylidene tert-butylamine
91.1⫾3.1
2-cyano-2-nitroadamantane
共307–368兲
70.0⫾1.9
4-nitrobenzylidene tert-butylamine N-oxide
116.5⫾3.1
5-phenylvaleric acid
共315–327兲
118.5⫾0.8
C
C
C
共298兲
ME
共298兲
C
共298兲
ME
共298兲
C
共298兲
C
共298兲
C
共298兲
C
共298兲
共386兲
共298兲
ME
ME
共398兲
共298兲
ME
ME
共384兲
共298兲
ME
ME
共397兲
共298兲
ME
ME
共391兲
共298兲
ME
ME
共390兲
LE
共298兲
C
共298兲
C
共337兲
共298兲
C
ME
共298兲
C
共338兲
T
共298兲
C
共321兲
ME
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
598
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C11H14O2
2-tert-butylbenzoic acid
共306 –322兲
3-tert-butylbenzoic acid
共318 –335兲
4-tert-butylbenzoic acid
共325–343兲
2,3,4,5-tetramethylbenzoic acid
共337–360兲
C11H14O2
C11H14O2
C11H14O2
C11H14O2
C11H14O2
C11H14O2
2,3,4,6-tetramethylbenzoic acid
共330–351兲
2,3,5,6-tetramethylbenzoic acid
共330–351兲
3,5-diethylbenzoic acid
共325–343兲
C11H14O2 S
p-tolyl but-1-enyl sulfone
C11H14O2 S
p-tolyl but-2-enyl sulfone
C11H14O2 S
p-tolyl but-3-enyl sulfone
C11H14O2 S
p-tolyl-isobutenyl sulfone
C11H14O2 S
p-tolyl 2-methylprop-2-enyl sulfone
C11H15N
1-adamantyl-1-carbonitrile
共294 –312兲
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
119.4⫾1.1
Method
Reference
共298兲
ME
99.8⫾0.4
共315兲
ME
103⫾0.5
共327兲
ME
103.8⫾0.4
共334兲
ME
113.4⫾0.6
115.9⫾0.6
共348兲
共298兲
ME
106.9⫾0.5
109.7⫾0.5
共341兲
共298兲
ME
104.6⫾0.8
106.1⫾0.8
共341兲
共298兲
ME
104.1⫾4.2
共334兲
关01/10兴
关1077-58-3兴
关79/4兴
关7498-54-6兴
关79/4兴
关98-73-7兴
关79/4兴
关2529-39-7兴
关88/10兴
关88/10兴
关2408-38-0兴
关88/10兴
关88/10兴
关2604-45-7兴
关88/10兴
关88/10兴
关3854-90-8兴
关74/15兴关77/1兴
关87/4兴
关111895-49-9兴
关69/11兴关70/1兴
关24931-66-6兴
关69/13兴关70/1兴
关17482-19-8兴
关69/13兴关70/1兴
关16192-03-3兴
关69/11兴关77/1兴
关16192-04-4兴
关69/13兴关70/1兴
关23074-42-2兴
关92/26兴
关92/26兴
关3376-24-7兴
关89/15兴
关18775-06-9兴
关89/11兴
关700-12-9兴
关94/13兴
关89/18兴
关82413-41-0兴
关83/14兴
关80/19兴关83/14兴
关80/19兴关83/14兴
关2409-55-4兴
关99/13兴
关99/13兴
关87/4兴关60/14兴
关88-60-8兴
关99/13兴
关99/13兴
关80-46-6兴
关99/13兴
关99/13兴
关31108-34-6兴
关87/4兴
关5511-18-2兴
关89/6兴
关89/6兴
关153495-36-4兴
关94/6兴
关768-91-2兴
关77/11兴
关75/2兴
106.3⫾2.5
B
107.5⫾2.5
B
113.4⫾2.9
B
102.1⫾2.5
B
106.7⫾2.9
C11H15NO
benzylidene tert-butylamine N-oxide
C11H15NS
N,N-diethylthiobenzamide
C11H16
pentamethylbenzene
C11H16N2 O2
C11H16O
C11H16O
C11H16O
C11H16O
C11H17NO
C11H17N5
C11H18
共296 –313兲
1,3-dimethyl-5,6-pentamethyleneuracil
共335–358兲
共323–338兲
共340–370兲
2-tert-butyl-4-methylphenol
共288 –318兲
共274 –294兲
2-tert-butyl-5-methylphenol
共277–294兲
4-tert-amylphenol
共293–333兲
1-共2,4,6-trimethylphenyl兲ethanol
共282–313兲
1-adamantyl carboxamide
共336 –354兲
6,9-dimethyl-8-butyladenine
共348 –354兲
1-methyladamantane
共300–342兲
共306 –336兲
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
67.1⫾0.8
67.2⫾0.8
共303兲
共298兲
ME
86.8⫾0.9
共298兲
C
91.4⫾3.2
共298兲
C
71.6⫾0.1
77.4⫾0.4
共298兲
共298兲
C
ME
111.9⫾0.2
108.8⫾5
113.4⫾1.3
共346兲
共330兲
共355兲
ME
QR
MS
82.6⫾0.5
82.9⫾0.5
77.4
共303兲
共298兲
共284兲
GS
80.4⫾1.3
79.7⫾1.3
共287兲
共298兲
GS
87.4⫾0.5
88.3⫾0.5
共313兲
共298兲
GS
U 5.7
共297兲
105.9⫾0.5
108.0⫾0.5
共345兲
共298兲
ME
106.0⫾0.1
共351兲
ME
67.8⫾1.3
67.6⫾0.5
共298兲
共321兲
BG
ENTHALPY OF SUBLIMATION
599
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C11H18
2-methyladamantane
共310–330兲
共300–340兲
bicyclo关3.3.3兴undecane
C11H20
C11H20O4
C11H22O2
C11H22O3
C11H23NO
C11H24
C12Cl8 O
C12Cl8 O2
C12F10
C12F18
C12Cl10
C12H2 Cl8
C12H4 Cl4 O
C12H4 Cl4 O
C12H4 Cl4 O2
C12H4 Cl6
C12H4 N4
C12H5 Cl3 O2
C12H5 Cl3 O2
C12H5 Cl5
C12H6 Cl2 O
C12H6 Cl2 O2
C12H6 Cl2 O2
C12H6 Cl2 O2
C12H6 Cl4
C12H6 Cl4
undecanedioic acid
共371–381兲
undecanoic acid
共303–308兲
peroxyundecanoic acid
共293–303兲
N-methyl decanamide
共303–325兲
undecane
(Tm /K)
67.5⫾2.1
68.2⫾1.3
共320兲
共298兲
63.6⫾0.8
共298兲
C
158.6⫾1.9
162.5⫾1.9
共376兲
共298兲
ME
121.3⫾1.3
共298兲
ME
125.9⫾3.4
共298兲
ME
102.8⫾0.8
共314兲
GS
共236兲
B
共423兲
T
共483兲
T
共310兲
ME
共299.5兲
I
共343兲
GS
共318兲
GS
共363兲
T
共323兲
T
91.5
octachlorodibenzofuran
共373– 474兲
149.4
octachlorodibenzo关b,e兴关1,4兴dioxin
共393–573兲
149.8
decafluorobiphenyl
共298 –323兲
85.3⫾2.3
hexakis(trifluoromethyl)tetracyclo关 2.2.0.02,6.02,5兴 hexane
共293–306兲
49.2
decachlorobiphenyl
共324 –363兲
121.8
2,2⬘ ,3,3 ⬘ ,5,5 ⬘ ,6,6 ⬘ -octachlorobiphenyl
共302–334兲
101.7
1,2,3,4-tetrachlorodibenzofuran
共333–393兲
118.5
2,3,7,8-tetrachlorodibenzofuran
共303–344兲
124.0
2,3,7,8-tetrachlorodibenzo关b,e兴关1,4兴dioxin
124.0
2,2⬘ ,4,4 ⬘ ,6,6 ⬘ -hexachlorobiphenyl
共263–303兲
103.4⫾2.3
7,7,8,8-tetracyanoquinodimethane
79.0
共452–553兲
108⫾2
共382– 464兲
122⫾2
126.1⫾1
共433– 499兲
104.8⫾9.2
1,3,7-trichlorodibenzo关b,e兴关1,4兴dioxin
共310–373兲
1,2,4-trichlorodibenzo关b,e兴关1,4兴dioxin
共310–374兲
2,2⬘ ,4,5,5⬘ -pentachlorobiphenyl
共303–313兲
3,6-dichlorodibenzofuran
共305–374兲
2,3-dichlorodibenzo关b,e兴关1,4兴dioxin
共306 –374兲
2,7-dichlorodibenze关b,e兴关1,4兴dioxin
共314 –374兲
2,8-dichlorodibenzo关b,e兴关1,4兴dioxin
共305–363兲
2,2⬘ ,5,5 ⬘ -tetrachlorobiphenyl
共303–312兲
2,3,4,5-tetrachlorobiphenyl
CAS registry number
⌬ subH m /kJ mol⫺1
Method
共578兲
共283兲
GS
共500兲
共423兲
共413兲
共465兲
TGA
T
ME
ME,TE
MG
116.2
共342兲
T
118.8
共342兲
T
92.7
共308兲
GS
110.9
共340兲
T
108.6⫾1.0
107.2⫾0.8
108.6⫾1.0
106.2
共298兲
共358兲
共298兲
共340兲
C
C
105.5
共344兲
T
109.0
共334兲
T
94.6
共308兲
GS
T
Reference
关700-56-1兴
关75/2兴
关77/11兴
关180-43-8兴
关75/7兴关77/1兴
关1852-04-6兴
关99/10兴
关99/10兴
关112-37-8兴
关68/2兴关70/1兴
关676-08-4兴
关80/23兴
关59/4兴关87/4兴
关1120-21-4兴
关63/6兴
关39001-02-2兴
关89/20兴关86/7兴
关3268-87-9兴
关89/20兴关86/7兴
关434-90-2兴
关74/9兴关87/4兴
关22736-20-5兴
关87/4兴关70/24兴
关2051-24-3兴
关84/26兴
关2136-99-4兴
关84/26兴
关24478-72-6兴
关89/20兴关86/7兴
关51207-31-9兴
关89/20兴关86/7兴
关1746-01-6兴
关85/19兴
关33976-03-2兴
关94/1兴
关1518-16-7兴
关95/35兴
关84/23兴
关84/23兴
关80/22兴
关63/4兴关70/1兴
关80/23兴关87/4兴
关67028-17-5兴
关89/20兴关86/7兴
关39227-58-2兴
关89/20兴关86/7兴
关37680-73-2兴
关81/19兴
关74919-40-4兴
关89/20兴关86/7兴
关29446-15-9兴
关99/38兴
关98/10兴
关98/10兴
关89/20兴关86/7兴
关33857-26-0兴
关89/20兴关86/7兴
关38964-22-6兴
关89/20兴关86/7兴
关35693-99-3兴
关81/19兴
关33284-53-6兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
600
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C12H7 ClO2
共253–393兲
1-chlorodibenzo关b,e兴关1,4兴dioxin
C12H7 ClO2
C12H8
C12H8 Cl2
C12H8 Cl6
C12H8 Cl6 O
C12H8 F2
C12H8 F2
C12H8 N2
C12H8 N2
C12H8 N2
C12H8 N2 O
C12H8 N2 O4
88.7⫾1.2
Reference
共273兲
GS
95.2⫾1.1
95.2
98.6
共298兲
C
共321兲
T
97.2
97.2⫾0.6
97.2
共298兲
共298兲
共327兲
C
C
T
70.0
77.2
73.2⫾0.5
73.0⫾0.4
71.1⫾1.3
共298兲
共383兲
共303兲
共298兲
CGC–DSC
GS
GS
C
共383兲
共319兲
共298兲
GS
共371–381兲
82.7
U 104.5
87.3⫾0.3
83.8⫾.3
U 128.9⫾2
2,2⬘ -dichlorobiphenyl
共310–328兲
共310–328兲
96.1
96.2⫾4.2
共314兲
共298兲
ME
ME
共283兲
共331兲
共298兲
GS
ME
ME
关94/1兴
关39227-53-7兴
关99/38兴
关98/27兴
关89/20兴关86/7兴
关39227-54-8兴
关99/38兴
关96/13兴
关89/20兴关86/7兴
关208-96-8兴
关98/5兴
关95/7兴
关83/11兴
关72/1兴
关70/1兴关87/4兴
关65/3兴
关259-79-0兴
关95/7兴
关89/9兴
关80/27兴
关72/1兴
关55/1兴关70/1兴
关87/4兴
关13029-08-8兴
关64/8兴
关64/8兴关70/1兴
关87/4兴
关2050-68-2兴
关94/1兴
关64/8兴关87/4兴
关64/8兴关70/1兴
共326兲
GS
关309-00-2兴
关82/23兴
共328兲
共303兲
GS
GS
共310兲
共298兲
ME
共306兲
共298兲
ME
ME
共303–338兲
2-chlorodibenzo关b,e兴关1,4兴dioxin
共305–348兲
acenaphthylene
共286 –318兲
C12H8 Cl2
(Tm /K)
Method
共313– 453兲
共238 –323兲
C12H8
CAS registry number
⌬ subH m /kJ mol⫺1
biphenylene
共313– 453兲
共309–336兲
4,4⬘ -dichlorobiphenyl
共263–303兲
95.3⫾1.3
共303–360兲
103.7
共303–360兲
103.8⫾4.2
1,2,3,4,10,10-hexachloro-1,4,4a,5,8,8a-hexahydro-endo-exo1,4:5,8-dimethylnaphthalene 共aldrin兲
共309–343兲
91.8
1,2,3,4,10,10-hexachloro-6,7-epoxy-1,4,4a,5,6,7,8,8a-octahydro1,4-endo-exo-5,8-dimethanonaphthalene 共dieldrin兲
共308 –348兲
93.8
共293–313兲
98.7
2,2⬘ -difluorobiphenyl
共301–319兲
95.1
共301–318兲
95⫾4.2
4,4⬘ -difluorobiphenyl
共294 –318兲
91.4
共294 –318兲
91.2⫾4.2
1,10-phenanthroline
98.3
phenazine
92.7⫾0.4
97.0⫾0.4
91.8⫾2.1
共280–318兲
92.4
99.9⫾2.5
共303–328兲
90.4⫾2.5
共303–323兲
90.0⫾1.5
共281–293兲
90.4⫾1.7
U 81.5
benzo关c兴cinnoline
共320–360兲
101.7⫾.2
113
phenazine-N-oxide
100.⫾1.3
4,4⬘ -dinitrobiphenyl
共441– 428兲
104.6⫾1.8
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
B
C
共376兲
ME
共354兲
共298兲
共298兲
共295兲
共298兲
共298兲
C
ME,GS
TE
TCM
LE
共340兲
ME
ME
共298兲
C
共420兲
ME
关60-57-1兴
关82/23兴
关69/4兴
关388-82-9兴
关87/4兴关64/8兴
关64/8兴关70/1兴
关2050-68-2兴
关64/8兴
关64/8兴关70/1兴
关66-71-7兴
关72/10兴
关92-82-0兴
关91/4兴
关91/4兴
关90/9兴
关87/4兴
关80/6兴
关75/5兴
关U/1兴关75/5兴
关75/1兴
关46/1兴
关230-17-1兴
关77/14兴关87/4兴
关72/10兴
关304-81-4兴
关90/9兴
关1528-74-1兴
关53/10兴关60/1兴
ENTHALPY OF SUBLIMATION
601
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
⌬ subH m /kJ mol⫺1
Polymorph
Temperature range 共K兲
C12H8 N4
bicyclo关2.2.2兴oct-5-ene-2,2,3,3-tetracarbonitrile
111.7⫾5.4
dibenzo-1,3a,4,6a-tetraazapentalene
共363– 433兲
70.3⫾1.7
dibenzo-1,3a,6,6a-tetraazapentalene
共363– 443兲
42.3⫾3.4
dibenzofuran
84.4⫾0.7
76.5⫾0.2
共304 –343兲
85.6
共303–343兲
79.1
88.7⫾2.1
dibenzo关b,e兴关1,4兴dioxin
89.6⫾0.7
89.6⫾0.7
共303–333兲
92.3
dibenzothiophene
85.1⫾0.4
共303–348兲
91.2
共336 –366兲
90.7
thianthrene
103.6⫾0.4
共338 –368兲
98.6⫾0.5
99.4⫾0.6
共358 – 426兲
98.0
共338 –368兲
97.5⫾6.3
4-chlorobiphenyl
共253–303兲
86.0⫾0.9
共306 –346兲
73.7⫾0.7
carbazole
共346 –364兲
101.2⫾1.1
103.3⫾1.1
97.7⫾0.3
84.5⫾.8
phenothiazine
共336 –395兲
86
4-nitroazobenzene
110.0
4-hydroxy-4⬘-nitroazobenzene
140.1
共417– 444兲
143.8⫾1.3
144⫾2.5
136.8
N-共2,4-dinitrophenyl兲-N-phenylamine
共402– 420兲
147.6⫾1.7
149⫾3.0
131.8
N-共2,4-dinitrophenyl兲-N-共4-hydroxyphenyl兲amine
共440– 470兲
155.6⫾4.2
154.0
N-共4-aminophenyl兲-N-共2,4-dinitrophenyl兲amine
共437– 460兲
156.5⫾2.1
154⫾2.9
139.3
acenaphthene
84.6
共313– 453兲
83.2
共283–323兲
86.8⫾0.9
83.4⫾1.0
82.4
共327–356兲
84.7⫾2.7
共290–340兲
86.2⫾0.8
共291–310兲
82.1⫾0.4
C12H8 N4
C12H8 N4
C12H8 O
C12H8 O2
C12H8 S
C12H8 S2
C12H9 Cl
C12H9 N
C12H9 NS
C12H9 N3 O2
C12H9 N3 O3
C12H9 N3 O4
C12H9 N3 O5
C12H9 N4 O4
C12H10
CAS registry number
(Tm /K)
Method
Reference
共433兲
关1017-93-2兴
关72/13兴关77/1兴
共400兲
关67/6兴
共403兲
关67/6兴
关132-64-9兴
关90/6兴
关87/10兴
关89/20兴关86/7兴
关86/8兴
关58/2兴
关262-12-4兴
关99/38兴
关97/37兴
关89/20兴关86/7兴
关132-65-0兴
关87/10兴关79/2兴
关86/8兴
关81/14兴
关92-85-3兴
关93/1兴
关89/4兴
关89/4兴
关81/14兴
关79/7兴
关2051-62-9兴
关94/1兴
关83/25兴
关86-74-8兴
关90/8兴
关90/8兴
关87/10兴
关55/2兴关70/1兴
关92-84-2兴
关87/4兴关42/1兴
关2491-52-3兴
关87/19兴关91/18兴
关1435-60-5兴
关87/19兴关91/18兴
关87/4兴关70/4兴
关70/4兴
关68/10兴关88/24兴
关961-68-2兴
关87/4兴关70/4兴
关70/4兴
关68/10兴关88/24兴
关119-15-3兴
关70/4兴关87/4兴
关68/10兴关88/24兴
关961-68-2兴
关87/4兴关70/4兴
关70/4兴
关68/10兴关88/24兴
关83-32-9兴
关98/5兴
关95/7兴
关83/11兴
关75/8兴关77/7兴
关75/8兴
关74/9兴
关65/3兴关70/1兴
关59/2兴关87/4兴
共298兲
共298兲
共324兲
共323兲
T
GS
共298兲
共318兲
共318兲
C
C
T
共298兲
共325兲
C
GS
共350兲
共353兲
共298兲
共393兲
共353兲
IPM
共278兲
共326兲
GS
TE,ME
共355兲
共298兲
共298兲
ME
ME
C
GS
HSA
共351兲
GS
共430.5兲
GS
TE
TE,ME
共411兲
TE
TE,ME
共455兲
TE,ME
共448.5兲
TE
TE,ME
共298兲
共383兲
共303兲
共298兲
共366兲
共341兲
CGC–DSC
GS
GS
共300兲
B,IPM
ME
ME
V
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
602
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C12H10
共258 –308兲
biphenyl
共297兲
共301兲
共302兲
共292兲
ME
QF
92.9
92.9⫾1.2
U 74.9
共288兲
共328兲
共318兲
ME
ME
94.1⫾0.8
93.6⫾1.9
92.1⫾0.9
96.9⫾0.8
94.9⫾0.8
93.8⫾1.2
U74.9
共298兲
共298兲
共319兲
共308兲
共308兲
共323兲
共318兲
B
ME
TE,ME
TE
ME
ME
98.6⫾0.9
共298兲
C
100.9⫾2.1
101.9⫾1.7
108.4
共340.5兲
TE
TE,ME
130.6⫾1.3
126.2⫾1.6
120.9
4,5-dimethy1-1,1,2,2-tetracyanocyclohex-4-ene
107.9⫾4.2
4-amino-4 ⬘ -nitroazobenzene
共403– 465兲
123
140.1
127.6
136.4
140.2⫾1.2
134.3
共404 – 424兲
137.7⫾0.8
共392.5兲
TE
TE,ME
共287–307兲
共288 –314兲
共278 –307兲
cis-azobenzene
共273–323兲
共298 –357兲
共303–333兲
trans-azobenzene
共298 –302兲
共298 –341兲
共299–317兲
共299–317兲
共298 –347兲
共303–333兲
C12H10N2 O
trans-diphenyldiazene-N-oxide
C12H10N2 O2
N-共2-nitrophenyl兲-N-phenylamine
共335–346兲
C12H10N4
C12H10N4 O2
C12H10O
C12H10O
81.6
75.1⫾1.7
81.6⫾1.7
72.8⫾3
68.6⫾0.8
共279–299兲
C12H10N2 O2
N-共4-nitrophenyl兲-N-phenylamine
共382– 403兲
共404 – 423兲
2-acetylnaphthalene
共295–316兲
diphenyl ether
共310兲
共298兲
共289兲
2-phenylphenol
共301–328兲
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
CGC–DSC
GS
EM
C
C
TSGC
HSA
ME
ME
C
共378兲
共434兲
共414兲
GS
GS
UV
ME
TE,ME
ME
TE
136.4⫾5.0
共413兲
ME
87.9⫾0.4
共305兲
V
82⫾2.1
C12H10O
Method
共298兲
共383兲
共311兲
共318兲
共298兲
共298兲
共298兲
共319兲
共306 –332兲
共273–313兲
共298 –323兲
共298 –318兲
C12H10N2
CAS registry number
(Tm /K)
82.9
81.8
83.4
U 113.3
81.5⫾0.2
77.9⫾0.3
81.8⫾0.2
80.4⫾1.6
76.0⫾4.0
83.6⫾2.5
75.2
81.8⫾0.4
75.8⫾0.6
81.6⫾2
共313– 453兲
共283–338兲
共303–333兲
C12H10N2
⌬ subH m /kJ mol⫺1
87.6⫾0.9
88.5⫾0.9
E
共314兲
共298兲
T
Reference
关58/1兴
关92-52-4兴
关98/5兴
关95/7兴
关89/1兴
关89/9兴
关89/5兴
关79/3兴
关78/34兴
关75/2兴
关75/3兴
关74/9兴
关74/6兴
关72/1兴
关55/3兴
关53/1兴关70/1兴
关60/1兴
关53/10兴
关53/13兴
关51/1兴
关38/1兴
关1080-16-6兴
关87/4兴
关77/14兴
关50/3兴关60/1兴
关17082-12-1兴
关96/11兴
关92/4兴
关84/18兴
关77/4兴
关77/4兴
关77/14兴
关50/3兴关60/1兴
关87/4兴
关21650-65-7兴
关86/10兴
关119-75-5兴
关87/4兴关70/4兴
关70/4兴
关68/10兴关88/24兴
关836-30-6兴
关87/4兴关70/4兴
关70/4兴
关68/10兴关88/24兴
关69155-29-9兴
关72/13兴关77/1兴
关730-40-5兴
关89/29兴
关87/19兴关91/18兴
关84/39兴关84/40兴
关80/25兴关91/18兴
关70/4兴
关68/10兴关88/24兴
关67/7兴关87/4兴
关70/4兴
关67/7兴关66/18兴
关93-08-3兴
关59/2兴关87/4兴
关101-84-8兴
关58/2兴关70/1兴
关90-43-7兴
关98/9兴
关98/9兴
ENTHALPY OF SUBLIMATION
603
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C12H10O
共292–314兲
4-phenylphenol
共333–368兲
C12H10O2
C12H10O2
C12H10O2 S
C12H10O4
C12H10S2
C12H10S2 O4
C12H11N
C12H11NO
C12H11N3
C12H12
C12H12
C12H12
C12H12
共327–348兲
2,2⬘ -dihydroxybiphenyl
共334 –363兲
4,4⬘ -dihydroxybiphenyl
共354 –388兲
共279–304兲
2,7-dimethylnaphthalene
共333–369兲
C12H12N2 O
4,4⬘ -diaminodiphenyl oxide
C12H14O2
C12H14O4
82.9
共303兲
106.6⫾1.0
109.8⫾1.0
97.0
共351兲
共298兲
共337.5兲
T
111.4⫾1.2
114.4⫾1.2
共349兲
共298兲
T
138.6⫾2.0
143.0⫾2.0
共371兲
共298兲
T
106.3⫾2.9
quinhydrone 共quinone–hydroquinone兲
共317–334兲
89.1
共300–325兲
88.6⫾1
U 181.2
NA
diphenyldisulfide
95.⫾3.0
diphenyldisulfone
91.7
diphenylamine
96.7⫾2.5
99.2
共298 –323兲
96.7⫾2.5
N-acetyl-1-naphthylamine
共337–360兲
94.1
4-aminoazobenzene
106.3
109.4
共356 –373兲
110.9⫾1.7
1,8-dimethylnaphthalene
共328 –336兲
77.9
79.6
82.7⫾0.3
2,3-dimethylnaphthalene
共333–373兲
82.8
共287–300兲
82.2⫾0.4
81.0
共278 –301兲
79.9⫾0.4
2,6-dimethylnaphthalene
共350–383兲
84.4⫾1.9
共333–368兲
4,4⬘ -dimethyl-2,2⬘ -bipyridyl
C12H12O6
(Tm /K)
Method
diphenyl sulfone
C12H12N2
C12H12N2 O2
CAS registry number
⌬ subH m /kJ mol⫺1
共325.5兲
共313兲
ME,TE
E
E
TE,ME
共310兲
QF
共348.5兲
GS
共364兲
ME
共332兲
共336兲
共298兲
IPM
B,IPM
C
共348兲
共294兲
共290兲
IPM
ME
B,IPM
V
共366兲
IPM
82.5
84.1
共383兲
共291兲
B,IPM
V
83.8⫾1
83.2
84.6
共345兲
共369兲
共348兲
IPM
B,IPM
IPM
99.7⫾2.3
共298兲
C
62.8
1-共4-dimethylaminophenyl兲-1H-pyrrole-2,5-dione
共350–370兲
122.6⫾0.9
1,3,5-trimethoxycarbonylbenzene
共350–368兲
115.9⫾0.4
118.9⫾0.4
117.5⫾0.8
ethyl trans-2-phenylcyclopropanecarboxylate
96.9⫾0.4
1,1-diacetoxy-1-phenylethane
C
共359兲
共298兲
共298兲
ME
共298兲
C
Reference
关87/4兴关60/14兴
关92-69-3兴
关98/9兴
关98/9兴
关87/4兴关60/14兴
关1806-29-7兴
关98/9兴
关98/9兴
关92-88-6兴
关98/9兴
关98/9兴
关127-63-9兴
关U/3兴关70/1兴
关106-34-3兴
关87/4兴
关81/4兴
关53/10兴关60/1兴
关51/6兴
关882-33-7兴
关62/5兴关70/1兴
关10409-06-0兴
关64/5兴
关122-39-4兴
关70/4兴
关68/10兴关88/24兴
关53/5兴关70/1兴
关575-36-0兴
关87/4兴关60/21兴
关60-09-3兴
关87/19兴关91/18兴
关84/40兴
关56/2兴关87/4兴
关569-4-5兴
关87/4兴关75/8兴
关75/8兴关79/5兴
关74/14兴关77/1兴
关581-40-8兴
关87/4兴关75/8兴
关79/5兴
关75/8兴
关59/2兴关87/4兴
关581-42-0兴
关77/7兴关75/8兴
关87/4兴
关75/8兴
关59/2兴关87/4兴
关582-16-1兴
关77/7兴关75/8兴
关75/8兴
关75/8兴关87/4兴
关1134-35-6兴
关97/27兴
关101-80-4兴
关75/11兴
关6953-81-7兴
关98/25兴
关2672-58-4兴
关95/6兴
关95/6兴
关67/8兴关95/6兴
关946-39-4兴
关98/24兴
关28153-24-4兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
604
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C12H15N3 O2
共308 –338兲
3,6-bis共dimethylamino兲phthalimide
共400– 457兲
C12H15N3 O6
C12H16N2 O2
C12H16N2 O5
C12H16N3 O3 PS2
C12H16O2
C12H16O4
C12H17NO2
C12H18
(C12H18) –
(C6 H3 N2 ClO4 )
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
94.4⫾2.2
共318兲
105
135.3
2,4,6-trinitro-1,3-dimethyl-5-tert-butylbenzene
共312–348兲
100.4
N-benzoyl-N⬘,N⬘-diethylurea
132.2⫾2.8
1-methyl-4-tert-butyl-3-methoxy-2,6-dinitrobenzene
共293–353兲
102.9
azinphos-ethyl
共326 – 420兲
86.8
pentamethylbenzoic acid
共347–363兲
111.5⫾1.7
113.4⫾1.8
benzo-12-crown-4
104.3⫾2.6
2,6-diisopropylnitrobenzene
81.0⫾1.0
80.6⫾1.0
hexamethylbenzene
80
81.4⫾0.1
共288 –304兲
85.0⫾0.2
74.9⫾0.6
共303–338兲
85.2
86.1
共314 –364兲
83.2
74.7⫾2
80.8
80.8
共hexamethylbenzene兲-共picryl chloride兲
Method
Reference
GS
关96/14兴
关5972-07-6兴
关87/4兴
关58/4兴
关81-15-2兴
关87/4兴关56/3兴
共415兲
RG
共327兲
共298兲
C
共341兲
共355兲
共298兲
ME
共298兲
CGC–DSC
共286兲
共298兲
GS
GS
共298兲
共298兲
共320兲
共298兲
共329兲
TGA
C
ME
DSC
A
A
ME
93.7
C12H18
C12H18O
C12H18O
C12H18O
C12H18O
C12H18O2
C12H18O2
C12H18O2
C12H19F3 N2 O4
C12H20
C12H20
C12H20N2
C12H20N2 O2
E,E,E-1,5,9-cyclododecatriene
共273–307兲
75.2
74.7⫾0.8
共288兲
1-adamantyl methyl ketone
共287–305兲
84.2⫾0.6
共298兲
exo-4-hydroxy-endo-endo-tetracyclo关 6.2.1.1.3,6.02,7兴 dodecane
共303–343兲
79.0⫾2.5
共298兲
exo-4-hydroxy-exo-endo-tetracyclo关 6.2.1.1.3,6.02,7兴 dodecane
共323–353兲
74.3⫾1.8
76.3⫾2.0
共298兲
exo-4-hydroxy-exo-exo-tetracyclo关 6.2.1.1.3,6.02,7兴 dodecane
共313–353兲
73.9⫾2
75.9⫾2.2
共298兲
1-adamantyl-1-carboxylic acid methyl ester
共267–283兲
84.3⫾0.6
共275兲
82.4⫾0.6
共298兲
trans-syn-trans decahydro-3-hydroxy-2-naphthalene acetic ␥-lactone
共240–310兲
NA
trans-anti-trans decahydro-3-hydroxy-2-naphthalene acetic ␥-lactone
共240–310兲
NA
N关共N-trifluoroacetyl兲valyl兴alanine ethyl ester
共323– 424兲
115.5
共338兲
2,2-dimethyladamantane
共300–360兲
73.6⫾1.3
共298兲
1,3-dimethyladamantane
67.8⫾1.3 共liq兲
共298兲
1-共1-piperidinyl兲cyclohexanecarbonitrile
87.8⫾0.6
共298兲
N,N⬘ -ethylenebis共4-aminopent-3-ene-2-one兲
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
ME
TSGC
TSGC
TSGC
ME
关00/28兴
关83-66-9兴
关53/7兴关60/1兴
关2642-71-9兴
关87/4兴
关2243-32-5兴
关88/10兴
关88/10兴
关14174-08-4兴
关00/11兴
关00/25兴
关00/25兴
关87-85-4兴
关97/29兴
关94/13兴
关89/18兴
关84/2兴
关76/2兴
关76/2兴关93/16兴
关69/24兴
关65/4兴关70/1兴
关57/1兴关60/1兴
关49/8兴
关49/8兴
关676-22-2兴
关87/4兴
关73/16兴关77/1兴
关1660-04-4兴
关92/2兴
关7273-98-5兴
关80/16兴
关107133-43-7兴
关80/16兴
关80/16兴
关74007-11-7兴
关80/16兴
关80/16兴
关711-01-3兴
关92/26兴
关92/26兴
ME
关57/10兴
ME
关57/10兴
BG
EB
关87/4兴关60/20兴
关19740-34-2兴
关77/11兴
关702-79-4兴
关77/11兴
关3867-15-0兴
关97/28兴
关6310-76-5兴
ENTHALPY OF SUBLIMATION
605
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
Compound
Temperature range 共K兲
共358 –374兲
C12H20O2
C12H22O
C12H22O
C12H22O4
C12H22O11
C12H24
C12H24N2 O2
C12H24O2
C12H24O3
C12H24O6
C12H25NO
C12H26
C12H26O
C12H26O
C13H4 Cl6 O
C13H7 NO2
C13H8 O
C13H8 O
C13H8 OS
C13H8 O2
C13H8 O2
C13H9 ClO2
C13H9 N
⌬ subH m /kJ mol⫺1
128.2⫾0.7
131.6
bicyclo关2.2.1兴heptane-7-one 2,2-dimethylpropylene ketal
84.0⫾0.9
cyclododecanone
83.2⫾0.3
trans 2-cyclohexylcyclohexanol
共293–325兲
98.6⫾0.5
dodecanedioic acid
共375–296兲
153.1⫾2.9
D cellobiose
共474 – 488兲
302⫾44.0
cyclododecane
76.2
76.4⫾1.7
dicyclohexyl ammonium nitrite
共290–298兲
99.1
U161.8
共308 –339兲
105.9
dodecanoic acid 共lauric acid兲
共293–303兲
127.9
共293–308兲
132.6
共296 –314兲
140.2⫾3.3
共293–313兲
117.2⫾2.9
peroxydodecanoic acid
共293–303兲
131.4⫾1.7
18 crown-6
128.1⫾2.3
dodecanamide
共349–368兲
152.7⫾0.8
n-dodecane
100.2
101.7
1-dodecanol
共285–294兲
130.1⫾1.2
129.3
di-tert-butyl-isopropylmethanol
59.3⫾0.8
1,2,4,5,7,8-hexachloroxanthene
共353– 449兲
147
benz关g兴isoquinoline-5,10-dione
共334 –381兲
108.1⫾1.6
perinaphthenone
共326 –348兲
97.2⫾2.5
fluorenone
共324 –349兲
91.6⫾1.6
93.9⫾1.6
87.6⫾0.3
88.4⫾0.4
共298 –343兲
92.2
thioxanthone
114.8⫾0.4
xanthone
98.57⫾0.4
3-hydroxy-1H-phenalen-1-one
共402– 432兲
151.5⫾4.7
5-chloro-2-hydroxybenzophenone
共293–367兲
91.9
acridine
86
89.5⫾0.2
91.7⫾0.4
94.5
CAS registry number
(Tm /K)
共366兲
共298兲
Method
Reference
ME
关95/12兴
关95/12兴
关217467-40-8兴
关98/26兴
关850-1-7兴
关96/16兴
共298兲
共298兲
ME
共320兲
ME
共386兲
ME
共481兲
ME
共298兲
CGC–DSC
共294兲
TE
共324兲
共298兲
共300兲
共304兲
共303兲
ME
ME
ME
共298兲
ME
共298兲
CGC–DSC
共358.5兲
ME
共298兲
共263兲
B
B
共290兲
共298兲
ME
共298兲
共401兲
T
共358兲
ME
共337兲
ME
共336兲
共298兲
共319兲
共298兲
共320兲
GS
GS
C
C
GS
共298兲
C
共298兲
C
共417兲
ME
共308兲
UV
共430兲
共333兲
共298兲
共298兲
TGA
C
C
关97/5兴
关693-23-2兴
关60/4兴关70/1兴
关528-50-7兴
关99/1兴
关294-62-2兴
关98/5兴
关57/1兴
关3129-91-7兴
关87/4兴关65/19兴
关85/20兴
关61/6兴
关143-07-7兴
关87/4兴
关68/2兴
关61/1兴
关57/3兴
关2388-12-7兴
关80/23兴
关17455-13-9兴
关00/11兴
关1120-16-7兴
关59/3兴关87/4兴
关112-40-3兴
关72/1兴
关63/6兴
关112-53-8兴
关65/6兴关87/4兴
关65/6兴
关5457-42-1兴
关98/22兴
关38178-99-3兴
关86/7兴
关46492-08-4兴
关98/3兴
关548-39-0兴
关98/3兴
关486-25-9兴
关98/21兴
关98/21兴
关88/5兴
关88/5兴
关86/8兴
关492-22-8兴
关92/27兴
关90-47-1兴
关88/13兴
关5472-84-4兴
关98/3兴
关85-19-8兴
关87/4兴关60/24兴
关260-94-6兴
关98/36兴
关94/14兴
关94/14兴
关89/26兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
606
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
Compound
Temperature range 共K兲
共280–328兲
共303–328兲
共303–326兲
共281–298兲
共306 –345兲
C13H9 N
3,4-benzoquinoline 共phenanthridine兲
共288 –323兲
共288 –323兲
C13H9 N
C13H9 N
5,6-benzoquinoline
共288 –323兲
C13H9 NO
acridone
C13H9 NO2
N-methyl-1,8-naphthalimide
共379–398兲
共318 –333兲
共348 –388兲
共283–323兲
共350–388兲
C13H10N2
共286 –300兲
共306 –323兲
共306 –322兲
9-aminoacridine
C13H10N2 O2
N-phenyl 4-nitrobenzaldehyde imine
C13H10N4
1,5-diphenyltetrazole
共348 –363兲
2,5-diphenyltetrazole
共333–353兲
benzophenone
共299–320兲
C13H10O
92.6
90.8⫾1.3
93.3⫾0.8
91.6⫾2.5
92.8⫾1.3
78.7
共295兲
共298兲
共298兲
共290兲
共298兲
100.1⫾10.1
98.6
94.6⫾4
107.5
共306兲
共298兲
共308兲
ME
83.1⫾3.6
106.3
共308兲
ME
ME
90.2⫾2.0
80.8⫾2.5
100.4
共298兲
共308兲
136.2⫾0.5
共298兲
C
107.4⫾0.8
109.7⫾0.8
共389兲
共298兲
ME
ME
87.6
84.9
84.9⫾0.4
85.1⫾0.4
87.0⫾1.0
80.2⫾0.2
78.9
88.4⫾0.6
83.1⫾1.3
81.8
80.3⫾0.8
82.8
82.8
共298兲
共383兲
共343兲
共298兲
共318兲
共298兲
共363兲
共303兲
CGC–DSC
GS
GS
共388兲
共293兲
共315兲
B
TE
115
共520兲
TGA
126⫾1.3
共298兲
121.5⫾4.2
共355兲
ME
119.7⫾4.2
共343兲
ME
92.4⫾2.2
93.1⫾2.2
94.7⫾1
92⫾0.83
95.0⫾0.2
96.1
84.4⫾1.13
93.9⫾0.5
95.0⫾1.5
92.9⫾0.8
77.0⫾2.5
89.96
94.6⫾0.8
93.4⫾0.3
96.1
91.2
78.2⫾1.2
共309兲
共298兲
共321兲
共298兲
共304兲
GS
GS
DM
C
ME
共298兲
共307兲
共305兲
共306兲
共298兲
共308兲
共298兲
共298兲
共306兲
C
TE,ME
TE
ME
ME
ME
TCM
C
Method
TE
TCM
LE
ME
E
ME
ME
ME
ME
fluorene
共313– 453兲
共323–363兲
C13H10N4
(Tm /K)
7,8-benzoquinoline
共293–323兲
C13H10
CAS registry number
⌬ subH m /kJ mol⫺1
共295–313兲
共297–317兲
共293–318兲
共294 –318兲
共278 –311兲
共298 –318兲
共295–304兲
共293–319兲
共290–315兲
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
共303兲
PG
C
IPM
GS
Reference
关87/4兴
关75/5兴
关U/1兴关75/5兴
关75/1兴
关U/2兴关75/5兴
关46/1兴
关260-27-3兴
关98/3兴
关89/26兴
关75/15兴关87/4兴
关65/6兴
关85-02-9兴
关75/15兴关87/4兴
关72/10兴
关230-27-3兴
关89/26兴
关75/15兴关87/4兴
关72/10兴
关598-95-0兴
关92/27兴
关2382-08-3兴
关00/9兴
关00/9兴
关86-73-7兴
关98/5兴
关95/7兴
关94/2兴
关94/2兴
关88/26兴
关87/10兴
关87/4兴关75/8兴
关83/11兴
关77/7兴关75/8兴
关75/8兴
关60/2兴
关53/13兴关87/4兴
关53/1兴关60/1兴
关90-45-9兴
关98/29兴
关785-80-8兴
关97/18兴
关7477-73-8兴
关51/3兴关70/1兴
关18038-45-7兴
关51/3兴关70/1兴
关119-61-9兴
关98/21兴
关98/21兴
关83/2兴
关74/20兴关83/2兴
关80/14兴
关78/15兴
关78/13兴
关77/4兴
关75/5兴
关75/6兴
关74/5兴
关87/4兴关74/6兴
关73/1兴
关72/1兴
关56/3兴
关50/2兴
关38/1兴关34/1兴
ENTHALPY OF SUBLIMATION
607
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
C13H10O
C13H10O2
Compound
Temperature range 共K兲
共273–320兲
dibenzopyran
共305–353兲
(Tm /K)
95⫾2.5
Method
Reference
共298兲
TE
91.2⫾1.6
共298兲
ME
92.5
112.1⫾2.1
共329兲
T
99.0⫾0.4
89.5⫾4.2
96.2⫾1.7
共298兲
90⫾8.4
共298兲
E
109.1
92⫾4.2
共294兲
UV
134
共327兲
UV
关32/1兴关70/1兴
关60/1兴
关25/1兴
关229-95-8兴
关86/7兴
关58/2兴关70/1兴
关93-99-2兴
关71/2兴
关71/11兴关77/1兴
关47/2兴关70/1兴
关102-09-0兴
关71/2兴关77/1兴
关118-55-8兴
关87/4兴关60/24兴
关47/2兴关70/1兴
关131-56-6兴
关87/4兴关60/24兴
关1470-79-7兴
关99/22兴
关131-55-5兴
关99/22兴
关87/4兴关60/24兴
关538-51-2兴
关97/18兴
关97/18兴
关86/10兴
关48/2兴
关1484-12-4兴
关90/8兴
关90/8兴
关1137-98-8兴
关86/10兴
关779-84-0兴
关87/4兴
关58/1兴
关1689-73-2兴
关87/4兴
关58/1兴
关93-98-1兴
关87/4兴关60/21兴
关20357-59-9兴
关86/10兴
关2440-22-4兴
关87/4兴关60/24兴
关101-81-5兴
关99/23兴
关99/23兴
关89/1兴
关86/1兴
关59/2兴关70/1兴
关51/1兴关60/1兴
关38/1兴
关644-08-6兴
关97/27兴
关102-07-8兴
关87/2兴
phenyl benzoate
C13H10O3
diphenyl carbonate
C13H10O3
phenyl salicylate
共279–315兲
C13H10O3
CAS registry number
⌬ subH m /kJ mol⫺1
C13H10O4
2,4-dihydroxybenzophenone
共312–353兲
2,4,4 ⬘ -trihydroxybenzophenone
C13H10O5
2,2⬘ ,4,4 ⬘ -tetrahydroxybenzophenone
C13H11N
共363– 471兲
N-phenyl-benzaldehyde imine
共294 –326兲
139.0
C13H11N
C13H11NO
C13H11NO
C13H11NO
C13H11NO
C13H11NO2
C13H11N3 O
C13H12
C13H12
C13H12N2 O
C13H12N4 O2
C13H12O
C13H12O
C13H13N
9-methylcarbazole
共313–332兲
TGA
178.5
143.4
共378兲
97.4⫾1.2
98.1⫾1.2
93.7⫾0.9
85.5⫾2.1
共309兲
共298兲
共298兲
共293兲
T
共322兲
共298兲
ME
共298兲
C
95.0
95.5
N-phenylmethylene benzenamine N-oxide
115.0⫾0.8
2-hydroxybenzaldehyde N-phenylimine
共288 –325兲
115.9
共348 – 408兲
129.9
4-hydroxybenzaldehyde N-phenylimine
共348 – 408兲
127.9
共288 –338兲
116
benzanilide
共352–369兲
99.2
N-共2-hydroxyphenylmethylene兲benzenamine N-oxide
116.5⫾1.4
2-共2 ⬘ -hydroxy-5 ⬘ -methylphenyl兲benzotriazole
共293–333兲
125.2
diphenylmethane
共273–295兲
88.5⫾0.8
87.6⫾0.8
共273–298兲
71.5
共276 –295兲
83.3⫾3.3
82.4⫾8
共278 –299兲
64.0
72.0⫾0.8
4-methylbiphenyl
80.2⫾1.4
1,3-diphenylurea
共445– 484兲
152⫾6
4 ⬘ -nitro-2-methylaminoazobenzene
134.7
diphenylmethanol
105.7⫾0.7
4-benzylphenol
共313–335兲
97.4
N-phenyl benzylamine
B
UV
C
共303兲
共378兲
共363兲
共313兲
共360.5兲
共298兲
C
共308兲
UV
共284兲
共298兲
共286兲
共286兲
GS
EM
HSA
V
共297兲
共298兲
C
共464兲
TE
GS
共298兲
共324兲
关87/19兴关91/18兴
关91-01-0兴
关98/22兴
关101-53-1兴
关87/4兴关60/14兴
关103-32-2兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
608
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
Compound
Temperature range 共K兲
共293–312兲
C13H14N2
C13H16N2
C13H16N2 O3
C13H17NO3
C13H19NO2
C13H21NO
C13H21NO2
C13H22
C13H22O3
C13H26O
C13H26O2
C13H26O2
C13H26O3
C13H27NO
C13H28
C13H28
C13H28O
plastic
crystalline
C14H6 Cl2 N2 O4
C14H6 N2 O6
C14H6 N6 O12
C14H7 NO4
C14H8 Cl4
C14H8 Cl6
C14H8 O2
2,2⬘ -diaminodiphenylmethane
共343– 403兲
␣-phenyl-1-piperidineacetonitrile
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
103.6⫾1.6
51.3
共303兲
111.3
共358兲
73.2⫾0.4
共298兲
hexahydro-1-共3-nitrobenzoyl兲-1H-azepine 共compound is called hexamethyleneimine
m-nitrobenzoate in paper兲
共310–321兲
113.0
共315兲
104.6
morpholine cinnamate
共298 –349兲
118.8
共313兲
cyclohexyl ammonium benzoate
共289–298兲
103.1
共293.5兲
N,N-dimethyl-1-adamantylcarboxamide
共303–322兲
96.9⫾0.3
共313兲
97.5⫾0.3
共298兲
N-共3-phenoxy-2-hydroxypropyl兲-butylamine
共323–348兲
133.9
共335.5兲
1,3,5-trimethyladamantane
共300–360兲
77.8⫾1.3
共298兲
dicyclohexyl carbonate
共293–313兲
66.5⫾4.2
共303兲
7-tridecanone
共287–293兲
103.8
共290兲
methyl dodecanoate
共262–273兲
121.8⫾2.1
共267兲
tridecanoic acid
共282–299兲
170
peroxytridecanoic acid
共293–303兲
142.7⫾5
共298兲
N-methyl dodecanamide
共323–337兲
116.6⫾0.8
共330兲
n-tridecane
91.4
共298兲
tri-tert-butylmethane
55.4
共298兲
共265–319兲
57.0⫾0.4
共288兲
共273–306兲
57.7⫾2.8
共290兲
61.1⫾1.3
共295–330兲
7.7⫾0.1
共311兲
tri-tert-butylmethanol
共278 –318兲
56.5⫾1.0
共298兲
共269–300兲
63.2⫾1.2
共298兲
1-amino-4-nitro-5,8-dichloroanthraquinone
158.2
1,4-dinitroanthraquinone
131.0
1,2-bis共2,4,6-trinitrophenyl兲ethylene
共434 – 479兲
179.9
共449兲
180.3
1-nitroanthraquinone
共407– 440兲
139.7
共422兲
108.9⫾2.1
共396兲
137.9⫾1.7
115.5
1,1-dichloro-2,2-bis共4-chlorophenyl兲ethylene
74.2
1,1,1-trichloro-2-chloro-2,2-bis共4-chlorophenyl兲ethane
89.4
9,10-anthraquinone
111.3
108.4
共402兲
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
Method
Reference
T
关97/10兴
关80/8兴
关6582-52-1兴
关87/4兴
关5766-79-0兴
关97/28兴
关37000-08-1兴
ME
ME
ME
BG
ME
ME
ME
TPTD
ME
GS
B
CGC–DSC
T
HSA
TE
TE
LE
TE
C
TE,ME
GS
C
关72/8兴
关70/22兴关72/8兴
关87/4兴
关3129-92-8兴
关87/4兴关65/19兴
关1502-00-7兴
关93/18兴关95/11兴
关95/11兴
关3246-04-6兴
关87/4兴
关707-35-7兴
关77/11兴
关4427-97-8兴
关71/11兴关77/1兴
关462-18-0兴
关38/3兴
关111-82-0兴
关65/6兴关87/4兴
关638-53-9兴
关01/15兴
关40915-96-6兴
关80/23兴
关27563-67-3兴
关59/4兴关87/4兴
关629-50-5兴
关72/1兴
关35660-96-9兴
关98/5兴
关97/7兴
关95/16兴
关95/16兴
关86/2兴
关41902-42-5兴
关83/18兴
关83/18兴
关66121-41-3兴
关68/10兴关88/24兴
关66121-37-7兴
关68/10兴关88/24兴
关20062-22-0兴
关87/4兴关69/12兴
关68/14兴关66/11兴
关82-34-8兴
关87/4兴关70/4兴
关82/3兴
关70/4兴
关68/10兴关88/24兴
关72-55-9兴
关95/32兴关89/32兴
关3563-45-9兴
关95/32兴关89/32兴
关84-65-1兴
关97/19兴关91/18兴
关82/3兴
ENTHALPY OF SUBLIMATION
609
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
Compound
Temperature range 共K兲
共373– 453兲
共397– 471兲
共355–356兲
共470–590兲
共343– 403兲
C14H8 O2
C14H8 O3
C14H8 O3
C14H8 O4
共393– 453兲
2,2⬘ -biphenyldicarboxylic anhydride
共433– 490兲
1,2-dihydroxyanthraquinone
共368 – 498兲
C14H9 ClN2 O4
C14H9 Cl5
108.1
132
共289兲
共383兲
C
113.1
120.6
101.3⫾0.4
共358兲
共407兲
136.8
153.1
共408兲
91.4
共448兲
123.8
121.9⫾0.5
121.5⫾0.4
123.9
共383兲
共469兲
共469兲
共403兲
114.6
102.4⫾4.4
89.1
121.9⫾0.8
121.1⫾4
U 94.5
123.5
103.5⫾1.3
共363兲
共413兲
共429兲
共429兲
共338兲
共376兲
共409兲
123.2⫾7
126.8
111.3
117.6
共398兲
共456兲
共298兲
116.8
123
U 96.5
105.8⫾8
109.6⫾8
共368兲
共345兲
共404兲
共298兲
ME
ME
GS
HSA
GS
C
ME
ME
GS
GS
ME
C
TGA
ME
HSA
ME
ME
1,8-dihydroxyanthraquinone
共333– 403兲
共335–356兲
C14H8 O6
ME
关77/20兴关78/35兴
关73/10兴
关73/10兴
关73/10兴
关71/17兴
关71/6兴
关71/6兴
关70/4兴
关68/10兴关88/24兴
关58/1兴关87/4兴
关56/5兴关70/1兴
关56/1兴
关54/3兴
关52/3兴
关52/3兴
关84-11-7兴
关89/21兴
关56/5兴关70/1兴
关129-43-1兴
关87/19兴关91/18兴
关58/1兴关87/4兴
关56/1兴
关605-32-3兴
关87/19兴关91/18兴
关87/4兴
关6050-13-1兴
关87/4兴
关72-48-0兴
关87/4兴
关73/4兴
关73/4兴
关58/1兴
关81-64-1兴
关87/19兴关91/18兴
关84/35兴
关77/20兴关78/35兴
关73/4兴
关73/4兴
关71/17兴
关58/1兴关87/4兴
关56/1兴
关117-12-4兴
关73/10兴
关58/1兴关87/4兴
关56/1兴
关56/1兴
关117-10-2兴
关73/10兴
关58/1兴关87/4兴
关71/17兴
关56/1兴
关56/1兴
关84-60-6兴
关58/1兴关87/4兴
关81-60-7兴
关58/1兴关87/4兴
关12217-79-7兴
关87/4兴
关50-29-3兴
关94/1兴
关87/4兴
关80/35兴
关72/11兴
1,5-dihydroxyanthraquinone
共363– 433兲
C14H8 O4
共373兲
共298兲
共298兲
共298兲
共367兲
共298兲
共298兲
GS
C
ME
ME
TGA
C
C
ME,TE
1,4-dihydroxyanthraquinone
共324 –351兲
C14H8 O4
共413兲
共298兲
共434兲
Reference
2-hydroxy-9,10-anthraquinone
共353–373兲
共373– 453兲
共394 – 463兲
C14H8 O4
98.3
113⫾0.8
107.5⫾0.8
107.9⫾0.8
U 105.9
127.0⫾3.0
136.6⫾3
116.1⫾1.7
115.1
126.4
112.1
110.9
107.9
104.6
108.0
Method
1-hydroxy-9,10-anthraquinone
共434 –505兲
C14H8 O4
(Tm /K)
9,10-phenanthraquinone
共333–383兲
C14H8 O3
CAS registry number
⌬ subH m /kJ mol⫺1
2,6-dihydroxyanthraquinone
共463–533兲
173.8
共498兲
1,4,5,8-tetrahydroxyanthraquinone
共403– 473兲
151.6
共438兲
1,5-diaminochloro-4,8-dihydroxyanthraquinone 共C.I. disperse blue 56兲
共483–533兲
93.3
共498兲
1,1-bis共-4-chlorophenyl兲-2,2,2-trichloroethane (p,p ⬘ -DDT)
共273–313兲
120.2⫾1.0
共293兲
共323–363兲
115
共338兲
共293–353兲
110
共304兲
共293–313兲
117.8
共303兲
ME
ME
TGA
HSA
GS
GS
GS
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
610
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
C14H9 F3 O2
C14H9 NO2
C14H9 NO2
C14H9 NO3
C14H9 N3 O4
C14H10
Compound
Temperature range 共K兲
⌬ subH m /kJ mol⫺1
共323–363兲
117.5
共313–363兲
84
共339–373兲
118
4,4,4-trifluoro-1-共2-naphthyl兲-butane-1,3-dione
108.7⫾0.6
1-aminoanthraquinone
121.8
共413– 443兲
126.5⫾1.3
共368 –393兲
116.3⫾3.9
共373– 453兲
103.3
共361–386兲
U 90.9
125.9⫾2.5
131.0
113⫾0.4
2-aminoanthraquinone
136.8
143.5⫾2.9
162.3
1-hydroxy-4-aminoanthraquinone
127.2
共418 – 438兲
131.3⫾1.7
共444 – 473兲
144
119.6
133.5⫾2.1
120.1
1,4-diamino-5-nitroanthraquinone
共373– 453, not crystalline兲
U50.2
anthracene
共423– 488兲
94.5
99.4
共318 –363兲
100.0⫾2.8
共343– 448兲
84.0⫾3.0
共313– 453兲
99.7
共318 –373兲
98.7
共313–363兲
102.6
共353–399兲
94.3
共283–323兲
91.8⫾0.9
共323–353兲
91.2
97.4⫾1.1
97.8⫾0.1
共337–361兲
104.5⫾1.5
共358 –393兲
94.8
共363– 448兲
98.8⫾0.4
共328 –372兲
97.2
97.1
共323–353兲
102.9⫾4.8
共283–323兲
95.8⫾6
共353– 432兲
101.0⫾0.5
99.7
共290–358兲
84.1
共342–359兲
98.3⫾2.1
共327–346兲
90⫾1.3
100.8
共303–373兲
103.4⫾2.9
100.8⫾4.2
共396 – 421兲
97.5⫾2
共339–353兲
102.1
共338 –353兲
102.1⫾2.1
92.0⫾2.1
90.4
95.4
95.0
共378 –398兲
97.3⫾1.2
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
CAS registry number
(Tm /K)
Method
Reference
共338兲
共338兲
共356兲
GS
GS
TE
共298兲
ME
关56/4兴关60/1兴
关49/10兴
关47/1兴
关893-33-4兴
关97/33兴
关82-45-1兴
关87/19兴关91/18兴
关87/4兴关70/4兴
关84/35兴
关77/20兴关78/35兴
关71/17兴
关70/4兴
关68/10兴关88/24兴
关56/1兴
关117-79-3兴
关87/19兴关91/18兴
关70/4兴
关68/10兴关88/24兴
关116-85-8兴
关87/19兴关91/18兴
关87/4兴关70/4兴
关87/4兴
关84/40兴
关70/4兴
关68/10兴关88/24兴
关82-33-7兴
关77/20兴关78/35兴
关120-12-7兴
关99/40兴
关98/5兴
关98/3兴
关97/38兴
关95/7兴
关86/7兴
关86/8兴
关83/3兴
关83/11兴
关82/23兴
关81/3兴
关80/3兴
关80/1兴
关79/27兴
关77/8兴
关76/8兴
关75/20兴
关75/5兴
关73/15兴
关73/2兴
关73/2兴
关72/9兴关71/6兴
关64/3兴关70/1兴
关60/2兴
关58/1兴关70/1兴
关58/1兴关70/1兴
关58/1兴关70/1兴
关53/2兴
关53/13兴
关53/1兴关70/1兴
关52/3兴
关51/12兴
关51/6兴
关50/5兴
关49/3兴
共428兲
共380兲
共413兲
共374兲
共463兲
GS
TE
GS
TGA
TE,ME
HSA
GS
TE,ME
共428兲
共458.5兲
GS
TE
TE,ME
共413兲
共298兲
共341兲
共298兲
共383兲
共346兲
共338兲
共376兲
共303兲
共338兲
共298兲
共376兲
共298兲
共393兲
共337兲
GS
MEM
CGC–DSC
ME
TGA
GS
GS
GS
GS
GS
GS
GS,C
HSA
TE,ME
GS
HSA
ME
C
TE
LE
ME
C
ME,C
TE
HSA
共346兲
共364兲
共353兲
ME
ME
RG
ENTHALPY OF SUBLIMATION
611
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
C14H10
Compound
Temperature range 共K兲
(Tm /K)
104.6⫾4.2
93.3⫾4.2
共353兲
95.3
95.1⫾1.1
90.0⫾4.5
88.7⫾1.25
共298兲
共298兲
共310兲
共313兲
92⫾1
90.5
95.0⫾4.4
88.9
87.2⫾1.1
90.9⫾1.7
82⫾2
95.0⫾0.6
92.5⫾2
87.2
87.2
87.4⫾0.8
86.6⫾0.8
90.9⫾0.4
84.1⫾2.5
95.9
86.6
共298兲
共318兲
共383兲
共350兲
共298兲
共340兲
共303兲
共298兲
共345兲
共372兲
共298兲
共298兲
共298兲
共297兲
共303兲
共317–362兲
共283–323兲
共315–335兲
共325–364兲
共300–330兲
共312–326兲
共279–315兲
共273–333兲
共310–323兲
90.7⫾1.2
81.6
92.9
84.1⫾0.8
C14H10F4
C14H10N2 O2
C14H10N2 O2
C14H10O
C14H10O2
CGC–DSC
ME
HSA
phenanthrene
共303–333兲
共313– 453兲
C14D10
Method
diphenylacetylene
共298 –316兲
共299–321兲
共299–321兲
C14H10
CAS registry number
⌬ subH m /kJ mol⫺1
phenanthrene-d10
共283–323兲
92.2⫾1.1
1,1,2,2-tetrafluoro-1,2-diphenylethane
101.8
1,4-diaminoanthraquinone
143.0
共448 – 474兲
151.2⫾1.3
136.0
共378 – 403兲
102.6⫾9.7
共473– 453兲
123
149.2⫾2.5
123.4
138.1
1,5-diaminoanthraquinone
共405– 427兲
118.5⫾4.8
anthrone
共333–368兲
103.0⫾0.8
106.1⫾0.8
103.3
99.6
benzil
共319–340兲
98.4⫾1.1
共315兲
共323兲
LE
CGC–DSC
ME
GS
DSC
DSC
TE
GS
TE,ME
GS
B
TE
TCM
C
TE
ME
ME
共313兲
共303兲
GS
共298兲
GS
共461兲
共390兲
共413兲
GS
TE,ME
GS
共416兲
共350兲
共298兲
共298兲
共354兲
GS
GS
C
共329兲
82.8
C14H10O3
C14H10O4
C14H10O4
benzoic anhydride
benzoyl peroxide
共310–340兲
共293–313兲
diphenyl oxalate
96.2⫾4.2
96.7⫾4.2
共298兲
B
97.9⫾2.5
89.7⫾4.2
共298兲
共303兲
ME
ME
Reference
关49/6兴关70/1兴
关38/1兴
关501-65-5兴
关98/5兴
关93/5兴
关86/1兴
关38/1兴
关38/2兴关60/1兴
关85-01-8兴
关98/38兴
关98/5兴
关98/3兴
关95/7兴
关88/4兴
关88/4兴
关83/27兴
关83/11兴
关80/1兴
关79/27兴
关75/8兴
关75/5兴
关U/1兴关75/5兴
关72/1兴关77/1兴
关60/2兴
关58/1兴关70/1兴
关53/1兴关70/1兴
关60/1兴
关52/3兴
关51/12兴
关49/6兴关70/1兴
关38/1兴
关1517-22-2兴
关83/11兴
关425-32-1兴
关97/34兴
关128-95-0兴
关87/19兴关91/18兴
关87/4兴关70/4兴
关84/40兴
关84/35兴
关77/20兴关78/35兴
关70/4兴
关68/10兴关88/24兴
关67/16兴关91/18兴
关129-44-2兴
关84/35兴
关90-44-8兴
关98/21兴
关98/21兴
关91/12兴
关91/12兴
关134-81-6兴
关59/2兴关70/1兴
关87/4兴
关38/1兴关38/2兴
关60/1兴
关93-97-0兴
关71/2兴关77/1兴
关47/2兴关70/1兴
关94-36-0兴
关75/9兴
关71/11兴关77/1兴
关3155-16-6兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
612
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
C14H10O4
C14H10O5
C14H11FO3
C14H11FO3
C14H11FO3
C14H11F3
C14H11N3 O2
C14H12
C14H12
Compound
Temperature range 共K兲
102.5⫾8.4
2,2 ⬘ -biphenyldicarboxylicacid
共433– 493兲
166.1
O-phenyl-O,O-benzoyl peroxycarbonate
97.9⫾2.5
133.9⫾4.2
2 ⬘ -fluoro-2-hydroxy-4-methoxybenzophenone
共307–318兲
109.3
3 ⬘ -fluoro-2-hydroxy-4-methoxybenzophenone
共322–343兲
U 17.3
4 ⬘ -fluoro-2-hydroxy-4-methoxybenzophenone
共322–343兲
U 37.7
1,1,2-trifluoro-1,2-diphenylethane
93.1
1,4,5-triaminoanthraquinone
共373– 453兲
U70.3
9,10-dihydroanthracene
共313– 453兲
93.9
共318 –379兲
92.4⫾4
94.2⫾0.8
共319–377兲
92.2⫾0.6
93.9⫾0.6
共279–328兲
93.3⫾4
89.5
trans-diphenylethene
102.0
共298 –343兲
99.6
U 61.1
共293–338兲
103.8⫾2.5
100.7⫾0.4
共310–340兲
C14H12
共303–315兲
9-methylfluorene
共318 –358兲
C14H12F2
1,1-difluoro-1,2-diphenylethane
C14H12N2
N-methyl-9-acridinamine
C14H12N2
10-methyl-9-acridinimine
C14H12N2
dibenzylideneazine
C14H12N2 O2
C14H12N2 S2
C14H12N4 O2
C14H12O
C14H12O2 S
C14H12O3
C14H12O4
⌬ subH m /kJ mol⫺1
CAS registry number
(Tm /K)
Reference
B
关71/2兴关77/1兴
关482-05-3兴
关87/4兴
关962-16-3兴
关75/9兴关77/1兴
关71/11兴关77/1兴
关3119-88-8兴
关87/4兴关66/6兴
关3506-35-2兴
关87/4兴关66/6兴
关3602-47-9兴
关87/4兴关66/6兴
关68936-77-6兴
关97/34兴
关6407-69-8兴
关77/20兴关78/35兴
关613-31-0兴
关95/7兴
关75/12兴关87/4兴
关75/12兴
关75/12兴关87/4兴
关75/12兴
关58/1兴关70/1兴
关51/2兴关60/1兴
关103-30-0兴
关98/5兴
关87/4兴
关83/9兴
关83/16兴
关83/1兴
共448兲
E
共312.5兲
EV
共332.5兲
EV
共332.5兲
EV
共298兲
共413兲
GS
共383兲
GS
ME
ME
C
C
共298兲
共298兲
共304兲
共388兲
共298兲
共313兲
CGC–DSC
MS
共315兲
共298兲
SRFG
TE,ME,DM
TE
TCM
99.6⫾1.7
102.1⫾0.6
99.2⫾0.4
86.5⫾0.1
共298兲
共309兲
TM
82.8⫾0.3
82.8⫾0.3
共338兲
共298兲
B
94.7⫾0.9
共298兲
107
共480兲
TGA
94
共550兲
TGA
93.3⫾2.1
共293兲
cis-5a,6,11a,12-tetrahdro关1,4兴benzothiazino关3,2-b兴关1,4兴benzoxazine
共383–392兲
122.0
共387兲
129.0⫾1.3
共298兲
cis-5a,6,11a,12-tetrahdro关1,4兴benzothiazino关3,2-b兴关1,4兴-benzothiazine
共383–392兲
118.0
共387兲
123.3⫾1.2
共298兲
1,4,5,8-tetraminoanthraquinone
共373– 453兲
U82
共413兲
desoxybenzoin
99.3⫾4.2
E-共2-phenylethenyl兲sulfonylbenzene
共phenyl trans-B-styrylsulfone兲
105⫾3.8
2-hydroxy-4-methoxybenzophenone
共281–337兲
118.9
共296兲
共308 –323兲
U39.7
共315兲
2,2⬘ -dihydroxy-4-methoxybenzophenone
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
Method
ME
ME
GS
B
UV
EV
关75/5兴
关73/1兴
关72/1兴
关55/5兴
关2523-37-7兴
关94/2兴
关94/2兴
关350-62-9兴
关97/34兴
关22739-29-3兴
关98/29兴
关5291-44-1兴
关98/29兴
关588-68-1兴
关48/2兴
关192998-96-2兴
关97/1兴
关97/1兴
关165454-33-1兴
关97/1兴
关97/1兴
关2475-45-8兴
关77/20兴关78/35兴
关451-40-1兴
关47/2兴关70/1兴
关16212-06-9兴
关69/11兴关77/1兴
关131-57-7兴
关87/4兴关60/24兴
关66/6兴
关131-53-3兴
ENTHALPY OF SUBLIMATION
613
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
C14H12O4
C14H13N
C14H13NO
C14H13NO2
C14H14
C14H14
C14H14
C14H14
C14H14FN3
C14H14FN3 O2 S
C14H14NO3
C14H14N2
C14H14N2 O
C14H14N2 O2
C14H14N4 O2
C14H14N4 O2
C14H14O
C14H14O2 S
C14H14O2 S
C14H14O8
C14H14S
C14H15N3
C14H15N3
Compound
Temperature range 共K兲
⌬ subH m /kJ mol⫺1
103.8
共303–342兲
228
2,4-dihydroxy-4 ⬘ -methoxybenzophenone
138.3
N-ethylcarbazole
共310–329兲
98.4⫾0.3
99.1⫾0.3
N,N-diphenylacetamide
共343–376兲
122.7
N-共4-methoxyphenylmethylene兲 benzenamine N-oxide
130.6⫾1.2
2,2⬘ -dimethylbiphenyl
共283–288兲
65.7
3,3⬘ -dimethylbiphenyl
共288 –308兲
71.9
4,4⬘ -dimethylbiphenyl
95.1⫾2.0
1,2-diphenylethane
共293–323兲
92.9
共273–318兲
91.2⫾0.4
91.5⫾0.7
91.4⫾0.5
共286 –307兲
84.1⫾0.4
共290–317兲
72.4⫾1.3
73.2
N,N-dimethyl-4-关共4-fluorophenyl兲azo兴benzenamine
91.2
4-关关4-共dimethylamino兲phenyl兴azo兴benzenesulfonyl chloride
105.6
bis共4-methoxyphenyl兲nitrogen oxide
共328 –363兲
100.7
N,N⬘ -diphenylacetamidine
共343–383兲
122.6⫾3.8
p-azoxyanisole
134.8⫾3.7
4-共2-hydroxyethoxy兲azobenzene
120.9
3-nitro-4 ⬘ -共N,N-dimethylamino兲azobenzene
共388 – 412兲
133.9⫾3.8
共392– 410兲
133.1⫾3.8
4-nitro-4 ⬘ -共N,N-dimethylamino兲azobenzene
共413– 425兲
134.3⫾7.5
共414 – 428兲
135.1⫾0.9
134.3
1,1-diphenylethanol
105.0⫾0.8
dibenzyl sulfone
125.5⫾2.9
di-p-tolyl sulfone
109.6⫾2.9
1,2,4,5-tetramethoxycarbonylbenzene
共371–391兲
140.4⫾0.8
143.3⫾0.8
135.9⫾1.3
dibenzyl sulfide
93.3⫾5
4-共N,N-dimethylamino兲azobenzene
共346 –354兲
117.6⫾1.7
共352–354兲
115.9⫾1.3
120.9⫾1.7
共E兲 4-共N,N-dimethylamino兲azobenzene
132⫾8
CAS registry number
(Tm /K)
共318兲
Method
Reference
B
UV
关99/22兴
关87/4兴关60/24兴
关131-53-3兴
关99/22兴
关86-28-2兴
关90/8兴
关90/8兴
关519-87-9兴
关87/4兴
关3585-93-1兴
关86/10兴
关605-39-0兴
关74/6兴关87/4兴
关612-75-9兴
关74/6兴
关613-33-2兴
关97/27兴
关103-29-7兴
关89/1兴
关83/16兴
关80/27兴
关72/1兴
关59/2兴关70/1兴
关51/1兴
关38/1兴关60/1兴
关38/2兴
关150-74-3兴
关84/39兴
关4644-89-7兴
关84/39兴
关2643-00-7兴
关87/4兴关65/7兴
关621-09-0兴
关58/12兴
关1562-94-3兴
关93/11兴
B
共319兲
共298兲
ME
ME
共358兲
共298兲
C
共285兲
ME
共298兲
ME
共298兲
C
共308兲
共295兲
共298兲
共298兲
EM
共304兲
B
C
V
ME
UV
UV
共343兲
共363兲
ME
共298兲
C
GS
共400兲
共401兲
ME
TE
共419兲
共421兲
ME
TE
ME
共298兲
共381兲
共298兲
共298兲
ME
E
共350兲
共353兲
共373兲
ME
TE
ME
共381兲
TE
关56/14兴关91/18兴
关3837-55-6兴
关67/7兴
关67/7兴关87/4兴
关2491-74-9兴
关67/7兴关66/18兴
关67/7兴关87/4兴
关56/14兴关91/18兴
关599-67-7兴
关98/22兴
关620-32-6兴
关U/3兴关70/1兴
关599-66-6兴
关U/3兴关70/1兴
关635-10-9兴
关95/6兴
关95/6兴
关67/8兴关95/6兴
关538-74-9兴
关62/5兴关70/1兴
关60-11-7兴
关67/7兴
关67/7兴
关56/2兴关87/4兴
关25548-37-2兴
关85/22兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
614
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C14H15N3
2,3⬘ -dimethyl-4-aminoazobenzene
C14H16
1,4,5,8-tetramethylnaphthalene
⌬ subH m /kJ mol⫺1
CAS registry number
(Tm /K)
112.5
C14H16ClN3 O2
C14H16O5
C14H18N2 O5
C14H18O
C14H18O2
C14H20
C14H20
C14H20
C14H20O
C14H20O
C14H20O
C14H20O5
C14H21F3 N2 O4
C14H21NO
C14H22
C14H22O
C14H22O
C14H22O
C14H22O
C14H22O2
C14H22O2
C14H22O6
99.8⫾1.4
共298兲
兵1-共4-chlorophenoxy兲-3,3-dimethyl-1-共1H-1,2,4-triazol-1-y1兲其butanone
共Triadimefon兲
共298 –343兲
111.1⫾2.2
共303兲
benzoyl共3-cyclohexyloxy兲carbonyl peroxide
共293–313兲
96.2⫾4.2
共303兲
2,6-dimethyl-3,5-dinitro-4-tert-butylacetophenone
共293–353兲
107.9
共323兲
diamantanone
103.1⫾.62
共320兲
6,6-dimethyl-1-phenyl-4,8-dioxaspiro关2.5兴octane
97.5⫾0.3
共298兲
1,8-cyclotetradecadiyne
共315–364兲
87.6⫾1.0
共338兲
94.3
共298兲
共317–332兲
166.0⫾3.2
共325兲
1,2,3,4,5,6,7,8-octahydroanthracene 共octhracene兲
共438 – 499兲
82.3⫾1.2
共298兲
diadamantane
共305–333兲
96.0⫾0.8
共319兲
117.2⫾8
diamantan-1-ol
共319–349兲
118.⫾0.6
共334兲
diamantan-3-ol
共323–354兲
116.1⫾4.4
共338兲
diamantan-4-ol
共322–353兲
117.8⫾0.2
共337兲
benzo-15-crown-5
123.2⫾2.0
共298兲
proline, 1-关N-共trifluoroacetyl兲-1-leucyl兴methyl ester
共313–366兲
121.3
共328兲
4-isopropylbenzylidene t-butylamine N-oxide
101.8⫾4.1
共298兲
1,4-di-tert-butylbenzene
共288 –333兲
82.1⫾0.4
共310兲
82.8⫾0.4
共298兲
共285–325兲
82.8
共305兲
2,6-di-tert-butylphenol
84.6⫾0.5
共298兲
81.5⫾2.3
共298兲
U110.9
共298兲
2,4-di-tert-butylphenol
共288 –327兲
86.1⫾0.3
共308兲
86.7⫾0.3
共298兲
92.9⫾2.8
共298兲
3,5-di-tert-butylphenol
97.7⫾3.7
共298兲
共302–325兲
68.2
共313.5兲
4-tert-octylphenol
共297–351兲
96.3⫾0.9
共324兲
97.9⫾0.9
共298兲
3,5-di-tert-butyl-1,2-dihydroxybenzene
共313–346兲
103.7⫾0.5
共330兲
104.7⫾0.5
共298兲
100.1⫾0.6
共298兲
2,5-di-tert-butyl-1,4-dihydroxybenzene
共333–368兲
108.8⫾1.7
共351兲
122.4⫾1.7
共298兲
dicyclohexyl peroxydicarbonate
100.4⫾4.2
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
Method
Reference
GS
关87/19兴关91/18兴
关2717-39-7兴
关74/14兴关77/1兴
C
GS
ME
ME
TSGC
HSA
CGC–DSC
ME
BG
TSGC
B
CGC–DSC
C
T
ME,RG
GS
C
C
GS
C
GS
GS
C
GS
关43121-43-3兴
关97/6兴
关20666-86-8兴
关71/11兴关77/1兴
关81-14-1兴
关53/7兴关60/1兴
关30545-23-4兴
关80/4兴
关180988-52-7兴
关98/26兴
关1540-80-3兴
关98/5兴
关98/5兴
关64/1兴关70/1兴
关1079-71-6兴
关71/1兴关77/1兴
关2292-79-7兴
关75/2兴
关71/9兴
关30545-14-3兴
关80/4兴关75/2兴
关30545-24-5兴
关80/4兴关75/2兴
关30651-03-7兴
关80/4兴关75/2兴
关14098-44-3兴
关00/11兴
关87/4兴关60/20兴
关121678-88-4兴
关89/15兴
关1012-72-2兴
关98/14兴
关98/14兴
关51/5兴关87/4兴
关128-39-2兴
关99/17兴
关99/21兴
关71/24兴关99/17兴
关96-76-4兴
关99/13兴
关99/13兴
关99/21兴
关1138-52-9兴
关01/17兴
关87/4兴
关124765-79-3兴
关99/13兴
关99/13兴
关1020-31-1兴
关00/21兴
关00/21兴
关84/20兴
关88-58-4兴
关99/28兴
关99/28兴
关1561-49-5兴
关71/11兴关77/11兴
ENTHALPY OF SUBLIMATION
615
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
Compound
Temperature range 共K兲
C14H26O
共293–313兲
trans-anti-trans perhydroanthracene
共269–313兲
共275–313兲
trans-syn-trans perhydroanthracene
共293–335兲
共335–393兲
1,3,5,7-tetramethyladamantane
共310–350兲
共295–315兲
cyclotetradecanone
C14H28
cyclotetradecane
C14H28O
共300–321兲
共295–307兲
共285–290兲
2-tetradecanone
C14H24
C14H24
C14H24
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
100.4⫾8.3
Method
Reference
共303兲
ME
66.1
72.7⫾3.3
共284兲
共294兲
ME
88.1
87.4⫾2.4
共308兲
共365兲
ME
83.7⫾1.3
81.1⫾10.9
共298兲
共305兲
BG
TSGC
95.6
97.9⫾1.7
134.8⫾1.5
89.3⫾0.4
共298兲
共310兲
共301兲
共287兲
CGC–DSC
HSA
ME
TM
130.9⫾0.5
共298兲
C
174
139.7⫾3.8
共318兲
TPTD
ME
关62/3兴关70/1兴
关28071-99-0兴
关87/4兴
关63/2兴关70/1兴
关1755-19-7兴
关87/4兴
关63/2兴关70/1兴
关1687-36-1兴
关77/11兴
关75/2兴
关295-17-0兴
关38/1兴关60/1兴
关295-17-0兴
关98/5兴
关92/1兴
关64/1兴关70/1兴
关55/5兴
关2345-27-9兴
关79/8兴
关544-63-8兴
关01/15兴
关61/1兴关70/1兴
关19816-73-0兴
关80/23兴
关638-58-4兴
关59/3兴关87/4兴
关629-59-4兴
关72/1兴
关112-72-1兴
关77/17兴
关65/6兴
关886-38-4兴
关85/3兴
关76/9兴关87/4兴
80.75
C14H30
tetradecanoic acid 共myristic acid兲
共282–305兲
共312–325兲
peroxytetradecanoic acid
共293–303兲
tetradecanamide
共248 –375兲
n-tetradecane
C14H30O
1-tetradecanol
C14H28O2
C14H28O3
C14H29NO
C15H10O
C15H10O2
C15H10O3
C15H10O3
C15H11F3 O3
C15H11F3 O3
C15H11F3 O3
C15H11N
C15H11NO2
C15H11NO2
C15H11NO4
共293–307兲
diphenylcyclopropenone
共353–378兲
共323–343兲
␣-benzoyloxyphthalide
共343–388兲
1-methoxy-9,10-anthraquinone
156.0⫾4.1
ME
167.4⫾2.5
共352兲
ME
117.6
共298兲
B
126.0⫾0.6
143.9
共300兲
ME
119.7⫾8
141⫾4
共365兲
共333兲
HSA
ME
U 125.3
共366兲
128.0
106.6
共385兲
GS
HSA
共419兲
GS
HSA
共338兲
EV
共318兲
EV
共323兲
EV
共344兲
共298兲
ME
2-methoxy-9,10-anthraquinone
124.7
118.4⫾0.4
2-hydroxy-2 ⬘ -trifluoromethyl-4-methoxybenzophenone
共323–363兲
U 13.3
2-hydroxy-3 ⬘ -trifluoromethyl-4-methoxybenzophenone
共313–323兲
103.8
2-hydroxy-4 ⬘ -trifluoromethyl-4-methoxybenzophenone
共313–333兲
91
2-phenylquinoline
共337–351兲
103.1⫾0.8
105.4⫾0.9
1-amino-2-methyl-9,10-anthraquinone
共360–388兲
124.6⫾7.3
1-共N-methylamino兲-9,10-anthraquinone
112.6
共363–383兲
115.9⫾3.5
共384 – 405兲
123.8⫾3.3
123.8⫾3.2
115.5⫾0.4
114.7⫾3
1-amino-2-methoxy-4-hydroxy-9,10-anthraquinone
132.0
共374兲
共373兲
共395兲
共461兲
共406兲
ME
ME
HSA
HSA
关89/9兴
关82-39-3兴
关87/19兴关91/18兴
关56/1兴
关3274-20-2兴
关87/19兴关91/18兴
关56/1兴
关3119-86-6兴
关87/4兴关66/6兴
关7396-89-6兴
关87/4兴关66/6兴
关7396-90-9兴
关87/4兴关66/6兴
关612-96-4兴
关97/14兴
关82-28-0兴
关84/35兴
关82-38-2兴
关84/40兴
关84/35兴
关60/8兴关87/4兴
关64/11兴关91/18兴
关66/18兴
关56/1兴
关56/1兴
关84/40兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
616
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
⌬ subH m /kJ mol⫺1
CAS registry number
(Tm /K)
Polymorph
Temperature range 共K兲
C15H11N3 O2
4-hydroxy-3-共phenylazo兲-2(1H)-quinolinone 共Disperse Yellow 4兲
127.2
9-methylanthracene
98.9
1-amino-4-共N-methylamino兲anthra-9,10-quinone
140.6
1,4-diamino-2-methoxyanthra-9,10-quinone
147.0
151.9
dibenzosuberone
109.3
共298兲
5,7-dihydro-6H-dibenzo关a,c兴cyclohepten-6-one
共333–347兲
93.4⫾0.8
共340兲
95.6⫾0.8
共298兲
dibenzoylmethane
115.7⫾0.9
共298兲
gallocyanine 共C.I. Disperse Blue 95兲
共433– 493兲
88.2
共448兲
N-benzoyl-N-methylbenzamide
共246 –269兲
116.8⫾0.4
共356兲
120.1⫾0.4
共298兲
4-共N-methyl-N-2-hydroxyethylamino兲-4 ⬘ -nitro-2 ⬘ ,6⬘ -dichloroazobenzene
135.1
N,N-dimethyl-4-关关4-共trifluoromethyl兲phenyl兴azo兴benzenamine
95.8
N,N-dimethyl-4-关关4-共trifluoromethoxy兲phenyl兴azo兴benzenamine
96.8
N,N-dimethyl-4-关关4-关共trifluoromethyl兲thio兴phenyl兴azo兴benzenamine
100.8
N,N-dimethyl-9-acridinamine
86
共510兲
N-methyl-10-methylacridinimine
72
共480兲
4,5,6-trimethylbenzoxalene
139.7⫾2.5
1,3-diphenyl-2-propanone
89.1⫾5
C15H12
C15H12N2 O2
C15H12N2 O3
C15H12O
C15H12O
C15H12O2
C15H13ClN2 O5
C15H13NO2
C15H14Cl2 N4 O3
C15H14F3 N3
C15H14F3 N3 O
C15H14F3 N3 S
C15H14N2
C15H14N2
C15H14O
C15H14O
C15H14O2
C15H14O2 S
C15H14O2 S
C15H14O4
C15H14O5
C15H15N3 O2
C15H16N4 O2
C15H16N4 O2
C15H16O2
C15H17NO2
Method
RG
GS
GS
B
GS
GS
ME
ME
UV
UV
UV
TGA
TGA
2,2-diphenyl-1,3-dioxalane
99.7⫾1.1
共Z兲-1-methyl-4-共2-phenylethenyl兲sulfonyl benzene
116.3⫾3.8
共E兲-1-methyl-4-共2-phenylethenyl兲sulfonyl benzene
108.4⫾2.5
2-hydroxy-4,4⬘ -dimethoxybenzophenone
121.1
2,2⬘ -dihydroxy-4,4⬘ -dimethoxybenzophenone
130.2
147.0
N-关4-关共2-hydroxy-5-methylphenyl兲azo兴phenyl兴acetamide
共Disperse Yellow 3兲
共403– 465兲
107
140.6
3-methyl-3 ⬘ -nitro-4-N,N-dimethylaminoazobenzene
共368 –393兲
101.7⫾1.7
共370–388兲
98.7⫾2.5
3-methyl-4 ⬘ -nitro-4-N,N-dimethylaminoazobenzene
共369–392兲
125.5⫾1.3
共371–390兲
126.4⫾3.8
dimethoxydiphenylmethane
103.9⫾1.7
N-共2-hydroxy-3-phenoxypropyl兲phenylamine
共323–333兲
99.9
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
共298兲
B
B
B
B
UV
共434兲
GS
共381兲
共379兲
ME
TE
共381兲
共381兲
TE
ME
共298兲
共328兲
Reference
关6407-80-3兴
关68/10兴关88/24兴
关779-02-2兴
关58/4兴
关1220-94-6兴
关67/16兴关91/18兴
关2872-48-2兴
关84/40兴
关67/16兴关91/18兴
关1210-35-1兴
关98/21兴
关1139-82-8兴
关98/21兴
关98/21兴
关120-46-7兴
关92/28兴
关1562-85-2兴
关87/4兴
关23825-32-3兴
关97/12兴
关97/12兴
关6232-56-0兴
关68/10兴关88/24兴
关405-82-3兴
关84/39兴
关1494-75-3兴
关84/39兴
关1494-77-5兴
关84/39兴
关3295-59-8兴
关98/29兴
关213623-43-9兴
关98/29兴
关10435-68-4兴
关66/3兴关70/1兴
关102-04-5兴
关54/2兴关77/1兴
关70/1兴
关4359-34-6兴
关98/26兴
关54897-33-5兴
关69/11兴关77/1兴
关16212-08-1兴
关69/11兴关77/1兴
关631-38-0兴
关99/22兴
关131-54-4兴
关99/22兴
关60/24兴
关2832-40-8兴
关89/29兴
关68/10兴关88/24兴
关4313-14-8兴
关67/7兴
关67/7兴
关92114-99-3兴
关67/7兴关87/4兴
关67/7兴
关2235-01-0兴
关98/26兴
关16112-55-3兴
关87/4兴
ENTHALPY OF SUBLIMATION
617
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
C15H18N2
C15H21NO
C15H22
C15H22
C15H22
C15H22O2
C15H24
C15H24O
Compound
Temperature range 共K兲
113.8⫾2.1
4-isopropylaminodiphenylamine
共323–348兲
120.7
2-methyl-1-phenyl-2-N-piperidinyl-1-propanone
94.8⫾1.3
1-methyldiamantane
共310–333兲
80.7⫾0.4
3-methyldiamantane
共305–327兲
103.1⫾1.0
4-methyldiamantane
共310–333兲
79.4⫾1.25
3,5-di-tert-butylbenzoic acid
共339–357兲
108.4⫾4.2
1,3-di-tert-butyl-5-methylbenzene
共275–301兲
C15H28O2
CAS registry number
(Tm /K)
共335兲
Method
GS
B
共321兲
TSGC
共316兲
TSGC
共321兲
TSGC
共348兲
ME
82.4⫾0.5
81.8⫾0.5
共288兲
共298兲
T
91.9⫾3.2
86.8⫾0.8
88.0⫾0.8
87.8
U117.3
共298兲
共319兲
共298兲
共318兲
共298兲
C
GS
GS
GS
C
86.0⫾0.6
77.4
共305兲
ME
81.3
共300兲
ME
139.3⫾1.6
共298兲
C
137.7⫾2.1
共281兲
ME
2,6-di-tert-butyl-4-methylphenol
共303–343兲
C15H28O
⌬ subH m /kJ mol⫺1
cyclopentadecanone
共296 –315兲
pentadecanolide
共290–310兲
C15H30
cyclopentadecane
C15H30O
2-pentadecanone
C15H30O2
methyl tetradecanoate
C15H30O2
pentadecanoic acid
共283–305兲
N-methyl tetradecanamide
共332–347兲
n-pentadecane
74.6⫾0.4
C15H31NO
C15H32
C16F34
C16H6 Br4 N2 O2
C16H9 BrN2 O2
C16H10
C16H10
178
130.4⫾0.8
TPTD
共340兲
107.8
共298兲
n-perfluorohexadecane
共288 –303兲
104.6
共295兲
5,7-dibromo-2-共5,7-dibromo-1,3-dihydro-3-oxo-2H-indol-2-ylidene兲1,2-dihydro-3H-indol-3-one 共C.I. Vat Blue 5兲
共519– 634兲
129
共577兲
5-bromo-2-共1,3-dihydro-3-oxo-2H-indol-2-ylidene兲-1,2-dihydro-3Hindol-3-one 共C.I. Vat Blue 3兲
共519– 634兲
57
共577兲
fluoranthene
共313– 453兲
98.3
共383兲
共283–323兲
84.6⫾0.9
共303兲
99.2⫾0.8
共298兲
共328 –353兲
102.1⫾2
共340兲
共298 –358兲
102.6
共328兲
pyrene
共308 –398兲
103.1⫾6.5
共353兲
共313– 453兲
97.9
共383兲
共369–383兲
100.3⫾0.3
共353兲
共283–323兲
91.2⫾0.5
共303兲
共398 – 423兲
100.2⫾0.4
共410兲
101.0⫾0.5
GS
B
ME
Reference
关76/19兴
关101-72-4兴
关71/19兴
关13430-30-3兴
关94/11兴
关26460-76-4兴
关75/2兴
关38375-86-2兴
关75/2兴
关30545-18-9兴
关75/2兴
关16225-26-6兴
关74/15兴关87/4兴
关77/1兴
关15181-11-0兴
关98/14兴
关98/14兴
关128-37-0兴
关01/17兴
关99/17兴
关99/17兴
关87/4兴关71/19兴
关71/24兴关99/17兴
关502-72-7兴
关97/13兴
关38/1兴关60/1兴
关70/1兴
关32539-85-8兴
关87/4兴关60/1兴
关54/4兴
关295-48-7兴
关57/1兴关70/1兴
关2345-28-0兴
关79/8兴
关124-10-7兴
关65/6兴
关1002-84-2兴
关01/15兴
关7438-09-7兴
关59/4兴关87/4兴
关629-62-9兴
关72/1兴
关355-49-7兴
关51/9兴关87/4兴
关2475-31-2兴
GS
关86/14兴
关6492-73-5兴
GS
关86/14兴
关206-44-0兴
关95/7兴
关83/11兴
关72/1兴关77/1兴
关65/3兴关70/1兴
关58/1兴
关129-00-0兴
关98/3兴
关95/7兴
关88/26兴
关83/11兴
关80/26兴
关74/4兴
GS
GS
C
ME
ME
GS
PG
GS
IPM
C
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
618
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
Compound
Temperature range 共K兲
共348 – 419兲
C16H10O
C16H10N2 O2
C16H10O
C16H10S
C16H12N2 O
C16H12O
C16H12S2
C16H13N
C16H13N
C16H13NO
C16H13NO
C16H13NO2
C16H13NO3
C16H13NO5
C16H14
C16H14
C16H14
C16H14
C16H14
C16H14
C16H14
C16H14Cl2 O2
C16H14F4 N4 O2
C16H14N2 O2
C16H15NO
C16H16
⌬ subH m /kJ mol⫺1
CAS registry number
(Tm /K)
100.8⫾1.5
95.7
共298 –363兲
100.5
共330兲
共345–358兲
100.1⫾1.7
共351兲
1-hydroxypyrene
共369–394兲
129.0⫾3.2
共382兲
2-共1,3-dihydro-3-oxo-2H-indol-2-ylidene兲-1,2-dihydro-3H-indol-3-one
共C.I. Vat Blue 1兲
共519– 634兲
136
共577兲
2,3,5,6-dibenzoxalene 共benz关b兴indeno关1,2-e兴pyran兲
共375–388兲
125.9
共381.5兲
129.4⫾1.3
1,2-benzodiphenylene sulfide
共325–373兲
111.9⫾1.2
共349兲
2-hydroxy-1-phenylazonaphthalene
共350–374兲
116.7⫾5.4
共362兲
2,5-diphenylfuran
102
共340兲
3,6-diphenyl-1,2-dithiin
174.5⫾2.5
共355兲
183.1⫾2.5
共298兲
N-phenyl-1-naphthylamine
共313–333兲
96.5
共323兲
N-phenyl-2-naphthylamine
共333–363兲
115.8
共348兲
9-acetamidoanthracene
共446 –500兲
134.8
共461兲
N-共4-hydroxyphenyl兲-2-naphthylamine
共373– 408兲
126.8
共390兲
1-共dimethylamino兲-9,10-anthraquinone
共396 – 408兲
U 3.6
共402兲
1-共2-hydroxyethylamino兲-9,10-anthraquinone
共403– 417兲
152.7⫾3.8
共410兲
1-amino-2-hydroxyethyl-4-hydroxy-9,10-anthraquinone
135.2
9,10-dimethylanthracene
共372–382兲
114.6
共377兲
共381– 434兲
103.2
共396兲
2,7-dimethylphenanthrene
106.7⫾0.8
4,5-dimethylphenanthrene
共313– 453兲
85.7
共383兲
104.6⫾1.3
9,10-dimethylphenanthrene
119.5⫾1.3
1-phenylnaphthalene
共313– 453兲
88.6
共383兲
1,4-diphenylbutadiene
87.0
4,5,9,10-tetrahydropyrene
共385– 410兲
90.4
共400兲
1,1-dichloro-2,2-bis-共4-methoxyphenyl兲ethylene
79.2
N-methyl-N-共2,2,3,3-tetrafluoropropyl兲-4-关共4-nitrophenyl兲azobenzenamine
100.8
1,4-bis共N-methylamino兲anthra-9,10-quinone
共385– 413兲
151.8⫾3.9
共399兲
150.2
3-anilino-1-phenylbut-2-enone
126.8⫾3.0
共298兲
关2.2兴-para-cyclophane
共353– 409兲
96.4⫾1.5
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
Method
Reference
ME
ME
关74/4兴
关53/1兴关77/1兴
关70/1兴
关58/1兴
关52/3兴
关5315-79-7兴
关98/3兴
ME
ME
ME
GS
ME
GS
GS
RG
GS
ME
RG
ME
GS
ME
GS
RG
IPM
UV
GS
C
TSGC
关482-89-3兴
关86/14兴
关243-24-3兴
关87/4兴
关66/3兴关70/1兴
关239-35-0兴
关98/3兴
关842-07-9兴
关84/35兴
关955-83-9兴
关89/7兴
关16212-85-4兴
关73/23兴关77/1兴
关73/23兴关77/1兴
关90-30-2兴
关87/4兴关71/19兴
关135-88-6兴
关87/4兴关71/19兴
关37170-96-0兴
关58/4兴关87/4兴
关93-45-8兴
关71/19兴
关5960-55-4兴
关87/4兴
关4465-58-1兴
关60/8兴关66/18兴
关84/40兴
关781-43-1兴
关87/4兴
关58/4兴关87/4兴
关1576-69-8兴
关65/5兴关70/1兴
关3674-69-9兴
关95/7兴
关65/5兴关70/1兴
关604-83-1兴
关66/3兴关70/1兴
关605-02-7兴
关95/7兴
关866-65-7兴
关58/4兴
关781-17-9兴
关93/7兴
关4359-34-6兴
关95/32兴关89/32兴
关80135-84-8兴
关84/39兴
关2475-44-7兴
关84/35兴
关67/16兴关91/18兴
关18594-93-9兴
关93/24兴
关1633-22-3兴
关80/15兴
ENTHALPY OF SUBLIMATION
619
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
C16H16
C16H16
Compound
(Tm /K)
共343–383兲
96.3⫾4.2
92.9⫾0.84
共363兲
ME
关2.2兴-meta-cyclophane
共308 –332兲
91.6⫾1.7
共320兲
ME
92.0⫾2
共298兲
ME
86.6
共336兲
ME
87.5⫾0.9
共298兲
ME
101.0⫾1.4
共298兲
92.3
共398兲
IPM
43.1⫾4.2
共303兲
ME
共401兲
共298兲
ME
Temperature range 共K兲
关2.2兴-meta-para-cyclophane
共311–328兲
C16H16
1,1-bis-共4-methylphenyl兲ethane
C16H16
1,2,3,6,7,8-hexahydropyrene
共390– 405兲
␣,␣-dimethylbenzyl perbenzoate
共293–313兲
pentamethoxycarbonylbenzene
共389– 413兲
C16H16O3
C16H16O10
C16H17ClN4 O3
C16H17F
C16H17NO
C16H17NO
C16H18
C16H18
C16H18NO5
C16H18N2 O3
C16H18N2 O2
C16H18N4 O2
C16H18N4 O3
C16H19N3
C16H23N
C16H24N2 O2
C16H26O
C16H28
CAS registry number
⌬ subH m /kJ mol⫺1
160.0⫾0.8
165.1⫾0.8
4-共N-ethyl-N-2-hydroxyethylamino兲-4 ⬘ -nitro-2 ⬘ -chloroazobenzene
142.7
2-fluoro-2-methyl-1,3-diphenylpropane
102.2⫾1.1
1,2-diphenyl-2-N,N-dimethylamino-1-ethanone
140.1⫾1.9
N-共4-isopropylphenylmethylene兲 benzenamine N-oxide
127.2⫾1.7
共dl兲 1,3-diphenylbutane
共288 –303兲
73.6
2,3-diphenylbutane
共293–348兲
96.7
bis共2,4-dimethoxyphenyl兲nitrogen oxide
共333–363兲
144.1⫾11.4
p-azoxyphenetole
126.2⫾2.7
2,2⬘ ,6,6 ⬘ -tetramethylazobenzene-N,N-dioxide
107⫾12
4-共N,N-diethylamino兲-4 ⬘ -nitroazobenzene
146.0
共422– 441兲
151.5⫾4.2
4-共N-ethyl-N-2-hydroxyethylamino兲-4 ⬘ -nitroazobenzene
136.8
189.5
共420– 433兲
176.6⫾1.3
4-共N,N-diethylamino兲azobenzene
132.2
共330–353兲
91.4⫾2.9
106.4
103.4
N-cyclohexyl-共2,4,6-trimethyl兲benzaldehyde imine
104.9⫾0.8
N-benzoyl-N⬘ ,N⬘ -diisobutylurea
137.5⫾4.4
2,4,5-triisopropylbenzyl alcohol
共313–346兲
113.0
tricyclo关 8.2.2.24,7兴 hexadecane
共316 –338兲
85.2⫾1.3
C16H30N2
共316 –338兲
tetracyclopropylsuccinonitrile
C16H30O
cyclohexadecanone
91.6⫾2.1
110.2⫾1.5
Method
Reference
共298兲
B
关73/13兴关77/1兴
关66/11兴关87/4兴
关70/1兴
关2319-97-3兴
关69/6兴关77/1兴
关87/4兴
关69/6兴关77/1兴
关5385-36-4兴
关69/6兴关77/1兴
关87/4兴
关69/6兴关77/1兴
关2919-20-2兴
关99/19兴
关1732-13-4兴
关93/7兴
关7074-00-2兴
关71/11兴关77/1兴
关3327-06-8兴
关95/6兴
关67/8兴关95/6兴
关3180-81-2兴
关68/10兴关88/24兴
关193472-70-7兴
关97/34兴
关15582-77-5兴
关94/11兴
关99081-88-6兴
关86/10兴
关1520-44-1兴
关74/6兴关87/4兴
关5789-35-5兴
关84/16兴
关3788-15-6兴
关87/4兴关65/7兴
关4792-83-0兴
关93/11兴
关101225-69-8兴
关93/3兴
关3025-52-3兴
关87/19兴关91/18兴
关60/8兴
关2872-52-8兴
关84/39兴关84/40兴
关68/10兴关88/24兴
关60/8兴关66/18兴
关2481-94-9兴
关87/19兴关91/18兴
关84/35兴
关84/39兴
关84/40兴
关199394-72-4兴
关97/18兴
共298兲
C
关00/28兴
共298兲
B
共298兲
C
共296兲
ME
共326兲
共348兲
共298兲
C
共298兲
ME
共431兲
GS
ME
UV
共426兲
ME
GS
共342兲
UV
共330兲
共327兲
ME
共298兲
ME
关63/13兴
关283-68-1兴
关69/6兴关77/1兴
关87/4兴
关69/6兴关77/1兴
关19219-01-3兴
关84/22兴
关2550-52-8兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
620
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C16H30O4
hexadecanedioic acid
共377–398兲
⌬ subH m /kJ mol⫺1
CAS registry number
(Tm /K)
Method
82
C16H32
cyclohexadecane
C16H32O2
hexadecanoic acid 共palmitic acid兲
共294 –316兲
共320–333兲
151.0⫾3.3
155.4⫾3.3
共388兲
共298兲
ME
81.8⫾0.4
C16H33NO
C16H34
C16H34O
C17H10O
hexadecanamide
共364 –378兲
hexadecane
共288 –290兲
1-hexadecanol
共323–335兲
共308 –320兲
benzanthrone
共389– 409兲
共353–388兲
C17H12
C17H12
C17H13N
C17H14N2 O2
C17H16F4 N4 O2
C17H16F4 N4 O3
C17H16OS
C17H16O4
C17H17N5 O2
C17H18O3
C17H18O4
C17H20O2
C17H21NO4
C17H32O
C17H34
benzo关a兴fluorene
共313– 453兲
benzo关b兴fluorene
共344 –398兲
共313– 453兲
N-methyl-2,3,5,6-dibenzazalene
154
154.4⫾4.2
共326兲
TPTD
ME
181.6⫾1.3
共371兲
ME
135.1
134.9
83.4⫾8
共298兲
共291兲
B
B
ME
109.4 共liq兲
167.4⫾2.1
169.5⫾2.1
共329兲
共314兲
共298兲
121.6⫾0.6
126.6⫾0.6
129.7⫾2.1
119.7⫾5.4
124.6⫾6.0
114.2⫾0.8
115.5
共399兲
共298兲
共298兲
共370兲
共298兲
105.4
共383兲
GS
119.3⫾1.3
111.2
共371兲
共383兲
ME
GS
66.1⫾0.6
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
ME
QR
ME
QR
共398兲
131.8⫾1.3
1-关共2-methoxyphenyl兲azo兴-2-hydroxynaphthalene
共374 –388兲
142.4⫾2.2
共381兲
N-ethyl-N-共2,2,3,3-tetrafluoropropyl兲-4-关4-nitrophenyl兴azobenzenamine
103.0
2-关关4-关共4-nitrophenyl兲azo兴phenyl兴共2,2,3,3-tetrafluoropropyl兲amino兴-ethanol
103.0
tetrahydro-2,6-diphenyl-4H-thiopyran-4-one
136.0
共375兲
144⫾3
共298兲
diphenylmethylene diacetate
共348 –388兲
122.1⫾1.2
共368兲
4-nitro-4 ⬘ -共N-2-cyanoethyl-N-ethylamino兲azobenzene
147.3
4-(tert-butylphenyl兲salicylate
共293–336兲
137.4
共308兲
2-hydroxy-4,4⬘ -diethoxybenzophenone
134.9
共298兲
diethoxydiphenylmethane
97.1⫾1.1
共298兲
cocaine
127.2
共294 –314兲
112.3⫾2.8
共304兲
cycloheptadecanone
75.7
cycloheptadecane
ME
UV
UV
ME
ME
GS
UV
B
GS
GS
Reference
关38/1兴关60/1兴
关505-54-4兴
关60/4兴关87/4兴
关60/4兴关99/10兴
关295-65-8兴
关57/1兴关70/1兴
关57-10-3兴
关01/15兴
关61/1兴关70/1兴
关87/4兴
关629-54-9兴
关59/3兴关87/4兴
关544-76-3兴
关72/1兴
关63/6兴
关49/1兴
关36653-82-4兴
关87/4兴
关65/6兴关87/4兴
关65/6兴
关82-05-3兴
关99/11兴
关99/11兴
关99/24兴
关84/12兴
关84/12兴
关79/28兴
关52/3兴关60/1兴
关238-84-6兴
关95/7兴
关243-17-4兴
关98/3兴
关95/7兴
关6626-64-8兴
关66/3兴关70/1兴
关1229-55-6兴
关84/35兴
关91488-84-5兴
关84/39兴
关1543-74-4兴
关84/39兴
关37014-01-0兴
关72/15兴
关72/15兴关77/1兴
关54334-63-3兴
关96/14兴
关84/40兴
关87-18-3兴
关87/4兴关60/24兴
关101595-31-7兴
关99/22兴
关6397-77-9兴
关98/26兴
关50-36-2兴
关96/19兴
关84/27兴
关3661-77-6兴
关38/1兴关60/1兴
关70/1兴
关295-97-6兴
关57/1兴关70/1兴
ENTHALPY OF SUBLIMATION
621
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C17H34O2
C17H36
methyl hexadecanoate
共291–301兲
heptadecanoic acid 共margaric acid兲
共291–316兲
N-methyl hexadecanamide
共345–355兲
heptadecane
C17H36O
共288 –293兲
1-heptadecanol
C17H34O2
C17H35NO
C18H10
C18H10BrNO3
C18H10Cl2 O2 S2
C18H10Cl2 O2 S2
C18H10O2
C18H10O2
C18H10O4
C18H11NO3
C18H12
C18H12
C18H12
(Tm /K)
152.3⫾2
共296兲
168
Method
ME
TPTD
144.5⫾0.8
共350兲
GS
125.1
131.3⫾13
共298兲
共290兲
ME
169.5⫾2.2
benzo关3,4兴cyclobuta关1,2-a兴biphenylene 共关3兴phenylene兲
115.1⫾0.8
2共4-bromo-3-hydroxy-2-quinolinyl兲-1H-indene-1,3(2H)-dione
共C. I. Disperse Yellow 64兲
共483–523兲
130.6
共498兲
6-chloro-2-共6-chloro-4-methyl-3-oxobenzo关b兴thien-2(3H)-ylidine兲4-methyl-benzo关b兴thiophen-3(2H)-one 共C.I. Vat Red 1兲
共519– 634兲
148
共577兲
5-chloro-2-共5-chloro-7-methyl-3-oxobenzo关b兴thien-2(3H)-ylidine兲7-methyl-benzo关b兴thiophen-3(2H)-one 共C.I. Vat Violet 2兲
共519– 634兲
93
共577兲
1,2-benzanthra-9,10-quinone
82.8⫾4.0
5,12-tetracenequinone
108.8⫾5.0
6,11-dihydroxy-5,12-naphthacenedione
共426 – 446兲
144.2⫾1.4
共436兲
2-共3-hydroxy-2-quinolinylidene兲-indeno-1,3-dione 共Disperse Yellow 54兲
125.2⫾0.4
共483–513兲
139
共498兲
benz关a兴anthracene 共1,2-benzanthracene, tetraphene兲
共313– 453兲
115.5
共383兲
共330–390兲
113.4
共345兲
104⫾2
共351兲
共283–323兲
U 81.3⫾2.5
共303兲
共373–396兲
123.3⫾3
共298兲
共357– 454兲
120.5
共405兲
共377– 403兲
104.6⫾4.2
共390兲
共333–393兲
119.7
共363兲
U 109.2
triphenylene
共313– 453兲
114.5
共383兲
共381– 406兲
126.5⫾4
共298兲
共363– 468兲
107.6
共378兲
共338 –398兲
118⫾4
共368兲
107.1
共425兲
naphthacene 共tetracene兲
共386 – 472兲
126.1⫾9.0
共429兲
共313– 453兲
126.5
共383兲
共419– 446兲
143.7⫾0.5
共298兲
124.7⫾4
共422兲
共433– 493兲
共433– 483兲
C18H12
CAS registry number
⌬ subH m /kJ mol⫺1
128.8
132.6
117.2
U92.0
124.3
benzo关c兴phenanthrene 共3,4-benzophenanthrene兲
106.3⫾4.2
共473兲
共468兲
共459兲
共384兲
Reference
关112-39-0兴
关65/6兴关87/4兴
关506-12-7兴
关01/15兴
关7388-58-1兴
关59/4兴关87/4兴
关629-78-7兴
关72/1兴
关49/1兴关60/1兴
关1454-85-9兴
关65/6兴关70/1兴
关65513-20-4兴
关00/18兴
关10319-14-9兴
关87/4兴
关2379-74-0兴
GS
关86/14兴
关5462-29-3兴
GS
关86/14兴
关2498-66-0兴
关56/5兴关70/1兴
关1090-13-7兴
关56/5兴关70/1兴
关1785-52-0兴
关98/3兴
关7576-65-0兴
关98/38兴
关73/6兴
关56-55-3兴
关95/7兴
关87/4兴关74/30兴
关83/27兴
关83/11兴
关80/1兴
关67/2兴
关64/3兴关87/4兴
关58/1兴
关51/2兴关60/1兴
关217-59-4兴
关95/7兴
关80/1兴
关87/4兴
关58/1兴关70/1兴
关67/2兴
关92-24-0兴
关98/3兴
关95/7兴
关80/1兴
关67/2兴关77/1兴
关70/1兴
关65/15兴
关64/10兴
关52/3兴关60/1兴
关51/12兴
关51/2兴关60/1兴
关195-19-7兴
关51/2兴关70/1兴
关67/2兴
ME
LE
GS
ME
TE
GS
ME
ME
GS
TE,ME
ME
ME
GS
TE,M
ME
HSA
HSA
ME
ME
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
622
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C18H12
chrysene
共313– 453兲
共353– 418兲
C18H12N2
C18H12O
C18H14
2,2⬘ -biquinoline
共393– 411兲
2-phenylindeno关2,1-b兴pyran
共394 – 424兲
5,12-dihydrotetracene
共338 –398兲
C18H14
diphenylfulvene
C18H14
o-terphenyl
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
118.8
131⫾4
117.6⫾4
121.4
117.6
共383兲
共298兲
共400兲
共385兲
GS
TE,ME
ME
129.5⫾0.8
134.7⫾1.3
96.6⫾0.9
共402兲
共298兲
ME
132.8
共409兲
115.9⫾4
120.5
共368兲
104.6⫾8.3
C18H14
C18H14
C18H14O
C18H15N
C18H15NO2
m-terphenyl
共329–353兲
共313–363兲
p-terphenyl
共353–383兲
共333–393兲
2,6-diphenylphenol
共334 –363兲
triphenylamine
共322–373兲
9-diacetylaminoanthracene
E
101.2⫾0.5
97⫾1
共298兲
共298兲
B
B
115.5⫾1.6
118.1⫾1.6
120⫾1
119
共341兲
共298兲
共298兲
共338兲
T
116.2⫾2.4
120.4⫾2.4
113⫾2
118.4
120.6
共368兲
共298兲
共298兲
共397兲
共363兲
T
116.1⫾1.1
119.1⫾1.1
共348兲
共298兲
T
87.9⫾1.3
共337兲
106.4
C18H15OP
C18H15P
triphenylphosphine oxide
共385– 408兲
triphenyl phosphate
C18H15PS
triphenylphosphine sulfide
共388 – 419兲
C18H18
dihydrodibenzotetra-aza-annulene
共443–583兲
2,4,5,7-tetramethylphenanthrene
C18H18
3,4,5,6-tetramethylphenanthrene
C18H18
9-butylanthracene
共293–313兲
3-diphenylmethyl-2,4-pentanedione
共348 –383兲
2,2⬘ -diphenyl-bi-共1,3-dioxolan-2-yl兲
共320–362兲
hexamethoxycarbonylbenzene
C18H18O2
C18H18O4
C18H18O12
B
ME
RG
131⫾2
66⫾6
共399兲
共298兲
113.2⫾3.0
109.2⫾1.1
96.2⫾8.4
共298兲
共350兲
共298兲
114.4⫾2.6
共298兲
B
136.8⫾6.1
142.8⫾6.8
共403兲
共298兲
HSA
81.5⫾6.4
共513兲
T
ME,TE
B
triphenylphosphine
C18H15PO4
C18H16N4
Method
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
114.2⫾1.7
ME
133.5⫾3.8
ME
108.1
共303兲
112.8⫾0.4
共366兲
T
132.8⫾2.1
共341兲
T
Reference
关218-01-9兴
关95/7兴
关80/1兴
关67/2兴关70/1兴
关58/1兴
关51/2兴关60/1兴
关119-91-5兴
关97/14兴
关97/14兴
关85/6兴
关10435-67-3兴
关87/4兴关66/3兴
关959-02-4兴
关58/1兴关70/1兴
关51/2兴关60/1兴
关2175-90-8兴
关57/2兴关70/1兴
关84-15-1兴
关97/15兴
关71/8兴
关92-06-8兴
关97/15兴
关97/15兴
关71/8兴
关58/1兴
关92-94-4兴
关97/15兴
关97/15兴
关71/8兴
关67/2兴
关58/1兴
关92-69-3兴
关98/9兴
关98/9兴
关603-34-9兴
关78/2兴关87/4兴
关3808-37-5兴
关58/4兴
关791-28-6兴
关89/28兴
关78/11兴
关603-35-0兴
关88/21兴
关84/13兴
关82/20兴关60/9兴
关115-86-6兴
关89/23兴
关3878-45-3兴
关96/9兴
关96/9兴
关22119-35-3兴
关83/29兴
关7396-38-5兴
关65/5兴关70/1兴
关7343-06-8兴
关65/5兴关70/1兴
关1498-69-7兴
关87/4兴关64/15兴
关19672-37-8兴
关95/2兴
关25062-95-7兴
关95/13兴
关6237-59-8兴
ENTHALPY OF SUBLIMATION
623
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
Compound
Temperature range 共K兲
共403– 422兲
C18H20
C18H20O4
C18H21N
C18H22
C18H22N2 O2
C18H22N4
C18H22O2
C18H22O4
C18H24
C18H29NO
C18H29NO2
C18H30
C18H30
C18H30
C18H30
C18H30O
C18H30O4
C18H31N
C18H34O
C18H36O2
C18H36O2
C18H37NO
C18H38
C18H38
关3.3兴para-cyclophane
共322–343兲
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
140.7⫾1.1
154.3⫾1.2
97.8⫾0.8
共322–343兲
103.3⫾1.0
2-hydroxy-4-butoxy-4 ⬘ -methoxybenzophenone
126.3
N-benzyl-pivalophenone imine
109.7⫾3.3
2,3-dimethyl-2,3-diphenylbutane
共293–348兲
96.7⫾0.8
2,2⬘ ,4,4 ⬘ ,6,6 ⬘ -hexamethylazobenzene-N,N-dioxide
107⫾12
2,3-dimethyl-2,3-bis共phenylazo兲butane
113.8⫾1.8
共dl兲-2,3-dimethoxy-2,3-diphenylbutane
共322–355兲
114.2⫾6.3
1,2-diphenyl-1,1,2,2-tetramethoxyethane
共351–399兲
77.6⫾0.6
1,2,3,4,4a,7,8,9,10,11,12,12a-dodecahydrochrysene
共293–313兲
115.4
2,4,6-tri-tert-butylnitrosobenzene
91.0⫾3.2
2,4,6-tri-tert-butylnitrosobenzene
94.8⫾1.0
96.4⫾1.0
81.4⫾1.8
1,3,5-tri-tert-butylbenzene
共298 –341兲
79.9⫾0.3
81.2⫾0.3
共273–315兲
79.7⫾0.4
hexaethylbenzene
共327–352兲
95.0⫾4.0
U 41.3⫾0.9
perhydrochrysene
共273–353兲
82.3 共liq兲
1-phenyldodecane
135.1
2,4,6-tri-tert-butylphenol
87.5⫾0.4
共295–339兲
85.6⫾0.4
共415–551兲
63.2 共liq兲
U128.1
共292–313兲
83.9
84.2⫾0.5
4-diacetylbenzene diethyl ketal
共306 –327兲
112.5
2,4,6-tri-tert-butylaniline
92.5⫾1.1
cyclooctadecanone
77.4
octadecanoic acid 共stearic acid兲
共296 –319兲
158
共331–340兲
166.5⫾4.2
ethyl palmitate
共286 –294兲
150.8
octadecanamide
共367–379兲
195.8⫾4.2
1,1,2,2-tetra-tert-butylethane
共303–366兲
71.9
74.3
n-octadecane
Method
Reference
共413兲
共298兲
ME
共332兲
ME
共298兲
ME
关95/6兴
关95/6兴
关2913-24-8兴
关69/6兴关77/1兴
关87/4兴
关69/6兴关77/1兴
关39716-92-2兴
关99/22兴
B
共298兲
B
共320兲
共298兲
ME
B
共339兲
共375兲
T
共303兲
共298兲
C
共351兲
共298兲
共298兲
GS
GS
C
共319兲
共298兲
共294兲
T
共340兲
HSA
DSC
ME
共288兲
共298兲
共298兲
共317兲
共430兲
共298兲
共302兲
共298兲
GS
ME
C
V
共316.5兲
共298兲
GS
共336兲
TPTD
ME
共290兲
ME
共373兲
ME
共341兲
共298兲
关97/18兴
关1889-67-4兴
关83/16兴
关100046-00-2兴
关93/3兴
关133930-64-0兴
关93/14兴
关41047-48-7兴
关90/17兴
关39787-30-9兴
关95/13兴
关1610-22-6兴
关87/4兴关64/15兴
关24973-59-9兴
关95/20兴
关4074-25-3兴
关00/25兴
关00/25兴
关95/20兴
关1460-02-2兴
关98/14兴
关98/14兴
关65/6兴关87/4兴
关604-88-6兴
关86/1兴
关84/2兴
关2090-14-4兴
关87/4兴关64/15兴
关123-01-3兴
关00/10兴
关732-26-3兴
关99/17兴
关65/6兴关87/4兴
关87/4兴
关71/24兴关99/17兴
关60/14兴
关60/14兴关99/17兴
关47189-08-2兴
关78/9兴关87/4兴
关961-38-6兴
关00/6兴
关6907-37-5兴
关38/1兴关60/1兴
关57-11-4兴
关01/15兴
关61/1兴关70/1兴
关628-97-7兴
关87/4兴关67/18兴
关124-26-5兴
关59/3兴关87/4兴
关62850-21-9兴
关84/15兴
关84/15兴
关593-45-3兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
624
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
Compound
Temperature range 共K兲
共288 –298兲
C18H38O
C19H15N
C19H15N3
C19H16
C19H16F8 N4 O2
C19H16O
C19H16O2
C19H17NO2
C19H18O2
C19H20O2
C19H21NO
C19H34
C19H36O
C19H38O2
C19H38O2
C19H40
C20H12
C20H12
C20H12
C20H12
C20H12
1-octadecanol
共318 –329兲
N-phenyl benzophenone imine
共348 –387兲
triphenylazidomethane
共335–363兲
triphenylmethane
(Tm /K)
152.7
153.0⫾5
Method
Reference
共298兲
共293兲
C
ME
187.4⫾1.3
191.2⫾1.3
共324兲
共298兲
ME
115.5⫾1.8
119.7⫾1.8
共367兲
共298兲
T
120.6
共349兲
关72/1兴
关49/1兴关60/1兴
关70/1兴
关112-92-5兴
关65/6兴关87/4兴
关65/6兴
关574-45-8兴
关97/18兴
关97/18兴
关14309-25-2兴
关87/4兴关74/31兴
关519-73-3兴
关99/25兴
关98/5兴
关89/1兴
关86/8兴
关59/2兴关70/1兴
关86/17兴关36/2兴
关74/31兴
关91488-85-6兴
109.1
112.0
共343–363兲
113.9
共303–358兲
106.8
共325–349兲
100⫾0.4
100.7
105⫾0.8
N-ethyl-4-关共4-nitrophenyl兲azo兴-N-共2,2,3,3,4,4,5,5-octafluoropentyl兲benzenamine
112.6
triphenylmethanol
121.8⫾1.7
共353–373兲
122
2-fluorenyl-2-methyl-1,3-cyclopentandione
共353–388兲
122.3⫾1.6
1-piperidinoanthraquinone
共383–392兲
U 18.3 共387.5兲
2-diphenylmethyl-2-methyl-1,3-cyclopentandione
共355–393兲
120.2⫾1.1
3-diphenylmethyl-3-methyl-2,4-pentandione
114.4⫾0.6
共⫾兲1,2-diphenyl-2-N-piperidinyl-1-ethanone
147.1⫾1
tricyclohexylmethane
共301–321兲
117.4
cyclononadecanone
82.4
methyl octadecanoate
共299–310兲
158.2⫾2.5
nonadecanoic acid
198.7⫾5
n-nonadecane
143.6
共288 –303兲
136.6
perylene
共391– 424兲
132.6⫾3.6
共313– 453兲
123.2
共443–518兲
145.2⫾2.5
125.5⫾4.2
共383– 453兲
139
129.6⫾2.1
121.3
benzo关b兴fluoranthene
共313– 453兲
119.2
benzo关k兴fluoranthene
共363– 430兲
130
120⫾10
benzo关a兴pyrene
共313– 453兲
122.5
共358 – 431兲
118.3
benzo关e兴pyrene
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
CAS registry number
⌬ subH m /kJ mol⫺1
共298兲
共298兲
共353兲
共330兲
共339兲
共298兲
GS
CGC–DSC
EM
GS
V
UV
共298兲
共363兲
GS
共371兲
T
共374兲
T
共298兲
T,B
B
共311兲
共304兲
共298兲
共296兲
C
共408兲
共383兲
共298兲
共298兲
共418兲
共415兲
共370兲
ME
GS
C,ME
ME
共383兲
GS
ME
ME
共378兲
TE
共383兲
共373兲
GS
ME
关84/39兴
关76-84-6兴
关98/22兴
关87/4兴
关160731-89-5兴
关95/2兴
关4946-83-2兴
关87/4兴
关160731-87-3兴
关95/2兴
关137932-36-6兴
关95/2兴
关127529-16-2兴
关94/11兴
关1610-24-8兴
关87/4兴关64/15兴
关38/1兴关60/1兴
关112-61-8兴
关65/6兴关87/4兴
关646-30-0兴
关68/2兴关70/1兴
关629-92-5兴
关72/1兴
关64/15兴
关198-55-0兴
关98/3兴
关95/7兴
关73/7兴
关67/2兴关70/1兴
关58/1兴关87/4兴
关52/3兴
关51/12兴
关205-99-2兴
关95/7兴
关207-08-9兴
关87/4兴
关83/28兴
关50-32-8兴
关95/7兴
关87/4兴关74/30兴
关192-97-2兴
ENTHALPY OF SUBLIMATION
625
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
C20H12BrNO4
C20H13NO4
C20H14
C20H14
C20H14
C20H14N2 O2
C20H14N2 O4
C20H14O4
C20H15F3
C20H16
C20H16
C20H16
C20H16
C20H16O4 S2
C20H17N3 O2
C20H18
C20H18O6
C20H20
C20H20O2
C20H20O6
C20H21ClN6 O2
C20H22O2
C20H24O6
C20H30
C20H38O4
Compound
Temperature range 共K兲
⌬ subH m /kJ mol⫺1
CAS registry number
(Tm /K)
Method
共313– 453兲
117.9
共383兲
GS
共359– 423兲
119.1
共373兲
ME
1-amino-2-共4-bromophenoxy兲-4-hydroxy-9,10-anthraquinone
共373– 453兲
163.6
共413兲
1-amino-4-hydroxy-2-phenoxy-9,10-anthraquinone 共Disperse Red 60兲
共359–366兲
152.5
共362.5兲
141.8
共373– 453兲
103.8
共413兲
9,10-dihydro-9,10-(1 ⬘ ,2⬘ ) benzoanthracene 共tryptycene兲
104.6⫾12.6
9-phenylanthracene
共313– 453兲
118.7
共383兲
GS
共352–395兲
119.7
TE
共353– 426兲
115.3
共368兲
binaphthalene
共313– 453兲
138.3
共383兲
GS
1-anilino-4-amino-9,19-anthraquinone
138.6
共373– 453兲
135.1
共413兲
GS
1-amino-2-共4-aminophenoxy兲-4-hydroxy-9,10-anthraquinone
共373– 453兲
U50.2
共413兲
resorcinol dibenzoate
共323–399兲
165.8
共338兲
UV
1,1,1-trifluoro-2,2,2-triphenylethane
112.3⫾1.0
共298兲
1 ⬘ ,9-dimethyl-1,2-benzanthracene
112.5⫾3.3
ME
3 ⬘ ,6-dimethyl-1,2-benzanthracene
112.5⫾3.3
ME
7,12-dimethylbenz关a兴anthracene
共379–390兲
135
共379–396兲
107.8 共vap兲
5,6-dimethylchrysene
130⫾1.3
134⫾1.3
共379– 408兲
135⫾2.4
共394兲
ME
6-ethoxy-2-共6-ethoxy-3-oxobenzo关b兴thien-2(3H)-ylidene兲benzo关b兴thiophen-3共2H兲-one 共C.I. Vat Orange 5兲
共519– 634兲
65
共577兲
GS
N-共benzoyl兲-4-共2-hydroxy-4-methylphenylazo兲benzenamine
共Disperse Yellow 50兲
共464 – 484兲
69
共474兲
GS
1,1,1-triphenylethane
108.6
共298兲
9-fluorenyl-tris共methoxycarbonyl兲methane
132.6
共298兲
GS
pagodane (undecacyclo关 9.9.0.01,5.02,12.02,18.03,7.06,10.08,12.011,15.013,17.016,20兴 eicosane)
共418 – 473兲
90.2⫾2.3
共446兲
T
2-diphenylmethyl-2-ethyl-1,3-cyclopentanedione
共342–377兲
122.8⫾0.7
共360兲
T
1,1,1-tris共methoxycarbonyl兲-2,2-diphenylethane
136.0
共298兲
GS
N-2-关共2-chloro-6-cyano-4-nitrophenly兲azo兴-5-共diethylamino兲phenyl-propanamide
共Disperse
Blue 165兲
共464 – 484兲
90.7
共474兲
GS
3-diphenylmethyl-3-ethyl-2,4-pentanedione
共349–387兲
122.3⫾1.5
共368兲
T
dibenzo-18-crown-6
178.8⫾6.9
共298兲
CGC–DSC
hexacyclopropylethane
109.0⫾2.1
eicosanedioic acid
共380–395兲
165.7⫾3.3
共388兲
ME
Reference
关95/7兴
关87/4兴关74/30兴
关59722-76-8兴
关78/35兴
关17418-58-5兴
关87/4兴
关84/40兴
关78/35兴
关477-75-8兴
关73/13兴关77/1兴
关602-55-1兴
关95/7兴
关74/33兴
关58/4兴
关11068-27-2兴
关95/7兴
关4395-65-7兴
关84/40兴
关77/20兴关78/35兴
关56405-27-7兴
关78/35兴
关94-01-9兴
关87/4兴关60/24兴
关68643-31-2兴
关97/34兴
关313-74-6兴
关65/5兴关70/1兴
关316-51-8兴
关65/5兴关70/1兴
关57-97-6兴
关87/4兴关64/3兴
关87/4兴关64/3兴
关3697-27-6兴
关66/3兴关70/1兴
关66/3兴关70/1兴
关64/3兴
关3263-31-8兴
关86/14兴
关89/29兴
关15271-39-6兴
关99/25兴
关170464-52-5兴
关95/29兴
关89683-62-5兴
关94/9兴
关160731-88-4兴
关95/2兴
关170464-52-5兴
关95/29兴
关89/29兴
关160731-83-9兴
关95/2兴
关14187-32-7兴
关00/11兴
关26902-55-6兴
关84/32兴
关2424-92-2兴
关60/4兴关87/4兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
626
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C20H40O2
eicosanoic acid
共337–346兲
ethyl stearate
共297–306兲
n-eicosane
C20H40O2
C20H42
C20H42O
C21H6 N12O18
C21H14N2 O3
C21H14N2 O3
C21H15BrN2 O2
C21H15NO3
C21H16
C21H16N2 O2
C21H17N3 O3
C21H18F2
C21H19F
C21H19F
C21H20Cl2 O3
C21H23NO5
C21H24O2
C21H26
C21H26O4
C21H30O
C21H42O2
C21H42O2
C21H44
C22H10O2
C22H12
C22H12
1-eicosanol
共327–341兲
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
170.0⫾3.3
共298兲
199.6⫾7.5
共342兲
ME
161.4
共301.5兲
ME
179.5⫾2.0
U152.3⫾5.0
170.4
共367兲
共298兲
共298兲
B
B
C
Method
218⫾3.8
共332兲
ME
223⫾3.8
共298兲
2,4,6-tris共2,4,6-trinitrophenyl兲-1,3,5-triazine
共479–551兲
167.9
共494兲
2-phenyl-3-benzoylquinoxaline-1,4-dioxide
167.4⫾4.0
共298兲
ME
1,4-diamino-2-benzoyl-9,10-anthraquinone
168.5
1-amino-2-bromo-4-关共4-methylphenyl兲amino兴-9,10-anthraquinone
共418 – 438兲
167.0⫾6.0
共428兲
2-hydroxy-4-关共4-methylphenyl兲amino兴-9,10-anthraquinone
共349–378兲
121.0⫾7.6
共363兲
关Note: Compound is listed as the 2-hydroxy-derivative in the paper; however, it is listed as the
1-hydroxy-derivative in Chem. Abstracts兴
3-methylcholanthrene
共401– 425兲
127.2⫾2.4
共413兲
1-anilino-4-共N-methylamino兲-9,10-anthraquinone
136.9
共5-cyano-3,4-diphenyl-6-oxo-1,6-dihydropyridazin-1-yl兲acetate
共396 – 414兲
131.9⫾9.3
共405兲
ME
1,1-difluoro-3,3,3-triphenylpropane
113.2⫾1.7
共298兲
1-fluoro-3,3,3-triphenylpropane
129.3⫾0.6
共298兲
2-fluoro-1,2,3-triphenylpropane
132.5⫾3.0
共298兲
共3-phenoxyphenyl兲methyl-cis-3-共2,2-dichloroethenyl兲-2,2-dimethylcyclopropanecarboxylate 共cis-permethrin兲
共313–333兲
108.8
共323兲
GS,A
diacetylmorphine 共heroin兲
共324 –339兲
144.5⫾4.0
共331兲
GS
3-diphenylmethyl-3-propyl-2,4-pentanedione
124.7
共298兲
T,B
关1,8兴-para-cyclophane
共354 –376兲
105⫾1.3
共365兲
ME
共354 –376兲
110.9⫾2.1
共298兲
ME
2-hydroxy-4,4⬘ -dibutoxybenzophenone
148.0
B
1,1-diadamantyl ketone
共362–379兲
109.0⫾1.8
共298兲
ME
methyl eicosanoate
共311–318兲
190.8⫾10
共314兲
ME
ethyl nonadecanoate
共302–308兲
149.7
共305兲
ME
heneicosane
141.8⫾10
共298兲
B
anthanthrone 共dibenzochrysene-6,12-dione兲
共450–550兲
152.2
共465兲
anthranthrene 共dibenzo关def,mno兴chrysene兲
135⫾5
共479兲
ME
benzo关ghi兴perylene
共313– 453兲
129.9
共383兲
GS
共389– 468兲
127.8
共404兲
ME
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
Reference
关60/4兴关99/10兴
关506-30-9兴
关61/1兴关70/1兴关87/4兴
关111-61-5兴
关87/4兴关67/18兴
关112-95-8兴
关94/8兴
关91/1兴
关72/1兴
关629-96-9兴
关65/6兴关87/4兴
关65/6兴
关49753-54-0兴
关87/4兴
关13494-38-7兴
关97/25兴
关84/40兴
关128-83-6兴
关84/35兴
关84/35兴
关56-49-5兴
关87/4兴关64/3兴
关84/40兴
关82232-20-0兴
关82/24兴
关193472-73-0兴
关97/34兴
关193472-69-4兴
关97/34兴
关193472-72-9兴
关97/34兴
关86/20兴
关561-27-3兴
关84/27兴
关160731-84-0兴
关95/2兴
关6169-94-4兴
关69/6兴关77/1兴
关69/6兴关77/1兴
关6127-74-8兴
关99/22兴
关38256-01-8兴
关92/2兴
关1120-28-1兴
关65/6兴关87/4兴
关18281-04-4兴
关87/4兴关67/18兴
关629-94-7兴
关91/1兴
关641-13-4兴
关87/4兴
关191-26-4兴
关52/3兴
关191-24-2兴
关95/7兴
关87/4兴关74/30兴
ENTHALPY OF SUBLIMATION
627
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
Polymorph
Temperature range 共K兲
C22H12O2
共450–510兲
共454 –502兲
6,13-pentacenequinone
C22H14
C22H14
C22H14
C22H14
C22H14
C22H16O
C22H17NO3 S
C22H18N2 O2
C22H18N2 O2
C22H18N2 O2
C22H20N2 O4
C22H20N2 O4
C22H20N2 O4
C22H21F
C22H22
C22H24N2 O2
C22H26
C22H26N2 O2
C22H26N2 O2
C22H28N2 O2
C22H28N2 O2
C22H28N2 O2
C22H28O
C22H28O
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
135.1
125.5
共465兲
共478兲
Method
ME
116.3⫾5.9
共298兲
1,2:6,7-dibenzophenanthrene 共benzo关b兴chrysene兲
136.4
共417兲
共398 –513兲
136.9
共413兲
pentacene
共443– 483兲
156.9⫾13.6
共463兲
共494 –526兲
154⫾5
共512兲
共495–530兲
184⫾10
共298兲
共455–555兲
157.7
共505兲
picene
共425– 488兲
140.1
共456兲
共409–527兲
140.7
共424兲
1,2:3,4-dibenzanthracene 共benzo关b兴triphenylene兲
共313– 453兲
135
共383兲
共425– 452兲
159⫾6
共298兲
1,2:5,6-dibenzanthracene 共dibenz关a,h兴anthracene兲
134.1
共436 – 462兲
162⫾6
共298兲
共417–502兲
141.8
共457兲
3,8-dimethylnaphtho关3,2,1-kl兴xanthene 共3,8-dimethylceroxene兲
共373– 433兲
138.2
共388兲
2-共3-methyoxypropyl兲-1H-xantheno关2,2,9-def兴isoquinoline-1,3(2H)-dione
共605– 647兲
111.8
共620兲
共647– 685兲
150.8
共662兲
1-amino-2-methyl-4-关共4-methylphenyl兲amino兴-9,10-anthraquinone
共418 – 435兲
142.2⫾2.3
共426兲
1-共N-methylamino兲-4-关共3-methylphenyl兲amino兴-9,10-anthraquinone
共418 – 434兲
129.0⫾4.7
共426兲
1-共N-methylamino兲-4-关共4-methylphenyl兲amino兴-9,10-anthraquinone
共403– 426兲
153.9⫾3.9
共414兲
N,N⬘ -bis共2-methoxyphenyl兲terephthalamide
共456 – 470兲
197.5⫾4.2
N,N⬘ -bis共3-methoxyphenyl兲terephthalamide
共456 – 470兲
209.2⫾8.4
N,N⬘ -bis共4-methoxyphenyl兲terephthalamide
227.6⫾8.4
2-benzyl-2-fluoro-1,3-diphenylpropane
127.5⫾0.8
共298兲
1,1,1-triphenylbutane
114.3
共298兲
N,N⬘ -ethylenebis共3-amino-1-phenylbut-2-en-1-one兲
共407– 426兲
192.9⫾5.3
共415兲
198.8⫾5.3
共298兲
1,1⬘ -diphenyl-1,1⬘ -bicyclopentyl
141.4
1,4-bis共N-butylamino兲-9,10-anthraquinone
共389–398兲
116.4⫾2.3
共394兲
1,4-bis共N-isobutylamino兲-9,10-anthraquinone
共368 –388兲
96.4⫾2.1
共378兲
(4R,4⬘ R,5R,5⬘ R)-5,5-diphenyl-3,3⬘ ,4,4 ⬘ -tetramethyl-2,2⬘ -bioxazolidine
共349–358兲
130.8⫾0.8
共356兲
共2R, 3R, 6R, 7R兲-2,6-diphenyl-3,4,7,8-tetramethyl-cis-perhydro-关1,4兴-oxazino关3,2-b兴-关1,4兴-oxazine
共353–364兲
116.6⫾1.0
共358兲
共2R, 3S, 6R, 7S兲-2,6-diphenyl-3,4,7,8-tetramethyl-cis-perhydro-关1,4兴-oxazino关3,2-b兴-关1,4兴-oxazine
共356 –364兲
123.1⫾1.6
共358兲
2,4,6-triisopropylbenzophenone
共353–364兲
116⫾7
共298兲
3 ⬘ ,5⬘ -diisopropyl-4,4-dimethyl-3-phenyl-1,2-benzocyclobuten-3-ol
ME
ME
ME,TE
ME,TE
ME
ME
GS
TE,ME
GS
TE,ME
ME
ME
ME
ME
ME
E,B
ME
Reference
关87/4兴
关67/2兴
关3029-32-1兴
关56/5兴关70/1兴
关214-17-5兴
关67/2兴
关87/4兴
关135-48-8兴
关98/3兴
关80/1兴
关80/1兴
关67/2兴
关213-46-7兴
关67/2兴
关87/4兴
关215-58-7兴
关95/7兴
关80/1兴
关53-70-3兴
关95/7兴
关80/1兴
关67/2兴
关87/4兴关59/14兴
关36245-88-2兴
关87/4兴
关87/4兴
关116-77-8兴
关84/35兴
关6408-50-8兴
关84/35兴
关128-85-8兴
关84/35兴
关36360-34-6兴
关73/21兴关77/1兴
关6957-81-9兴
关73/21兴关77/1兴
关7144-15-2兴
关73/21兴关77/1兴
关193472-71-8兴
关97/34兴
关43044-69-5兴
关99/25兴
关16087-30-2兴
关95/12兴
关95/12兴
关59358-70-2兴
关83/16兴
关17354-14-2兴
关84/35兴
关10720-45-7兴
关84/35兴
关145513-29-7兴
关95/19兴
关145438-85-3兴
ME
关95/19兴
关145438-85-3兴
ME
关95/19兴
关33574-11-7兴
关82/10兴
关33574-16-2兴
C
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
628
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
C22H38
C22H31NO4
C22H42
C22H42
C22H44O2
C22H46O
C22H46
C23H24O6
C23H25F
C23H26O6
C23H36N2 O2
C23H48
C24H12
C24H12
C24H12O2
C24H14
C24H14
C24H16N2 O2
C24H18
C24H24O4
Compound
Temperature range 共K兲
⌬ subH m /kJ mol⫺1
共354 –364兲
117.9
meso 3,4-di共1-cyclohexen-1-yl兲-2,2,5,5-tetramethylhexane
共347– 404兲
117.2⫾2.4
N,N-bis共3-phenoxy-2-hydroxypropyl兲butyl amine
共363– 411兲
114.3
146.0⫾4.2
meso-共E, E兲-5,6-di-tert-butyl-2,2,9,9-tetramethyl-3,7-decadiene
共297–353兲
110.0⫾1.7
共dl兲-共E, E兲-5,6-di-tert-butyl-2,2,9,9-tetramethyl-3,7-decadiene
共297–346兲
74.4⫾1.7
ethyl eicosanoate
共307–313兲
171.5
1-docosanol
共335–341兲
206.7⫾10
238.5⫾10
docosane
172.6⫾2.0
U 151.1⫾10
tris共ethoxycarbonyl兲-9-fluorenylmethane
143.2
1-adamantylfluorodiphenylmethane
共353–393兲
125.9⫾1.3
1,1,1-tris共ethoxycarbonyl兲-2,2-diphenylethane
140.1
共5␣,17␤兲-N-共1,1-dimethylethyl兲-3-oxo-4-azaandrost-1-ene-17carboxamide 共Finasteride兲
共463– 488兲
143.7
tricosane
U146.8⫾10
coronene
共421–504兲
133.1⫾5.1
共313– 453兲
143.2
共427–510兲
135.9
128.4
共433–513兲
147
共476 –555兲
143.2
148.5
bis-benzo关3,4兴cyclobuta关 1,2-a:1 ⬘ ,2⬘ -c兴 biphenylene 共关4兴phenylene兲
131.0⫾4.2
3,4:9,10-dibenzpyrene-5,8-quinone
112.5⫾5.4
dibenzo关a,e兴pyrene
共414 –506兲
146.4
共434 –526兲
137.6
dibenzo关fg,op兴naphthacene
共430–555兲
147.4
共454 –526兲
146.9
共called 1,2,6,7-dibenzpyrene in paper, which we have taken to be
based upon the melting point temperature reported in the paper兲
2,2⬘ -共1,4-phenylene兲bis共5-phenyl兲oxazole
140
共600– 680兲
94.4
1,3,5-triphenylbenzene
150.9
共364 –388兲
145.6⫾0.9
150.3⫾0.9
152⫾0.3
共410– 444兲
142
共384 – 400兲
142.2
149.7⫾4.1
syn 4,9-bis共methoxycarbonyl兲pagodane 共dimethyl undecacyclo
关 9.9.0.01,5.02,12.02,18.03,7.06,10.08,12.011,15.013,17.016,20兴 eicosane4-syn, 9-syn-dicarboxylate兲
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
CAS registry number
(Tm /K)
Method
Reference
共298兲
C
共376兲
T
关82/10兴
关62678-54-0兴
关93/6兴
关23257-62-7兴
关87/4兴
关76/19兴
共378兲
共325兲
T
关95/1兴
共307兲
T
共310兲
ME
共330兲
共298兲
ME
共391兲
共298兲
B
B
共298兲
GS
共373兲
T
关95/1兴
关18281-05-5兴
关87/4兴关67/18兴
关661-19-8兴
关65/6兴关87/4兴
关65/6兴
关629-97-0兴
关94/8兴
关91/1兴
关170464-53-6兴
关95/29兴
关154393-25-6兴
关94/10兴
共298兲
GS
关95/29兴
关98319-26-7兴
TGA
关97/36兴
关638-67-5兴
关91/1兴
关191-07-1兴
关98/3兴
关95/7兴
关87/4兴关74/30兴
关67/2兴
关58/1兴
关52/3兴
关51/12兴
关102234-01-5兴
关00/18兴
关3302-52-1兴
关56/5兴关70/1兴
关192-65-4兴
关87/4兴
关67/2兴
关192-51-8兴
关87/4兴
关67/2兴
共298兲
B
共463兲
共383兲
共468兲
ME
GS
ME
ME
共473兲
共407兲
共407兲
ME
ME
共429兲
共480兲
ME
共445兲
共490兲
ME
dibenzo关fg,op兴naphthacene
共480兲
共615兲
共298兲
共376兲
共298兲
共298兲
共425兲
共422兲
共298兲
CGC–DSC
T
C,ME
ME
ME
ME
关1806-34-4兴
关89/7兴
关87/4兴
关612-71-5兴
关98/5兴
关97/15兴
关97/15兴
关74/4兴
关74/4兴关87/4兴
关67/2兴
关58/1兴关70/1兴
关89702-41-0兴
ENTHALPY OF SUBLIMATION
629
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
C24H24O4
C24H26N2 O2
C24H28P2 O2
C24H30
C24H30O4
C24H32
C24H48O2
C24H50
C25H20
C25H36O2
C25H50O2
C25H52
C26H16
C26H18
C26H18
C26H20
C26H20N2 O2
C26H22
C26H22
C26H26
C26H38
C26H54
C27H48
Compound
Temperature range 共K兲
⌬ subH m /kJ mol⫺1
CAS registry number
(Tm /K)
共393– 447兲
146.1⫾3.0
共420兲
1,6-bis共methoxycarbonyl兲dodecahedrane 共dimethyl undecacyclo关 9.9.0.02,9.03,7.04,20.05,18.06,16.08,15.010,14.012,19.013,17兴 eicosane1,6-dicarboxylate兲
共395– 450兲
139.7⫾1.3
共422兲
1,5-dipiperidylanthraquinone
共408 – 458兲
173.3
共428兲
1,4-bis共diphenylphosphino兲butane
171.6
共443兲
1,1⬘-diphenyl-1,1⬘ -bicyclohexyl
150.2
2,2⬘ -diphenyl-bi-共5,5-dimethyl-1,3-dioxan-2-yl兲
共372– 420兲
130.2⫾1.8
共396兲
关6.6兴-para-cyclophane
共352–371兲
108.8⫾0.8
共361兲
115.1⫾2.1
共298兲
ethyl docosanoate
共313–318兲
196.5
共315.5兲
tetracosane
162⫾12
共298兲
tetraphenylmethane
140.0
共298兲
共396 – 466兲
150.6⫾4
共298兲
共404 – 466兲
143.3⫾1
共419兲
2,2⬘ -methylenebis共6-tert-butyl-4-methylphenol兲
共383– 403兲
114.0
共393兲
ethyl tricosanoate
共316 –322兲
175.2
共319兲
pentacosane
173.6⫾10
共298兲
dibenzo关g,p兴chrysene
共408 – 493兲
142.2
共423兲
共417–500兲
141.8
共458兲
9,10-diphenylanthracene
共313– 453兲
137.5
共383兲
116.4
共393– 433兲
143.6
共413兲
共481–502兲
156.9⫾4.2
共492兲
9,9⬘ -bifluorenyl
共383– 408兲
131.8⫾1.1
共395兲
132.6⫾1.1
共298兲
tetraphenylethene
共343–389兲
129.3⫾0.7
共366兲
133.4⫾0.7
共298兲
2,2⬘ -共1,4-phenylene兲bis共4-methyl-5-phenyl兲oxazole
150
共480兲
1,1,2,2-tetraphenylethane
136.8⫾2.9
共298兲
共370– 423兲
131.4⫾2.1
共396兲
1,1,1,2-tetraphenylethane
132.6⫾2.1
共298兲
共340– 400兲
128.7⫾2.1
共370兲
126.4⫾1.7
共434兲
pentacyclo关18.2.2.2共9,12兲.0共4,15兲.0共4,15兲.0共6,17兲兴hexacos-4,6共17兲,9,11,15,20,22,23,25-nonane 共triple layered 关2.2兴paracyclophane兲
共299– 412兲
119.1⫾1.5
125.9⫾2.5
共298兲
2,3-dimethyl-2,3-bis-共4-tert-butylphenyl兲-butane
161.9
hexacosane
177.2⫾10
共298兲
17-共1,5-dimethylhexyl兲-10,13-dimethyl-hexahydro-1H-cyclopenta关a兴phenanthrene 共5␣-cholestane兲
Method
Reference
T
关94/9兴
T
B
E,B
T
ME
ME
ME
B
TE,ME
ME
GS
ME
B
ME
GS
HSA
T
T
GS
GS
GS
GS
HSA
TSGC
TSGC
E,B
B
关124316-65-0兴
关94/9兴
关14580-70-2兴
关58/1兴关87/4兴
关7688-25-7兴
关89/28兴
关59358-71-3兴
关83/16兴
关167321-36-0兴
关95/13兴
关4384-23-0兴
关69/6兴关77/1兴
关69/6兴关77/1兴
关5908-87-2兴
关87/4兴关67/18兴
关646-31-1兴
关91/1兴
关630-76-2兴
关99/25兴
关72/5兴关77/1兴
关87/4兴关72/5兴
关119-47-1兴
关71/19兴
关18281-07-7兴
关87/4兴关67/18兴
关629-99-2兴
关91/1兴
关191-68-4兴
关87/4兴
关67/2兴
关1499-10-1兴
关95/7兴
关58/4兴
关58/1兴关87/4兴
关53/2兴关70/1兴
关1530-12-7兴
关94/2兴
关94/2兴
关632-51-9兴
关99/29兴
关99/29兴
关3073-87-8兴
关89/7兴
关632-50-8兴
关90/12兴
关90/12兴
关2294-94-2兴
关90/12兴
关90/12兴
关56/1兴
关35117-21-6兴
关80/15兴
关80/15兴
关5171-91-5兴
关83/16兴
关630-01-3兴
关91/1兴
关481-21-0兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
630
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Compound
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
133.8
共298兲
196.0⫾30
共298兲
B
Polymorph
Temperature range 共K兲
C27H56
heptacosane
C28H14
phenanthro关1,10,9,8-opqra兴perylene
共580– 630兲
C.I. Vat Blue 6
共519– 634兲
C.I. Vat Blue 4
共519– 634兲
9,9⬘ -bianthryl
180.5⫾5
共605兲
ME
199
共577兲
GS
167
共577兲
GS
共413– 473兲
128.4⫾0.2
127.9
148.1
共443兲
C28H12Cl2 N2 O4
C28H14N2 O4
C28H18
C28H18
9,9⬘ -biphenanthryl
C28H22
9,9⬘ -dimethyl-9,9⬘-bifluorenyl
共368 – 403兲
Method
151.5
C28H30N4
C28H38
C28H58
C30H14O2
C30H16
C30H46
C31H15NO3
C32H2 Br16N8
C32H2 Cl16N8
C32H14
C32H18N8
C32H50
C32H50
C32H66
C34H16O2
C34H16O2
C34H18
C34H18
C34H18
C34H18
118.7⫾1.3
119.7⫾1.3
2,3,7,8,12,13,17,18-octamethylporphyrin
共593– 653兲
268⫾11
1,1⬘-diphenyl-1,1⬘-bicyclooctyl
174.5
octacosane
208.9⫾10
8,16-pyranthenedione 共C. I. Vat Orange 9兲
共503–543兲
197.7
181.2
pyranthrene
194.5⫾6.7
3,4-diethyl-3,4-bis-共4-tert-butylphenyl兲-hexane
167.8
C.I. Vat Green 3
共519– 634兲
155
hexadecabromophthalocyanine
共438 – 493兲
109.2⫾16.3
hexadecachlorophthalocyanine
共398 – 443兲
141.0⫾17.6
ovalene
211.7⫾7.9
␤ -29H,31H-phthalocyanine
共598 – 698兲
223.8⫾1.3
2,4,5,7-tetramethyl-4,5-bis-共4-tert-butylphenyl兲-octane
182.8
4,5-diethyl-4,5-bis-共4-tert-butylphenyl兲-octane
182.4
dotriacontane
271.1⫾2.5
dibenzanthrone 共violanthrone兲
共513–548兲
208.8
202.9
isodibenzanthrone 共isoviolanthrone兲
共523–553兲
221.1
215.5
benzo关rst兴phenanthro关1,10,9-cde兴pentaphene
共478 – 603兲
154.1
violanthrene
223.8⫾8.8
violanthrene A 共melting point 478 °C兲
共562–724兲
195.8
violanthrene B 共melting point 330 °C兲
共555– 625兲
153.5
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
共386兲
共298兲
T
GS
E,B
共298兲
B
共518兲
共498兲
ME
共595兲
ME
E,B
共577兲
GS
共453兲
ME
共413兲
ME
共600兲
ME
ME
E,B
E,B
共528兲
共542兲
ME
共538兲
共537兲
ME
共493兲
共590兲
Reference
关00/10兴
关593-49-7兴
关91/1兴
关190-39-6兴
关87/4兴关52/3兴
关130-20-1兴
关86/14兴
关81-77-6兴
关86/14兴
关1055-23-8兴
关70/1兴关58/1兴
关58/1兴关87/4兴
关51/2兴关60/1兴
关20532-03-0兴
关51/2兴关60/1兴
关15300-82-0兴
关94/2兴
关94/2兴
关1257-25-6兴
关01/12兴
关59358-73-5兴
关83/16兴
关630-02-4兴
关91/1兴
关128-70-1兴
关87/4兴
关51/12兴
关191-13-9兴
关52/3兴
关85668-74-2兴
关83/16兴
关3271-76-9兴
关86/14兴
关28746-04-5兴
关87/4兴关70/7兴
关28888-81-5兴
关87/4兴关70/7兴
关190-26-1兴
关52/3兴
关574-93-6兴
关00/30兴
关85668-75-3兴
关83/16兴
关85668-73-1兴
关83/16兴
关544-85-4兴
关70/1兴
关116-71-2兴
关87/4兴
关51/12兴
关128-64-3兴
关87/4兴
关51/12兴
关190-93-2兴
关87/4兴
关81-31-2兴
关52/3兴关60/1兴
共653兲
ME
关67/2兴
共590兲
ME
关67/2兴
ENTHALPY OF SUBLIMATION
631
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
C34H18
C34H18
C34H54
C38H30
C38H30O2
C38H62
C42H28
C44H26Br4 N4
C44H26Br4 N4
C44H26Cl4 N4
C44H26F4 N4
C44H26F4 N4
C44H30N4
form I
form II
C48H38N4
C48H38N4
C48H38N4
C60
C60F16
C60F36
Compound
Temperature range 共K兲
⌬ subH m /kJ mol⫺1
CAS registry number
(Tm /K)
共Note: This entry is likely the original reference for benzo关rst兴phenanthro关1,10,9-cde兴pentaphene listed in reference 关87/4兴. Chemical Abstracts
cites 关67/2兴 as reporting the heat of sublimation of benzo关rst兴phenanthro关1,10,9-cde兴pentaphene.兲
isoviolanthrene A 共melting point 510 °C兲
共588 –724兲
218
共590兲
tetrabenzo关de,hi,op,st兴pentacene
共348 – 448兲
118.5
共363兲
4,5-dipropyl-4,5-bis-共4-tert-butylphenyl兲-octane
198.3
1-diphenylmethylene-4-triphenylmethyl-2,5-cyclohexadiene
共348 –394兲
114.6
共363兲
bis共triphenylmethyl兲peroxide
共392– 434兲
158.1
共407兲
5,6-dibutyl-5,6-bis-共4-tert-butylphenyl兲-decane
220.9
5,6,11,12-tetraphenyltetracene
共453–523兲
160.6⫾4.2
共488兲
5,10,15,20-tetrakis共3-bromophenyl兲porphine
204⫾4
5,10,15,20-tetrakis共4-bromophenyl兲porphine
135⫾4
5,10,15,20-tetrakis共4-chlorophenyl兲porphine
311⫾5
5,10,15,20-tetrakis共2-fluorophenyl兲porphine
225⫾8
5,10,15,20-tetrakis共4-fluorophenyl兲porphine
178⫾4
5,10,15,20-tetraphenylporphine
240⫾7
共540– 630兲
267⫾9
共630– 670兲
185⫾10
共588 – 678兲
110.9⫾5.0
共603兲
5,10,15,20-tetrakis共2-methylphenyl兲porphine
159⫾5
5,10,15,20-tetrakis共3-methylphenyl兲porphine
177⫾5
5,10,15,20-tetrakis共4-methylphenyl兲porphine
178⫾3
buckminsterfullerene
共775–1033兲
180⫾2
共298兲
共789–907兲
152.8⫾0.1
共897兲
183.5⫾1.0
共298兲
179.2⫾3.5
共298兲
共730–990兲
175.2⫾2.9
共860兲
181⫾2.0
共298兲
219.6
共546 –722兲
180⫾10.0
共634兲
158⫾3.0
共700兲
168.5⫾1.2
共298兲
181.1⫾2.6
共298兲
181.4⫾2.3
共700兲
158.6
共773兲
184.1⫾3.1
共298兲
183.2⫾3.5
共298兲
180.6⫾1.5
共298兲
共673– 873兲
159.0⫾4.2
⬎163 共powder兲
共640– 800兲
167.8⫾5.4
共707兲
U90.9
hexadecafluorobuckminsterfullerene
186⫾9
hexatriacontylfluorobuckminsterfullerene 共4 isomer average兲
Method
Reference
ME,TE
ME,TE
TGA
UV
ME
ME
ME
MS
ME
GS
ME
ME
ME
TGA
ME,MS
ME,MS
关4430-29-9兴
关52/3兴关60/1兴
关191-79-7兴
关87/4兴关67/2兴
关85668-72-0兴
关83/16兴
关18909-18-7兴
关87/4兴
关596-30-5兴
关87/4兴
关85668-76-4兴
关83/16兴
关517-51-1兴
关58/1兴关70/1兴
关68772-71-4兴
关00/36兴
关29162-73-0兴
关00/36兴
关22112-77-2兴
关00/36兴
关27185-62-2兴
关00/36兴
关37095-43-5兴
关00/36兴
关917-23-7兴
关00/36兴
关94/41兴
关94/41兴
关87/4兴关70/7兴
关37083-40-2兴
关00/36兴
关50849-45-1兴
关00/36兴
关14527-51-6兴
关00/36兴
关99685-96-8兴
关00/37兴
关98/4兴
关98/4兴
关96/20兴关98/4兴
关95/8兴
关95/8兴
关95/35兴
关94/18兴
关94/12兴
关94/12兴关98/4兴
关94/25兴关98/4兴
关94/15兴关92/22兴
关93/15兴
关92/21兴关98/4兴
关92/22兴关98/4兴
关92/23兴关98/4兴
关92/16兴
关92/10兴
关91/9兴
关90/20兴
ME,MS
关00/32兴
ME
ME
E,B
E,B
GS
GS
GS
GS
GS
GS
ME
GS
GS
GS
ME
GS
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
632
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 6. Reported enthalpies of sublimation of organic compounds, 1910–2001—Continued
Molecular formula
Polymorph
C60F36
C60F42
C60F44
C60F44O
C60F46
C60F48
C60H16
C60H36
C70
C76
C76H94N4
C84
Compound
Temperature range 共K兲
⌬ subH m /kJ mol⫺1
共422–525兲
134⫾6
hexatriacontylfluorobuckminsterfullerene
139⫾8
共408 –539兲
135⫾8.0
dotetracontylfluorobuckminsterfullerene
共430–510兲
110⫾10
tetratetracontylfluorobuckminsterfullerene
共430–510兲
112⫾6
tetracontylfluorobuckminsterfullerene
共430–510兲
111⫾3
hexatetracontylfluorobuckminsterfullerene
共430–510兲
114⫾7
octatetracontylfluorobuckminsterfullerene
共395–528兲
109⫾7.0
hexadecahydrobuckminsterfullerene
⭓186
hexatriacontylhydrobuckminsterfullerene
共560– 680兲
162⫾5
152
175
Fullerene—C70
共864 –1099兲
199⫾2
共783–904兲
189.8⫾3.1
200⫾6.0
174⫾3.0
193.4⫾1.5
186.6
共673– 873兲
188.3⫾4.2
共640– 800兲
180.0⫾9.2
Fullerene—C76
共637–911兲
190⫾7
共834 –1069兲
206⫾4.0
5,10,15,20-tetrakis共3,5-di-tert-butylphenyl兲porphine
209⫾5
Fullerene—C84
共658 –980兲
202⫾4.0
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
CAS registry number
(Tm /K)
Method
Reference
共473兲
MS
共466兲
ME,MS
ME,MS
关94/26兴关96/8兴
关150180-35-1兴
关00/8兴
关99/2兴
关150155-92-3兴
关00/14兴
关147771-02-6兴
关00/14兴
关337371-51-4兴
关00/14兴
关143471-96-9兴
关00/14兴
关143471-98-1兴
关99/2兴关00/34兴
E
关00/38兴关01/11兴
MS
关00/38兴关01/11兴
关01/11兴
关01/11兴
关115383-22-7兴
关00/37兴
关96/1兴
关96/1兴
关94/12兴
关94/15兴
关93/15兴
关92/16兴
关91/9兴
关135113-15-4兴
关98/30兴
关97/21兴
关89372-90-7兴
关00/36兴
关135113-16-5兴
关99/5兴
ME,MS
ME,MS
ME,MS
ME,MS
共476兲
共630兲
共298兲
共298兲
共844兲
共298兲
共740兲
共750兲
共788兲
ME
ME
共739兲
ME
MS
ME
ME
ME,MS
共764兲
共298兲
ME
TE
共853兲
ME
ENTHALPY OF SUBLIMATION
633
TABLE 7. Enthalpies of sublimation of some organometallic and inorganic compounds, 1910–2001
Element
Molecular formular/polymorph
A1
C5 H5 AlBr3 N
C15H3 AlF18O6
C15H12AlF9 O6
C15H21AlO6
C16H40Al2 N2
C18H15Al
C24H12AlF9 O6 S3
C27H18AlN3 O3
C30H18AlF9 O6
C30H27AlO6
C30H30F21AlO6
C32H16AlClN8
C32H16AlFN8
C33H57AlO6
Am
(C15H3 AmF18O6 ) – 2(C12H27O4 P)
(C15H12AmF9 O6 ) – 2(C12H27O4 P)
Compound
Temperature range 共K兲
⌬ subH m /kJ mol⫺1
CAS registry number
(Tm /K)
aluminum tribromide–pyridine complex
共501– 633兲
71.2⫾0.6
83.3
tris共1,1,1,5,5,5-hexafluoro-2,4-pentanedionato兲aluminum共III兲
共333–363兲
52
共324 –344兲
77.6⫾6.2
共334兲
79.0⫾6.5
共298兲
74.1⫾2.5
共323–347兲
109.6⫾3.8
共335兲
tris共1,1,1-trifluoro-2,4-pentanedionato兲aluminum共III兲
共373– 403兲
74
共363– 423兲
113.4⫾1.3
共369–392兲
102.7⫾3.2
108⫾2.0
43.1
共443兲
共354 –396兲
93.7⫾6.7
共375兲
41.0
40.0
tris共2,4-pentanedionato兲aluminum共III兲
共413– 443兲
93
120⫾3.0
共298兲
共432– 464兲
102.0⫾3.2
共448兲
47.1⫾1.0
118.9⫾7.9
24.3
共458兲
121.7⫾4.2
共298兲
共383– 413兲
66.1⫾3.3
共398兲
23.4
共417– 476兲
20.5
tetramethylbis关␮-关N-共1-methylethyl兲-2-propanaminto兴兴dialuminum共III兲
99.2
triphenylaluminum
共432– 477兲
172⫾5
共455兲
tris共1-共2-thenoyl兲-4,4,4-trifluoro-1/,3-butanedione兲aluminum共III兲
U46.4
tris共8-hydroxyquinolinato兲aluminum共III兲
137.7
tris共1-phenyl-4,4,4-trifluoro-1,3-butanedione兲aluminum共III兲
U55.2
tris共1-phenyl-1,3-butanedionato兲aluminum共III兲
共462– 478兲
186.8⫾2.1
共470兲
195.2⫾2.1
共298兲
326.5
共496兲
193.7⫾0.3
共298兲
tris共1,1,1,2,2,3,3-heptafluoro-7,7-dimethyl-4,6-octanedionato兲aluminum共III兲
共363–398兲
71.1⫾2.5
共381兲
aluminum共III兲–共phthalocyaninato兲chloro complex
共588 –703兲
236.4⫾1.7
aluminum共III兲–共phthalocyaninato兲fluoro complex
共658 –768兲
266.9⫾2.5
tris共2,2,6,6-tetramethyl-3,5-heptanedionato兲aluminum共III兲
共413– 443兲
88
119⫾3.0
tris共1,1,1,5,5,5-hexafluoro-2,4-pentanedionato兲americium共III兲2共tributylphosphate兲 complex
共425–511兲
133.9⫾1.7
共468兲
tris共1,1,1-trifluoro-2,4-pentanedionato兲americium共III兲2共tributylphosphate兲 complex
共509–545兲
222.6⫾29.2
共527兲
Method
T
B,E
TGA
BG
TGA
GS
TGA
ME
BG
ME
ME,TE
TGA
ME,TE
ME
ME
TGA
Reference
关15348-61-5兴
关89/24兴
关67/12兴
关17786-67-3兴
关00/35兴
关87/20兴关88/22兴
关87/20兴
关85/23兴关87/20兴
关72/17兴
关14354-59-7兴
关00/35兴
关85/16兴
关78/27兴
关77/18兴关88/16兴
关77/25兴
关72/17兴
关65/11兴
关60/17兴
关13963-57-0兴
关00/35兴
关77/18兴关88/2兴
关88/22兴
关81/13兴
关80/30兴
关77/25兴
关75/19兴
关72/17兴
关65/11兴
关60/17兴
关115381-27-6兴
关88/20兴
关841-76-9兴
关84/8兴
关14054-83-2兴
关60/17兴
关2085-33-8兴
关95/35兴
关14323-12-7兴
关60/17兴
关14376-06-8兴
关95/9兴
关95/9兴
关88/16兴
关83/20兴
关18716-26-2兴
关72/17兴
关14154-42-8兴
关00/30兴
关5196-93-4兴
关00/30兴
关14319-08-5兴
关00/35兴
关77/18兴关83/20兴
关58760-64-8兴
TRM
关78/32兴
关75101-27-8兴
TRM
关78/32兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
634
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 7. Enthalpies of sublimation of organometallic and inorganic compounds, 1910–2001—Continued
Element
Compound
⌬ subH m /kJ mol⫺1
CAS registry number
(Tm /K)
Molecular formula/polymorph
Temperature range 共K兲
(C24H30AmF9 O6 ) – 2(C12H27O4 P)
tris共1,1,1-trimethyl-5,5,5-trifluoro-2,4-pentanedionato兲americium共III兲2共tributylphosphate兲 complex
共438 – 493兲
129.7⫾23.4
共465兲
tris共2,2,6,6-tetramethyl-3,5-heptanedionato兲americium共III兲
共373– 423兲
200.8
tetrakis共trifluoromethyl兲tetraarsetane
共317–354兲
76.6
共335兲
tris共N,N-diethyldithiocarbamate兲arsenic共III兲
124⫾3
共298兲
triphenylarsine
98.3⫾8.4
triphenylarsine oxide
149.0⫾5.4
tris共dipropyldithiocarbamate兲arsenic共III兲
145.1⫾5.3
共298兲
tris共N,N-dibutyldithiocarbamate兲arsenic共III兲
128⫾3
共298兲
tris共N,N-diisobutyldithiocarbamate兲arsenic共III兲
128⫾2
共298兲
C33H57AmO6
As
C4 As4 F12
C15H30AsN3 S6
C18H15As
C18H15AsO
C21H42AsN3 S6
C27H54AsN3 S6
C27H54AsN3 S6
Au
C7 H10AuF3 O2
B
CH5 BO2
(CH5 N) – (BH3 )
(CH5N兲–共C3H9BO3兲
CH11B2NS1
(C2 H3 OF) – (BF3 )
(C2H5B3兲–共C3H9N兲
C2H6BF2N
(C2 H7 N) – (BH3 )
(C2H7N兲–共C3H9BO3兲
C2 H6 B4
C2 H12B10
C2 H12B10
C2 H12B10
(C3 H7 N) – (BH3 )
(C3H9B兲–共C2H9Nsi兲
(C3H9B兲–共C7H13N兲
(C3 H9 N) – (BF3 )
(C3 H9 ) – (B2 F4 )
Method
关75101-26-7兴
TRM
ME
DSC,E
DSC,E
dimethyl共1,1,1-trifluoro-2,4-pentanedionato兲gold共III兲
共265–300兲
83.5
dihydroxymethylborane
共293–362兲
64.1
共298 –338兲
65.2
methylamine–borane complex
共273–318兲
78.7⫾4.2
methylamine–methylborate complex
58.2
N-methyl-N-silylaminodiborane
共214 –230兲
36.6
methylfluorocarbonyl–trifluoroboron complex
共223–273兲
26.3
1,5-dicarbopentaborane共5兲–trimethylamine complex
共220–253兲
49.7
dimethylamino difluoroboron
共308 –359兲
76.5
dimethylamine–borane complex
共273–308兲
77.4⫾2.9
dimethylamine–methylborate complex
70.3
1,6-dicarbahexaborane
共190–209兲
31.2
1,2-dicarbadodecaborane 共o-carborane兲
共283–333兲
50.3
共333– 423兲
49.4
65.4⫾1.0
1,7-dicarbadodecaborane 共m-carborane兲
共283–333兲
67.5
共333– 423兲
63.3
58.5⫾1.0
1,12-dicarbododecaborane 共p-carborane兲
61.3⫾1.0
azetidine–borane complex
共297–321兲
67.9
trimethylboron–silyldimethylamine complex
共243–268兲
51.4
trimethylboron–azabicyclo关2.2.2兴octane complex
共273–388兲
79.6
trimethylamine–boron trifluoride complex
共373– 413兲
68.9
trimethylamine–diboron tetrafluoride 共tetramer兲
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
Reference
关78/32兴
关71817-66-8兴
关79/30兴
关7547-15-1兴
关66/14兴
关17767-20-3兴
关87/16兴
关603-32-7兴
关82/20兴关64/6兴
关1153-05-5兴
关94/31兴
关86431-46-1兴
关99/34兴
关48233-55-2兴
关94/31兴
关41582-74-5兴
关97/31兴
关00/33兴
共308兲
共318兲
ME
关13061-96-6兴
关87/4兴
关40/4兴
关1722-33-4兴
关59/16兴
关51/13兴
共222兲
共248兲
关50/7兴
关353-44-6兴
关57/8兴
共236兲
关72/28兴
共333兲
关54/13兴
关74-94-2兴
关69/16兴
ME
共298兲
关51/13兴
关20693-67-8兴
关87/4兴
关16872-09-6兴
关87/4兴
关87/4兴
关82/20兴关76/13兴
关16986-24-6兴
关87/4兴
关87/4兴
关82/20兴关76/13兴
关20644-12-6兴
关82/20兴关76/13兴
共309兲
关56/17兴
共255兲
关54/11兴
共194兲
共318兲
共348兲
共298兲
共298兲
共348兲
共298兲
共393兲
关48/3兴
关420-20-2兴
关87/4兴关43/5兴
关3801-72-7兴
ENTHALPY OF SUBLIMATION
635
TABLE 7. Enthalpies of sublimation of organometallic and inorganic compounds, 1910–2001—Continued
Element
Molecular formula/polymorph
C3 H9 B3 Cl3 N3
(C3 H9 N) – (BH3 )
(C3H9N兲–共C3H6BCl2N兲
C3 H10BN
C3 H12B10O2
C3 H12B10O2
C3 H12B10O2
C3 H14B10
C3 H14B10O
C3 H14B10O
C3 H14B10O
C4 H11BO2
C4 H12B2 Br4 N2
(C4H12GeO兲–共BF3兲
C4 H16B10
C4 H18B4 N2
(C5 H5 N) – (BBr3 )
(C5 H11N) – (BCl3 )
(C5 H11N) – (BH3 )
C5 H21B3 N2 S
C6 H12BNO3
(C7 H9 N) – (BH3 )
C7 H14BNO3
C8 H16BNO3
C8 H18BNO3
C8 H18B10O3
C8 H18B10O3
C8 H24B10
Compound
Temperature range 共K兲
⌬ subH m /kJ mol⫺1
CAS registry number
(Tm /K)
共366 –399兲
65.1
共382兲
2,4,6-trichloro-1,3,5-trimethylborazine
共363– 404兲
57.9
共383.5兲
trimethylamine–borane complex
共273–363兲
56.9⫾0.8
共296 –367兲
57
共311兲
trimethylamine–dimethylaminoboron dichloride complex
共293–342兲
66.1⫾1.7
共317兲
N-methylaminodimethylborane
56.9⫾0.8
共298兲
o-carboranecarboxylic acid
97.0⫾1.7
共298兲
m-carboranecarboxylic acid
97.7⫾0.7
共298兲
p-carboranecarboxylic acid
96.3⫾0.7
共298兲
methyl-o-carborane
63.8⫾0.6
共298兲
hydroxymethyl-o-carborane
77.0⫾1.3
共298兲
hydroxymethyl-m-carborane
78.3⫾1.3
共298兲
hydroxymethyl-p-carborane
83.9⫾1.3
共298兲
dihydroxy-n-butylborane
共303–340兲
69.9⫾0.8
共321兲
dibromo共dimethylamino兲borane dimer
87.4⫾22.2
trimethylmethoxygermane–boron trifluoride complex
共289–306兲
59.5
共297兲
dimethyl-o-carborane
65.3⫾07
共298兲
1,4-piperazinediyl bis共diborane共6兲兲
共318 –346兲
63.9
共332兲
boron tribromide–pyridine complex
共523– 602兲
65.8⫾0.2
105.5⫾1.1
共393兲
piperidine–boron trichloride complex
共448 – 457兲
76.1
共453兲
piperidine–borane complex
共342–380兲
87.8
共361兲
1,2,3,3,4,4,5,5,6,6-decahydro-1,3,3,5,5-pentamethyl-2H-1,3,5,2,4,6thiadiazatriborine
57.7
2,8,9-trioxa-5-aza-1-boratricyclo关 3.3.3.0 1,5兴 undecane
111.9⫾0.9
共418兲
2,6-dimethylpyridine–borane complex
共358 –378兲
83.8
共368兲
2,9,10-trioxa-5-aza-1-boratricyclo关 4.3.3.01,6兴 dodecane
105.2⫾0.6
共390兲
2,10,11-trioxa-5-aza-1-boratricyclo关 4.4.3.01,6兴 tridecane
102.2⫾1.0
共390兲
2,10,11-trioxa-5-aza-1-boratricyclo关 4.4.4.01,6兴 tetradecane
97.9⫾1.0
共418兲
1,2-dicarbadodecaborane共12兲-1-carboperoxoic acid 1,1-dimethyl-2propynyl ester
共329–343兲
120.7⫾7.4
1,7-dicarbadodecaborane共12兲-1-carboperoxoic acid 1,1-dimethyl-2propynyl ester
共317–334兲
80.1⫾6.1
1-hexyl-o-carborane
86.2⫾1.4
共298兲
Method
ME
BG
BG
SG
Reference
关58/8兴
关703-86-6兴
关87/4兴
关75-22-9兴
关59/16兴
关87/4兴关37/1兴
关52/8兴
关4023-40-9兴
关88/16兴关66/7兴
关18178-04-6兴
关82/20兴关70/14兴
关18581-81-2兴
关82/20兴关70/14兴
关23087-98-1兴
关82/20兴关70/14兴
关16872-10-9兴
关82/20兴关76/13兴
关19610-34-5兴
关82/20兴关76/13兴
关53257-04-8兴
关82/20兴关76/13兴
关35795-98-3兴
关82/20兴关76/13兴
关4426-47-5兴
关56/12兴
关25928-66-9兴
关83/12兴
关61/9兴
关17032-21-2兴
关82/20兴关76/13兴
T
C
关68/16兴
关3022-54-6兴
关89/24兴
关89/24兴
GS
关60/19兴
关56/17兴
关37956-18-6兴
C
T
C
C
C
ME
ME
关72/27兴
关283-56-7兴
关84/14兴
关56/15兴
关283-62-5兴
关84/14兴
关283-64-7兴
关84/14兴
关283-65-8兴
关84/14兴
关146959-04-8兴
关99/43兴
关146959-05-9兴
关99/43兴
关20740-05-0兴
关82/20兴关78/23兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
636
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 7. Enthalpies of sublimation of organometallic and inorganic compounds, 1910–2001—Continued
Element
Compound
⌬ subH m /kJ mol⫺1
CAS registry number
(Tm /K)
Molecular formula/polymorph
Temperature range 共K兲
C11H24B10O3
1,2-dicarbadodecaborane共12兲-1-carboperoxoic acid 2-共1-methylethyl兲1,1-dimethyl-2-propynyl ester
共345–362兲
125.1⫾7.0
triphenylboron
103.8⫾2.5
共360兲
92.1⫾2.5
共298兲
81.6⫾2.1
tricyclohexylboron
81.6⫾4.2
共298兲
diboron tetrafluoride
共178 –209.5兲
35.5
共193兲
2,4,6-tribromoborazine
共342–395兲
86.2⫾0.4
2,4,6-trichloroborazine
共303–353兲
70.5⫾0.4
共313–357兲
71.1
2,4,6-trifluoroborazine
共273– 454兲
63.1⫾0.1
hexahydroborazine
共321–349兲
104.6⫾12.6
ammonia–triborane complex
共306 –328兲
71.5⫾0.4
共304 –327兲
71.5
C18H15B
C18H33B
B2 F4
B3 Br3 H3 N3
B3 Cl3 H3 N3
B3 F3 H3 N3
B3 H12N3
(NH3 ) – (B3 H7 )
Ba
(C10H2BaF12O4兲–共C12H24O6兲
C22H38BaO4
C34H42BaCu2 F24O8
C56H80BaF24O12Y2
Be
C10H2 BeF12O4
C10H8 BeF6 O4
C10H14BeO4
C12H18Be4 O13
monoclinic
form I
form II
C20H12BeF6 O4
C20H18BeO4
C22H38BeO4
Method
Reference
关146959-06-0兴
ME
TE,ME
I
I
I
ME
ME
关99/43兴
关960-71-4兴
关84/4兴
关78/2兴
关82/20兴关67/10兴
关1088-01-3兴
关82/20兴关67/10兴
关13965-73-6兴
关58/8兴
关13703-88-3兴
关66/9兴
关933-18-6兴
关66/9兴
关55/6兴
关13779-24-3兴
关66/9兴
关13871-09-5兴
关69/22兴关71/30兴
关59/16兴
关59/15兴
bis共1,1,1,5,5,5-hexafluoro-2,4-pentanedionato兲barium共II兲–18-crown-6
complex
共412– 468兲
104.9⫾1.3
共440兲
共428 – 473兲
115⫾2
共450兲
T
bis共2,2,6,6-tetramethylheptane-3,5-dionato兲barium共II兲
NA
共413– 473兲
90.2
共443兲
tetrakis共hexafluoroisopropoxy兲bis共2,2,6,6-tetramethylheptane-3,5-dionato兲
barium共II兲dicopper共II兲
共383– 448兲
102.7
共416兲
tetrakis共hexafluoroisopropoxy兲tetrakis共2,2,6,6-tetramethylheptane-3,5-dionato兲
barium共II兲diyttrium共III兲
共360– 403兲
84.8
共382兲
关143737-48-8兴
bis共1,1,1,5,5,5-hexafluoro-2,4-pentanedionato兲beryllium共II兲
共289–349兲
66.1
bis共1,1,1-trifluoro-2,4-pentanedionato兲berylium共II兲
共354 –383兲
85.3⫾6.3
88.0⫾6.5
U30.5
bis共2,4-pentanedionato兲berylium共II兲
94⫾1.0
95.3⫾2.0
82.3
91⫾1.4
85.3⫾3.5
U35.6
hexakis共aceto兲-oxotetraberyllium
共390– 451兲
115.3
115.3
共394 – 422兲
132.6
共426 – 446兲
113.4
bis共1-phenyl-4,4,4-trifluoro-1,3-butanedionato兲beryllium共II兲
U35.8
bis共benzoylacetonato兲berylium共II兲
共416 – 438兲
151.6⫾1.8
158.0⫾1.8
142.3⫾1.4
bis共2,2,6,6-tetramethylheptane-3,5-dionato兲berylium
关19648-82-9兴
关87/20兴
关13939-10-1兴
关87/20兴关88/22兴
关87/20兴
关60/17兴
关10210-64-7兴
关77/18兴关88/2兴
关88/25兴
关88/22兴
关85/5兴
关83/10兴
关60/17兴
关19049-40-2兴
关87/4兴
关59/17兴
关55/9兴
关55/9兴
关14052-07-4兴
关60/17兴
关14128-75-7兴
关95/9兴
关95/9兴
关83/20兴
关36915-22-7兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
共319兲
BG
共368兲
共298兲
BG
共298兲
共298兲
共298兲
共298兲
ME
BG
C
DSC
共420.5兲
共408兲
共436兲
I
共427兲
共298兲
共298兲
TE,ME
C
关95/22兴
关93/4兴
关155138-07-1兴
关94/40兴
关93/9兴
关16034-35-2兴
关96/7兴
关160669-81-8兴
关96/7兴
ENTHALPY OF SUBLIMATION
637
TABLE 7. Enthalpies of sublimation of organometallic and inorganic compounds, 1910–2001—Continued
Element
Compound
Molecular formula/polymorph
Temperature range 共K兲
BeF2
beryllium fluoride
共713–795兲
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
84.2
Bi
C15H30BiN3 S6
C18H15Bi
C21H42BiN3 S6
C27H54BiN3 S6
C27H54BiN3 S6
BiCl3
Ca
C22H38CaO4
Cd
C4 H16CdCl2 N8 S4
C10H14CdCl2 N6 O2
C10H14CdO4
C10H20CdN2 S4
C14H28CdN2 S4
C18H12CdN2 O2
C18H36CdN2 S4
C18H36CdN2 S4
C20H16CdN2 O2
C44H28CdN4
Ce
C15H15Ce
CeBr3
CeCl3
CeI3
Cf
(C15H3CfF18O6兲–2共C6H14OS兲
(C15H3CfF18O6兲–2共C12H27OP兲
共750兲
共755兲
236.4⫾2.9
231.8⫾1.7
tris共N,N-diethyldithiocarbamate兲bismuth共III兲
213⫾3
triphenylbismuth
110.9⫾8.4
tris共dipropyldithiocarbamate兲bismuth共III兲
285.2⫾5.0
tris共N,N-dibutyldithiocarbamate兲bismuth共III兲
202⫾3
tris共N,N-diisobutyldithiocarbamate兲bismuth共III兲
147⫾3
bismuth 共III兲 chloride
共371– 468兲
124.7
共371– 468兲
118.8⫾0.4
Reference
BG
关88/22兴
关7787-49-7兴
关65/20兴
关65/20兴
TE
MS
共298兲
DSC,E
共420兲
ME
ME
关20673-31-8兴
关94/31兴
关603-33-8兴
关82/20兴关79/22兴
关57407-97-3兴
关99/34兴
关34410-99-6兴
关94/31兴
关90285-80-6兴
关97/31兴
关7787-60-2兴
关66/8兴关59/11兴
关59/11兴
GS
关3618-89-0兴
关90/15兴
共298兲
共298兲
DSC,E
共298兲
bis共2,2,6,6-tetramethylheptane-3,5-dionato兲calcium共II兲
72.0
关28813-21-0兴
关70/11兴
trans-dichloro-tetrakis共thiourea兲cadmium共II兲
共377– 405兲
75⫾20
关 cadmium(1-methylcytosine) 2 Cl2 兴
共483–503兲
135.3⫾20
145⫾20
bis共2,4-pentanedionato兲cadmium共II兲
共438 – 448兲
144.9⫾22
154⫾22
bis共diethyldithiocarbamate兲cadmium共II兲
共433– 469兲
133.2
bis共dipropyldithiocarbamate兲cadmium共II兲
199⫾1
bis共8-hydroxyquinolinato兲cadmium共II兲
201.7⫾7.5
共438 – 448兲
144.9⫾22
154⫾22
bis共dibutyldithiocarbamate兲cadmium共II兲
123⫾3
bis共diisobutyldithiocarbamate兲cadmium共II兲
281⫾2
bis共8-hydroxy-2-methylquinolinate兲cadmium共II兲
共537–554兲
190.9⫾7.3
203.3⫾7.3
5,10,15,20-tetraphenylporphine cadmium共II兲
222⫾6
tris共cyclopentadienyl兲cerium
共528 – 653兲
cerium共III兲 bromide
共887–1003兲
cerium共III兲 chloride
共955–1070兲
cerium共III兲 iodide
共910–1031兲
Method
共493兲
共298兲
ME
共443兲
共298兲
ME
共451兲
共298兲
DSC,E
共298兲
共443兲
共298兲
ME
ME
共298兲
DSC,E
共298兲
DSC,E
共546兲
共298兲
ME
GS
104.6⫾2.1
300⫾10
共298兲
TE
331⫾5
共298兲
TE
295⫾10
共298兲
TE
tris共1,1,1,5,5,5-hexafluoro-2,4-pentanedionato兲californium-249–
dipropyl sulfoxide 共1:2兲 complex
共402– 434兲
93.6⫾6.0
tris共1,1,1,5,5,5-hexafluoro-2,4-pentanedionato兲californium-249–
tributylphosphine oxide 共1:2兲 complex
共431– 485兲
130.6⫾1.9
关84/12兴
关84/12兴
关14689-45-3兴
关84/12兴
关84/12兴
关14239-68-0兴
关87/4兴
关55519-99-8兴
关92/19兴
关14245-29-5兴
关94/16兴
关84/12兴
关84/12兴
关14566-86-0兴
关91/15兴
关69090-75-1兴
关94/33兴
关15685-78-6兴
关98/8兴
关98/8兴
关14977-07-2兴
关00/36兴
关1298-53-9兴
关73/31兴
关14457-87-5兴
关00/19兴
关7790-86-5兴
关00/19兴
关7790-87-6兴
关00/19兴
关123611-97-2兴
GS,TRM
关89/31兴
关123628-36-4兴
GS,TRM
关89/31兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
638
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 7. Enthalpies of sublimation of organometallic and inorganic compounds, 1910–2001—Continued
Element
Compound
⌬ subH m /kJ mol⫺1
Molecular formula/polymorph
Temperature range 共K兲
(C15H3CfF18O6兲–2共C12H27O4P兲
tris共1,1,1,5,5,5-hexafluoro-2,4-pentanedionato兲californium-249–
tributylphosphate 共1:2兲 complex
共413– 451兲
133.0⫾6.1
Cl
HCl
Co
C4 H16Cl2 CoN8 S4
C8 Co2 O8
C8 H10Cl2 CoN6 O2
C9 CoMnO9
C9 CoO9 Re
C10BrCo3 O9
C10ClCo3 O9
C10H8 Cl4 CoN2
C10H8 Cl4 CoN2
C10H10Co
C10H14CoO4
C12Co4 O12
C12H14Cl2 CoN2
C14H10Br2 CoN2 S2
C15H3 CoF18O6
C15H12CoF9 O6
C15H21CoO6
C15H30CoN3 S6
hydrogen chloride
共121–133兲
共134 –150兲
19.7
19.6
trans-dichloro-tetrakis共thiourea兲cobalt共II兲
共356 –382兲
129⫾20
octacarbonyldicobalt
共264 –278兲
84.3⫾0.5
共288 –315兲
103.8
65.2⫾3.3
共207–287兲
75.3⫾6.3
关 cobalt(cytosine) 2 Cl2 兴
共483–523兲
151.8⫾14
162⫾14
nonacarbonylcobaltmanganese
85⫾2
72⫾2
nonacarbonylcobaltrhenium
94⫾4
83⫾4
共bromomethylidyne兲tricobaltenneacarbonyl
99.6⫾1.7
共chloromethylidyne兲tricobaltenneacarbonyl
117.6⫾2.5
关 cobalt(2-chloropyridine) 2 Cl2 兴
共345–365兲
101.2⫾6.7
关 cobalt(3-chloropyridine) 2 Cl2 兴
共345–365兲
77.0⫾4.2
dicyclopentadienyl cobalt
72.1⫾0.1
70.3⫾4.2
bis共2,4-pentanedionato兲cobalt共II兲
共433– 463兲
149
共322–371兲
130.1⫾6.3
118.7⫾2.2
81.2
U62.8
tetracobaltdodecacarbonyl
96.2⫾4.2
关 cobalt(2-methylpyridine) 2 Cl2 兴
共345–365兲
86.6⫾3.8
关 cobalt(benzothiazole) 2 Br2 兴
共381–399兲
127.7⫾4.1
tris共1,1,1,5,5,5-hexafluoro-2,4-pentanedionato兲cobalt共III兲
共333–363兲
73
tris共1,1,1-trifluoro-2,4-pentanedionato兲cobalt共III兲
共373– 403兲
119
114⫾4.0
共383– 433兲
108.8⫾0.4
tris共2,4-pentanedionato兲cobalt共III兲
共433– 463兲
138
NA
共318 –382兲
134.6⫾4.0
142.6⫾6.9
86.3
107.1
74.9⫾4.6
U13.0
tris共diethyldithiocarbamato兲cobalt共III兲
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
CAS registry number
(Tm /K)
Method
Reference
关123712-43-6兴
GS,TRM
共127兲
共142兲
共271兲
共301.5兲
共298兲
关90/33兴
关90/33兴
TE
EM
共503兲
共298兲
ME
共308兲
共298兲
C
共313兲
共298兲
C
共298兲
共298兲
共355兲
DSC
共355兲
DSC
共298兲
共298兲
共298兲
共370兲
TGA
ME
共298兲
共355兲
DSC
共390兲
DSC
TGA
TGA
共298兲
GS
TGA
共298兲
共471兲
共390兲
关89/31兴
ME
DSC
关22738-43-8兴
关70/11兴
关10210-68-1兴
关95/36兴
关87/4兴关68/15兴
关82/20兴关75/26兴
关73/26兴
关74543-51-4兴
关84/12兴
关84/12兴
关35646-82-3兴
关98/33兴
关98/33兴
关15039-80-2兴
关98/33兴
关98/33兴
关19439-14-6兴
关82/20兴关75/26兴
关13682-02-5兴
关82/20兴关75/26兴
关14361-73-0兴
关82/18兴
关14361-78-5兴
关82/18兴
关1277-43-6兴
关88/3兴
关82/20兴关75/23兴
关14024-48-7兴
关00/35兴
关90/21兴
关85/5兴
关70/10兴
关60/17兴
关17786-31-1兴
关82/20兴关74/26兴
关13869-67-5兴
关82/18兴
关21422-14-0兴
关73/28兴
关16702-37-7兴
关00/35兴
关16827-64-8兴
关00/35兴
关88/1兴
关85/16兴
关21679-46-9兴
关00/35兴
关94/34兴
关90/21兴
关87/13兴
关71/17兴
关70/10兴
关64/4兴
关61/8兴
关13963-60-5兴
ENTHALPY OF SUBLIMATION
639
TABLE 7. Enthalpies of sublimation of organometallic and inorganic compounds, 1910–2001—Continued
Element
Molecular formula/polymorph
C16H14Br2 CoN2 O2
C16H14Cl2 CoN2 O2
C16H14Br2 CoN2 S2
C16H14Cl2 CoN2 S2
C18H12CoN2 O2
Compound
Temperature range 共K兲
共448 –587兲
关 cobalt(2-methylbenzoxazole) 2 Br2 兴
共345–390兲
关 cobalt(2-methylbenzoxazole) 2 Cl2 兴
共345–390兲
关 cobalt(2-methylbenzothiazole) 2 Br2 兴
共335–354兲
关 cobalt(2-methylbenzothiazole) 2 Cl2 兴
共332–356兲
bis共8-hydroxyquinolinato兲cobalt共II兲
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
95⫾6
共518兲
111.1⫾4.2
共368兲
DSC
92.4⫾2.5
共368兲
DSC
115.1⫾4.1
共345兲
DSC
122.6⫾1.2
共345兲
DSC
205.3⫾4.0
共298兲
185.7⫾9
共551兲
200⫾10
共298兲
dibenzotetra-aza–annulene cobalt共II兲 complex
178.2⫾16.7
共360兲
关 cobalt(2,5-dimethylbenzoxazole) 2 Br2 兴
共345–390兲
95.4⫾4.6
共368兲
关 cobalt(2,5-dimethylbenzoxazole) 2 Cl2 兴
共345–390兲
104.6⫾5.8
共368兲
bis共8-hydroxy-2-methylquinolinate兲cobalt共II兲
共457– 473兲
196.1⫾5.9
共465兲
204.4⫾5.9
共298兲
bis共2,2,6,6-tetramethyl-3,5-heptanedionato兲cobalt共II兲
共433– 463兲
143
tris共1-共2-thenoyl兲-4,4,4-trifluoro-1,3-butanedione兲cobalt共III兲
45.6
tris共2-furoyltrifluoroacetonato兲cobalt共III兲
35.6
tris共1-phenyl-4,4,4-trifluoro-1,3-butanedionato兲cobalt共III兲
51.0
tris共1-phenyl-1,3-butanedionato兲cobalt共III兲
39.0
cobalt 共II兲 phthalocyanine
183.7⫾13.8
bis共2,2,6,6-tetramethyl-3,5-heptanedionato兲共2,2⬘-bipyridyl兲cobalt共II兲
126⫾4.0
130.3
124.4
tris共2,2,6,6-tetramethyl-3,5-heptanedionato兲cobalt共III兲
共433– 463兲
132
126⫾3.0
共298兲
cobalt共II兲 bromide
共764 –911兲
207⫾4.0
共802兲
216⫾1.0
共298兲
共533–569兲
C18H14CoN4
C18H18Br2 CoN2 O2
C18H18Cl2 CoN2 O2
C20H16CoN2 O2
C22H38CoO4
C24H12CoF9 O6 S3
C24H12CoF9 O9
C30H18CoF9 O6
C30H27CoO6
C32H16CoN8
C32H46CoN2 O4
C33H57CoO6
CoBr2
Cr
C6 CrO6
chromium hexacarbonyl
共266 –272兲
共323–391兲
共288 – 423兲
共240–280兲
共274 –301兲
共319– 411兲
C8 H3 CrNO5 S
C8 H4 CrN2 O5
C8 H9 CrNO5
65.7
68.5⫾1.1
68.5
68.9⫾2
70.0⫾2
71.6⫾1.7
69.5
72.0⫾4.2
71.5⫾0.8
69.3
71.9
63.6
共308 – 408兲
thiazole共pentacarbonyl兲chromium
共270–301兲
102.0⫾2.7
pyrazole共pentacarbonyl兲chromium
共270–303兲
88.4⫾1.8
trimethylamine共pentacarbonyl兲chromium
Method
ME
ME
DSC
DSC
ME
TGA
ME
B
UV/Vis
MEM
TGA
TE
共269兲
TE
共355.5兲
共298兲
共298兲
共260兲
共298兲
共298兲
共288兲
C
ME
C
共358兲
MM
共286兲
ME
共287兲
ME
BG
Reference
关79/20兴
关22974-96-5兴
关82/18兴关74/27兴
关52657-96-2兴
关82/18兴关74/27兴
关26225-02-5兴
关73/28兴
关26225-01-4兴
关73/28兴
关13978-88-6兴
关94/16兴
关84/12兴
关84/12兴
关41283-94-7兴
关82/25兴
关52230-48-5兴
关82/18兴关74/27兴
关52230-47-4兴
关82/18兴关74/27兴
关17992-18-6兴
关98/8兴
关98/8兴
关13986-53-3兴
关00/35兴
关41875-84-7兴
关61/8兴
关64137-83-3兴
关61/8兴
关31125-84-5兴
关61/8兴
关14524-55-1兴
关61/8兴
关3317-67-7兴
关70/7兴
关18347-53-8兴
关96/24兴
关96/24兴
关96/24兴
关14877-41-3兴
关00/35兴
关88/1兴
关7789-43-7兴
关97/20兴
关97/20兴
关13007-92-6兴
关95/36兴
关93/28兴
关87/4兴
关84/17兴
关83/20兴
关80/34兴关79/19兴
关75/20兴
关82/20兴关75/24兴
关66/17兴
关52/7兴
关35/2兴
关34/3兴
关55293-31-7兴
关79/19兴
关71127-65-6兴
关79/19兴
关15228-26-9兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
640
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 7. Enthalpies of sublimation of organometallic and inorganic compounds, 1910–2001—Continued
Element
Molecular formula/polymorph
C8 H9 CrO5 P
C8 H12CrMoO8
C8 H12Cr2 O8
C9 H4 CrN2 O5
C9 H5 ClCrO3
C9 H6 CrO3
C10H5 CrNO5
C10H8 CrO3
C10H8 CrO3
C10H8 CrO4
C10H10Cr
C10H14CrO4
C10H11CrNO5
C11H8 CrO4
C11H8 CrO4
C11H8 CrO5
C11H11CrNO3
C12H12Cr
C12H12CrO3
C12H12CrO3
C13H8 CrO3
C15H3 F18CrO6
C15H12CrF9 O6
Compound
Temperature range 共K兲
⌬ subH m /kJ mol⫺1
共248 –293兲
80.2⫾0.7
trimethylphosphine共pentacarbonyl兲chromium
91.2⫾1.6
chromium molybdenum tetraacetate
165.0⫾8.4
tetra-␮-acetatodichromium共II兲
共330–340兲
299.6⫾10
313.8⫾27.0
145
pyrazine共pentacarbonyl兲chromium
99.7
chlorobenzenechromium tricarbonyl
102.5⫾4.2
benzene chromium tricarbonyl
91.2
U58.6
共364 –370兲
97.9
pyridine共pentacarbonyl兲chromium
共294 –317兲
103.2⫾1.8
cycloheptatriene chromium tricarbonyl
94.1
␩ 6 -toluene共tricarbonyl兲chromium
93.0⫾2.0
94.6⫾4.2
␩ 6 -anisole共tricarbonyl兲chromium
104.2⫾2.0
dicyclopentadienyl chromium
71.0
62.8⫾4.2
69.9⫾1.7
bis共2,4-pentanedionato兲chromium共II兲
共330–370兲
129.8⫾8.7
111
piperidine共pentacarbonyl兲chromium
共265–298兲
93.5⫾1.9
norbornadienechromium tetracarbonyl
89.0⫾4.0
␩ 6 -acetophenone共tricarbonyl兲chromium
107.0⫾0.6
␩ 6 -methyl benzoate共tricarbonyl兲chromium
114.0⫾5.0
␩ 6 -N,N-dimethylaniline共tricarbonyl兲chromium
118.4⫾10
dibenzenechromium
共323–363兲
89.4
78.2⫾6.3
82.0⫾2.1
90.6⫾0.3
78.2⫾6.2
mesitylene chromium tricarbonyl
108.4
U64.4
共1,2,4-trimethylbenzene兲 chromium tricarbonyl
U33.5
共1,2,3,4,4a,8a-h-naphthalene兲tricarbonyl chromium
107⫾3
tris共1,1,1,5,5,5-hexafluoro-2,4-pentanedionato兲chromium共III兲
共333–363兲
46
112⫾4.0
共333–360兲
123.0⫾1.3
tris共1,1,1-trifluoro-2,4-pentanedionato兲chromium共III兲
共373– 403兲
71
182⫾4.0
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
CAS registry number
(Tm /K)
共271兲
Method
Reference
ME
关80/34兴
关26555-09-9兴
关80/34兴
关71561-64-3兴
关82/20兴
关15020-15-2兴
关84/20兴
关82/20兴
关79/23兴
关66179-02-0兴
关79/19兴
关12082-03-0兴
关82/20兴关75/20兴
关12082-08-5兴
关75/20兴
关61/4兴关73/29兴
关59/6兴关73/29兴
关14740-77-3兴
关79/19兴
关12125-72-3兴
关75/20兴
关12125-87-0兴
关84/17兴
关82/20兴关75/20兴
关12116-44-8兴
关84/17兴
关1271-24-5兴
关84/24兴
关82/20兴关75/23兴
关77/24兴
关14024-50-1兴
关90/21兴
关81/15兴
关15710-39-1兴
关79/19兴
关12146-36-0兴
关82/20兴关77/22兴
关12153-11-6兴
关84/17兴
关12125-87-0兴
关84/17兴
关12109-10-3兴
关84/17兴
关1271-54-1兴
关87/4兴
关82/20兴关73/29兴
关73/22兴
关69/21兴
关58/13兴
关12129-67-8兴
关75/20兴
关61/5兴关77/21兴
关32913-41-0兴
关61/5兴关77/21兴
关12110-37-1兴
关79/16兴
关14592-80-4兴
关00/35兴
关87/12兴
关72/17兴
关14592-89-2兴
关00/35兴
关87/12兴
ME
共335兲
共298兲
ME,TE
E
ME
共298兲
共298兲
C
TE
共306兲
ME
共298兲
C
共298兲
共298兲
C
共298兲
C
共298兲
共298兲
共298兲
共439兲
ME
T
共282兲
ME
共298兲
共298兲
C
共298兲
C
共298兲
C
共343兲
共298兲
ME
共298兲
共298兲
C
共298兲
C
TGA
共298兲
共335兲
共426兲
TGA
C
ENTHALPY OF SUBLIMATION
641
TABLE 7. Enthalpies of sublimation of organometallic and inorganic compounds, 1910–2001—Continued
Element
Molecular formula/polymorph
Compound
Temperature range 共K兲
⌬ subH m /kJ mol⫺1
117⫾4.0
115.1⫾0.8
112.5⫾4.8
53.6
共377– 413兲
108.8⫾1.3
hexamethylbenzene chromium tricarbonyl
123.0⫾4.0
tris共2,4-pentanedionato兲chromium共III兲
共413– 443兲
91
共350–375兲
126.8⫾4.2
共457– 486兲
113.0⫾4.8
132.1⫾1.9
28.9
112.1
共363–393兲
40.2⫾1.7
110.9⫾0.8
123⫾3.0
共373– 438兲
共403– 423兲
C15H18CrO3
C15H21CrO6
C18H24Cr
C20H16Cr
C23H15CrO5 P
C24H24Cr2 N4 O4
C24H36Cr
C30H27CrO6
C30H30F21CrO6
C33H57CrO6
CrI2
Cs
C5 H9 CsO2
CAS registry number
(Tm /K)
Method
共298兲
65
关87/12兴
关85/16兴
关78/29兴
关77/25兴
关72/17兴
关12088-11-8兴
关75/20兴关77/22兴
关21679-31-2兴
关00/35兴
关90/21兴
关88/22兴关87/21兴
关85/5兴
关77/25兴
关70/10兴
关72/17兴
关70/9兴关70/17兴
关77/18兴关88/2兴
关67/11兴
关1274-07-3兴
关79/16兴
关33085-81-3兴
关79/16兴
关14917-12-5兴
关80/34兴
关67634-82-6兴
关82/20兴关81/18兴
关12156-66-0兴
关79/16兴
关16432-36-3兴
关87/12兴
关17966-86-8兴
关72/17兴
关14434-47-0兴
关00/35兴
关87/12兴
关13478-28-9兴
关56/19兴
共298兲
共298兲
共298兲
共298兲
GS
T
T
MS
关20442-70-0兴
关98/31兴
关7789-17-5兴
关98/4兴
关85/15兴关98/4兴
关84/29兴关98/4兴
关84/28兴关98/4兴
共298兲
共458兲
C
GS
共447兲
共395兲
共298兲
共298兲
共298兲
共463兲
共390兲
共378兲
共298兲
共298兲
bis共␩ 6 -1,3,5-trimethylbenzene兲chromium
104⫾1
共298兲
bis共naphthalene兲chromium
105.0⫾10
triphenylphosphine共pentacarbonyl兲chromium
共324 –347兲
170.2⫾6.8
共336兲
tetrakis共6-methyl-2-hydroxypyridyl兲dichromium共II兲
150.0⫾4.0
共298兲
bis共␩ 6 -hexamethylbenzene兲chromium
119⫾4
共298兲
tris共1-phenyl-1,3-butanedionato兲chromium共III兲
186⫾2
共298兲
tris共1,1,1,2,2,3,3-heptafluoro-7,7-dimethyl-4,6-octanedionato兲chromium共III兲
共323–353兲
37.7⫾0.8
共338兲
tris共2,2,6,6-tetramethyl-3,5-heptanedionato兲chromium共III兲
共413– 443兲
85
133⫾2
共298兲
chromium II iodide
共943–1054兲
298.7
共298兲
C
TGA
ME
BG
C
HSA
ME
C
ME
C
TGA
cesium pivalate
163.5⫾7.2
CsI
cesium iodide
195.6
193.1
193.1
191.1
Cu
C6 H12CuN2 S4
C8 H12Cu2 O8
C8 H14CuN4 O4
bis共dimethyldithiocarbamato兲 copper complex
156.0⫾0.3
共443– 473兲
147.4⫾0.8
149.0⫾2.5
tetrakis共acetato兲dicopper共II兲
共321–360兲
106.1⫾0.9
C10H2 CuF12O4
C10H8 CuF6 O4
GC
共298兲
ME,
TE
共298兲
TE,
ME
共298兲
C
bis共dimethylglyoxime兲copper共II兲
93.1⫾0.8
bis共1,1,1,5,5,5-hexafluoro-2,4-pentanedionato兲copper共II兲
108⫾6
bis共1,1,1-trifluoro-2,4-pentanedionato兲copper共II兲
共373– 403兲
112
共342–359兲
113.3⫾2.4
115.9⫾2.4
共342–359兲
114.4⫾1.6
Reference
共350兲
共298兲
共350兲
TGA
TE
ME
关137-29-1兴
关95/21兴
关87/4兴关78/12兴
关76/21兴
关24411-13-0兴
关90/2兴
关14221-10-4兴
关90/2兴
关14781-45-4兴
关88/7兴
关14324-82-4兴
关00/35兴
关95/4兴
关95/4兴
关95/4兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
642
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 7. Enthalpies of sublimation of organometallic and inorganic compounds, 1910–2001—Continued
Element
Molecular formula/polymorph
Compound
Temperature range 共K兲
共383– 463兲
C10H14CuO4
bis共2,4-pentanedionato兲copper共II兲
共413– 443兲
共377–398兲
共377–398兲
共315–386兲
C10H20CuN2 S4
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
117.0⫾1.6
112⫾3.0
110.0⫾0.8
U50.6
共298兲
共298兲
120
122.5⫾1.2
122.5⫾1.2
122.6⫾0.7
127.1⫾1.2
122.3⫾1.1
127.0⫾1.1
116.6⫾2.0
115.1⫾2.1
142.6⫾6.9
107.1⫾5.7
127.5⫾3.2
154⫾22
109.9⫾3.4
57.1
109.6
106.1
109⫾6
57.3
62.8
共387兲
共298兲
共387兲
共298兲
共393兲
共298兲
共298兲
共298兲
共471兲
共492兲
共298兲
共298兲
共298兲
Method
C
GS
TGA
TE
ME
ME
C
DSC
C
TE
TG
共400兲
DSC
bis共diethyldithiocarbamate兲copper共II兲
162.6⫾5
共298兲
149.1⫾0.4
共442.5兲
103.8⫾2.4
116.2⫾1.3
149.0⫾2.5
87⫾1.7
bis共1,1,1-trifluorohexane-2,4-dione兲copper共II兲
119.1⫾1.7
共298兲
bis共3-methyl-2,4-pentanedionato兲copper共II兲
130.7⫾1
共396.7兲
135.6⫾1
共298兲
132.7⫾2.5
共298兲
bis共1,1,1-trifluoro-5-methylhexane-2,4-dione兲copper共II兲
122.4⫾0.9
共298兲
bis共dipropyldithiocarbamate兲copper complex
158.6⫾5
共298兲
118.4⫾3.3
bis共diisopropyldithiocarbamate兲copper complex
共440– 465兲
129.5⫾2.9
共452.5兲
bis共4,4,4-trifluoro-1-共2-furanyl兲butane-1,3-dione兲copper共II兲
161.1⫾2.1
共298兲
bis共1,1,1-trimethyl-5,5,5-trifluoro-2,4-pentanedionato兲copper共II兲
120.2⫾1.0
共298兲
共353–379兲
102⫾3
共366兲
共381– 443兲
76.5⫾2 共liq兲
共412兲
bis共1,1,1-trifluoro-5-methylheptane-2,4-dione兲copper共II兲
122.5⫾0.9
共298兲
bis共1,1,1-trimethyl-5,5,5-trifluoro-2,4-pentanedionato兲copper共II兲-15-crown-5
complex
共368 – 443兲
80.2⫾2 共liq兲
共405兲
bis共8-hydroxyquinolinato兲copper共II兲
168.7⫾7.3
共298兲
共478 –503兲
160.3⫾3
共491兲
170⫾3
共298兲
dibenzotetra-aza–annulene copper共II兲 complex
共493–553兲
99.7⫾8.7
共523兲
bis共2,2-dimethylheptane-3,5-dionato兲copper共II兲
共420– 465兲
C12H12CuF6 O4
C12H18CuO4
C14H16CuF6 O4
C14H28CuN2 S4
C14H28CuN2 S4
C16H8 CuF6 O6
C16H20CuF6 O4
C16H20CuF6 O4
(C16H20F6 O4 Cu)
(C10H20O5 )
C18H12CuN2 O2
C18H14CuN4
C18H30CuO4
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
I
ME
ME
C
ME
ME
ME
T
T
ME
T
ME
ME
T
Reference
关95/4兴
关88/7兴
关85/16兴
关60/17兴
关13395-16-9兴
关00/35兴
关95/4兴
关95/4兴
关95/4兴
关95/4兴
关95/4兴
关95/4兴
关94/7兴
关91/17兴
关87/12兴
关87/13兴
关85/5兴
关84/12兴
关84/11兴
关81/13兴
关72/24兴
关71/17兴
关70/10兴
关71/18兴
关62/8兴
关13681-87-3兴
关89/10兴
关87/4兴关78/12兴
关79/20兴
关79/14兴
关76/21兴
关69/15兴
关30133-85-8兴
关98/32兴
关14781-49-8兴
关92/8兴
关92/8兴
关92/8兴
关33896-35-4兴
关98/32兴
关14354-08-6兴
关89/10兴
关78/12兴
关14354-07-5兴
关87/4兴关78/12兴
关13928-10-4兴
关98/32兴
关150026-91-8兴
关98/32兴
关93/4兴
关93/4兴
关220869-88-5兴
关98/32兴
关93/4兴
关10380-26-6兴
关94/16兴
关84/12兴
关84/12兴
关41283-96-9兴
关83/29兴
关15321-96-7兴
ENTHALPY OF SUBLIMATION
643
TABLE 7. Enthalpies of sublimation of organometallic and inorganic compounds, 1910–2001—Continued
Element
Molecular formula/polymorph
Compound
Temperature range 共K兲
⌬ subH m /kJ mol⫺1
CAS registry number
(Tm /K)
共344 –364兲
C18H30CuO4
C20H12CuF6 O4
C20H16CuN2 O2
C20H18CuO4
C20H20CuF14O4
C20H34CuO4
C22H24CuN2 O2
C22H38CuO4
C28H16CuF6 O4
C32H16CuN8
C32H16CuN8
C39H59F12O8 CuY
C44H28CuN4
125.0⫾1.3
共354兲
127.8⫾1.3
共298兲
共344 –364兲
125.1⫾0.5
共354兲
127.9⫾0.5
共298兲
122.8⫾1.7
共298兲
bis共2,6-dimethylheptane-3,5-dionato兲copper共II兲
118.0⫾347
共298兲
bis共4,4,4-trifluoro-1-phenylbutane-1,3-dione兲copper共II兲
172.1⫾3.1
共298兲
bis共8-hydroxy-2-methylquinolinate兲copper共II兲
共402– 419兲
166.5⫾3.4
共410兲
172.1⫾3.4
共298兲
bis共1-phenylbutane-1,3-dionato兲copper共II兲
共429– 450兲
152.2⫾1.7
共439兲
159.3⫾1.7
共298兲
共429– 450兲
152.2⫾1.9
共439兲
159.3⫾1.9
共298兲
160⫾4
共298兲
bis共1,1,1,2,2,3,3-hetafluoro-7,7-dimethyloctane-4,6-dionato兲copper共II兲
122.8⫾0.7
共298兲
bis共2,2,6-trimethylheptane-3,5-dionato兲copper共II兲
共346 –362兲
127.4⫾0.7
共354兲
130.2⫾0.7
共298兲
共346 –362兲
127.8⫾1.5
共354兲
130.6⫾1.5
共298兲
129.0⫾1.3
共351兲
131.7⫾1.3
共298兲
126.4⫾1.1
共298兲
bis关共4-phenylimino-2-pentanoato兲兴copper共II兲
128.1⫾0.8
共298兲
bis共2,2,6,6-tetramethylheptane-3,5-dionato兲copper共II兲
共345–377兲
127.6⫾0.4
共361兲
共335–366兲
127.2⫾1.7
共351兲
共433– 463兲
120
共400– 430兲
74.8
共392– 415兲
100
共404兲
124.5⫾0.8
共372兲
129.1⫾0.8
共298兲
共362– 452兲
124.6
共407兲
共418 – 473兲
123.6
共445兲
105.9
111.6
122.8⫾6.5
共298兲
112
bis共4,4,4-trifluoro-1-共2-naphthalenyl兲butane-1,3-dione兲copper共II兲
208.4.1⫾4.9
共298兲
copper共II兲 ␣-phthalocyanine
114.0
copper共II兲 ␤-phthalocyanine
共618 –713兲
231.8⫾2.1
211.1
共657– 863兲
266.1
共657–722兲
266.1⫾5.1
bis共hexafluoroisopropoxy兲tris共2,2,6,6-tetramethylheptane-3,5-dionato兲
copper共II兲yttrium共III兲
共370– 410兲
81.2
共390兲
5,10,15,20-tetraphenylporphine copper共II兲
160⫾5
Dy
C15H15Dy
tris共cyclopentadienyl兲dysprosium共III兲
C30H30DyF21O6
105.0⫾2.1
tris共1,1,1,2,2,3,3-heptafluoro-7,7-dimethyloctane-4,6-dione兲dysprosium共III兲
Method
Reference
TE
关95/4兴
关95/4兴
关95/4兴
关95/4兴
关84/11兴
关17653-77-9兴
关84/11兴
关14126-89-7兴
关98/32兴
关14522-43-1兴
关98/8兴
关98/8兴
关14128-84-8兴
关95/4兴
关95/4兴
关95/4兴
关95/4兴
关79/21兴
关38926-19-1兴
关98/32兴
关141752-16-3兴
关95/4兴
关95/4兴
关95/4兴
关95/4兴
关95/4兴
关95/4兴
关84/11兴
关15214-38-7兴
关90/2兴
ME
ME
ME
TE
ME
C
ME
ME
TE
ME
ME,
TE
TE
TE
TGA
TGA,DTA
T
ME
GS
C
C
ME
关14040-05-2兴
关01/6兴
关01/6兴
关00/35兴
关96/29兴
关96/4兴
关95/4兴
关95/4兴
关93/9兴
关92/18兴
关90/15兴
关88/23兴关93/9兴
关84/11兴
关84/11兴
关30983-56-3兴
关98/32兴
ME
关95/35兴
关147-14-8兴
关00/30兴
关95/35兴
关69/23兴
关65/15兴关70/7兴
GS
关160364-36-3兴
关96/7兴
关14172-91-9兴
关00/36兴
TGA
ME
TGA
关12088-04-9兴
关73/32兴
关18232-98-3兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
644
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 7. Enthalpies of sublimation of organometallic and inorganic compounds, 1910–2001—Continued
Element
Molecular formula/polymorph
C33H57O6 Dy
DyBr3
DyCl3
DyI3
Er
C15H12ErF9 O6
C15H15Er
C24H33Er
C30H30ErF21O6
C33H57O6 Er
Eu
C33H57O6 Eu
Fe
C2 FeN2 O4
C4 FeI2 O4
C4 H16Cl2 FeN8 S4
C6 H5 FeIO3
C8 H6 Fe2 O6 S2
C9 Fe2 O9
C9 H12FeO
C10H10Fe
Compound
Temperature range 共K兲
⌬ subH m /kJ mol⫺1
共370–385兲
156.5⫾2.9
tris共2,2,6,6-tetramethylheptane-3,5-dionato兲dysprosium共III兲
共373–388兲
171.5
共388 – 413兲
152.7
共410– 456兲
133.5
dysprosium tribromide
共878 –1151兲
289⫾6.0
dysprosium trichloride
共924 –1214兲
283⫾5.0
dysprosium triiodide
共889–1157兲
282⫾4.0
CAS registry number
(Tm /K)
dicarbonyldinitrosyl iron
共272–291兲
irontetracarbonyl diiodide
47.2
86.0⫾4.0
trans-dichloro-tetrakis共thiourea兲iron共II兲
共372– 405兲
110⫾20
allylirontricarbonyl iodide
84.5⫾4.0
hexacarbonylbis共methanethiolato兲diiron
102.8
109.8
diiron nonacarbonyl
共296 –314兲
135.3
75.3⫾21.0
bis共1,3-butadiene兲ironcarbonyl
76.1⫾4.2
ferrocene
73.3⫾0.1
74.3⫾0.4
73.2⫾0.7
共292–300兲
72.5⫾1.0
72.4⫾1.0
共294 –302兲
70.3⫾1.0
共278 –309兲
72.1⫾0.4
71.9⫾0.4
共348 – 446兲
64.6
75.6⫾0.4
74.0⫾2
共328 –398兲
70.0⫾2
72.6⫾1.4
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
Reference
ME
关71/25兴
关15522-69-7兴
关81/21兴
关81/21兴
关69/19兴
关14456-48-5兴
关99/20兴
关10025-74-8兴
关99/20兴
关15474-63-2兴
关99/20兴
共380兲
共400兲
共433兲
ME
ME
BG
共298兲
TE
共298兲
TE
共298兲
TE
tris共1,1,1-trifluoro-2,4-pentanedionato兲erbium共III兲
共473– 494兲
79.5⫾11.5
共484兲
tris共cyclopentadienyl兲erbium共III兲
共503–558兲
97.2⫾3.2
共530兲
97.1⫾3.3
tris关共1,2,3,4,5-␩兲-1-共1-methylethyl兲-2,4-cyclopentadien-1-yl兴erbium共III兲
共464 –502兲
78.6⫾3.0
共483兲
tris共1,1,1,2,2,3,3-heptafluoro-7,7-dimethyloctane-4,6-dione兲erbium共III兲
共349–362兲
154.8⫾4.2
tris共2,2,6,6-tetramethylheptane-3,5-dionato兲erbium共III兲
130.8⫾2.2
共298兲
共471–505兲
93.9⫾4.6
共488兲
共363– 418兲
154.0
共390兲
共358 –381兲
149.3⫾1.7
共410– 454兲
133.2
共432兲
tris共2,2,6,6-tetramethylheptane-3,5-dionato兲europium共III兲
共363– 433兲
179.9
共373– 423兲
180.0
共430– 466兲
165.4
Method
共398兲
共448兲
ME
ME
BG
关70332-27-3兴
关96/27兴
关39330-74-0兴
关96/27兴
关73/32兴
关130521-76-5兴
关96/27兴
关17978-75-5兴
关71/25兴
关14319-09-6兴
关99/33兴
关96/27兴
关81/21兴
关71/25兴
关69/19兴
ME
ME
BG
关15522-71-1兴
关81/21兴
关79/30兴
关69/19兴
ME
DSC
共281.5兲
共298兲
共298兲
共333兲
共298兲
C
共305兲
共298兲
共298兲
共298兲
共298兲
共298兲
共296兲
共298兲
共298兲
共294兲
共298兲
共397兲
共298兲
共298兲
共298兲
C
ME
C
ME
ME
ME
TE,ME,DM
TE
C
ME
关13682-74-1兴
关87/4兴
关14878-30-9兴
关82/20兴关79/25兴
关28813-18-5兴
关70/11兴
关12189-10-5兴
关82/20兴关79/25兴
关14878-96-7兴
关95/34兴
关95/34兴
关15321-51-4兴
关87/4兴
关82/20兴关72/21兴
关82/20兴关76/16兴
关102-54-5兴
关01/5兴
关95/15兴
关95/15兴
关90/3兴
关90/3兴
关89/3兴关90/3兴
关88/3兴
关88/3兴
关87/4兴
关83/6兴
关81/10兴
关80/20兴
关80/24兴
ENTHALPY OF SUBLIMATION
645
TABLE 7. Enthalpies of sublimation of organometallic and inorganic compounds, 1910–2001—Continued
Element
Molecular formula/polymorph
Compound
Temperature range 共K兲
共385– 455兲
C10H10Fe2 O6 S2
C10H14FeO4
共323–367兲
共357– 455兲
hexacarbonylbis共ethanethiolato兲diiron
bis共2,4-pentanedionato兲iron共II兲
共330–368兲
C11H8 FeO3
cyclooctatetraeneirontricarbonyl
C12H12FeO
C12Fe3 O12
acetylferrocene
共329–358兲
triiron dodecacarbonyl
C13H16FeO
bis共1,3-cyclohexadiene兲ironcarbonyl
C14H14FeO2
C15H3 F18FeO6
C15H12F9 FeO6
C15H21FeO6
(Tm /K)
73.6⫾0.4
74.1⫾1.7
84.0⫾2
72.7⫾2
76.6⫾1
83.3
70.5
共298兲
共298兲
105.4
112.0
共340兲
共298兲
C
131.2⫾8.7
117.6
共298兲
共385兲
ME
87.0⫾4.0
共298兲
115.6⫾2.5
共298兲
96.0⫾21.0
共298兲
95.0⫾4.2
1,1⬘ -diacetylferrocene
共360– 400兲
91.9⫾2.5
tris共1,1,1,5,5,5-hexafluoro-2,4-pentanedionato兲iron共III兲
共333–363兲
60
tris共1,1,1-trifluoro-2,4-pentanedionato兲iron共III兲
共373– 403兲
96
共378 – 438兲
104.6⫾0.8
80.3
128.9
87.0
tris共2,4-pentanedionato兲iron共III兲
共413– 443兲
112
118
共369–388兲
124.6⫾0.9
128.6⫾0.9
共338 –355兲
114.2⫾1.5
共309–360兲
126.4⫾3.1
138.4⫾5.2
100
113.6⫾3.8
99⫾0.8
114.2
65.3⫾3.3
U23.4
81.6
C15H30FeN3 S6
C17H14FeO
C18H27FeO6
C20H30Fe
C24H12F9 FeO6 S3
C24H18FeO2
C30H27FeO6
C33H57FeO6
CAS registry number
⌬ subH m /kJ mol⫺1
共298兲
共298兲
共406兲
Method
TCM
C
ME
ME
ME
BG
共298兲
共298兲
TGA
TGA
GS
共433兲
共345兲
共378兲
共298兲
共298兲
共298兲
共395兲
TGA
TGA
TE,ME
ME
C
T
共385兲
共298兲
I
tris共diethyldithiocarbamoto兲iron共III兲
65.7⫾1.7
benzoylferrocene
共358 –382兲
116.3⫾6
tris共3-methylpentane-2,4-dionato兲iron共III兲
164.5
bis共␩ 5 -pentamethylcyclopentadienyl兲iron
96.8⫾0.6
tris共1-共2-thenoyl兲-4,4,4-trifluoro-1,3-butanedione兲ironIII兲
U46.4
1,1⬘ -dibenzoylferrocene
共358 –381兲
109.3⫾6
tris共benzoylacetonato兲iron共III兲
U45.6
tris共2,2,6,6-tetramethylheptane-3,5-dionato兲iron共III兲
共413– 443兲
111
共246兲
共298兲
TE,ME
共422兲
共298兲
C
共298兲
TE,ME
I
TGA
Reference
关82/20兴关75/23兴
关73/1兴
关71/6兴
关69/4兴
关62/7兴
关59/6兴
关52/6兴
关28829-01-8兴
关95/34兴
关95/34兴
关14024-17-0兴
关90/21兴
关70/10兴
关12093-05-9兴
关82/20兴关79/25兴
关1271-55-2兴
关81/10兴
关17685-52-8兴
关82/20兴关72/21兴
关34978-83-1兴
关82/20兴关76/16兴
关1273-94-5兴
关81/10兴
关17786-67-3兴
关00/35兴
关14526-22-8兴
关00/35兴
关85/16兴
关77/25兴
关70/10兴
关60/17兴
关14024-18-1兴
关00/35兴
关97/29兴
关96/3兴
关96/3兴
关92/11兴
关90/21兴
关85/5兴
关81/15兴
关80/30兴
关79/21兴关81/15兴
关70/17兴
关70/10兴
关82/20兴关68/13兴
关64/2兴
关60/17兴
关34768-31-5兴
关70/12兴
关1272-44-2兴
关83/15兴
关13978-46-6兴
关92/29兴
关12126-50-0兴
关01/5兴
关14319-78-9兴
关60/17兴
关12180-80-2兴
关83/15兴
关14323-17-2兴
关64/2兴
关14876-47-2兴
关00/35兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
646
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 7. Enthalpies of sublimation of organometallic and inorganic compounds, 1910–2001—Continued
Element
Molecular formula/polymorph
Compound
Temperature range 共K兲
共360–378兲
共316 –330兲
C45H33FeO6
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
128.5⫾0.9
129.3⫾1.2
136.1⫾1.9
106.7
共369兲
共298兲
iron共II兲 dibromide
共655– 833兲
共680–720兲
共673–962兲
FeCl2
共623–718兲
iron共II兲 dichloride
共693– 866兲
共694 –745兲
共621– 658兲
FeF2
iron共II兲 difluoride
共958 –1178兲
共848 –1142兲
Ga
C3 H9 Ga
C15H3 F18GaO6
C15H12F9 GaO6
C15H21GaO6
C16H36Ga4 S4
C16H36Ga4 Se4
C16H36Ga4 Te4
C20H44Ga4 S4
C20H44Ga4 Se4
C20H44Ga4 Te4
C24H52Ga4 S4
C24H52Ga4 Se4
C24H52Ga4 Te4
C28H60Ga4 S4
C28H60Ga4 Se4
C28H60Ga4 Te4
C33H57O6 Ga
Reference
TE,ME
关96/3兴
关96/3兴
关92/11兴
关73/18兴
关14405-49-3兴
关92/11兴
关64/2兴
关7789-46-0兴
关96/26兴
关96/26兴
关60/23兴关96/26兴
关55/12兴关96/26兴
关55/12兴关96/26兴
关55/12兴关96/26兴
关7758-94-3兴
关96/26兴
关96/26兴
关60/23兴关96/26兴
关58/22兴关96/26兴
关58/22兴关96/26兴
关7789-28-8兴
关96/26兴
关96/26兴
关76/22兴关96/26兴
关76/22兴关96/26兴
ME
tris共dibenzoylmethano兲iron共III兲
210⫾10
U31.8
FeBr2
Method
197.6⫾5
208⫾5
196⫾8
197⫾2
210⫾6
197⫾4
共744兲
共298兲
共700兲
共817兲
共298兲
共670兲
TE,ME
198.9⫾6
204⫾6
189⫾8
186⫾12
193⫾12
共780兲
共298兲
共719兲
共640兲
共298兲
TE,ME
263⫾4
271⫾4
263⫾3
270⫾3
共1068兲
共298兲
共995兲
共298兲
TE,ME
trimethyl gallium
共247–257兲
45.2
tris共1,1,1,5,5,5-hexafluoro-2,4-pentanedionato兲gallium共III兲
共333–363兲
53
tris共1,1,1-trifluoro-2,4-pentanedionato兲gallium共III兲
共373– 403兲
75
共378 – 433兲
118.8⫾1.7
共386 – 401兲
89.4⫾6.7
tris共pentane-2,4-dionato兲gallium共III兲
共413– 433兲
90
关 ((CH3兲3C兲Ga共␮3⫺S兲兴4
共367–380兲
110
关 ((CH3 ) 3 C)Ga( ␮ 3 ⫺Se) 兴 4
共375–388兲
119
关 ((CH3 ) 3 C)Ga( ␮ 3 ⫺Te) 兴 4
共391– 422兲
131
关 (C2 H5 (CH3 ) 2 C)Ga( ␮ 3 ⫺S) 兴 4
共369–382兲
124
关 (C2 H5 (CH3 ) 2 C)Ga( ␮ 3 ⫺Se) 兴 4
共395– 407兲
137
关 (C2 H5 (CH3 ) 2 C)Ga( ␮ 3 ⫺Te) 兴 4
共416 – 432兲
140
关 ((C2 H5 ) 2 (CH3 )C)Ga( ␮ 3 ⫺S) 兴 4
共407– 420兲
137
关 ((C2 H5 ) 2 (CH3 )C)Ga( ␮ 3 ⫺Se) 兴 4
共388 – 420兲
147
关 ((C2 H5 ) 2 (CH3 )C)Ga( ␮ 3 Te) 兴 4
共432– 447兲
151
关 ((C2 H5 ) 3 C)Ga( ␮ 3 ⫺S) 兴 4
共432– 444兲
149
关 ((C2 H5 ) 3 C)Ga( ␮ 3 ⫺Se) 兴 4
共452– 464兲
156
关 ((C2 H5 ) 3 C)Ga( ␮ 3 ⫺Te) 兴 4
共444 – 456兲
156
tris共2,2,6,6-tetramethylheptane-3,5-dionato兲gallium共III兲
共413– 443兲
87
102.1
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
I
TE
GS
ME
TE
MS
ME
共252兲
TGA
TGA
GS
TGA
共373兲
TGA
共381兲
TGA
共406兲
TGA
共375兲
TGA
共375兲
TGA
共324兲
TGA
共413兲
TGA
共404兲
TGA
共439兲
TGA
共438兲
TGA
共458兲
TGA
共450兲
TGA
TGA
ME
关1445-79-0兴
关87/4兴
关19648-92-1兴
关00/35兴
关15453-83-5兴
关00/35兴
关85/16兴
关78/27兴
关14405-43-7兴
关00/35兴
关135283-83-9兴
关97/29兴
关13528-84-0兴
关97/29兴
关135258-40-1兴
关97/29兴
关166331-96-0兴
关97/29兴
关176100-40-6兴
关97/29兴
关176100-41-7兴
关97/29兴
关166331-97-1兴
关97/29兴
关187612-49-3兴
关97/29兴
关176100-42-8兴
关97/29兴
关187612-47-1兴
关97/29兴
关187612-51-7兴
关97/29兴
关187612-52-8兴
关97/29兴
关34228-15-4兴
关00/35兴
关73/18兴
ENTHALPY OF SUBLIMATION
647
TABLE 7. Enthalpies of sublimation of organometallic and inorganic compounds, 1910–2001—Continued
Element
Compound
Molecular formula/polymorph
Temperature range 共K兲
(GaBr3 ) – (NH3 )
gallium tribromide–ammonia complex
⌬ subH m /kJ mol⫺1
CAS registry number
(Tm /K)
Method
关54955-92-9兴
关75/27兴
关50599-24-1兴
关75/27兴
67.4⫾1.3
(GaCl3 ) – (NH3 )
gallium trichloride–ammonia complex
75.6⫾1.3
Gd
C10H10ClGd
C15H15Gd
C30H30F21GdO6
C33H57O6 Gd
Ge
C3 H9 FGe
bis共cyclopentadienyl兲gadolinium chloride
共338 – 438兲
138.5⫾2.1
tris共cyclopentadienyl兲gadolinium
共513– 623兲
106.7⫾2.9
tris共1,1,1,2,2,3,3-heptafluoro-7,7-dimethyloctane-4,6-dione兲gadolinium共III兲
C8 H24Ge4 O4
C16H12Ge
diethynyldiphenylgermane
C16H18Ge
1,1-diphenylgermolane
C20H18Ge
triphenyl vinylgermanium
C24H20Ge
tetraphenylgermane
共402– 480兲
triphenyl phenylethynylgermane
C28H28Ge
tetrabenzylgermane
C32H16Cl2GeN8
germanium phthalocyanine dichloride
C36H30Ge2 O
bis共triphenyl germanium兲 oxide
C36H30Ge2
hexaphenyldigermane
GeCl4
germanium tetrachloride
共187–221兲
germanium difluoride
DSC
共400兲
共438兲
ME
ME
BG
40.0
共267兲
SG
关661-370-0兴
关87/4兴关61/9兴
68.2⫾4.2
共298兲
BE
104.6⫾2.8
共298兲
B
98.7⫾1.6
共298兲
ME,TE
148.6
156.9⫾4.2
共441兲
共298兲
107.5⫾1.5
共298兲
168.6⫾8.4
共298兲
ME,TE
147.4⫾12.4
GeF2
GeI4
HaOCl3
Hf
C10H10Cl2 Hf
C20H16F12HfO8
98.0⫾1.5
共298兲
209.2⫾4.2
共298兲
44.6⫾0.2
ME,TE
MG
82.8⫾4.2
93.3⫾10.5
共298兲
共298兲
87.1⫾3
86.7⫾3
76.5⫾5.7
共298兲
共298兲
共298兲
⭐120
共298兲
MS
germanium tetraiodide
共323– 420兲
Ha
HaCl5
TE
hahnium共V兲 pentachloride
hahnium共V兲 oxychloride
共298 – 607兲
关11087-14-2兴
关71/32兴
关1272-21-5兴
关73/31兴
共298兲
ME
133.9
C26H20Ge
ME
关17631-67-3兴
关71/25兴
关14768-15-1兴
关99/33兴
关96/31兴关00/16兴
关81/21兴
关73/18兴
关69/19兴
共362–385兲
154.8⫾0.8
tris共2,2,6,6-tetramethylheptane-3,5-dionato兲gadolinium共III兲
166.1⫾3.5
78.8⫾1.5
共383– 418兲
181.2
163.6
共420– 456兲
161.3
fluorotrimethylgermane
共250–284兲
octamethyltetragermoxane
Reference
152⫾18
107.3⫾2.4
bis共cyclopentadienyl兲hafnium dichloride
110.2⫾2.9
共394 – 447兲
100.3
106.7⫾2.1
100.4⫾1.3
tetrakis共1,1,1-trifluoro-2,4-pentanedionato兲hafnium共IV兲
共298兲
共298兲
共298兲
共420.5兲
共298兲
ME
关82/20兴关72/19兴
关1675-59-8兴
关75/28兴
关4514-06-1兴
关88/31兴
关4049-97-2兴
关88/8兴
关1048-05-1兴
关87/4兴
关82/20兴关69/17兴
关4131-49-1兴
关88/8兴
关1048-05-1兴
关82/20兴关70/15兴
关19566-97-3兴
关72/31兴
关2181-40-0兴
关88/8兴
关2816-39-9兴
关82/20兴关70/15兴
关10038-98-9兴
关64/12兴
关13940-63-1兴
关71/26兴
关71/26兴
关13573-08-5兴
关99/14兴
关99/14兴
关87/22兴
关146837-09-4兴
关96/25兴
关143928-41-0兴
关96/25兴
关68/19兴关01/3兴
关12116-66-4兴
关01/3兴
关87/4兴
关82/20兴关76/14兴
关77/23兴
关17475-68-2兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
648
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 7. Enthalpies of sublimation of organometallic and inorganic compounds, 1910–2001—Continued
Element
Molecular formula/polymorph
C20H28HfO8
HfCl4
Hg
CH3 BrHg
CH3 ClHg
CH3 HgI
C2 H5 BrHg
C2 H5 ClHg
C2 H5 HgI
C4 H16Cl2 HgN8 S4
C10H14Cl2 HgN6 O2
C10H20HgN2 S4
C12H12Hg
C14H14Hg
C14H28HgN2 S4
C16H10Hg
C18H36HgN2 S4
C18H36HgN2 S4
Ho
C15H15Ho
C33H57HoO6
In
C3 H9 In
C15H12F9 InO6
C15H30InN3 S6
C20H48In2 P4
C21H42InN3 S6
Compound
Temperature range 共K兲
⌬ subH m /kJ mol⫺1
共383– 438兲
129.7⫾3.8
共383– 438兲
124.7⫾3.8
tetrakis共pentane-2,4-dionato兲hafnium共IV兲
150.6⫾4.2
hafnium tetrachloride
共398 –500兲
97.9⫾1.2
共353– 433兲
107.9⫾0.8
methylmercuric bromide
共258 –297兲
methylmercuric chloride
共278 –307兲
CAS registry number
(Tm /K)
Method
Reference
GS
GS
关85/16兴
关85/16兴
关17475-67-1兴
关91/23兴
关13499-05-3兴
关94/22兴
关73/30兴
共499兲
T
67.6⫾1.6
共277.5兲
V
64.9⫾1.6
共298兲
V
methylmercuric iodide
共263–290兲
ethylmercuric bromide
共285–303兲
65.3⫾1.6
共276兲
V
76.5⫾2.9
共294兲
V
ethylmercuric chloride
共283–303兲
76.2⫾2.9
共293兲
V
ethylmercuric iodide
共286 –303兲
79.7⫾2.9
共294.5兲
V
共435兲
共298兲
ME
trans-dichloro-tetrakis共thiourea兲mercury共II兲
101⫾20
关 mercury(1-methylcytosine) 2 Cl2 兴
共428 – 443兲
150.8⫾19
159⫾19
bis共diethyldithiocarbamate兲 mercury complex
共378 – 403兲
47.6
diphenylmercury
共314 –303兲
112.8⫾0.8
bis共benzyl兲mercury
共350–390兲
88.7⫾2.1
bis共dipropyldithiocarbamate兲mercury共II兲
200⫾2
bis共phenylethynyl兲mercury
共350–390兲
99.2⫾1.4
bis共dibutyldithiocarbamate兲mercury共II兲
193⫾3
bis共diisobutyldithiocarbamate兲mercury共II兲
247⫾1
共390.5兲
共298兲
ME
ME,TE
共298兲
DSC,E
ME,TE
共298兲
DSC,E
共298兲
DSC,E
tris共cyclopentadienyl兲holmium共III兲
102.1⫾2.1
共338 –348兲
119.7⫾2.1
tris共2,2,6,6-tetramethylheptane-3,5-dionato兲holmium共III兲
131.0⫾2.9
共363– 418兲
152.7
共420– 458兲
131.4
ME
共390兲
共439兲
DSC
ME
BG
trimethyl indium
48.5⫾2.5
共298兲
共328 –362兲
57.7
共344兲
tris共1,1,1-trifluoro-2,4-pentanedionato兲indium共III兲
共378 – 428兲
112.1⫾1.3
共398 – 478兲
77.4⫾0.6 共liq兲
tris共diethyldithiocarbamate兲indium共III兲
176.7⫾3.3
共298兲
bis关␮-关bis共1,1-dimethylethyl兲phosphino兲兴兴tetramethyldiindium共III兲
130.0
tris共dipropyldithiocarbamate兲indium共III兲
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
GS
DSC,E
ME
关506-83-2兴
关87/4兴关51/14兴
关115-09-3兴
关87/4兴关82/20兴
关50/6兴关51/14兴
关143-36-2兴
关51/14兴
关107-26-6兴
关87/4兴关82/20兴
关51/10兴关51/14兴
关107-27-7兴
关87/4兴关82/20兴
关51/10兴关51/14兴
关2440-42-8兴
关87/4兴关82/20兴
关51/10兴关51/14兴
关28813-22-1兴
关70/11兴
关84/12兴
关84/12兴
关14239-51-1兴
关87/4兴
关587-85-9兴
关58/9兴
关780-24-5兴
关84/19兴
关21439-56-5兴
关92/19兴
关6077-10-7兴
关84/19兴
关21439-58-7兴
关91/15兴
关79001-48-2兴
关94/33兴
关1272-22-6兴
关73/32兴
关71/32兴关71/33兴
关15522-73-3兴
关93/26兴
关81/21兴
关69/19兴
关3385-78-2兴
关82/20兴关68/11兴
关87/4兴关41/4兴
关15453-87-9兴
关85/16兴
关78/27兴
关15741-07-8兴
关00/13兴
关115381-28-7兴
关88/20兴
关87052-01-5兴
ENTHALPY OF SUBLIMATION
649
TABLE 7. Enthalpies of sublimation of organometallic and inorganic compounds, 1910–2001—Continued
Element
Molecular formula/polymorph
C21H42InN3 S6
C27H54InN3 S6
C27H54InN3 S6
C33H57InO6
InBr3
InCl3
InI3
Ir
C7 H7 IrO4
C7 H13Cl2 IrO2
C9 H15IrO2
C11H19IrO2
C12O12Ir4
C13H19IrO6
C13H19IrO6
C15H21IrO6
La
C15H15La
C30H30F21LaO6
C33H57LaO6
Li
C2 H5 Li
C4 H9 Li
Compound
Temperature range 共K兲
⌬ subH m /kJ mol⫺1
372.8⫾3.4
tris共diisopropyldithiocarbamate兲indium共III兲
279.5⫾3.5
tris共dibutyldithiocarbamate兲indium共III兲
358.3⫾3.2
tris共diisobutyldithiocarbamate兲indium共III兲
182.0⫾3.3
tris共2,2,6,6-tetramethylheptane-3,5-dionato兲indium共III兲
129.3
indium共III兲 bromide
147⫾4
indium共III兲 chloride
共495– 648兲
152⫾4
158⫾4
150.4
161.1
共453–572兲
151.1⫾1.2
155.6⫾1.2
共478 –563兲
161.1⫾1.6
168.5⫾1.6
共623–773兲
156.3
166.6
indium共III兲 iodide
共399– 479兲
136⫾5.0
dicarbonyl-2,4-pentanedionato iridium complex
共286 –325兲
92.⫾1.3
bis共chloroethylene兲-2,4 –pentanedionato iridium complex
共281–298兲
89.5⫾4.2
bis共ethylene兲-2,4-pentanedionato iridium complex
共283–311兲
82.8⫾4.2
bis共propylene兲-2,4-pentanedionato iridium complex
共269–304兲
90⫾1.3
tetrairidiumdodecacarbonyl
104.6⫾20
bis共vinyl acetate兲-2,4-pentanedionato iridium complex
共325–344兲
120.5⫾2.9
bis共methyl acrylate兲-2,4-pentanedionato iridium complex
共311–335兲
117.2⫾5
tris共2,4-pentanedionato兲iridium共III兲
共423– 473兲
129.3⫾0.8
共383– 433兲
130.5⫾3.4
共387–513兲
101.6⫾1.8
共468 –518兲
86.6⫾1.7
NA
CAS registry number
(Tm /K)
Method
Reference
共298兲
DSC,E
共298兲
DSC,E
共298兲
DSC,E
共298兲
DSC,E
共298兲
TE
共570兲
共298兲
共710兲
共298兲
共489兲
共298兲
共524兲
共298兲
共698兲
共298兲
TE
共298兲
TE,ME
关00/13兴
关85883-33-6兴
关00/13兴
关23467-56-3兴
关00/13兴
关85129-27-7兴
关00/13兴
关34269-03-9兴
关73/18兴
关13465-09-3兴
关97/23兴
关10025-82-8兴
关98/35兴
关98/35兴
关94/37兴
关94/37兴关98/35兴
关88/30兴
关88/30兴关98/35兴
关88/30兴
关88/30兴关98/35兴
关74/29兴
关74/29兴关98/35兴
关13510-35-5兴
关97/22兴
共306兲
ME
关14023-80-4兴
关78/20兴关87/4兴
共290兲
ME
共297兲
ME
共287兲
ME
ME
MS
共298兲
共333兲
ME
共323兲
ME
GS
ME
MCV
SMZG
tris共cyclopentadienyl兲lanthanum
114.6⫾4.0
共298兲
共548 – 663兲
102.1⫾2.9
tris共1,1,1,2,2,3,3-heptafluoro-7,7-dimethyloctane-4,6-dione兲lanthanum共III兲
共387– 403兲
145.2⫾2.9
tris共2,2,6,6-tetramethylheptane-3,5-dionato兲lanthanum共III兲
156.0⫾4.6
116.1⫾8.4
107.9⫾4.6
共388 – 423兲
179.5
共405兲
164.4
共450–520兲
143.6
共485兲
ethyl lithium
共298 –333兲
butyl lithium
共333–368兲
116.6
共315.5兲
109.7
共350.5兲
ME
DSC
ME
ME
BG
关78/20兴关87/4兴
关52654-27-0兴
关78/20兴关87/4兴
关66467-05-8兴
关78/20兴关87/40兴
关11065-24-0兴
关82/20兴关74/26兴
关66467-07-0兴
关78/20兴
关66467-08-1兴
关78/20兴
关15635-87-7兴
关00/12兴
关00/12兴
关00/12兴
关00/12兴
关94/34兴
关1272-23-7兴
关82/20兴关74/23兴
关73/31兴
关19106-89-9兴
关71/25兴
关14319-13-2兴
关97/3兴关00/16兴
关96/17兴
关96/31兴关00/16兴
关81/21兴
关73/18兴
关69/19兴
关811-49-4兴
关87/4兴关62/9兴
关109-72-8兴
关87/4兴关62/12兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
650
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 7. Enthalpies of sublimation of organometallic and inorganic compounds, 1910–2001—Continued
Element
Compound
⌬ subH m /kJ mol⫺1
Molecular formula/polymorph
Temperature range 共K兲
C11H19LiO2
共2,2,6,6-tetramethylheptane-3,5-dionato兲lithium
174.5
lithium fluoride
共1073–1121兲
268.2⫾4.2
共957–1113兲
267.8⫾4.2
LiF
Lu
C15H15Lu
CAS registry number
(Tm /K)
Method
Reference
ME
关73/18兴
关7789-24-4兴
关59/18兴关58/20兴
关58/21兴
tris共cyclopentadienyl兲lutetium共III兲
123.0⫾2.9
C15H21LuO6
C33H57O6 Lu
Mg
C10H10Mg
tris共2,4-pentanedionato兲lutetium共III兲
共403– 433兲
79⫾13
tris共2,2,6,6-tetramethylheptane-3,5-dionato兲lutetium共III兲
135.8⫾2.9
共363– 413兲
154.8
共420– 448兲
134.2
C18H12MgN2 O2
C20H16MgN2 O2
MgF2
Mn
C4 H16Cl2 MnN8 S4
C5 BrMnO5
C5 ClMnO5
C5 IMnO5
C6 F3 MnO5
C6 H3 MnO5
C7 F3 MnO6
C7 H3 MnO6
C8 H5 MnO3
C8 H10Cl2 MnN6 O2
C10MnO10 Re
C10Mn2 O10
C10H6 Mn2 O8 S2
共298兲
共390兲
共434兲
DSC
ME
BG
bis共cyclopentadienyl兲 magnesium
68.2⫾1.3
C10H22Mg
共418兲
bis共2,2-dimethylpropyl兲magnesium
共318 –348兲
160.0⫾2.0
bis共8-hydroxyquinolinato兲magnesium共II兲
230.2⫾4.0
bis共8-hydroxy-2-methylquinolinate兲magnesium共II兲
共533–549兲
212.2⫾6.5
224.3⫾6.5
magnesium fluoride
共1220–1450兲
359.8
共1273–1513兲
327.3⫾4.3
348.2⫾4.3
trans-dichloro-tetrakis共thiourea兲manganese共II兲
共382– 409兲
133⫾20
bromo共pentacarbonyl兲manganese
58.6⫾8.4
88.0⫾2.0
chloro共pentacarbonyl兲manganese
58.6⫾8.4
91⫾9
iodo共pentacarbonyl兲manganese
77.4⫾1.4
pentacarbonyl共trifluoromethyl兲manganese
77.8⫾1.0
methyl共pentacarbonyl兲manganese
60.3⫾1.0
共293– 403兲
60.2
pentacarbonyl共trifluoroacetyl兲manganese
79⫾5
acetyl共pentacarbonyl兲manganese
80⫾7
cyclopentadienyl共tricarbonyl兲manganese
52.4⫾3.1
关manganese-(cytosine) 2 Cl2 兴
共433– 453兲
U 146⫾21
decacarbonylmanganeserhenium
109⫾4
86⫾4
共363– 440兲
68.6
decacarbonyldimanganese
80.3⫾4.2
92.3⫾2.1
共351– 428兲
80.3⫾2.1
62.8⫾4.2
bis共␮-methanethiolato兲octacarbonyldimanganese
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
共298兲
共333兲
ME
共298兲
ME
共541兲
共298兲
ME
共1330兲
共1400兲
共298兲
MS
TE
共298兲
共298兲
C
共298兲
共298兲
C
共298兲
C
共298兲
C
共298兲
C
共443兲
ME
共363兲
共298兲
共401兲
C
共298兲
共298兲
共390兲
MM
C
MM
关1272-24-8兴
关73/32兴
关17966-84-6兴
关83/22兴
关15497-45-2兴
关99/33兴
关81/21兴
关69/19兴
关1284-72-6兴
关82/20兴关67/9兴
关67/17兴
关19978-31-5兴
关83/19兴
关14639-28-2兴
关94/16兴
关14406-92-9兴
关98/8兴
关98/8兴
关7783-40-6兴
关62/10兴
关64/13兴
关64/13兴
关28813-17-4兴
关70/11兴
关14516-54-2兴
关82/20兴关72/21兴
关82/21兴
关14100-30-2兴
关82/20兴关72/21兴
关82/21兴
关14879-42-6兴
关82/21兴
关13601-14-4兴
关82/21兴
关13601-24-6兴
关82/20兴关74/25兴
关58/7兴
关14099-62-8兴
关82/21兴
关13963-91-2兴
关82/21兴
关12079-65-1兴
关82/20兴关65/12兴
关74543-44-5兴
关84/12兴
关14693-30-2兴
关98/33兴
关98/33兴
关71/20兴
关10170-69-1兴
关82/20兴关58/10兴
关82/21兴
关71/20兴
关60/15兴
关21321-38-0兴
ENTHALPY OF SUBLIMATION
651
TABLE 7. Enthalpies of sublimation of organometallic and inorganic compounds, 1910–2001—Continued
Element
Molecular formula/polymorph
C10H10Mn
C10H14MnO4
C11H5 MnO5
C12H5 MnO6
C12H7 MnO5
C15H12F9 MnO6
C15H21MnO6
C18H12MnN2 O2
C20H16MnN2 O2
C30H27MnO6
C33H57MnO6
C44H28MnN4
MnF2
Mo
C6 MoO6
C7 H3 MoNO5
C8 F12Mo2 O8
C8 H12CrMoO8
C8 H12Mo2 O8
C8 H12Mo2 O8
C8 H24MoN4
Compound
Temperature range 共K兲
⌬ subH m /kJ mol⫺1
114.2⫾0.8
bis共cyclopentadienyl兲manganese complex
共298 – 445兲
72.4
75.7⫾1.7
72.4
bis共2,4-pentanedionato兲 manganese共II兲
共390– 440兲
139.3⫾2.5
87
88.7
88.7
phenyl共pentacarbonyl兲manganese
84.9⫾4.4
benzoyl共pentacarbonyl兲manganese
123⫾3
benzyl共pentacarbonyl兲manganese
84.5⫾0.7
tris共1,1,1-trifluoro-2,4-pentanedionato兲 manganese共III兲
共378 – 413兲
120.5⫾9.2
117.3
77.8
tris共2,4-pentanedionato兲 manganese共III兲
共320–380兲
124.7⫾3.8
120⫾10
99
113.0
77.8⫾0.8
bis共8-hydroxyquinolinato兲 manganese共II兲
194.6⫾10.4
共615– 650兲
208.4⫾14
226⫾14
bis共8-hydroxy-2-methylquinolinate兲manganese共II兲
共521–541兲
199.6⫾7.2
211.2⫾7.2
tris共1-phenylbutane-1,3-dionato兲manganese共III兲
195⫾10
tris共2,2,6,6-tetramethylheptane-3,5-dionato兲manganese共III兲
140⫾10
5,10,15,20-tetraphenylporphine manganese 共II兲
175⫾1
manganese共II兲 fluoride
318.4⫾8.4
molybdenum hexacarbonyl
共265–300兲
共316 – 423兲
共240–285兲
77.7
69.1
76.9⫾0.9
73.8⫾1.0
共343–383兲
69.7
共323– 403兲
72.5
共292–308兲
72.8
68.2
acetonitrile molybdenum pentacarbonyl
共260–279兲
105.8⫾5.6
dimolybdenum tetratrifluoroacetate
共330–370兲
113.6⫾1.7
chromium molybdenum tetraacetate
165.0⫾8.4
dimolybdenum tetraacetate
共400– 420兲
170.5⫾7
tetra-␮-acetatodimolybdenum共II兲
165.0⫾8.4
tetrakis共dimethylamino兲molybdenum
72.4⫾6
CAS registry number
(Tm /K)
共340兲
Method
Reference
C
关95/18兴
关1271-27-8兴
关87/4兴
关82/20兴关71/22兴
关56/11兴
关14024-58-9兴
关90/21兴
关81/15兴
关72/24兴
关70/10兴
关13985-77-8兴
关82/21兴
关15612-92-7兴
关82/21兴
关14049-86-6兴
关82/21兴
关14526-24-0兴
关85/16兴
关71/17兴
关64/4兴
关14284-89-0兴
关90/21兴
关88/28兴
关81/15兴
关70/10兴
关82/20兴关68/12兴
关14495-13-7兴
关94/16兴
关84/12兴
关84/12兴
关14515-78-7兴
关98/8兴
关98/8兴
关14376-07-9兴
关88/28兴
关14324-99-3兴
关88/28兴
关31004-82-7兴
关93/27兴
关7782-64-1兴
关64/18兴
共371.5兲
共298兲
共298兲
共343兲
ME
共400兲
共298兲
C
共298兲
C
共298兲
C
GS
共298兲
共298兲
共392兲
共370兲
共298兲
ME
E
共298兲
共633兲
共298兲
ME
ME
共531兲
共298兲
ME
共298兲
E
共298兲
E
UV
共298兲
共331兲
共263兲
ME
ME
共363兲
共298兲
共350兲
ME,TE
共410兲
ME,TE
共298兲
共298兲
C
关13939-06-5兴
关00/33兴
关87/4兴
关79/19兴关80/34兴
关75/22兴关74/24兴
关60/18兴
关52/7兴
关47/5兴
关35/2兴
关17594-16-0兴
关80/31兴
关36608-07-8兴
关84/20兴
关71561-64-3兴
关82/20兴
关84/20兴
关14221-06-8兴
关82/20兴关79/23兴
关100207-68-9兴
关79/18兴关82/20兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
652
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 7. Enthalpies of sublimation of organometallic and inorganic compounds, 1910–2001—Continued
Element
Compound
⌬ subH m /kJ mol⫺1
Molecular formula/polymorph
Temperature range 共K兲
C9 H9 MoN3 O3
tris共acetonitrile兲 molybdenum tricarbonyl
共283–308兲
111.3⫾3.0
96.0⫾10.0
pyridine共pentacarbonyl兲molybdenum
共283–299兲
102.0⫾2.0
cycloheptatriene共tricarbonyl兲molybdenum
88.0⫾4.0
dichlorobis共␩ 5 -2,4-cyclopentadien-1-yl兲molybdenium
100.4⫾4.2
bis共␩ 5 -2,4-cyclopentadien-1-yl兲diiodomolybdenium
100.4⫾4.2
piperidine共pentacarbonyl兲molybdenum
共275–289兲
121.9⫾5.1
bis共␩ 5 -2,4-cyclopentadien-1-yl兲dihydromolybdenium
81.4⫾1.0
92.5⫾2.1
norbornadienemolybdenumtetracarbonyl
92.0⫾4.0
dibenzene molybdenum
94.6⫾8
dimethyldicyclopentadienylmolybdenum
70.4⫾4.2
hexakis共dimethylamine兲dimolybdenum共II兲
111⫾8
di-␮-acetatobis共pentane-2,4-dionato兲dimolybdenum共II兲
163.0⫾5.0
di共6-methyl-2-hydroxypyridyl兲diacetatodimolybdenum共II兲
161.0⫾4.0
tris共pyridine兲tricarbonylmolybdenum
142.0⫾10.0
hexakis共isopropoxy兲dimolybdenum
113⫾10
tetrakis共6-methyl-2-hydroxypyridyl兲dimolybdenum共II兲
157.0⫾3.0
octakis共isopropoxy兲dimolybdenum共II兲
137.0⫾15
C10H5 MoNO5
C10H8 MoO3
C10H10Cl2 Mo
C10H10I2 Mo
C10H11MoNO5
C10H12Mo
C11H8 MoO4
C12H12Mo
C12H16Mo
C12H36Mo2 N6
C14H20Mo2 O8
C16H14Mo2 N2 O4
C18H15MoN3 O3
C18H42Mo2 O6
C24H24Mo2 N4 O4
C24H56Mo2 O8
N
NH3
NH3 O
NH4 Br
NH4 Cl
ammonia
共177–195兲
hydroxylamine
共261–280兲
共273–298兲
ammonium bromide
NH4 I
ammonium iodide
NH4 CN
ammonium cyanide
NH4 SCN
ammonium thiocyanate
NO
nitric oxide
共94 –109兲
hydrazine
N2 H4 O3
共298兲
共298兲
共291兲
ME
共298兲
共298兲
E
共298兲
E
共282兲
ME
ME
共298兲
共298兲
共298兲
C
sulfamide
共347–358兲
ammonium nitrate
共349– 438兲
共298兲
关82/20兴关81/18兴
关15279-79-5兴
关82/20兴关78/25兴
关62521-20-4兴
关81/16兴
关67634-80-4兴
关82/20兴关81/18兴
关79376-50-4兴
关81/16兴
共298兲
共298兲
C
共298兲
共298兲
C
共285兲
183.7
187.9
共550兲
共298兲
I
168.6
176.6⫾0.4
177.0
共550兲
I
TE
182.0
共298兲
84.5
共298兲
133.9
共298兲
16.6
共101兲
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
178.7
关15038-48-9兴
关80/31兴
关82/20兴关78/25兴
关14324-76-6兴
关79/19兴
关12125-77-8兴
关82/20兴关77/22兴
关12184-22-4兴
关76/20兴
关12184-29-1兴
关76/20兴
关19456-57-6兴
关79/19兴
关1291-40-3兴
关90/30兴
关76/20兴
关12146-37-1兴
关82/20兴关77/22兴
关12129-68-9兴
关70/1兴关61/4兴
关39333-52-3兴
关82/20兴关80/37兴
关51956-20-8兴
关79/18兴关81/16兴
关82/20兴关79/23兴
64.2
U46.5
101.5⫾1.0
Reference
共298兲
31.2
U 46.0
N2 H4 O2 S
Method
ammonium chloride
共308 –363兲
N2 H4
CAS registry number
(Tm /K)
共298兲
关7664-41-7兴
关37/4兴
关7803-49-8兴
关65/18兴
关41/5兴
关12124-97-9兴
关71/28兴
关55/11兴
关12125-02-9兴
关71/28兴
关61/7兴
关55/11兴
关12027-06-4兴
关55/11兴
关55/11兴
关1762-95-4兴
关55/11兴
关10102-43-9兴
关29/2兴
关302-01-2兴
关41/2兴关01/8兴
关7803-58-9兴
关97/32兴关59/12兴
关6484-52-2兴
关62/11兴
ENTHALPY OF SUBLIMATION
653
TABLE 7. Enthalpies of sublimation of organometallic and inorganic compounds, 1910–2001—Continued
Element
Compound
Molecular formula/polymorph
Temperature range 共K兲
N2 O
nitrous oxide
共68 – 80兲
共148 –182兲
共103–123兲
Na
C4 H9 ONa
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
174.9
共298兲
25.1⫾0.4
24.6
23.6
共74兲
共161兲
共113兲
Method
Reference
LE
关55/11兴
关10024-97-2兴
关74/13兴
关35/5兴
关30/5兴
MG
sodium tert-butoxide
NA
C6 H13ONa
sodium methyldiethylmethoxide
C7 H15ONa
sodium triethylmethoxide
NA
C32H40F12NaO8 Pr
C32H40F12NaO8 Tb
C32H40F12NaO8 Y
Nb
C5 H15NbO5
C10H10Cl2 Nb
NbBr5
NbCl5
NbCl3 O
Nd
C15H15Nd
C30H30F21NdO6
C33H57O6 Nd
Ni
C4 H16Cl2 N8 NiS8
C4 NiO4
C6 H12N2 NiS4
C8 F18NiO2 P2
C8 F28NiP4
C10H8 F6 NiO4
C10H10Ni
NA
sodium tetrakis共1,1,1-trimethyl-5,5,5-trifluoro-2,4-pentanedionato兲-praseodymate
共423– 483兲
155⫾2
共453兲
T
sodium tetrakis共1,1,1-trimethyl-5,5,5-trifluoro-2,4-pentanedionato兲-terbate
共418 – 473兲
163⫾3
共445兲
T
sodium tetrakis共1,1,1-trimethyl-5,5,5-trifluoro-2,4-pentanedionato兲-yttrate
共418 –503兲
130⫾3
共460兲
T
共463–503兲
142⫾12
共483兲
niobium pentamethoxide
80.3⫾10.5
bis共cyclopentadienyl兲niobium dichloride
127.4⫾4.4
niobium共V兲 pentabromide
共298 – 479兲
115⫾18
112.5
niobium共V兲 pentachloride
共298 – 479兲
94.0
95⫾16
niobium共V兲 oxychloride
共298 – 607兲
128.5
124⫾16
ME,E
共298兲
共298兲
共298兲
共298兲
共298兲
共298兲
共298兲
tris共cyclopentadienyl兲neodymium共III兲
共533– 633兲
108.8⫾3.8
共338 – 438兲
134.7⫾2.1
tris共1,1,1,2,2,3,3-heptafluoro-7,7-dimethyloctane-4,6-dione兲neodymium共III兲
共387– 402兲
155.2⫾2.9
tris共2,2,6,6-tetramethylheptane-3,5-dionato兲neodymium共III兲
159.1⫾3.4
共298兲
92.9⫾2.5
共378 – 423兲
177.0
共400兲
共430– 491兲
158.4
共460兲
trans-dichloro-tetrakis共thiourea兲nickel共II兲
共409– 447兲
74⫾20
nickel tetracarbonyl
41.6⫾0.5
bis共dimethyldithiocarbamato兲 nickel complex
共448 – 478兲
139.9⫾2.1
151.9⫾2.1
dicarbonylbis关tris共trifluoromethyl兲phosphine兴nickel
共293–302兲
47.2
tetrakis关bis共trifluoromethyl兲phorphinous fluoride兴nickel
共305–331兲
66.6
bis共1,1,1-trifluoro-2,4-pentanedionato兲nickel共II兲
共416 – 473兲
157.7⫾3.3
bis共cyclopentadienyl兲 nickel
71.5⫾0.6
70.2⫾1.5
共353– 419兲
72.4⫾1.3
ME
ME
ME
DSC
ME
BG
共463兲
GC
共298兲
共318兲
GS
共298兲
共298兲
MM
关865-48-5兴
关90/22兴
关67638-48-6兴
关90/22兴
关53535-82-3兴
关90/22兴
关93557-93-8兴
关93/4兴
关12576-88-4兴
关93/4兴
关12576-89-5兴
关93/4兴
关93/4兴
关1066-25-7兴
关72/23兴关77/21兴
关12793-14-5兴
关01/3兴
关13478-45-8兴
关96/25兴
关96/25兴关91/22兴
关10026-12-7兴
关96/25兴关91/22兴
关96/25兴
关113597-20-1兴
关96/25兴关91/22兴
关96/25兴
关1273-98-9兴
关73/31兴
关71/32兴关71/33兴
关17978-76-6兴
关71/25兴
关15492-47-4兴
关99/33兴
关96/31兴关00/16兴
关81/21兴
关69/19兴
关28813-19-6兴
关70/11兴
关13463-39-3兴
关53/9兴
关15521-65-0兴
关87/4兴关78/12兴
关76/21兴
关15188-79-1兴
关66/15兴
关14917-18-1兴
关66/15兴
关14324-83-5兴
关85/16兴
关1271-28-9兴
关88/3兴
关84/24兴
关82/20兴关75/23兴
关67/17兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
654
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 7. Enthalpies of sublimation of organometallic and inorganic compounds, 1910–2001—Continued
Element
Compound
Molecular formula/polymorph
Temperature range 共K兲
C10H14NiO4
bis共2,4-pentanedionato兲nickel共II兲
共357– 420兲
共378 – 403兲
C10H20N2 NiS4
C12H8 N2 NiO4
C13H6 F24N2 Ni2 O3 P4
C14H10NiO4
C14H12N2 NiO2
C14H12N2 NiO4
C14H28N2 NiS4
C14H28N2 NiS4
C16H14N2 NiO2
C18H12N2 NiO2
C18H14N4 Ni
C18H36N2 NiS4
C18H36N2 NiS4
C20H16N2 NiO2
C22H38NiO4
C32H16N8 Ni
C44H28N4 Ni
NiBr2
NiF2
bis共diethyldithiocarbamato兲nickel共II兲
共448 – 478兲
共440– 478兲
共507– 650兲
共443–543兲
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
126.4⫾4.4
108.2⫾5
108.2⫾4.9
155⫾80
127.7⫾10
132⫾10
69.0
95.4
69.0
共298兲
共207兲
共480兲
共298兲
共381兲
共298兲
157.3⫾6.0
152⫾0.8
98.8⫾6
91.9⫾6
151.9⫾2.1
61.1⫾1.7
Method
ME
DSC
DSC
C
ME
ME
I
共400兲
C
共459兲
共579兲
共493兲
DSC
DSC
I
Reference
关3264-82-2兴
关90/21兴
关87/13兴
关87/12兴
关85/5兴
关84/12兴
关84/12兴
关71/17兴
关70/10兴
关60/17兴
关14267-17-5兴
关89/16兴
关87/4兴关78/12兴
关79/20兴
关79/20兴
关76/21兴
关69/15兴
bis共picolinato兲nickel共II兲
76.6
␮-carbonyldicarbonylbis关␮-关共methylimino兲bis关bis共trifluoromethyl兲phophine兴兴兴dinickel
共370–390兲
92.3
bis共salicyladehydato兲nickel共II兲
85.4
bis共salicyliminato兲nickel共II兲
158.2
bis共salicylaldoximato兲nickel共II兲
共403– 423兲
106.6⫾29
112⫾29
bis共dipropyldithiocarbamate兲nickel complex
147.2⫾5.0
126.1⫾0.8
bis共diisopropyldithiocarbamate兲 nickel complex
148.⫾5.0
共442– 477兲
143.4⫾2.1
N,N-bis共salicylidene兲ethylenediaminonickel共II兲
共459–545兲
149.8⫾7.0
bis共8-hydroxyquinolinato兲nickel共II兲
175.4⫾6.7
共468 –503兲
129.9⫾6
139⫾6
dibenzotetra-aza-annulene nickel共II兲 complex
共463–553兲
116.6⫾5.5
bis共dibutyldithiocarbamate兲nickel共II兲
132.6⫾5.0
bis共diisobutyldithiocarbamate兲nickel共II兲
133.6⫾5.0
共423– 443兲
152.1⫾1.3
bis共8-hydroxy-2-methylquinolinate兲nickel共II兲
共489–505兲
170.9⫾3.7
180.9⫾3.7
bis共2,2,6,6-tetramethylheptane-3,5-dionato兲nickel共II兲
共453– 493兲
111
145.2⫾10
nickel共II兲 phthalocyanine
144.6
5,10,15,20-tetraphenylporphine nickel共II兲
152⫾4
nickel共II兲 bromide
共714 –969兲
207⫾4.0
226⫾1.0
nickel共II兲 fluoride
共1054 –1106兲
332.2⫾4.1
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
I
共380兲
关68/17兴
I
关63/7兴
I
关63/7兴
关14363-30-5兴
关84/12兴
关84/12兴
关14516-30-4兴
关89/16兴
关78/12兴
关15694-55-0兴
关89/16兴
关87/4兴关78/12兴
关14167-20-5兴
关99/39兴
关14100-15-3兴
关94/16兴
关84/12兴
关84/12兴
关39251-81-5兴
关83/29兴
关13927-77-0兴
关89/16兴
关28371-07-5兴
关89/16兴
关87/4兴关78/12兴
关15200-70-1兴
关98/8兴
关98/8兴
关14481-08-4兴
关99/40兴
关78/22兴
关14055-02-8兴
关95/35兴
关14172-92-0兴
关00/36兴
关13462-88-9兴
关97/20兴
关97/20兴
关10028-18-9兴
关64/19兴
共413兲
共298兲
C
C
共459.5兲
ME
共298兲
共486兲
共298兲
ME
ME
共508兲
T
C
C
共433兲
共496兲
共298兲
ME
MEM
ME
TGA
GS
共841兲
共298兲
关63/7兴
关14402-98-3兴
TE
ME
ENTHALPY OF SUBLIMATION
655
TABLE 7. Enthalpies of sublimation of organometallic and inorganic compounds, 1910–2001—Continued
Element
Molecular formula/polymorph
Np
(C10H2F12NpO6兲–共C3H9OP兲
C20H4 F24NpO8
(C20H4F24NpO8兲–共C3H9OP兲
C32H40F12NpO8
C40H40F28NpO8
Os
C10H10Os
C12O12Os3
Compound
Temperature range 共K兲
CAS registry number
(Tm /K)
Method
bis共1,1,1,5,5,5-hexafluoro-2,4-pentanedionato兲neptunium共IV兲 dioxidetrimethylphospine oxide adduct
共370– 418兲
90⫾3
tetrakis共1,1,1,5,5,5-hexafluoro-2,4-pentanedionato兲neptunium共IV兲
共314 –375兲
81⫾3
tetrakis共1,1,1,5,5,5-hexafluoro-2,4-pentanedionato兲neptunium共IV兲trimethylphospine oxide adduct
共353– 404兲
100⫾4
tetrakis共1,1,1-trimethyl-5,5,5-hexafluoro-2,4-pentanedionato兲neptunium共IV兲
共374 – 424兲
106⫾3
tetrakis共1,1,1,2,2,3,3-heptafluoro-7,7-dimethyloctane-4,6-dione兲neptunium共IV兲
共350–368兲
147.7⫾2.9
共359兲
ME
bis共cyclopentadienyl兲osmium
共393–506兲
72.9⫾1.4
80.5⫾1.7
75.3
共298兲
104.6⫾20
108.4
共298兲
共483兲
CH3 Cl2 OP
difluoro共trichloromethyl兲phosphine
共264 –283兲
methylphosphonic dichloride
36.8共liq兲
共274兲
CH5 O3 P
methylphosphonic acid
62.3
C2 HF6 OP
C2 HF6 PS2
C2 H6 ClP
C2 H7 O3 P
C3 F9 P3 S5
C3 N3 P
C3 H6 F3 PS
C3 H9 OP
C3 H9 PS
C4 F12P4
C4 H8 Cl3 O4 P
C4 H13NP2
C5 H11P
C6 F18NP3
C9H12N3P
C10H14NO5 PS
C12H16N3 O3 PS2
48.1⫾4.2
phosphinous acid, bis共trifluoromethyl兲 ester
共233–251兲
46.6
共242兲
phosphinodithioic acid, bis共trifluoromethyl兲 ester
共273–287兲
41.9
共280兲
chlorodimethylphosphine
共233–268兲
55.5
共253兲
ethylphosphonic acid
50.6⫾4.2
2,4,5-tris共trifluoromethyl兲-1,3,2,4,5-dithiatriphospholane-2,4,5-trisulfide
共363–373兲
96.6
共368兲
tricyanophosphine
共293–323兲
78.3
共308兲
75.3⫾2.9
共298兲
dimethyl共trifluoromethyl兲phospine sulfide
共300–320兲
68.0
共310兲
trimethylphosphine oxide
50.2⫾4.2
trimethylphospine sulfide
共366 –394兲
70.3
共380兲
1,2,3,4-tetrakis共trifluoromethyl兲tetraphosphetane
共292–339兲
65.3
共307兲
共1-hydroxy-2,2,2-trichloroethyl兲phosphonic acid dimethyl ester
共293–357兲
107
共308兲
bis共dimethylphosphino兲amine
共300–310兲
61.7
共305兲
phoshorinane
共250–291兲
43.3
共276兲
共294 –345兲
39.9 共liq兲
共309兲
nitrilotris关bis共trifluoromethyl兲phosphine兴
共273–309兲
68.4
共291兲
tris共2-cyanoethyl兲phosphine
共397– 427兲
105.7⫾2
共413兲
ethyl parathion 共O,O-diethyl-O-4-nitrophenylthiophosphate兲
共298 –318兲
100.6
共308兲
azinphos-ethyl
Reference
关106617-32-7兴
关88/15兴关87/23兴
关110900-26-0兴
关88/15兴关87/23兴
关110934-11-7兴
关88/15兴关87/23兴
关99791-99-8兴
关88/15兴
关70/23兴
关1273-81-0兴
关84/31兴
关84/31兴
关59/10兴
关15696-40-9兴
关82/20兴关74/26兴
关74/35兴
triosmium dodecacarbonyl
共423–543兲
P
CCl3 F2 P
⌬ subH m /kJ mol⫺1
ME
E
T
T
ME,TE
关1112-03-4兴
关87/4兴
关676-97-1兴
关70/1兴关55/4兴
关993-13-5兴
关55/4兴关70/1兴
关359-65-9兴
关87/4兴关62/13兴
关18799-75-2兴
关87/4兴
关811-62-1兴
关87/4兴关58/16兴
关15845-66-6兴
关55/4兴关70/1兴
关26349-17-7兴
关70/21兴
关1116-01-4兴
关87/4兴关76/17兴
关95/30兴关76/17兴
关26348-92-5兴
关70/20兴
关676-96-0兴
关82/20兴关60/10兴
关2404-55-9兴
关66/13兴
关393-02-2兴
关87/4兴关58/17兴
关52-68-6兴
关87/4兴
关53/14兴
关4743-40-2兴
关87/4兴关66/16兴
关87/4兴关66/16兴
关65/21兴
关4023-54-4兴
关81/22兴
关56-38-2兴
关79/10兴关83/5兴
关2642-71-9兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
656
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 7. Enthalpies of sublimation of organometallic and inorganic compounds, 1910–2001—Continued
Element
Molecular formula/polymorph
C15H30N3 PS6
C18H15OP
C18H15P
C18H15O4 P
C18H15PS
C20H20NP
C21H42N3 PS6
C28H28P
C27H54N3 PS6
PH3
PBr3 S
P3 Cl6 N3
P3 F6 N3
P4 F8 N4
Pb
C10H2 F12O4 Pb
C10H14O4 Pb
C10H20N2 PbS4
C12H10Br2 Pb
C16H20F6 O4 Pb
C18H12N2 PbO2
C18H15BrPb
C18H15IPb
C20H20F14O4 Pb
C22H38O4 Pb
C24H20Pb
Compound
Temperature range 共K兲
⌬ subH m /kJ mol⫺1
共326 – 420兲
86.8
phosphorus-tris共N,N-diethyldithiocarbamate兲
143⫾2
triphenylphosphine oxide
131⫾2
66⫾6
triphenylphosphine
113.2⫾3.0
109.2⫾1.1
96.2⫾8.4
triphenylphosphate
114.4⫾2.6
triphenylphosphine sulfide
共388 – 419兲
136.8⫾6.1
142.8⫾6.8
N-ethyl triphenylphosphine imine
75.3⫾8.4
tris共dipropyldithiocarbamate兲phosphorous
127.4⫾4.2
1,4-bis共diphenylphosphino兲butane
171.6⫾2.5
tris共diisobutyldithiocarbamate兲phosphorous
138⫾3
phosphine
共129–140兲
17.2
thiophosphoryl bromide
共273–309兲
61.2
phosphonitrilic chloride 共trimer兲
76.1
phosphonitrilic fluoride 共trimer兲
共273–300兲
53.6
共273–298兲
53.6
phosphonitrilic fluoride 共tetramer兲
共273–303兲
58.2
共283–303兲
57.7
CAS registry number
(Tm /K)
共341兲
共298兲
共399兲
共298兲
ME,TE
B
共298兲
共350兲
共298兲
共298兲
B
共403兲
共298兲
HSA
共298兲
DSC,E
共443兲
B
DSC,E
MM
共291兲
bis共1,1,1,5,5,5-hexafluoro-2,4-pentanedionato兲lead共II兲
共368 – 413兲
111.7⫾1.3
bis共2,4-pentanedionato兲lead共II兲
共393– 444兲
102.4⫾5.0
87.0
bis共diethyldithiocarbamate兲lead complex
共444 – 482兲
129.9⫾2.5
共463兲
diphenyl lead dibromide
共298 –398兲
141.8⫾0.8
共298兲
bis共1,1,1-trimethyl-5,5,5-trifluoro-2,4-pentanedionato兲lead共II兲
共393– 463兲
117.5⫾2.8
bis共8-hydroxyquinolinato兲lead共II兲
187.1⫾6.2
共298兲
triphenyl lead bromide
共298 –398兲
134.7⫾3.3
共298兲
triphenyl lead iodide
共298 –398兲
130.1⫾0.4
共298兲
bis共6,6,7,7,8,8,8-heptafluoro-2,2-dimethyl-3,5-octanedionato兲lead共II兲
75
bis共2,2,6,6-tetramethyl-3,5-heptanedionato兲lead共II兲
共373–398兲
117.5⫾2.8
66.9
86
74.1
tetraphenyl lead
共412– 480兲
151
共446兲
共412– 474兲
159⫾1
共298兲
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
Method
GSM
T
ME
T
GS
GS
LE
ME
GS
ME
ME
ME
GS
LE
ME
ME,TE
Reference
关87/4兴
关17767-20-3兴
关87/16兴
关791-28-6兴
关89/28兴
关78/11兴
关603-35-0兴
关88/21兴
关84/13兴
关82/20兴关60/9兴
关115-86-6兴
关89/23兴
关3878-45-3兴
关96/9兴
关96/9兴
关47182-04-7兴
关82/20兴关60/10兴
关100575-31-3兴
关99/34兴
关7688-25-7兴
关89/28兴
关194281-16-8兴
关97/31兴
关7803-51-2兴
关37/3兴
关3931-89-3兴
关41/1兴
关940-71-6兴
关43/6兴
关15599-91-4兴
关58/15兴
关58/19兴
关14700-00-6兴
关58/15兴
关58/19兴
关19648-88-5兴
关97/35兴
关15282-88-9兴
关97/35兴
关94/35兴关97/35兴
关17549-30-3兴
关87/4兴关78/12兴
关3134-29-6兴
关88/16兴关76/15兴
关21751-12-2兴
关97/35兴
关14976-96-6兴
关94/16兴
关894-06-4兴
关88/16兴关76/15兴
关894-07-5兴
关88/16兴关76/15兴
关21600-78-2兴
关92/9兴
关21319-43-7兴
关97/35兴
关94/35兴关97/35兴
关92/9兴
关73/18兴
关595-89-1兴
关87/4兴
关77/19兴
ENTHALPY OF SUBLIMATION
657
TABLE 7. Enthalpies of sublimation of organometallic and inorganic compounds, 1910–2001—Continued
Element
Molecular formula/polymorph
Compound
Temperature range 共K兲
共298 –316兲
C32H16N8 Pb
lead共II兲 phthalocyanine
PbF2
共542– 663兲
lead共II兲 fluoride
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
194.6⫾6.3
U 80.2
82.8
共298兲
共298兲
共298兲
156.3
195.7
Method
Reference
E
ME
关82/20兴关72/20兴
关62/6兴
关72/22兴
关15187-16-3兴
关95/35兴
关84/7兴
关7783-46-2兴
关71/27兴
关10101-63-0兴
关96/23兴
关96/23兴关85/14兴
关96/23兴关79/26兴
关96/23兴关64/7兴
关96/23兴关39/1兴
关96/23兴关29/1兴
关12069-00-0兴
关93/20兴
TGA
267.8
PbI2
PbSe
Pd
C10H2 F12O4 Pd
C8 H10Pd
C10H8 F6 O4 Pd
C10H10F6 N2 O2 Pd
C10H14O4 Pd
C10H20N2 PdS4
C16H20F6 O4 Pd
C16H20F6 O6 Pd
C18H12N2 O2 Pd
C20H12F6 O4 Pd
C20H18O4 Pd
C22H38O4 Pd
C44H28N4 Pd
Pm
C33H57O6 Pm
Pr
C15H15Pr
C33H57O6 Pr
lead共II兲 iodide
共598 – 640兲
共474 –582兲
共900–1150兲
共563– 613兲
共579– 650兲
共923–1073兲
lead selenide
共835–1047兲
173.1⫾1.6
167.7⫾1.3
182.5⫾1.0
165.2⫾1.8
166.4⫾1.0
165.5⫾3.0
共298兲
共298兲
共298兲
共298兲
共298兲
共298兲
226⫾1
ME
MS
ME
ME
GS
TE
bis共1,1,1,5,5,5-hexafluoro-2,4-pentanedionato兲palladium共II兲
共293–313兲
84.6⫾1.6
共cyclopentadienyl兲allyl palladium
共291–333兲
49.9
共312兲
bis共1,1,1-trifluoro-2,4-pentanedionato兲palladium共II兲
共332–378兲
115.2⫾1.4
共423– 448兲
105.0⫾0.8
bis共1,1,1-trifluoro-4-imino-2-pentanonato兲palladium共II兲
共332–386兲
110.9⫾0.7
bis共2,4-pentanedionato兲palladium共II兲
共347– 416兲
130.1⫾2.8
共330–394兲
122.7⫾8.6
共298兲
共363–393兲
127.6⫾17
共378兲
132⫾17
共298兲
bis共diethyldithiocarbamate兲palladium共II兲
153.1⫾1.9
bis共1,1,1-trimethyl-5,5,5-trifluoro-2,4-pentanedionato兲palladium共II兲
共315–357兲
131.4⫾1.9
bis共1,1-dimethyl-1-methoxy-5,5,5-trifluoro-2,4-pentanedionato兲palladium共II兲
共315–369兲
113.8⫾1.2
bis共8-hydroxyquinolinato兲palladium共II兲
共483–503兲
158.5⫾4
共493兲
168⫾4
共298兲
bis共4,4,4-trifluoro-1-phenyl-1,3-butanedionato兲palladium共II兲
共386 – 452兲
148.6⫾1.4
bis共1-phenyl-1,3-butanedionato兲palladium共II兲
共410– 471兲
152.9⫾1.4
bis共2,2,6,6-tetramethyl-2,4-heptanedionato兲palladium共II兲
共343– 401兲
125.4⫾1.4
5,10,15,20-tetraphenylporphine palladium共II兲
207⫾5
ME
ME
GS
ME
ME
ME
ME
ME
ME
ME
ME
ME
GS
关64916-48-9兴
关00/29兴
关1271-03-0兴
关87/4兴关76/18兴
关63742-52-9兴
关00/29兴
关85/16兴
关203874-01-5兴
关00/29兴
关14024-61-4兴
关00/29兴
关91/17兴
关84/12兴
关84/12兴
关15170-78-2兴
关99/37兴
关77964-87-5兴
关00/29兴
关301198-67-4兴
关00/29兴
关14638-30-3兴
关84/12兴
关84/12兴
关85159-01-9兴
关00/29兴
关15186-07-9兴
关00/29兴
关15214-66-1兴
关00/29兴
关76775-77-4兴
关00/36兴
tris共2,2,6,6-tetramethylheptane-3,5-dionato兲promethium共III兲
共433– 463兲
131.8
关67840-53-3兴
关79/29兴
tris共cyclopentadienyl兲praseodymium
关11077-59-1兴
关82/20兴关74/23兴
关73/31兴
关71/32兴关71/33兴
关15492-48-5兴
关96/31兴关00/16兴
关93/26兴关00/16兴
关81/21兴
关69/19兴
125.5⫾3.0
共298兲
共533– 653兲
113.0⫾1.7
共338 – 438兲
131.0⫾2.1
tris共2,2,6,6-tetramethylheptane-3,5-dionato兲praseodymium共III兲
104.3⫾2.6
163.0⫾3.6
共383– 423兲
178.7
共403兲
共450– 495兲
165.4
共473兲
ME
DSC
ME
BG
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
658
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 7. Enthalpies of sublimation of organometallic and inorganic compounds, 1910–2001—Continued
Element
Compound
⌬ subH m /kJ mol⫺1
CAS registry number
(Tm /K)
Molecular formula/polymorph
Temperature range 共K兲
C32H40F12O8 NaPr
sodium tetrakis共1,1,1-trimethyl-5,5,5-trifluoro-2,4-pentanedionato兲praseodymate
共423– 483兲
155⫾2
共453兲
praseodymium共III兲 bromide
288⫾4
共900兲
306⫾4
共298兲
292
共298兲
praseodymium共III兲 chloride
317⫾4
共1000兲
340⫾4
共298兲
324
共298兲
praseodymium共III兲 iodide
263⫾4
共900兲
280⫾4
共298兲
275
共298兲
PrBr3
PrCl3
PrI3
Pt
C8 H14Pt
C10H20N2 PtS4
C12H16Pt
Pu
C40H40F28O8 Pu
Rb
C5 H9 O2 Rb
bis共2,4-pentanedionato兲platinum共II兲
共363–383兲
129.4⫾9
133⫾9
bis共diethyldithiocarbamate兲platinum共II兲
157.1⫾2.0
dicyclopentadienyldimethylplatinum
83.7⫾3.5
T
TE
TE
TE
共298兲
共373兲
共298兲
ME
共298兲
rubidium pivalate
关70205-79-7兴
关98/31兴
bis共␮-acetato兲tetrabromodirhenium stereoisomer
cis
trans
C4 H6 Cl4 O4 Re2
共410–510兲
66.6
共410–510兲
59.9
bis共␮-acetato兲tetrachlorodirhenium stereoisomer
cis
trans
C5 BrO5 Re
共450–560兲
共450–560兲
bromopentacarbonylrhenium
C5 ClO5 Re
chloropentacarbonylrhenium
72.8
64.7
92.1⫾2
C10O10Re2
Rh
C7 H7 O4 Rh
C9 H13Cl2 O2 Rh
C9 H15O2 Rh
关1271-07-4兴
关82/20兴关77/21兴
关15170-57-7兴
关84/12兴
关84/12兴
关15730-38-8兴
关99/37兴
关42613-14-9兴
关82/20兴关77/21兴
关28041-99-8兴
关70/23兴
Re
C4 H6 Br4 O4 Re2
C6 H3 O5 Re
关93/4兴
关13536-53-3兴
关00/27兴
关00/27兴
关00/27兴
关10361-79-2兴
关00/27兴
关00/27兴
关00/27兴
关13813-23-5兴
关00/27兴
关00/27兴
关00/27兴
tetrakis共1,1,1,2,2,3,3-heptafluoro-7,7-dimethyloctane-4,6-dione兲plutonium共IV兲
共349–363兲
153.5⫾7.9
共356兲
ME
167.1⫾5.6
C5 HO5 Re
Reference
关93557-93-8兴
cyclopentadienyltrimethylplatinum
77.8⫾2.0
C10H14O4 Pt
Method
110.9⫾2
rhenium hydride pentacarbonyl complex
共279–369兲
45.1
rhenium methylpentacarbonyl complex
共315–380兲
65.2
70.0⫾2
65.3⫾1.0
共313–383兲
64.9
dirhenium decacarbonyl
100.9⫾2
93.3⫾4.2
共363– 450兲
77.6
79.5
dicarbonyl-2,4-pentanedionatorhodium complex
共276 –301兲
87⫾2.9
bis共chloroethylene兲-2,4-pentanedionatorhodium complex
共275–288兲
117.2⫾7.1
bis共ethylene兲-2,4-pentanedionatorhodium complex
共282–301兲
97.9⫾7.1
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
C
C
共324兲
共347.5兲
共298兲
共298兲
C
共298兲
共298兲
共406兲
MM
共289兲
ME
共281兲
ME
共292兲
ME
关75027-96-2兴;
关75081-56-0兴
关84/36兴
关84/36兴
关62320-69-8兴;
关100495-10-1兴
关84/36兴
关84/36兴
关14220-21-4兴
关83/21兴
关14099-01-5兴
关83/21兴
关16457-30-0兴
关87/4兴
关14524-92-6兴
关87/4兴关60/22兴
关83/21兴
关82/20兴关74/25兴
关58/7兴
关14285-68-8兴
关83/21兴
关82/20兴关74/25兴
关71/20兴
关61/10兴关71/20兴
关14874-82-9兴
关78/20兴关87/4兴
关12282-04-1兴
关78/20兴关87/4兴
关12082-47-2兴
关78/20兴关87/4兴
ENTHALPY OF SUBLIMATION
659
TABLE 7. Enthalpies of sublimation of organometallic and inorganic compounds, 1910–2001—Continued
Element
Compound
Molecular formula/polymorph
Temperature range 共K兲
C10H14O4 Rh
bis共2,4-pentanedionato兲rhodium共II兲
C11H19O2 Rh
C13H19O6 Rh
C13H19O6 Rh
C16O16Rh6
Ru
C10H10Ru
C10H14O4 Ru
C15H3 F18O6 Ru
C15H12F9 O6 Ru
C15H21O6 Ru
S
H2 S
SF6
NA
共383– 447兲
173.2⫾7.0
bis共propylene兲-2,4-pentanedionatorhodium complex
共270–296兲
86.2⫾1.7
bis共vinylacetate兲-2,4-pentanedionatorhodium complex
共309–328兲
121.3⫾3
bis共methyl acrylate兲-2,4-pentanedionatorhodium complex
共311–327兲
111.7⫾4.6
hexarhodiumhexadecacarbonyl
117.2⫾20.0
bis共cyclopentadienyl兲ruthenium
共383– 479兲
C18H15Sb
C21H42N3 S6 Sb
C27H54N3 S6 Sb
C27H54N3 S6 Sb
Sc
C15H3 F18O6 Sc
C15H12F9 O6 Sc
C15H15Sc
C15H21O6 Sc
C33H57O6 Sc
76.2⫾1.4
82.7⫾1.7
77.6⫾1.6
bis共2,4-pentanedionato兲ruthenium共II兲
共398 – 413兲
139.7⫾2.5
145.1⫾2.5
tris共1,1,1,5,5,5-hexafluoro-2,4-pentanedionato兲ruthenium共III兲
共299–313兲
114.1⫾1.0
114.5⫾1.0
tris共1,1,1-trifluoro-2,4-pentanedionato兲ruthenium共III兲
共350–369兲
126.8⫾1.0
129.9⫾1.0
共383– 423兲
90.0⫾3.0
tris共2,4-pentanedionato兲ruthenium共III兲
共423– 493兲
127.0⫾0.9
hydrogen sulfide
共128 –142兲
共165–188兲
sulfur hexafluoride
共175–207兲
Sb
C15H30N3 S6 Sb
⌬ subH m /kJ mol⫺1
CAS registry number
(Tm /K)
Method
共298兲
共283兲
ME
共319兲
ME
共319兲
ME
共298兲
共298兲
共406兲
共298兲
ME
ME
共306兲
共298兲
ME
ME
共360兲
共298兲
ME
ME
22.5
22.5
共135兲
共176兲
MG
23.2⫾0.01
23.3
共186兲
共191兲
tris共N,N-diethyldithiocarbamate兲antimony共III兲
160⫾2
triphenylantimony
106.3⫾8.4
tris共dipropyldithiocarbamate兲antimony共III兲
169.5⫾6.1
tris共N,N-dibutyldithiocarbamate兲antimony共III兲
179⫾3
tris共N,N-diisobutyldithiocarbamate兲antimony共III兲
157⫾3
tris共1,1,1,5,5,5-hexafluoro-2,4-pentadionato兲scandium共III兲
共333–363兲
55
共313–348兲
60.2⫾1.2
tris共1,1,1-trifluoro-2,4-pentadionato兲scandium共III兲
共373– 403兲
78
共363– 433兲
117.6⫾1.7
共366 – 413兲
53.2⫾1.0
tris共cyclopentadienyl兲scandium
97.1⫾3.5
tris共2,4-pentanedionato兲scandium共III兲
共413– 443兲
95
共393– 453兲
58.2⫾0.8
99.6⫾0.8
tris共2,2,6,6-tetramethylheptane-3,5-dionato兲scandium共III兲
共413– 443兲
90
79.6⫾2.4
共298兲
共298兲
DSC,E
共298兲
共298兲
DSC,E
TGA
I
TGA
I
共298兲
共298兲
TGA
I
HSA
TGA
Reference
关69047-66-1兴
关94/34兴
关91/17兴
关12282-38-1兴
关78/20兴关87/4兴
关31724-87-5兴
关78/20兴
关31724-88-6兴
关78/20兴
关28407-51-4兴
关82/20兴关75/25兴
关1287-13-4兴
关84/31兴
关84/31兴
关67/17兴
关71263-16-6兴
关93/25兴
关93/25兴
关16827-63-7兴
关01/13兴
关01/13兴
关16702-38-8兴
关01/13兴
关01/13兴
关96/30兴
关14284-93-6兴
关96/30兴
关7783-06-4兴
关51/16兴
关36/5兴
关2551-62-4兴
关94/23兴
关32/2兴
关22914-48-3兴
关94/31兴
关603-36-1兴
关82/20兴关60/11兴
关226980-30-9兴
关99/34兴
关14907-93-8兴
关94/31兴
关41594-79-0兴
关97/31兴
关18990-42-6兴
关00/35兴
关78/26兴
关14634-68-5兴
关00/35兴
关85/16兴
关78/26兴
关1298-54-0兴
关82/20兴关74/23兴
关14284-94-7兴
关00/35兴
关78/26兴
关70/9兴关70/17兴
关15492-49-6兴
关00/35兴
关97/3兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
660
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 7. Enthalpies of sublimation of organometallic and inorganic compounds, 1910–2001—Continued
Element
Molecular formula/polymorph
Se
CSe2
C4 H4 N2 O2 Se
C4 H4 Se
C8 H6 N2 Se
C12H12Se2
C14H14Se2
SeF6
Compound
Temperature range 共K兲
carbon diselenide
共218 –229兲
selenobarbituric acid
共449– 486兲
selenophene
共208 –243兲
4-phenyl-1,2,3-selenadiazole
共275–343兲
共327–345兲
diphenyl diselenide
共302–324兲
dibenzyl diselenide
共291–330兲
selenium hexafluoride
共194 –226兲
Si
(CH3Cl3Si兲–2共C6H15N3兲
CH3 NSi
C2 H3 F3 O2 Si
C2 H9 NSi
C6 H18O3 Si3
C7 H15NO3 Si
C8 H15NO3 Si
C8 H17NO3 Si
C8 H17NO3 Si
C8 H17NO4 Si
C8 H24O4 Si4
C8 H24O12Si8
C9 H19NO3 Si
C9 H19NO3 Si
C9 H19NO3 Si
C10H21NO3 Si
2(C6 H15N3 )•Cl4 Si
C12H36Si5
C13H19NO4 Si
C14H19NO5 Si
C14H21NO3 Si
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
46.3
共224兲
141⫾4.0
共466兲
47.1
共225兲
91.2⫾1.7
94.1⫾0.8
90.7
共309兲
共298兲
共336兲
ME
GS
116.7⫾2.5
共313兲
ME
130.5
24.96⫾0.04
23.5
TE
ME
共205兲
共210兲
bis-1,3,5-trimethyl-1,3,5-triazacyclohexane-methyltrichlorosilane
共298 –354兲
74.0⫾2.8
isocyano silane
共253–304兲
48.8
共279兲
silyl trifluoroacetate
共273–293兲
30.7 共liq兲
共283兲
dimethylaminosilane
共228 –264兲
58.8
共246兲
hexamethylcyclotrisiloxane
共297–335兲
55.2⫾0.4
共316兲
1-methyl-2,8,9-trioxa-5-aza-1-silabicyclo关3.3.3兴undecane
82⫾0.8
1-ethenyl-2,8,9-trioxa-5-aza-1-silabicyclo关3.3.3兴undecane
85⫾0.8
1-ethyl-2,8,9-trioxa-5-aza-1-silabicyclo关3.3.3兴undecane
81⫾0.9
1,7-dimethyl-2,8,9-trioxa-5-aza-1-silabicyclo关3.3.3兴undecane
92⫾0.8
1-ethoxy-2,8,9-trioxa-5-aza-1-silabicyclo关3.3.3兴undecane
81⫾0.8
octamethylcyclotetrasiloxane
64⫾2
octamethyldodecaoxooctasilicon
共463–563兲
110.5
共513兲
1-propyl-2,8,9-trioxa-5-aza-1-silabicyclo关3.3.3兴undecane
84⫾0.8
1-共1-methylethyl兲-2,8,9-trioxa-5-aza-1-silabicyclo关3.3.3兴undecane
92⫾0.9
1,3,7-trimethyl-2,8,9-trioxa-5-aza-1-silabicyclo关3.3.3兴undecane
101⫾0.8
1,3,7,10-tetramethyl-2,8,9-trioxa-5-aza-1-silabicyclo关3.3.3兴undecane
115⫾0.9
bis-1,3,5-trimethyl-1,3,5-triazacyclohexane•tetrachlorosilane
共298 –354兲
76.1⫾4.6
tetrakis共trimethylsilyl兲silane
83.7⫾20.9
共298兲
1-共2-phenoxylmethyl兲-2,8,9-trioxa-5-aza-1-silabicyclo关3.3.3兴undecane
108⫾0.8
2,8,9-trioxa-5-aza-1-silabicyclo关3.3.3兴undecane-1-methanol benzoate ester
109⫾0.9
1-共2-phenylethyl兲-2,8,9-trioxa-5-aza-1-silabicyclo关3.3.3兴undecane
108⫾0.9
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
Method
C
B
Reference
关506-80-9兴
关87/4兴关66/12兴
关92754-59-1兴
关99/6兴
关288-05-1兴
关51/17兴
关25660-64-4兴
关74/5兴
关73/25兴
关87/4兴
关1666-13-3兴
关80/33兴
关1482-82-2兴
关74/5兴关73/25兴
关7783-79-1兴
关96/22兴
关32/2兴
关84/5兴
关18081-38-4兴
关87/4兴关56/16兴
关6876-44-4兴
关87/4兴关67/20兴
关2875-98-1兴
关87/4兴关54/11兴
关541-05-9兴
关53/11兴
关2288-13-3兴
关89/12兴
关2097-18-9兴
关89/12兴
关2097-16-7兴
关89/12兴
关18225-19-9兴
关89/12兴
关3463-21-6兴
关89/12兴
关556-67-2兴
关53/11兴关60/1兴
关70/1兴
关57348-79-5兴
关87/4兴关75/29兴
关26053-77-0兴
关89/12兴
关2097-17-8兴
关89/12兴
关56492-01-4兴
关89/12兴
关71229-51-1兴
关89/12兴
关84/5兴
关4098-98-0兴
关82/20兴关72/18兴
关63071-93-2兴
关89/12兴
关79791-55-2兴
关89/12兴
关63330-92-7兴
关89/12兴
ENTHALPY OF SUBLIMATION
661
TABLE 7. Enthalpies of sublimation of organometallic and inorganic compounds, 1910–2001—Continued
Element
Compound
⌬ subH m /kJ mol⫺1
CAS registry number
(Tm /K)
Molecular formula/polymorph
Temperature range 共K兲
C15H21NO5 Si
4-methylbenzoic acid 2,8,9-trioxa-5-aza-1-silabicyclo关3.3.3兴undec-1ylmethyl ester
123⫾0.9
4-methoxybenzoic acid 2,8,9-trioxa-5-aza-1-silabicyclo关3.3.3兴undec-1-ylmethyl ester
143⫾0.9
ethoxytriphenylsilane
142.7⫾1.0
tetraphenylsilane
共428 – 484兲
51.2
共456兲
156.9⫾1.7
共298兲
149.4⫾1.7
共298兲
ME,TE
共428 – 489兲
51.0
MG
51.0
共298兲
tetraphenoxysilane
124.7⫾1.2
silicon phthalocyanine dichloride
115.3⫾11.5
hexaphenyldisilane
209.2⫾2.1
共298兲
ME,TE
silicon tetrachloride
共175–204兲
43.3⫾0.1
MG
silicon tetrafluoride
共148 –183兲
25.8
1,1,1-trifluorodisilane
共195–209兲
39.2
共202兲
关89/12兴
关94697-86-6兴
关89/12兴
关1516-80-9兴
关88/27兴
关1048-08-4兴
关87/4兴
关78/24兴
关74/12兴
关73/14兴
关72/22兴关86/17兴
关1174-72-7兴
关88/27兴
关19333-10-9兴
关72/31兴
关1450-23-3兴
关74/12兴
关10026-04-7兴
关64/12兴
关7783-61-1兴
关30/4兴
关15195-26-3兴
关72/29兴
tris共cyclopendienyl兲samarium共III兲
共513– 633兲
109.6⫾1.7
tris共2,4-pentanedionato兲samarium共III兲
共293– 413兲
U 20⫾2
tris共1,1,1,2,2,3,3-heptafluoro-7,7-dimethyloctane-4,6-dione兲samarium共III兲
共379–394兲
158.6⫾1.7
tris共2,2,6,6-tetramethylheptane-3,5-dionato兲samarium共III兲
149.7⫾3.3
共298兲
共378 – 418兲
180.7
共398兲
共430– 468兲
150.6
共447兲
关1298-55-1兴
关73/31兴
关14589-42-5兴
关85/18兴
关17631-69-5兴
关71/25兴
关15492-50-9兴
关99/33兴
关81/21兴
关69/19兴
C15H21NO6 Si
C20H20OSi
C24H20Si
C24H20O4 Si
C32H16Cl2N8Si
C36H30 Si2
SiCl4
SiF4
F3 H3 Si2
Sm
C15H15Sm
C15H21O6 Sm
C30H30F21O6 Sm
C33H57O6 Sm
Sn
C16H18Sn
Method
ME
DSC
ME
BG
1,1-diphenylstannolane
C17H20Sn
hexahydro-1,1-diphenylstannin
C20H18Sn
triphenyl vinyl tin
C24H20Sn
tetraphenyl tin
共393– 461兲
106.8⫾5.5
共298兲
B
75.0⫾1.5(liq)
共298兲
ME
114.1
共428 – 454兲
共393– 461兲
C27H20Sn
共298 –316兲
triphenyl phenylethynyl tin
C32H16Cl2 N8 Sn
tin共IV兲 phthalocyanine dichloride
C32H16N8 Sn
tin共II兲 phthalocyanine
C36H30Sn2
hexaphenyl ditin
C44H26N8 Sn
diphenyl tin共IV兲 phthalocyanine
SnBr4
tin共IV兲 bromide
共257–299兲
tin共IV兲 iodide
151.7
161.1⫾4.2
152.5⫾0.6
151.8⫾1.1
59.5
U 66.0⫾21.2
共427兲
共298兲
TE
ME
共298兲
共298兲
ME
137.6
218.4⫾17.6
ME
123.4⫾10.0
ME
188.3⫾4.2
共298兲
174.9⫾18.8
SnI4
62.4
ME,TE
ME
共278兲
Reference
关100446-65-9兴
关53561-93-6兴
关88/11兴
关19814-46-1兴
关88/11兴
关2117-48-8兴
关85/12兴
关595-90-4兴
关87/4兴
关82/20兴关69/18兴
关69/16兴
关69/16兴
关72/22兴关86/17兴
关62/6兴关70/13兴
关1247-08-1兴
关85/12兴
关18253-54-8兴
关70/7兴
关15304-57-1兴
关70/7兴
关1064-10-4兴
关69/16兴
关219130-47-0兴
关70/7兴
关7789-67-5兴
关41/7兴
关7790-47-8兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
662
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 7. Enthalpies of sublimation of organometallic and inorganic compounds, 1910–2001—Continued
Element
Molecular formula/polymorph
Compound
Temperature range 共K兲
共366 – 414兲
Sr
SrCl2
Ta
C5 H15O5 Ta
CAS registry number
⌬ subH m /kJ mol⫺1
(Tm /K)
75.6
共390兲
328.9⫾4.8
共298兲
TaI5
Tb
C15H15Tb
C32H40F12NaO8 Tb
C33H57O6 Tb
Te
TeCl4
TeF6
Th
C20H16F12O8 Th
C40H40F28O8 Th
␣ form
␤ form
C44H76O8 Th
Ti
C2 H3 Cl4 NTi
C2 H3 Cl4 NTi
C4 H8 Cl4 OTi
C4 H8 Cl4 OTi
C4 H8 Cl4 STi
C4 H8 Cl4 STi
C5 H5 Cl3 Ti
C5 H10Cl4 OTi
C5 H10Cl4 OTi
C8 H8 Cl4 OTi
C8 H8 Cl4 OTi
C13H10Cl4 OTi
LE
tantalum pentamethoxide
ME,E
tantalum共V兲 pentabromide
127⫾18
121.9
tantalum共V兲 pentaiodide
共573– 655兲
共298兲
共298兲
120.9
T
DSC
ME
ME
BG
tellurium hexafluoride
共194 –233兲
共298兲
25.6
共214兲
tetrakis共1,1,1-trifluoropentane-2,4-dionato兲thorium共IV兲
154.6
共298兲
tetrakis共1,1,1,2,2,3,3-heptafluoro-7,7-dimethyloctane-4,6-dione兲thorium 共IV兲
151.2
共298兲
130.6
共298兲
共344 –367兲
138.5⫾3.3
共355兲
tetrakis共2,2,6,6-tetramethylheptane-3,5-dionato兲thorium共IV兲
共391– 409兲
152.3⫾3.3
共400兲
titanium trichloride–acetonitrile 共1:1 complex兲
29.4⫾5.0
titanium trichloride–acetonitrile 共1:2 complex兲
41.0⫾5.0
titanium trichloride–tetrahydrofuran 共1:1 complex兲
33.5⫾5.0
titanium trichloride–tetrahydrofuran 共1:2 complex兲
49.1⫾5.0
titanium trichloride–tetrahydrothiophene 共1:1 complex兲
29.7⫾5.0
titanium trichloride–tetrahydrothiophene 共1:2 complex兲
43.3⫾5.0
cyclopentadienyltitanium trichloride
共354 – 404兲
89.8
104.6⫾8.4
89.1⫾0.8
titanium trichloride–tetrahydropyran 共1:1 complex兲
33.5⫾5.0
titanium trichloride–tetrahydropyran 共1:2 complex兲
73.0⫾5.0
titanium trichloride–acetophenone 共1:1 complex兲
39.1⫾5.0
titanium trichloride–acetophenone 共1:2 complex兲
66.4⫾5.0
titanium trichloride–benzophenone 共1:1 complex兲
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
关865-35-0兴
关72/23兴关77/21兴
关13451-11-1兴
关96/25兴
关96/25兴关91/22兴
关14693-81-3兴
关78/30兴
关93/4兴
关15492-51-0兴
关99/33兴
关81/21兴
关81/21兴
关69/19兴
关10026-07-0兴
关94/32兴
关7783-80-4兴
关32/2兴
tellurium tetrachloride
105⫾2
关10476-85-4兴
关65/17兴
关1272-25-9兴
关73/32兴
关12576-88-4兴
tris共cyclopentadienyl兲terbium共III兲
103.8⫾1.7
sodium tetrakis共1,1,1-trimethyl-5,5,5-trifluoro-2,4-pentanedionato兲terbate
共418 – 473兲
163⫾3
共445兲
tris共2,2,6,6-tetramethylheptane-3,5-dionato兲terbium共III兲
138.4⫾2.6
共298兲
共373– 420兲
173.6
共396兲
共420– 433兲
151.0
共426兲
共420– 454兲
141.5
共437兲
Reference
关41/7兴
strontium chloride
88.3⫾13.4
TaBr5
Method
GS,HA
GS,HA
ME
关17500-72-0兴
关86/9兴
关23841-30-7兴
关86/9兴
关86/9兴
关70/23兴
ME
关70/23兴
GS,HA
T
T
T
T
T
T
共379兲
共298兲
T
T
T
T
关13682-81-0兴
关70/18兴
关15227-64-2兴
关70/18兴
关15005-09-1兴
关70/18兴
关31011-57-1兴
关70/18兴
关14281-72-2兴
关70/18兴
关16893-00-8兴
关70/18兴
关1270-98-0兴
关87/4兴
关82/20兴关77/21兴
关77/23兴
关22538-12-1兴
关70/18兴
关31011-56-0兴
关70/18兴
关31011-60-6兴
关70/18兴
关31011-61-7兴
关70/18兴
关23368-15-2兴
ENTHALPY OF SUBLIMATION
663
TABLE 7. Enthalpies of sublimation of organometallic and inorganic compounds, 1910–2001—Continued
Element
Molecular formula/polymorph
C13H10Cl4 OTi
C10H10Ti
C10H10Cl2 Ti
C12H10O2 Ti
C12H16Ti
C14H10F6 O4 Ti
C22H20Ti
C24H20O4 Ti
C24H24Ti
C30H28Fe2 Ti
TiBr4
TiF3
Tl
C3 H9 Tl
TlF
Tm
C15H15Tm
C33H57O6 Tm
U
C6 H18O6 U
C10H2 F12O6 U
C15H15ClU
C16H16U
C20H20F30O10U2
C20H22Cl2 F12O6 U
Compound
Temperature range 共K兲
⌬ subH m /kJ mol⫺1
CAS registry number
(Tm /K)
59.6⫾5.0
titanium trichloride–benzophenone 共1:2 complex兲
68.8⫾5.0
bis共cyclopentadienyl兲titanium
58.5⫾8.0
共298兲
bis共cyclopentadienyl兲titanium dichloride
124.4⫾2.9
共298兲
共418 –533兲
124.4
共475.5兲
118.8⫾2.1
共298兲
111.7⫾1.7
96.2
102⫾13
共298兲
bis共cyclopentadienyl兲dicarbonyl titanium
84.2⫾3.5
共298兲
bis共cyclopentadienyl兲dimethyltitanium
79.5⫾8.4
共298兲
bis共cyclopentadienyl兲titanium bis共trifluoroacetate兲
108.0⫾8.0
共298兲
bis共cyclopentadienyl兲diphenylltitanium
88⫾8
bis共benzoato兲bis共␩ 5 -2,4-cyclopentadien-1-yl兲titanium
112⫾8
bis共cyclopentadienyl兲dibenzyltitanium
83.7⫾8.4
共298兲
关Note: There is no reference to 关77/21兴 in Chemical Abstracts under the
given chemical name. Rather, Chemical Abstracts lists the paper under
bis共cyclopentadienyl兲diphenyltitanium.兴
bis共cyclopentadienyl兲diferrocenyl titanium
150⫾15
titanium共IV兲 tetrabromide
共283–306兲
62.4
294
titanium共III兲 fluoride
共759– 865兲
237.2⫾1.7
共810兲
trimethyl thallium
共258 –304兲
thallium共I兲 fluoride
57.3
共285兲
142.7
共298兲
Method
Reference
T
关70/18兴
关31011-63-9兴
关70/18兴
关1271-29-0兴
关82/20兴关71/22兴
关1271-19-8兴
关01/3兴
关87/4兴
关82/20兴关77/21兴
关77/23兴
关69/20兴
关68/19兴关01/3兴
关12129-51-0兴
关87/18兴
关1271-66-5兴
关82/20兴关77/21兴
关1282-45-7兴
关82/20兴关81/17兴
关1273-09-2兴
关82/22兴
关12156-48-8兴
关81/17兴
关See Note兴
关82/20兴关77/21兴
T
ME
ME
关65274-19-3兴
关82/22兴
关7789-68-6兴
关41/7兴
关13470-08-1兴
关67/13兴
CATH
DSC
ME
BG
关1272-26-0兴
关82/20兴关74/23兴
关73/32兴
关71/32兴关71/33兴
关15631-58-0兴
关99/33兴
关81/21兴
关69/19兴
ME
关69644-82-2兴
关91/23兴
关67316-66-9兴
关87/4兴
关78/28兴
关11087-14-2兴
关71/32兴关71/33兴
tris共cyclopentadienyl兲thulium
111.3⫾3.5
98.7⫾1.7
共338 – 438兲
109.2⫾2.1
tris共2,2,6,6-tetramethylheptane-3,5-dionato兲thulium共III兲
131.3⫾2.9
共363– 418兲
156.1
共410– 446兲
131.4
共298兲
ME
共298兲
共390兲
共428兲
uranium hexamethoxide
102.9⫾8.4
bis共1,1,1,5,5,5-hexafluoro-2,4-pentanedionato兲uranium dioxide complex
共370– 425兲
147
共397.5兲
共370– 425兲
147⫾4
tris共cyclopentadienyl兲uranium chloride
共338 –348兲
115.9⫾2.1
bis共cyclooctatetraene兲uranium
共400–500兲
107.9⫾3.3
114.2⫾4.8
共298兲
bis关pentakis共trifluoroethoxy兲兴diuranium
NA
bis共1,1,1,5,5,5-hexafluoro-2,4-pentanedionato兲dichlorouraniumbis共tetrahydropyran兲
共316 –387兲
79.1
共352兲
关3003-15-4兴
关65/13兴关87/4兴
关7789-27-7兴
关67/14兴
关79/31兴关77/26兴
关79/31兴关77/26兴
关137220-74-7兴
关91/19兴
关136211-24-0兴
T
关91/16兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
664
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 7. Enthalpies of sublimation of organometallic and inorganic compounds, 1910–2001—Continued
Element
Compound
⌬ subH m /kJ mol⫺1
CAS registry number
(Tm /K)
Molecular formula/polymorph
Temperature range 共K兲
C20H28O8 U
tetrakis共pentane-2,4-dionato兲uranium共IV兲
148.1⫾4.6
bis共2,2,6,6-tetramethylheptane-3,5-dionato兲dioxouranium
共370– 412兲
151.6⫾1.9
共404兲
156.9⫾1.9
共298兲
126⫾9
tetrakis共1,1,1,2,2,3,3-heptafluoro-7,7-dimethyloctane-4,6-dione兲
uranium共IV兲
68.2
64.3⫾3.2
共343–367兲
143.5⫾1.3
共355兲
tetrakis共2,6-dimethyl-2-methoxy-3,5-heptanedionato兲uranium共IV兲
共344 –377兲
121.7⫾18
共350兲
tetrakis共2,2,6,6-tetramethyl-3,5-heptanedionato兲uranium共IV兲
共372– 478兲
152.2⫾3.3
共425兲
共392– 409兲
149.0⫾1.3
共400兲
tetrakis共2,6,6-trimethyl-2-methoxy-3,5-heptanedionato兲uranium共IV兲
共387– 428兲
160.7⫾6.3
共408兲
C22H38O6 U
C40H40F28O8 U
C40H68O12U
C44H76O8 U
C44H76O12U
V
C10H8 F6 O5 V
C10H10Cl2 V
C10H10V
C10H14O5 V
C10H17NO5 V
C12H12V
C14H16V
C15H12F9 O6 V
C15H18V
C15H18BrNO5 V
C15H19NO5 V
C15H21O6 V
C16H18N2 O5 V
C16H18N2 O5 V
C16H21NO5 V
C16H20V
C18H24V
W
C6 O6 W
bis共1,1,1-trifluoro-2,4-pentanedionato兲oxovanadium共IV兲
共423– 473兲
119.7⫾0.8
bis共cyclopentadienyl兲vanadium dichloride
140.1⫾7.4
bis共cyclopentadienyl兲vanadium
共323–338兲
57.4
58.6⫾4.2
bis共2,4-pentanedionato兲oxovanadium共IV兲
140.7⫾4.0
共418 – 443兲
91.5
140.4⫾1.1
aminebis共pentane-2,4-dionato兲oxovanadium
29.0
bis共benzene兲vanadium
70⫾10
benzene共ethylbenzene兲vanadium
共453– 483兲
69.5
tris共1,1,1-trifluoro-2,4-pentanedionato兲vanadium共III兲
共383– 433兲
118.4⫾2.1
benzene共isopropylbenzene兲vanadium
共453– 483兲
83.7
3-bromopyridinebis共acetylacetonato兲oxovanadium
59.4
pyridinebis共acetylacetonato兲oxovanadium
47.8
tris共2,4-pentanedionato兲vanadium共III兲
102.9⫾0.8
3-cyanopyridinebis共acetylacetonato兲oxovanadium
79.0
4-cyanopyridinebis共acetylacetonato兲oxovanadium
75.6
4-methylpyridinebis共acetylacetonato兲oxovanadium
56.9
bis共ethylbenzene兲vanadium
共453– 483兲
72.0
bis共isopropylbenzene兲vanadium
共453– 483兲
86.2
tungsten hexacarbonyl
共265–288兲
共338 – 423兲
共333– 433兲
共250–292兲
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
77.7
74.9⫾1.3
74.4
78.9⫾1.1
73.2
共298兲
Method
Reference
ME
关65137-03-3兴
关91/23兴
关50707-86-9兴
关93/2兴
关93/2兴
关78/28兴
关23797-50-4兴
BG
C
ME
关77/27兴
关77/27兴
关70/23兴
关133952-93-9兴
关91/11兴
ME
ME
关77/29兴
关70/23兴
关133952-92-8兴
关91/11兴
ME
共330.5兲
共298兲
共493兲
共430.5兲
共298兲
DSC
共370兲
DSC
C
共468兲
共468兲
共402兲
DSC
共404兲
DSC
共298兲
HSA
共391兲
DSC
共399兲
DSC
共421兲
DSC
共468兲
共468兲
共276兲
TE
共348兲
共271兲
共298兲
ME
C
关52081-94-4兴
关85/16兴
关12083-48-6兴
关01/3兴
关1277-47-0兴
关87/4兴
关82/20兴关71/22兴
关3153-26-2兴
关87/14兴
关87/4兴
关86/13兴
关122343-53-7兴
关89/22兴
关12129-72-5兴
关82/20兴
关36955-47-2兴
关72/30兴
关15695-88-2兴
关85/16兴
关36955-49-4兴
关72/30兴
关24263-16-9兴
关89/22兴
关24263-31-8兴
关89/22兴
关13476-99-8兴
关70/9兴关70/17兴
关24263-13-6兴
关89/22兴
关24263-14-7兴
关89/22兴
关24263-33-0兴
关89/22兴
关36955-48-3兴
关72/30兴
关36472-53-4兴
关72/30兴
关14040-11-0兴
关95/36兴
关93/28兴
关87/4兴
关80/34兴关79/19兴
关75/20兴
ENTHALPY OF SUBLIMATION
665
TABLE 7. Enthalpies of sublimation of organometallic and inorganic compounds, 1910–2001—Continued
Element
Molecular formula/polymorph
Compound
Temperature range 共K兲
共339– 410兲
C7 H3 NO5 W
C8 H4 N2 O5 W
C8 H6 N2 O4 W
C8 H9 NO5 W
C8 H9 O5 PW
C9 H4 N2 O5 W
C9 H4 N2 O5 W
C9 H9 N3 O3 W
C10H5 NO5 W
C10H8 O3 W
C10H10Cl2 W
C10H10I2 W
C10H11NO5 W
C10H12W
C12H12W
C12H16W
C12H36N6 W
C12H36N6 W2
C23H15O5 PW
C23H15O8 PW
WCl4O
Y
C15H3 F18O6 Y
C15H15Y
C15H21O6 Y
C33H57O6 Y
⌬ subH m /kJ mol⫺1
CAS registry number
(Tm /K)
Method
76.5⫾1.3
69.7
74.1
acetonitrile tungsten pentacarbonyl
共271–303兲
98.1⫾2.0
pyrazole共pentacarbonyl兲tungsten
共287–327兲
112.5⫾2.4
bis共acetonitrile兲tetracarbonyltungsten
共294 –313兲
131.0⫾6.0
trimethylamine共pentacarbonyl兲tungsten
89.1⫾2.1
trimethylphosphine共pentacarbonyl兲tungsten
共283–327兲
93.8⫾1.5
pyrazine共pentacarbonyl兲tungsten
共287–321兲
108.4⫾1.3
pyridazine共pentacarbonyl兲tungsten
106.4⫾2.5
tris共acetonitrile兲 tungsten tricarbonyl
共308 –333兲
103.4⫾6.0
pyridine共pentacarbonyl兲tungsten
共285–313兲
109.7⫾2.7
cycloheptatrienetungstentricarbonyl
92.0
dichlorobis共␩ 5 -2,4-cyclopentadien-1-yl兲tungsten
120.7⫾8.6
104.6⫾4.2
bis共␩ 5 -2,4-cyclopentadien-1-yl兲diiodotungsten
104.6⫾4.2
piperidine共pentacarbonyl兲tungsten
共289–327兲
106.4⫾1.0
dicyclopentadienyltungsten dihydride
共313–323兲
84.6⫾1.6
96.2⫾2.1
共298兲
共307兲
ME
共298兲
共305兲
ME
共304兲
ME
共298兲
共299兲
ME
共298兲
C
共298兲
ME
共308兲
ME
ME
共298兲
dibenzene tungsten
106
bis共␩ 5 -2,4-cyclopentadien-1-yl兲dimethyltungsten
74.6⫾4.2
hexakis共dimethylamino兲tungsten
89.1⫾7
hexakis共dimethylamino兲ditungsten
113.3⫾6
triphenylphosphine共pentacarbonyl兲tungsten
共340–364兲
162.2⫾8.3
triphenylphosphite共pentacarbonyl兲tungsten
共308 –348兲
120.2⫾6.6
tungsten共IV兲 oxychloride
共396 – 447兲
63.7⫾1.7
tris共1,1,1,5,5,5-hexafluoro-2,4-pentanedionato兲yttrium共III兲
共310–365兲
91.6⫾8.5
tris共cyclopentadienyl兲yttrium
111.7⫾3.5
99.2⫾3.3
tris共2,4-pentanedionato兲yttrium共III兲
98⫾16
tris共2,2,6,6-tetramethylheptane-3,5-dionato兲yttrium共III兲
共358 –387兲
151.0⫾0.8
共357–377兲
153.1⫾0.4
共403– 433兲
135.9
117
共298兲
ME
共298兲
C
共298兲
C
共352兲
ME
共328兲
ME
共421兲
56
ME
共298兲
共372兲
共366兲
TE
TE
TG,DTA
Reference
关75/22兴
关52/7兴
关35/2兴
关15096-68-1兴
关80/31兴
关39017-11-3兴
关79/19兴
关16800-45-6兴
关80/31兴
关15228-32-7兴
关79/19兴关80/32兴
关80/34兴
关26555-11-3兴
关80/34兴
关65761-19-5兴
关79/19兴
关65761-20-8兴
关79/19兴关80/32兴
关80/34兴
关16800-47-8兴
关80/31兴
关14586-49-3兴
关79/19兴
关12128-81-3兴
关77/22兴关82/20兴
关12184-26-8兴
关01/3兴
关76/20兴
关12184-31-5兴
关76/20兴
关31082-68-5兴
关79/19兴
关1271-33-6兴
关90/30兴
关82/20兴关79/24兴
关76/20兴
关12089-23-5兴
关74/37兴
关39333-53-4兴
关80/37兴
关68941-84-4兴
关79/18兴
关54935-70-5兴
关79/18兴
关26555-11-3兴
关80/34兴
关23306-41-4兴
关80/34兴
关13520-78-0兴
关83/30兴
关18911-76-7兴
关99/39兴
关1294-07-1兴
关82/20兴关74/23兴
关73/32兴
关15554-47-9兴
关84/34兴
关15632-39-0兴
关01/6兴
关01/6兴
关97/8兴
关97/3兴
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
666
J. S. CHICKOS AND W. E. ACREE, JR.
TABLE 7. Enthalpies of sublimation of organometallic and inorganic compounds, 1910–2001—Continued
Element
Molecular formula/polymorph
Compound
Temperature range 共K兲
⌬ subH m /kJ mol⫺1
CAS registry number
(Tm /K)
共382– 412兲
共353– 433兲
共353– 433兲
C32H40F12O8 NaY
Yb
C15H15Yb
126
共397兲
117
115.7
138.5
66.5 共liq兲
共363– 418兲
156.9
共388兲
130.8
sodium tetrakis共1,1,1-trimethyl-5,5,5-trifluoro-2,4-pentanedionato兲-yttrate
共418 –503兲
130⫾3
共460兲
共463–503兲
142⫾12
共483兲
C30H30F21O6 Yb
C33H57O6 Yb
Zn
C4 H16Cl2 N8 S4 Zn
C10H14O4 Zn
C10H20N2 S4 Zn
C14H28N2 S4 Zn
C18H12N2 O2 Zn
C18H36N2 S4 Zn
C18H36N2 S4 Zn
C20H16N2 O2 Zn
C22H38O4 Zn
C22H44N2 S4 Zn
C44H28N4 Zn
Zr
C10H10Cl2 Zr
C12H16Zr
C20H4 F24O8 Zr
Reference
T
关96/4兴
关93/9兴
关93/9兴
关90/15兴
关90/15兴
关81/21兴
关73/18兴
关12576-89-5兴
关93/4兴
关93/4兴
GS
GS
ME
ME
T
tris共cyclopentadienyl兲ytterbium
108.8⫾3.5
96.2⫾2.9
C15H21O6 Yb
Method
共298兲
tris共2,4-pentanedionato兲ytterbium共III兲
共364 – 404兲
93.3
tris共1,1,1,2,2,3,3-heptafluoro-7,7-dimethyloctane-4,6-dione兲ytterbium共III兲
共339–356兲
154.8⫾3.3
tris共2,2,6,6-tetramethylheptane-3,5-dionato兲ytterbium共III兲
131.1⫾2.7
共298兲
共363– 413兲
156.9
共388兲
共410– 444兲
133.3
共427兲
trans-dichloro-tetrakis共thiourea兲 zinc共II兲
共351–382兲
90⫾20
bis共2,4-pentanedionato兲zinc共II兲
132.6⫾8
117⫾3
bis共diethyldithiocarbamate兲zinc共II兲
115⫾15
共401– 444兲
143.1
142.7⫾2.5
bis共dipropyldithiocarbamate兲zinc共II兲
147⫾2
bis共8-hydroxyquinolinato兲zinc共II兲
183.2⫾6.3
共473–513兲
167.9⫾6
178⫾6
bis共dibutyldithiocarbamate兲zinc共II兲
107⫾3
bis共diisobutyldithiocarbamate兲zinc共II兲
283⫾2
bis共8-hydroxy-2-methylquinolinate兲zinc共II兲
共437–556兲
172.0⫾5.0
179.4⫾5.0
bis共2,2,6,6-tetramethylheptane-3,5-dianato兲zinc共II兲
136.0
bis共dipentyldithiocarbamate兲zinc共II兲
127⫾3
5,10,15,20-tetraphenylphorphine zinc 共II兲
共563– 663兲
213⫾3
109
DSC
ME
BG
共298兲
C
共298兲
共422.5兲
DSC,E
GC
共298兲
DSC,E
共298兲
共493兲
共298兲
ME
ME
共298兲
DSC,E
共298兲
DSC,E
共541兲
共298兲
ME
ME
共298兲
DSC,E
共666兲
UV/Vis
bis共cyclopentadienyl兲zirconium dichloride
108.5⫾4.6
共298兲
共393– 457兲
100.3
共425兲
105.0⫾2.1
共298兲
100.4⫾1.7
96.7
103⫾13
共298兲
bis共cyclopentadienyl兲dimethylzirconium
81.2⫾2.1
共298兲
tetrakis共1,1,1,5,5,5-hexafluoro-2,4-pentanedionato兲zirconium共IV兲
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
ME
ME
关1295-20-1兴
关82/20兴关74/23兴
关73/32兴
关14284-98-1兴
关81/7兴
关18323-96-1兴
关71/25兴
关15492-52-1兴
关99/33兴
关81/21兴
关69/19兴
关28813-20-9兴
关70/11兴
关14024-63-6兴
关85/5兴
关80/30兴
关14324-55-1兴
关00/40兴
关87/4兴
关76/21兴
关15694-56-1兴
关92/19兴
关13978-85-3兴
关94/16兴
关84/12兴
关84/12兴
关136-23-2兴
关91/15兴
关36190-62-2兴
关94/33兴
关14128-73-5兴
关98/8兴
关98/8兴
关14363-14-5兴
关73/18兴
关15337-18-5兴
关00/40兴
关14074-80-7兴
关94/38兴关01/2兴
关71/29兴关01/2兴
关1291-32-3兴
关01/3兴
关87/4兴
关82/20兴关76/14兴
关77/23兴
关69/20兴
关68/19兴关01/3兴
关1291-32-3兴
关82/20兴关76/14兴
关19530-02-0兴
ENTHALPY OF SUBLIMATION
667
TABLE 7. Enthalpies of sublimation of organometallic and inorganic compounds, 1910–2001—Continued
Element
Compound
Molecular formula/polymorph
C20H16F12O8 Zr
C20H28O8 Zr
C22H20Zr
C32H40F12O8 Zr
C44H28N4 Zn
C44H76O8 Zr
ZrCl4
ZrF4
Temperature range 共K兲
⌬ subH m /kJ mol⫺1
共333–363兲
59
共366 – 456兲
48.6⫾0.6共liq兲
tetrakis共1,1,1-trifluoro-2,4-pentanedionato兲zirconium共IV兲
共373– 403兲
94
共368 –398兲
133.6⫾2.0
118.7⫾3.1
共383– 438兲
126.4⫾1.7
共383– 438兲
119.2⫾1.7
tetrakis共2,4-pentanedionato兲zirconium共IV兲
共413– 443兲
126
共403– 433兲
138.8⫾2
125.8⫾2.9
132.0⫾6.8
116⫾34
bis共cyclopentadienyl兲diphenylzirconium
92.0⫾4.2
tetrakis共1,1,1-trimethyl-5,5,5-trifluoro-2,4-pentanedionato兲
zirconium共IV兲
共388 – 423兲
134.9⫾1.6
5,10,15,20-tetraphenylporphine zinc共II兲
208⫾4
tetrakis共2,2,6,6-tetramethylheptane-3,5-dionato兲zirconium共IV兲
共413– 443兲
120
zirconium tetrachloride
共405–518兲
98.9⫾0.5
zirconium tetrafluoride
共696 – 856兲
240.0⫾0.1
共796兲
243.0
共983–1177兲
241.1⫾0.1
共681–913兲
242.6⫾1.7
共713– 873兲
232.3⫾1.2
共983–1081兲
239.9⫾0.2
共890–1150兲
241.8⫾0.6
6. References to Tables 6 and 7
1910
10/1 L. Holborn and A. Bauman, Ann. Physik. 31, 945–
970 共1910兲.
1913
13/1 C. F. Mündel, Z. Phys. Chem. 85, 435– 465 共1913兲.
1916
16/1 J. W. Terwen, Physik. Chem. 91, 469– 499 共1916兲.
1920
20/1 G. P. Baxter, F. K. Bezzenberger, and C. H. Wilson,
J. Am. Chem. Soc. 42, 1386 –1392 共1920兲.
1925
25/1 M. Volmer and P. Kirchhoff, Z. Phys. Chem. 115,
223–228 共1925兲.
25/2 J. H. Perry and D. C. Bardwell, J. Am. Chem. Soc.
47, 2629–2632 共1925兲.
25/3 T. H. Swan and H. Mack, Jr., J. Am. Chem. 47,
2112–2116 共1925兲.
1926
26/1 D. H. Andrews, G. Gynn, and J. Johnston, J. Am.
Chem. Soc. 48, 1274 –1287 共1926兲.
26/2 M. R. Andrews, J. Phys. Chem. 30, 1497–1500
共1926兲.
CAS registry number
(Tm /K)
共411兲
共383兲
共298兲
共418兲
共298兲
共463兲
共406兲
Method
Reference
TGA
T
关00/35兴
关96/2兴
关17499-68-2兴
关00/35兴
关96/2兴
关92/7兴
关85/16兴
关85/16兴
关17501-44-9兴
关00/35兴
关96/2兴
关92/7兴
关87/14兴
关84/34兴
关51177-89-0兴
关76/14兴
关56044-44-1兴
TGA
SMZG
C
GS
GS
TGA
SMZG
C
SMZG
GS
TGA
共512兲
T
共298兲
共298兲
共298兲
共298兲
共298兲
共298兲
共298兲
TE
MS
MS
GS
关96/2兴
关14074-80-7兴
关00/36兴
关18865-74-2兴
关00/35兴
关10026-11-6兴
关94/22兴
关7783-64-4兴
关94/36兴
关65/14兴关94/36兴
关64/9兴关94/36兴
关63/9兴关94/36兴
关63/8兴关94/36兴
关58/11兴关94/36兴
关54/9兴关94/36兴
26/3 W. A. Noyles, Jr. and D. E. Webbe, J. Am. Chem.
Soc. 48, 1882–1887 共1926兲.
26/4 J. H. Perry and F. Porter, J. Am. Chem. Soc. 48,
299–302 共1926兲.
1927
27/1 O. E. May, J. F. T. Berliner, and D. F. J. Lynch, J.
Am. Chem. Soc. 49, 1012–1016 共1927兲.
27/2 A. S. Coolidge and M. S. Coolidge, J. Am. Chem.
Soc. 49, 100–104 共1927兲.
27/3 S. Klosky, L. P. L. Woo, and R. J. Flanigan, J. Am.
Chem. Soc. 49, 1280–1284 共1927兲.
1928
28/1 L. E. Steiner and J. Johnston, J. Phys. Chem. 32,
912–939 共1928兲.
1929
29/1 K. Jellinek and A. Rudat, Z. Phys. Chem. 143,
55– 61 共1929兲.
29/2 H. L. Johnston and W. F. Giauque, J. Am. Chem.
Soc. 51, 3194 –3214 共1929兲.
1930
30/1 A. S. Coolidge, J. Am. Chem. Soc. 52, 1874 –1887
共1930兲.
30/2 G. V. Cunningham, Power 72, 374 共1930兲; as cited
in 关89/5兴.
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
668
J. S. CHICKOS AND W. E. ACREE, JR.
30/3 C. Drucker and Th. Flade, Z. Wiss. Phot., Schaum
Festschr. 29, 29– 42 共1930兲.
30/4 W. I. Patnode and J. Papish, J. Phys. Chem. 34,
1494 –1496 共1930兲.
30/5 H. K. Black, G. van Praagh, and B. Topley, Trans.
Faraday Soc. 26, 196 –197 共1930兲.
30/6 O. A. Nelson, Ind. Eng. Chem. 22, 971–972
共1930兲.
1931
31/1 V. E. Cosslett, Z. Anorg. Allgem. Chem. 201,
75– 80 共1931兲; Chem. Abstr. 26, 1535 共1932兲.
31/2 A. E. Hill, J. Am. Chem. Soc. 53, 2598 –2608
共1931兲.
31/3 C. A. Crommelin, W. J. Bijleveld, and E. G. Brown,
Proc. Acad. Sci. Amsterdam 34, 1314 –1317 共1931兲; Chem.
Abstr. 26, 2904 共1932兲.
31/4 E. G. Lindner, J. Phys. Chem. 35, 531–535 共1931兲.
1932
32/1 K. Neumann and E. Volker, Z. Phys. Chem. A161,
33– 45 共1932兲.
32/2 W. Klemm and P. Henkel, Z. Anorg. Allgem. Chem.
207, 73– 86 共1932兲.
1933
33/1 L. F. Broadway and R. G. J. Fraser, J. Chem. Soc.
429– 430 共1933兲.
33/2 D. M. Yost and W. E. Stone, J. Am. Chem. Soc. 55,
1889–1895 共1933兲.
33/3 H. Tanneberger, Chem. Ber. 66B, 484 – 486 共1933兲;
Chem. Abstr. 27, 3374 共1933兲.
33/4 V. R. Deitz, J. Am. Chem. Soc. 55, 472– 475
共1933兲.
33/5 W. Menzel and F. Mohry, Z. Anorg. Allgem. Chem.
210, 257–263 共1933兲.
33/6 F. C. Whitmore and G. H. Fleming, J. Am. Chem.
Soc. 55, 3803–3806 共1933兲.
1934
34/1 K. L. Wolf and H. G. Trieschmann, Z. Phys. Chem.
共B兲 27, 376 –380 共1934兲.
34/2 H. Hirsbrunner, Helv. Chim. Acta 17, 477–504
共1934兲.
34/3 M. M. Windsor and A. A. Blanchard, J. Am. Chem.
Soc. 56, 823– 825 共1934兲.
34/4 L. Rotinjanz and N. Nagornow, Z. Phys. Chem. 共A兲
169, 20–30 共1934兲.
1935
35/1 H. G. Trieschmann, Ph.D. dissertation, Inst. Fur Phys.
Chem. and Electrochem. der Universitat Kiel, Germany,
1935.
35/2 W. Hieber and E. Romberg, Z. Anorg. Allgem.
Chem. 221, 332–336 共1935兲; Chem. Abstr. 29, 2467 共1935兲.
35/3 P. J. Lee, Z. Anorg. Allgem. Chem. 223, 213–217
共1935兲; Chem. Abstr. 29, 6118 共1935兲.
35/4 J. L. Carrico and R. G. Dickinson, J. Am. Chem.
Soc. 57, 1343–1348 共1935兲.
35/5 R. W. Blue and W. F. Giauque, J. Am. Chem. Soc.
57, 991–997 共1935兲.
1936
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
36/1 J. G. Aston and G. H. Messerly, J. Am. Chem. Soc.
58, 2354 –2361 共1936兲.
36/2 G. R. Cuthbertson and H. E. Bent, J. Am. Chem.
Soc. 58, 2000–2003 共1936兲.
36/3 J. H. De Boer, Trans. Faraday Soc. 32, 10 共1936兲.
36/4 M. A. Grekhnev, Lesokhim. Prom. 5, 11–12
共1936兲; Chem. Abstr. 32, 5271 共1938兲.
36/5 W. F. Giauque and R. W. Blue, J. Am. Chem. Soc.
58, 831– 837 共1936兲.
1937
37/1 A. B. Burg and H. I. Schlesinger, J. Am. Chem.
Soc. 59, 780–787 共1937兲.
37/2 J. H. de Wilde, Z. Anorg. Allgem. Chem. 233, 411–
414 共1937兲.
37/3 C. C. Stephenson and W. F. Giauque, J. Chem.
Phys. 5, 149–158 共1937兲.
37/4 R. Overstreet and W. F. Giauge, J. Am. Chem. Soc.
59, 254 –259 共1937兲.
37/5 W. F. Giauque and C. J. Egan, J. Chem. Phys. 5,
45–54 共1937兲.
37/6 H. Dunken and K. L. Wolf, Z. Phys. Chem. 共B兲 38,
441– 450 共1937–1938兲.
1938
38/1 K. L. Wolf and H. Weghofer, Z. Phys. Chem. 共B兲
39, 194 –208 共1938兲.
38/2 H. Weghofer, Ph.D. dissertation, Phys. Chem. Institut der Universitat Halle, Germany, 1938.
38/3 A. R. Ubbelohde, Trans. Faraday Soc. 34, 282–292
共1938兲.
1939
39/1 K. Niwa, M. Sato, and M. Yosiyama, J. Chem. Soc.
Jpn. 60, 918 –928 共1939兲.
39/2 R. A. Ruehrwein and W. F. Giauque, J. Am. Chem.
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1940
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1976
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1977
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77/25 S. V. Volkov, E. A. Mazurenko, and Zh. N. Bublik,
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1978
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83/24 S. Skoulika and R. Sabbah, Thermochim. Acta 61,
203–214 共1983兲.
83/25 D. Ferro, V. Piacente, and P. Scardala, Thermochim. Acta 68, 329–339 共1983兲.
83/26 G. Al-Takhin, G. Pilcher, J. Bickerton, and A. A.
Zaki, J. Chem. Soc., Dalton Trans. 2657–2659 共1983兲.
83/27 D. Ferro, P. Imperatori, and C. Quangliata, J.
Chem. Eng. Data 28, 242–244 共1983兲.
83/28 D. Ferro, C. Quagliata, and M. R. Conte, Thermochim. Acta 60, 211–217 共1983兲.
83/29 V. V. Zvezdina, O. R. Motorina, G. Yu. Guara, V.
P. Bochin, O. A. Golubchikov, and B. D. Berezin, Russ. J.
Phys. Chem. 57, 1422–1424 共1983兲.
83/30 A. E. Castro Luna, M. I. Ponzi, and J. B. Rivarola,
J. Chem. Eng. Data 28, 349–350 共1983兲.
1984
84/1 M. Colomina, P. Jimenez, M. V. Roux, and C. Turrion, J. Chem. Thermodyn. 16, 379–384 共1984兲.
84/2 M. R. Holdiness, Thermochim. Acta 78, 435– 436
共1984兲.
84/3 J. Bickerton, M. E. Minas Da Piedade, and G.
Pilcher, J. Chem. Thermodyn. 16, 661– 668 共1984兲.
84/4 S. W. Govorchin, A. S. Kana’an, and J. M. Kanameuller, J. Chem. Thermodyn. 16, 703–709 共1984兲.
84/5 G. S. Gol’din, E. I. Levites, A. I. L’vov, and N. L.
Sin’ko, Koord. Khim. 20, 563–564 共1984兲.
84/6 J. Bickerton, G. Pilcher, and G. Al-Takhin, J.
Chem. Thermodyn. 16, 373–378 共1984兲.
84/7 A. Mrwa, M. Starke, and C. Harmann, Z. Phys.
Chem. 共Leipzig兲 265, 577–581 共1984兲.
ENTHALPY OF SUBLIMATION
84/8 S. W. Govorchin and A. S. Kana’an, J. Chem. Thermodyn. 16, 437– 443 共1984兲.
84/9 M. Colomina, P. Jimenez, M. V. Roux, and C. Turrion, J. Chem. Thermodyn. 16, 1121–1127 共1984兲.
84/10 M. D. M. C. Ribeiro Da Silva, M. A. V. Ribeiro
Da Silva, and G. Pilcher, J. Chem. Thermodyn. 16, 1149–
1155 共1984兲.
84/11 M. D. M. C. Ribeiro Da Silva, M. A. V. Ribeiro
Da Silva, A. P. S. M. C. Carvalho, M. J. Akello, and G.
Pilcher, J. Chem. Thermodyn. 16, 137–144 共1984兲.
84/12 P. M. Burkinshaw and C. T. Mortimer, J. Chem.
Soc. Dalton Trans. 75–77 共1984兲.
84/13 A. A. Grigor’ev, Yu. V. Kontrat’ev, and A. V. Suvorov, Zh. Obshch. Khim. 54, 1935 共1984兲; as cited by D. R.
Kirklin and E. S. Domalski, J. Chem. Thermodyn. 20, 743–
754 共1988兲.
84/14 V. P. Vorob’eva, E. A. Miroshnichenko, I. I. Solomennikova, G. I. Zelchan, E. Lukevits, and Yu. A. Lebedev, Bull. Acad. Sci. USSR, Div. Chem. Sci. 33, 1372–
1376 共1984兲.
84/15 M. A. Flamm-Ter Meer, H.-D. Beckhaus, and C.
Ruechardt, Thermochim. Acta 80, 81– 89 共1984兲.
84/16 H.-D. Beckhaus, C. Ruechardt, and M. Smisek,
Thermochim. Acta 79, 149–159 共1984兲.
84/17 G. Al-Takhin, J. A. Connor, H. A. Skinner, and M.
T. Zafarani-Moattan, J. Organomet. Chem. 260, 189–197
共1984兲.
84/18 J. A. Bouwstra, H. A. J. Oonk, J. G. Blok, and C.
G. De Kruif, J. Chem. Thermodyn. 16, 403– 409 共1984兲.
84/19 A. S. Carson and J. A. Spencer, J. Chem Thermodyn. 16, 423– 426 共1984兲.
84/20 A. S. Carson, J. Chem Thermodyn. 16, 427– 429
共1984兲.
84/21 W. Hessler, Wissenschaftliche Zeitschrift der
Wilhelm-Piech Universitat, Rostich 33, 9 共1984兲.
84/22 W. Bernloehr, H.-D. Beckhaus, and C. Ruechardt,
Chem. Ber. 117, 1026 –1033 共1984兲.
84/23 F. Kersten and H. Oppermann, Z. Phys. Chem.
共Leipzig兲 265, 1207–1212 共1984兲.
84/24 A. K. Baev, A. A. Barkatin, and L. M. Dyagileva,
Vesti Akad. Navuk. Belarus. SSR, Ser. Khim. Navuk. 60– 62
共1984兲.
84/25 E. S. Domalski, W. H. Evans, and E. D. Hearing,
J. Phys. Chem. Ref. Data 13, Suppl. 1 共1984兲.
84/26 L. P. Burkhard, D. E. Armstrong, and A. Andren,
J. Chem. Eng. Data 29, 248 –250 共1984兲.
84/27 A. H. Lawrence, L. Elias, and M. Authier-Martin,
Can. J. Chem. 62, 1886 –1888 共1984兲.
84/28 R. Viswanathan and K. Hilpert, Ber. Bunsenges.
Phys. Chem. 88, 125–131 共1984兲.
84/29 E. H. P. Cordfunke, Thermochim. Acta 108,
45–55 共1984兲.
84/30 N. D. Lebedeva, N. M. Gutner, N. M. Katin Yu. A.
Kozlova, N. N. Kiseleva, E. F. Machinya, and S. L. Dobychin, Zh. Prikl. Khim. 共Lenningrad兲 57, 2297–2301
共1984兲.
685
84/31 A. K. Baev and A. A. Barkatin, Russ. J. Phys.
Chem. 58, 195–198 共1984兲.
84/32 W. Bernloehr, H.-D. Beckhaus, K. Peters, H. G.
von Schnering, and C. Ruechardt, Chem. Ber. 117, 1013–
1025 共1984兲.
84/33 Y. H. Kim. J. E. Woodrow, and J. N. Seiber, J.
Chromatogr. 314, 37–53 共1984兲.
84/34 G. V. Trembovetskii, S. S. Berdonosov, I. A.
Murav’eva, and L. I. Martynenko, Zh. Neorg. Khim. 29,
2159–2162 共1984兲; Chem. Abstr. 101, 137451w 共1984兲.
84/35 G. Krien, Thermochim. Acta 81, 29– 43 共1984兲.
84/36 A. V. Steblevskii, A. S. Alikhanyan, L. G. Vedenkina, A. V. Shtemenko, A. S. Kotel’nikova, and V. I. Gorgoraki, Koord. Khim. 10, 72–76 共1984兲.
84/37 H. Ebeling and E. U. Franck, Ber. Bunsenges.
Phys. Chem. 88, 862– 865 共1984兲.
84/38 A. Zielenkiewicz, W. Zielenkiewicz, L. F.
Sukhodub, O. T. Glukhova, A. B. Teplitsky, and K. L.
Wierzchowski, J. Solution Chem. 13, 757–765 共1984兲.
84/39 V. V. Karpov, G. N. Rodionova, I. V. Krutovskaya,
L. Z. Gandel’sman, L. A. Khomenko, and L. M.
Yagupol’skii, Dyes Pigments 5, 285–293 共1984兲.
84/40 V. V. Karpov, I. V. Krutovskaya, and G. N. Rodionova, Zh. Prikl. Khim. 共Leningrad兲 57, 1348 –1351 共1984兲.
1985
85/1 M. Colomina, P. Jimenez, M. V. Roux, and C. Turrion, J. Chem. Thermodyn. 17, 1091–1096 共1985兲.
85/2 J.-R. Cao and R. A. Back, Can. J. Chem. 63, 2945–
2948 共1985兲.
85/3 W. V. Steele, B. E. Gannon, N. K. Smith, A. Greenburg, J. S. Chickos, and J. F. Liebman, J. Chem. Thermodyn.
17, 505–511 共1985兲.
85/4 B. F. Rordorf, Thermochim. Acta 85, 435– 438
共1985兲.
85/5 S. Murata, M. Sakiyama, and S. Seki, Thermochim.
Acta 88, 121–126 共1985兲.
85/6 H. A. Skinner, G. Pilcher, and G. Al-Takhin, personal comment to M. Faour and T. S. Akasheh, J. Chem. Soc.
Perkin Trans. II 811– 813 共1985兲.
85/7 D. Ferro and V. Piacente, Thermochim. Acta 90,
387–389 共1985兲.
85/8 H. K. Yan, J. K. Gu, and R. H. Fu, Wuli Huaxue
Xuebao 1, 543–546 共1985兲; H. Yan, J. Gu, X. An, and R. Hu,
Huaxue Xuebao 45, 1184 –1187 共1987兲; Chem. Abstr. 108,
138790n 共1988兲.
85/9 E. Kaiserberger, W. Hadrich, and W.-D. Emmerich,
Thermochim. Acta 95, 331–336 共1985兲.
85/10 O. T. Glukhova, N. M. Arkhangelova, A. B.
Teplitsky, L. F. Sukhodub, I. K. Yanson, and M. Kaminski,
Thermochim. Acta 95, 133–138 共1985兲.
85/11 N. Matsubara and T. Kuwamoto, Thermochim.
Acta 83, 193–202 共1985兲.
85/12 A. S. Carson, P. G. Laye, and J. A. Spencer, J.
Chem. Thermodyn. 17, 277–281 共1985兲.
85/13 W. Brostow, J. C. Iniguez, M. A. Shmorhun, and J.
A. Valdez, Mater. Chem. Phys. 12, 557–569 共1985兲.
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
686
J. S. CHICKOS AND W. E. ACREE, JR.
85/14 K. Hilpert, L. Bencivenni, and B. Saha, Ber. Bunsenges. Phys. Chem. 89, 1292–1300 共1985兲.
85/15 V. Venugopal, R. Prasad, and D. D. Sood, J. Nucl.
Mater. 130, 115–121 共1985兲.
85/16 N. Matsubara and T. Kuwamoto, Inorg. Chem. 24,
2697–2701 共1985兲.
85/17 K. Kusano, Thermochim. Acta 88, 109–120
共1985兲.
85/18 G. B. Sergeev, V. V. Zagorskii, A. M. Kosolapov,
and S. E. Kondakov, Zh. Neog. Khim. 30, 3212–3214
共1985兲; Chem. Abstr. 104, 121894u 共1986兲.
85/19 J. M. Schroy, F. D. Hileman, and S. C. Cheng,
Chemosphere 14, 877– 880 共1985兲.
85/20 V. I. Trusov, I. M. Krasikova, A. A. Grigor’ev, A.
I. Altsybeeva, A. V. Suvorov, A. A. Khonikevich, and P. A.
Vinogradov, Zashch. Met. 21, 299–301 共1985兲; Chem. Abstr.
102, 173623h 共1985兲.
85/21 M. Kaminski and W. Zielenkiewicz, Calorim.
Anal. Therm. 16, 281–286 共1985兲; Chem. Abstr. 104, 96844t
共1986兲.
85/22 A. R. Campanelli, D. Ferro, and N. V. Pavel, Thermochim. Acta 87, 231–238 共1985兲; Chem. Abstr. 103,
93861q 共1985兲.
85/23 I. K. Igumenov, T. Yu. Gerasimenko, and V. G.
Isakova, Izv. Sib. Otdel Akad. Nauk SSSR, Ser. Khim. Nauki
42– 44 共1985兲.
1986
86/1 J. S. Chickos, R. S. Annunziata, L. H. Ladon, A. S.
Hyman, and J. F. Liebman, J. Org. Chem. 51, 4311– 4314
共1986兲.
86/2 M. A. Flamm-Ter Meer, H.-D. Beckhaus, and C.
Ruechardt, Thermochim. Acta 107, 331–338 共1986兲.
86/3 M. D. M. C. Ribeiro Da Silva, M. A. V. Ribeiro Da
Silva, and G. Pilcher, J. Chem. Thermodyn. 18, 295–300
共1986兲.
86/4 M. Colomina, P. Jimenez, M. V. Roux, and C. Turrion, An. Quim. 82, 126 –130 共1986兲.
86/5 J. P. Pedley, R. D. Naylor, and S. P. Kirby, Thermochemical Data of Organic Compounds, 2nd ed. 共Chapman
and Hall, New York, NY, 1986兲.
86/6 A. P. Krasulin and A. A. Kozyro, Proceedings 11th
All-Union Conference on Calorimetry and Chemical Thermodynamics, Novosibirsk, USSR, June 17, 1986, p. 129;
关90/5兴.
86/7 B. F. Rordorf, Chemosphere 15, 1325–1332
共1986兲.
86/8 P. C. Hansen and C. A. Eckert, J. Chem. Eng. Data
31, 1–3 共1986兲.
86/9 G. Gärtner, P. Janiel, H. Rau, H. A. M. van Hal, and
H. J. P. Nabben, Ber. Bunsenges. Phys. Chem. 90, 459– 463
共1986兲.
86/10 J. J. Kirchner, W. E. Acree, Jr., G. Pilcher, and S.
Li, J. Chem. Thermodyn. 18, 793–799 共1986兲.
86/11 L. Nunez, L. Barral, L. S. Gavelanes, and G.
Pilcher, J. Chem. Thermodyn. 18, 575–579 共1986兲.
86/12 W. Hessler and W. Lichtenstein, Wissenschaftliche
J. Phys. Chem. Ref. Data, Vol. 31, No. 2, 2002
Zeitschrift der Wilhelm-Piech Universitat, Rostich 35, 27
共1986兲.
86/13 E. H. Jamea and G. Pilcher, Thermochim. Acta 97,
77– 84 共1986兲.
86/14 K. Nishida, Y. Ando, S. Sunagawa, A. Ogihara, I.
Tanaka, and A. Koukitsu, J. Soc. Dyers Colour. 102, 18 –20
共1986兲.
86/15 P. Jimenez, M. V. Roux, C. Turrion, and F. Gomis,
J. Calorim., Anal. Therm. Thermodyn. Chim. 17, 469– 470
共1986兲.
86/16 G. Barone, D. Ferro, P. Fiorani, C. A. Mattia, and R.
Puliti, J. Calorim., Anal. Therm. Thermodyn. Chim. 17,
471– 473 共1986兲.
86/17 Y. Marcus and A. Loewenschuss, J. Chem. Soc.,
Faraday Trans. 1 82, 993–1006 共1986兲.
86/18 B. F. Rordorf, L. P. Sarna, and G. R. B. Webster,
Chemosphere 15, 2073–2076 共1986兲.
86/19 A. P. Krasulin, A. A. Kozyro, and S. V. Dalidovich, Zh. Fiz. Khim. 60, 2580–2583 共1986兲.
86/20 D. Wells, B. T. Grayson, and E. Langner, Pestic.
Sci. 17, 473– 476 共1986兲.
1987
87/1 X. An, I. Zhu, and R. Hu, Thermochim. Acta 121,
473– 477 共1987兲.
87/2 D. Ferro and G. Della Gatta, Thermochim. Acta
122, 189–195 共1987兲.
87/3 P. H. Allot, A. Finch, G. Pilcher, L. Numez, and L.
Barral, J. Chem. Thermodyn. 19, 771–779 共1987兲.
87/4 R. M. Stephenson and S. Malanowski, Handbook of
the Thermodynamics of Organic Compounds 共Elsevier, New
York, 1987兲. The data in this listing was obtained directly
from this compendium which does not contain literature references. The sublimation enthalpies were calculated from the
vapor pressures obtained from the Antoine constants reported
in this compendium. In cases where the Antoine constant C
⫽0, the Antoine Equation (log10P⫽A⫺B/(C⫹T)) reduces
to the integrated form of the Clausius Clapeyron equation
directly. This was the case for most sublimation enthalpies.
In those cases where this condition was not met, vapor pressures were calculated over a 30 K temperature range closest
to 298 K and the temperature dependence was reformulated
in terms of the integrated form of the Clausius Clapeyron
equation.
87/5 D. Ferro, G. Della Gatta, and V. Piacente, J. Chem.
Thermodyn. 19, 915–923 共1987兲.
87/6 P. Fiorani and D. Ferro, Thermochim. Acta 112,
387–389 共1987兲.
87/7 M. Kaminski and W. Zielenkiewicz, Bull. Polish
Acad. Sciences Chem. 35, 583–587 共1987兲.
87/8 M. L. C. C. H. Ferrao and G. Pilcher, J. Chem.
Thermodyn. 19, 543–548 共1987兲.
87/9 P. Jimenez, M. V. Roux, C. Turrion, and F. Gomis,
J. Chem. Thermodyn. 19, 985–992 共1987兲.
87/10 R. Sabbah and I. Antipine, Bull. Soc. Chim. Fr.
392– 400 共1987兲.
87/11 M. Colomina, P. Jimenez, R. Perez-Ossorlo, M. V.
ENTHALPY OF SUBLIMATION
Roux, and C. Turrion, J. Chem. Thermodyn. 19, 155–162
共1987兲.
87/12 M. A. V. Ribeiro da Silva and M. L. C. C. H.
Ferrao, J. Chem. Thermodyn. 19, 645– 652 共1987兲.
87/13 J. P. Murray and J. O. Hill, Thermochim. Acta
109, 383–390 共1987兲.
87/14 J. P. Murray and J. O. Hill, Thermochim. Acta
109, 391–396 共1987兲.
87/15 M. Colomina, P. Jimenez, M. V. Roux, and C. Turrion, J. Chem. Thermodyn. 19, 1139–1144 共1987兲.
87/16 C. Airoldi and A. G. DeSouza, J. Chem. Soc., Dalton Trans. 2955–2958 共1987兲.
87/17 M. Meier, B. Dogan, H. D. Beckhaus, and C.
Rüchardt, New J. Chem. 11, 1– 6 共1987兲.
87/18 A. R. Dias, P. B. Dias, H. P. Diogo, A. M. Galvao,
M. E. Minas de Piedade, and J. A. Martinho Simoes, Organometallics 6, 1427–1432 共1987兲.
87/19 T. Shimizu, S. Ohkubo, M. Kimura, I. Tabata, and
T. Hori, J. Soc. Dyers Colour. 103, 132–137 共1987兲.
87/20 Ya. Kh. Grinberg, V. B. Lazarev, V. V. Petukhov,
G. Ya. Novikova, G. A. Sharpataya, and Z. P. Ozerova, Dokl.
Akad. Nauk SSSR 297, 633– 637 共1987兲.
87/21 Ya. Kh. Grinberg and V. B. Lazarev, Zh. Neorg.
Khim. 32, 3110–3112 共1987兲.
87/22 D. Ferro and S. Stranges, Thermochim. Acta 119,
373–375 共1987兲.
87/23 N. R. Grebenshchikov, G. V. Sidorenko, and D. N.
Suglobov, Radiokhim. 29, 296 –302 共1987兲.
1988
88/1 M. A. V. Ribeiro da Silva and M. L. C. C. H. Ferrao, Bull. Chem. Soc. Jpn. 61, 1755–1759 共1988兲.
88/2 M. A. V. Ribeiro da Silva and M. L. C. C. H. Ferrao, Pure Appl. Chem. 60, 1225–1234 共1988兲.
88/3 L. A. Torres-Gomez, G. Barreiro-Rodriguez, and F.
Mendez-Ruiz, Thermochim. Acta 124, 179–183 共1988兲.
88/4 L. A. Torres-Gomez, G. Barreiro-Rodriguez, and A.
Galarza-Mondragon, Thermochim. Acta 124, 229–233
共1988兲.
88/5 R. Sabbah, L. El Watik, and C. Minadakis, C. R.
Acad. Sci. Paris 307 共Series II兲, 239–244 共1988兲.
88/6 D. Ferro, G. Della Gatta, and G. Barone, J. Thermal
Analysis 34, 835– 841 共1988兲.
88/7 M. A. V. Ribeiro da Silva, M. L. C. C. H. Ferrao,
and C. C. H. Luisa, J. Chem. Thermodyn. 20, 359–361
共1988兲.
88/8 A. S. Carson, E. H. Jamea, P. G. Laye, and J. A.
Spencer, J. Chem. Thermodyn. 20, 1223–1229 共1988兲.
88/9 M. A. V. Ribeiro da Silva, M. D. M. C. Ribeiro da
Silva, and G. Pilcher, J. Chem. Thermodyn. 20, 969–974
共1988兲.
88/10 M. Colomina, P. Jimenez, R. Perez-Ossorio, M. V.
Roux, and C. Turrion, J. Chem. Thermodyn. 20, 575–580
共1988兲.
88/11 A. S. Carson, E. H. Jamea, P. G. Laye, and J. A.
Spencer, J. Chem. Thermodyn. 20, 923–926 共1988兲.
88/12 A. Imamura, S. Murata, and M. Sakiyama, J.
Chem. Thermodyn. 20, 389–396 共1988兲.
687
88/13 R. Sabbah and L. El Watik, Bull. Soc. Chim. Fr.
626 – 630 共1988兲.
88/14 F. Galan-Estella, J. Gonzalez-Julian, and P.
Aquado-Rodriquez, Phytochemistry 27, 3069–3073 共1988兲;
Chem. Abstr. 110, 102153h 共1989兲.
88/15 N. R. Grebenshchikov, G. V. Sidorenko, D. N. Suglobov, L. L. Shcherbakova, and V. M. Adamov, Inorg.
Chim. Acta 145, 315–325 共1988兲.
88/16 O. F. Golovanova, G. V. Sitonina, V. I. Pepekin,
and F. I. Korsunskii, Izv. Akad. Nauk. SSSR, Ser. Khim.
1012–1016 共1988兲; Chem. Abstr. 110, 38466j 共1989兲.
88/17 M. A. V. Ribeiro Da Silva, A. M. V. Reis, and G.
Pilcher, Thermochim. Acta 124, 319–328 共1988兲.
88/18 L. Nunez, L. Barral, and G. Pilcher, J. Chem.
Thermodyn. 20, 1211–1216 共1988兲.
88/19 L. Shaofeng and G. Pilcher, J. Chem. Thermodyn.
20, 463– 465 共1988兲.
88/20 D. C. Bradley, M. M. Faktor, D. M. Frigo, and K.
V. Young, Chemtronics 3, 50–53 共1988兲; Chem. Abstr. 109,
43735e 共1988兲.
88/21 D. R. Kirklin and E. S. Domalski, J. Chem. Thermodyn. 20, 743–754 共1988兲.
88/22 V. B. Lazarev, Ya. Kh. Grinberg, Z. P. Ozerova,
and G. A. Sharpataya, J. Thermal Anal. 33, 797–799 共1988兲.
88/23 N. E. Fedotova, A. A. Voityuk, A. A. Blitznyuk,
and I. K. Igumenov, Koordinatsionnaya Khimiya 14, 1493–
1496 共1988兲.
88/24 G. L. Baughman and T. A. Perenich, Environmental Toxicology Chem. 7, 183–199 共1988兲.
88/25 M. A. V. Ribeiro da Silva, G. Pilcher, and R. J.
Irving, J. Chem. Thermodyn. 20, 95–102 共1988兲.
88/26 K. Sasse, J. Jose, and J.-C. Merlin, Fluid Phase
Equilibria 42, 287–304 共1988兲.
88/27 M. G. Voronkov, V. P. Baryshok, V. A. Klyuchnikov, T. F. Danilova, V. I. Pepekin, A. N. Korchagina, and Y.
I. Khudobin, J. Organometallic Chem. 345, 27–38 共1988兲.
88/28 M. A. V. Ribeiro da Silva and M. L. C. C. H.
Ferrao, Can. J. Chem. 66, 651– 654 共1988兲.
88/29 V. L. Khudyakov, Russ. J. Phys. Chem. 62, 1743–
1744 共1988兲.
88/30 F. Defoort, C. Chatillon, and C. Bernard, J. Chem.
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P. Semyannikov, and I. K. Igumenov, Russ. J. Coordin.
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00/30 P. P. Semyannikov, T. V. Basova, V. M. Grankin,
and I. K. Igumenov, J. Porphyrins Phthalocyanines 4, 271–
277 共2000兲.
00/31 H. A. J. Oonk, A. C. G. van Genderen, J. G. Blok,
and P. R. van der Linde, Phys. Chem. Chem. Liq. 2, 5614 –
5618 共2000兲.
00/32 V. Yu. Markov, O. V. Boltalina, A. A. Gorjunkov,
A. Y. Lukonin, L. N. Sidorov, G. Gigli, G. Balducci, and R.
Taylor, Proc.-Electrochem. Soc. 2000–12, 109–120 共2000兲;
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00/33 T. Ohta, F. Cicoira, P. Doppelt, L. Beitone, and P.
Hoffman, Chem. Vap. Deposition 7, 33–37 共2000兲; Chem.
Abstr. 134, 153247w 共2001兲.
00/34 O. V. Boltalina and N. A. Galeva, Russ. Chem.
Rev. 69, 609– 621 共2000兲.
00/35 B. D. Fahlman and A. R. Barron, Adv. Mater. Optics Electron. 10, 223–232 共2000兲.
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Abstr. 134, 121606w 共2001兲.
00/38 M. V. Korobov, P. A. Dorozhko, A. S. Lobach, A.
A. Popov, and V. M. Senyavin, Schr. Forschungszent. Juelich
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00/39 P. O. Dunstan, Thermochim. Acta 356, 19–25
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00/40 J. A. de A. Imeida Sales, A. G. Souza, G. F. Goncalves de Freitas, S. Prasad, M. F. S. Trindade, L. H. Carvalho, and P. O. Dunstan, Thermochim. Acta 356, 9–17
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ENTHALPY OF SUBLIMATION
00/41 S. Brownridge, H. Du, S. A. Fairhurst, R. C. Haddon, H. Oberhammer, S. Parson, J. Passmore, M. J. Schriver,
L. H. Sutcliffe, and N. P. C. Westwood, J. Chem. Soc., Dalton Trans. 3365–3382 共2000兲.
2001
01/1 M. D. M. C. Ribeiro da Silva, J. M. Goncalves, S.
C. C. Ferreira, L. C. M. da Silva, M. J. Sottomayor, G.
Pilcher, W. E. Acree, Jr., and L. E. Roy, J. Chem. Thermodyn. 33, 1263–1275 共2001兲.
01/2 R. Patino, M. Campos, and L. A. Torres, J. Chem.
Thermodyn. 共submitted for publication, 2001兲.
01/3 H. P. Diogo, M. E. Minas de Piedade, J. M. Goncalves, M. J. S. Monte, and M. A. V. Ribeiro da Silva, Eur. J.
Inorg. Chem. 257–262 共2001兲.
01/4 M. D. M. C. Ribeiro da Silva, S. C. C. Ferreira, I.
A. P. Rodrigues, L. C. M. da Silva, W. E. Acree, Jr., S.
Pandey, and L. E. Roy, J. Chem. Thermodyn. 33, 1227–1235
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01/5 T. Kiyobayashi and M. E. Menas da Piedade, J.
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01/6 C. Colominas, K. H. Lau, D. L. Hildenbrand, S.
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450 共2001兲.
01/7 M. J. S. Monte and D. M. Hillesheim, J. Chem.
Thermodyn. 33, 103–112 共2001兲.
01/8 D. Giordano, J. Chem. Eng. Data 46, 486 –505
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01/9 M. A. V. Ribeiro da Silva, M. D. M. C. Ribeiro da
Silva, L. C. M. da Silva, F. Dietz, E. Hoyer, L. Beyer, B.
Schröder, A. M. Damas, and J. F. Liebman, J. Chem. Soc.,
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01/10 M. J. S. Monte and D. M. Hillesheim, J. Chem.
Eng. Data 46, 1601–1604 共2001兲.
01/11 P. A. Dorozhko, A. S. Lobach, A. A. Popov, V. M.
Senyavin, and M. V. Korobov, Chem. Phys. Lett. 336, 39– 46
共2001兲.
01/12 G. E. Nikitina, B. Suleiman, A. S. Semeikin, and
O. A. Golubchikov, Russ. J. Phys. Chem. 75, 675–758
共2001兲.
01/13 M. A. V. Ribeiro da Silva, M. J. S. Monte, and E.
Giera, J. Chem. Thermodyn. 33, 369–376 共2001兲.
01/14 M. V. Roux, P. Jimenez, J. Z. Davalos, R. Notario,
and E. Juaristi, J. Org. Chem. 66, 5343–5351 共2001兲.
01/15 S. Chattopadhyay, H. J. Tobias, and P. J. Ziemann,
Anal. Chem. 73, 3797–3803 共2001兲.
01/16 M. V. Roux, P. Jimenez, P.-A. Mayorga, J. Z.
Davalos, S. Böhm, and O. Exner, J. Phys. Chem. A 105,
7926 –7932 共2001兲.
01/17 M. A. V. Ribeiro da Silva, M. A. R. Matos, M. S.
Miranda, M. H. F. A. Sousa, R. M. Borges dos Santos, M. M.
Bizarro, and J. A. Martinho Simoes, Struct. Chem. 12, 171–
181 共2001兲.
01/18 M. A. V. Ribeiro da Silva, M. D. M. C. Ribeiro da
Silva, L. C. M. da Silva, F. Dietz, and E. Hoyer, Thermochim. Acta 378, 45–50 共2001兲.
01/19 K. C. Albyn, J. Chem. Eng. Data 46, 1415–1416
共2001兲.
697
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Thermodyn. 33, 745–754 共2001兲.
2002
02/1 B. Brunetti, G. Portalone, and V. Piacente, J. Chem.
Eng. Data 47 17–19 共2002兲.
Unpublished Results
U/1 C. G. DeKruif 共unpublished results兲.
U/2 C. H. D. van Ginkel, C. G. DeKruif, and F. E. B. de
Waal 共unpublished results兲.
U/3 H. Mackle, W. V. Steele, and D. V. McNally 共unpublished results兲.
U/4 D. Stull 共unpublished results兲.
U/5 J. S. Chickos 共unpublished results兲.
7. Acknowledgments
J.S.C. would like to thank the past and present students in
Chemistry 202, Introduction to the Chemical Literature, who
have contributed to this compilation through their term papers.
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