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ANALYTICALß'
BIOANALYTICAL
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Addresses of Editor
S. Daunert
P. Garrigues
G. Gauglitz
K. G. Heumann
K. Jinno
A. Roda
A. Sanz-Medel
S. A. Wise
Sylvia Daunert
Dept. Chemistry & Dept. Pharmaceutical Sciences
University of Kentucky, Lexington, KY 40506-0055, USA
Tel.: +1-859-257-7060,e-mail: [email protected]
Philippe Garrigues
Institut des Sciences Moléculaires (ISM), UMR 5255 CNRS
Bâtiment A12. Université de Bordeauxl, 33405 Talence Cedex, France
Tel.: +33-5-40006283,e-mail: [email protected]
Regional Editor Central Europe
M. Jarosz
Central Editorial Office
Springer
Tiergartenstrasse 17
69121 Heidelberg, Germany
Managing Editor
Christina Dyllick
Associate Editor
Andrea Pfeifer
Assistant Editor
Ingrid März
Editorial Assistants
Maite Menés
Patricia Vogt
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Fax: +49-6221-48768377
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Günter Gauglitz
Inst. Physikalische & Theoretische Chemie, Universität Tübingen
Auf der Morgenstelle 8,72076 Tübingen, Germany
Tel.: +49-7071-29-76927 or -74667, e-mail: [email protected]
Klaus G. Heumann
Inst. Anorg. Chemie & Analytische Chemie, Johannes Gutenberg-Universität
Duesbergweg 10-14, 55099 Mainz, Germany
Tel.: +49-6131-39-25882, e-mail: [email protected]
Kiyokatsu Jinno
School of Materials Science, Toyohashi University of Technology
Toyohashi 441-8580,Japan
Tel.: +81-532-446805, e-mail: jinnoSchrom.tutms.tut.ac.jp
Aldo Roda
Laboratory of Analytical and Bioanalytical Chemistry
Dept. of Pharmaceutical, Sciences, Alma Mater Studiorum-University of Bologna,
Via Belmeloro 6,40126 Bologna, Italy
Tel. and Fax: +39-051-343398, e-mail: [email protected]
Alfredo Sanz-Medel
Dept. Physical & Analytical Chemistry, University of Oviedo
CI Julián Claveria 8, 33 006 Oviedo, Spain
Tel.: +34-985-103474, e-mail: [email protected]
Stephen A. Wise
National Inst. of Standards & Technology
100 Bureau Drive, Stop 8390, Gaithersburg, MD 20899-8390, USA
Tel.: +1-301-975-3108, e-mail: [email protected]
Address of Regional Editor
Maciej Jarosz
Faculty of Chemistry
Warsaw University of Technology
Noakowskiego 3
00-664 Warsaw, Poland
Tel. and Fax: +48-22-234-7408, e-mail: [email protected]
A4
Bibliografische Informationen
http://d-nb.info/1002786940
digitalisiert durch
ANALYTICALcSr
BIOANALYTICAL
CHEMISTRY
Volume 397 Number 1 May 2010
ANALYTICAL CHALLENGE
Avogadro constant challenge
W.B. Jensen • J. Meija 1
Solution to the beryllium valence challenge
J. Meija 3
Euroanalysis XV
The European Conference
on Analytical Chemistry
Guest Editors: Wolfgang Buchberger •
Wolfgang Lindner
EDITORIAL
Euroanalysis XV, 2009: The European conference
on analytical chemistry
W. Buchberger • W. Lindner 5
ABCS OF TEACHING ANALYTICAL SCIENCE
E-learning in applied instrumental analysis: the example
of cultural heritage preservation
E.A. Varella 7
FEATURE ARTICLE
Some people and places important in the history
of analytical chemistry in Austria
D.T. Burns 11
Application of the novel 5-chloro-2,2,3,3,4,4,5,5octafluoro-1-pentyl chloroformate derivatizing agent
for the direct determination of highly polar water
disinfection byproducts
M. Vincenti • F. Fasano • M.C. Valsania • P. Guarda •
S.D. Richardson 43
ORIGINAL PAPERS
Food Analysis
An inimunochemical test for rapid screening
of zearalenone and T-2 toxin
E.Y. Basova • I.Y. Goryacheva • T.Y. Rusanova •
N.A. Burmistrova • R. Dietrich • E. Märtlbauer •
C. Detavernier • C. Van Peteghem • S. De Saeger 55
Direct chiral determination of free amino acid
enantiomers by two-dimensional liquid chromatography:
application to control transformations in E-beam
irradiated foodstuffs
V. Guillén-Casla • M.E. León-González • L.V. Pérez-Arribas •
L.M. Polo-Diez 63
Exploiting automatic on-line renewable molecularly
imprinted solid-phase extraction in lab-on-valve format
as front end to liquid chromatography: application to
the determination of riboflavin in foodstuffs
H.M. Oliveira • M.A. Segundo • J.L.F.C. Lima • M. Miró •
V. Cerdà 77
Determination of aflatoxin Bj in alcoholic beverages:
comparison of one- and two-photon-induced
fluorescence
C. Rasch • M. Böttcher • M. Kumke 87
TRENDS
PAPERS IN FOREFRONT
Development and validation of a LC-MS/MS method
for the simultaneous determination of aflatoxins, dyes
and pesticides in spices
C. Ferrer Amate • H. Unterluggauer • R.J. Fischer •
A.R. Fernández-Alba • S. Masseiter 93
The principle of exhaustiveness versus the principle
of parsimony: a new approach for the identification
of biomarkers from proteomic spot volume datasets
based on principal component analysis
E. Marengo • E. Robotti • M. Bobba • F. Gosetti 25
Fluctuation in the ergosterol and deoxynivalenol content
in barley and malt during malting process
V. Dohnal • A. Jezkova • L. Pavlikova • K. Musilek •
D. Jun • K. Kuca 109
The environmental challenge for analytical sciences
M. Grasserbauer 17
Springer
ANALYTICAL
BIOANALYTICAL
CHEMISTRY
Comparison of two derivatization-based methods for
solid-phase microextraction-gas chromatography-mass
spectrometric determination of bisphenol A, bisphenol S
and biphenol migrated from food cans
P. Viñas • N. Campillo • N. Martinez-Castillo •
M. Hernández-Córdoba 115
Validated HPAEC-PAD method for prebiotics
determination in synbiotic fermented milks during
shelf life
C. Borromei • A. Cavazza • C. Corradini • C. Vatteroni •
A. Bazzini • R. Ferrari • P. Menisi 127
Pharmaceutical Analysis
Identification of a new co-crystal of salicylic acid and
benzamide of pharmaceutical relevance
M.A. Elbagerma • H.G.M. Edwards • T. Munshi •
IJ. Scowen 137
Quantitative LC-ESI-MS/MS metabolic profiling
method for fatty acids and lipophilic metabolites in
fermentation broths from ß-lactam antibiotics
production
S. Schiesel • M. Lämmerhofer • W. Lindner 147
Development of an LC-MS/MS method for analysis
of interconvertible Z/E isomers of the novel anticancer
agent, Bp4eT
J. Stariat • P. Kovaríková • J. Klimes • D.S. Kalinowski •
D.R. Richardson 161
Determination of adrenolytic drugs by SPME-LC-MS
B. Buszewski • P. Olszowy • T. Ligor • M. Szultka •
J. Nowaczyk • M. Jaworski • M. Jackowski 173
Quantification of chlorpheniramine maléate
enantiomers by ultraviolet spectroscopy and
chemometric methods
P. Valderrama • A.L. Romero • P.M. Imamura •
I.R.S. MagaMes • P.S. Bonato • R.J. Poppi 181
Electrochemical evaluation and determination of
antiretroviral drug fosamprenavir using boron-doped
diamond and glassy carbon electrodes
M. Gumustas • S.A. Ozkan 189
Biological Analysis
Determination of insoluble avian eggshell matrix
proteins
I. Miksik • P. Sedláková • K. Lacinová • S. Pataridis •
A. Eckhardt 205
Springer
Raman spectroscopic analysis of minerals and organic
molecules of relevance to astrobiology
A.I. Alajtal • H.G.M. Edwards • I.J. Scowen 215
Determination of heterocyclic amines in urine samples
by capillary liquid chromatography with evaporated
light-scattering detection
F. De Andrés • M. Zougagh • G. Castañeda • A. Ríos 223
Voltammetric detection of damage to DNA caused by
nitro derivatives of fluorene using an electrochemical
DNA biosensor
V. Vyskocil • J. Labuda • J. Barek 233
Environmental Analysis
Simultaneous determination by ultra-performance
liquid chromatography-atmospheric pressure chemical
ionization time-of-flight mass spectrometry of nitrated
and oxygenated PAHs found in air and soot particles
G. Mirivel • V. Riffault • J.-C. Galloo 243
Determination of brominated diphenyl ethers (from
mono- to hexa- congeners) in indoor dust by pressurised
liquid extraction with in-cell clean-up and gas
chromatography-mass spectrometry
M.P. Martinez • J.D. Carrillo • M.T. Tena 257
Determination of organic UVfiltersin water by stir
bar sorptive extraction and direct analysis in real-time
mass spectrometry
M. Haunschmidt • C.W. Klampfl • W. Buchberger •
R. Hertsens 269
Method for the simultaneous determination of the most
problematic families of organic pollutants in compost
and compost-amended soil
M.M. González • J.L. Santos • I. Aparicio • E. Alonso 277
Holistic visualisation of the multimodal transport
and fate of twelve Pharmaceuticals in biosolid
enriched topsoils
L. Barron • E. Nesterenko • K. Hart • E. Power • B. Quinn •
B. Kelleher • B. Pauli 287
Capillary liquid chromatography with off-line mid-IR
and Raman micro-spectroscopic detection: analysis
of chlorinated pesticides at ppb levels
S. Armenta • B. Lendl 297
GC-MS determination of polycyclic aromatic
hydrocarbons evolved from pyrolysis of biomass
D. Fabbri • A. Adamiano • C. Torri 309
Miscellaneous
Multimethod analysis of Iranian Ilkhanate ceramics from
the Takht-e Soleyman palace
L. Osete-Cortina • M.T. Doménech-Carbó • A. Doménech •
DJ. Yusá-Marco • H. Ahmadi 319
Screen-printed sensor for batch and flow injection
potentiometric chromium(VI) monitoring
R.A. Sánchez-Moreno • MJ. Gismera • M.T. Sevilla •
J.R. Procopio 331
Determination of vanadium(V) in the particulate matter
of emissions and working areas by sequential dissolution
and solid-phase extraction
M. Sturini • F. Maraschi • L. Cucca • G. Spini •
G. Talamini • A. Profumo 395
Ultra-fast HPLC-ICP-MS analysis of oxaliplatin
in patient urine
G. Koellensperger • S. Hann 401
Investigation of selective molecular interactions using
two-dimensional Fourier transform IR spectroscopy
X. Liu • T. Zhou • X. Wang • J. Zhang
339
Characterisation of steroids in wooden crates of veal
calves by accelerated solvent extraction (ASE®)
and ultra-high performance liquid chromatography
coupled to triple quadrupole mass spectrometry
(U-HPLC-QqQ-MS-MS)
K. Verheyden • H. Noppe • J. Vanden Bussche • K. Wille •
K. Bekaert • L. De Boever • J. Van Acker • C.R. Janssen •
H.F. De Brabander • L. Vanhaecke 345
Identification of additives in poly(vinylacetate) artist's
paints using PY-GC-MS
M.F. Silva • M.T. Doménech-Carbó • L. Fuster-López •
M.F. Mecklenburg • S. Martin-Rey 357
Volatile organic compounds in paper—an approach
for identification of markers in aged books
E.M. Gaspar • J.C. Santana • J.F. Lopes • M.B. Diniz 369
CMOS arrays as chemiluminescence detectors on
microfluidic devices
E.R.G.O. Rodrigues • R.A.S. Lapa 381
TECHNICAL NOTES
Application of the new electroanalytical technique
AGNES for the determination of free Zn concentration
in river water
F. Zavarise • E. Companys • J. Galceran • G. Alberti •
A. Profumo 389
Indexed in/abstracted by Current Contents, Science
Citation Index, Analytical Abstracts, Chemical Abstracts,
BIOSIS, Aquatic Sciences and Fisheries Abstracts, Food
Science and Technology Abstracts, Life Science Collection,
Pascal, Index Medicus and Mediine
Instructions for Authors for Anal Bioanal Chem are
available at http^/www.springer.com/abc
Cover image: SEM backscattered electron image of
the metallic sheet fixed on the glaze of the sample
CI7VC (reference 20986-10). Metallic sheet on the top,
and glaze at the bottom. (From L. Osete-Cortina,
M.T. Doménech-Carbó, A. Doménech, DJ. Yusá-Marco,
H. Ahmadi 'Multi-method analysis of Iranian Ilkhanate
ceramics from the Takht-e Soleyman palace'.
Anal Bioanal Chem (2010) 397: 319-329)
Springer