Carbon
Carbon-13 benchtop
NMR NMR
Carbon-13
benchtop
For organic chemists 13C NMR
backbone of routine molecular analysis. Spinsolve Carbon has
For organic chemists 13Cforms
NMRtheforms
the backbone of routine molecular analysis.
outstanding resolution and unique sensitivity that enables the power of proton-carbon NMR in a benchtop
Now you can have the power of proton-carbon NMR in a benchtop instrument that
instrument. This best-in-class spectrometer is the most flexible and cost effective way to get carbon-13
canlaboratory.
use in your lab.
NMRyou
in your
5 6
9 8
4 7
14
15
10 16
11 17
12
16,17
10,11
14,15
12
6,7,8
HETCOR spectrum of lidocaine
HETCOR spectrum of lidocaine
Who
Who
•Synthetic Chemists
•Medicinal Chemists
• Medicinal
and Pharmaceutical
• Organic Chemistry
Lecturers •Structure
Elucidation
•Organic
ChemistryChemists
Education
• Small Molecule Research Scientists • Synthetic Chemists monitoring reactions
• Academics running practical laboratory classes • Post Graduate Chemistry Students
Why
Why
$
•No cryogens •Low cost
•Low maintenance
• No cryogens
• Low cost
• Low maintenance
• Fast
• Accessible • Easy to operate
•Fast
•Easy to operate
•Accessible
• Convenient
• Robust
• Exceptional performance
•Convenient
•Robust
•Exceptional performance
Carbon
Example
NMR
Spectra of Lidocaine using Spinsolve Carbon
13C NMR
Spectroscopy
13C13
Spectroscopy
13C NMR
C 13
NMR
Spectroscopy
C
NMR
Spectroscopy
NMR
Spectroscopy
Example NMR Spectra
of Lidocaine using Spinsolve Carbon.
Example NMR Spectra of Lidocaine using Spinsolve Carbon.
Example
NMR
Spectra
of Lidocaine
Spinsolve
Carbon.
Example
NMR
Spectra
of Lidocaine
using
Spinsolve
Carbon.
Example
NMR
Spectra
of
Lidocaine
usingusing
Spinsolve
Carbon.
2
10,11
10,11
10,11
10,11
6
7
8
6
7
86
6
7
8
7
8
3
3
3
10,11
2
CH3
6
7
8
16
17
14
15
12
12 14
15
14
15
14
15
12
12
14
1416
10
15
14
11
1517
1215
10 10
16
16
10
11 16
17
11 17
11 17
12
12
CH3
CHCH
3
3
CH2
CH2
CH2 CH2
CH2
CH
3
10 16
11 17
14
15
CH3
16
17
16 12 16
16
17
1417
15
1217
14
15
12
3
2
5 6
5 6
9 8
5 65 69 8
7 6
4 5
2 9 8
9 84 7
9 8
2
7
4 7 4 4 7
CH
CH
CH
1D Proton with1D
peak
assignments.
Carbon shows
peaks of
all carbons
Proton
with peak assignments. 1D CH
1D Carbon
shows
peaks of(top).
all carbons (top).
1DSpectral
Carbon
shows
ofofall signals
carbons
usingpeaks
DEPT
selects
of (top).
Spectral editing
using editing
DEPT
selects
signals
CH
,
CH
and
CH
groups
(rows
2-4).
CH1D
and
CH
(rows
2-4).
1D Proton
withassignments.
peak assignments.
Carbon
shows
peaks
of DEPT
all carbons
(top).signals
1D Proton
with peak
Carbon
shows
peaks
of
all
carbons
(top).
Spectral
editing
using
selects
3 groups
2
3, CH
21D
Spectral
editing
using
DEPT
selects
signals
of
Spectral
editing
using
DEPT
selects
signals
of
and
CH
groups
(rows
2-4)
,
CH
of
CH
10,11
10,11
3
2
10,11
10,11
16
16
16
16
CH
,
CH
and
CH
groups
(rows
2-4).
,
CH
and
CH
groups
(rows
2-4).
CH
14
14
3
2
3
2
Proton6,7,8
with peak assignments.
1D6,7,8
Carbon shows
of all carbons
(top).
6,7,8 peaks
14
6,7,8 14
17
17
1D Proton with peak assignments.
1D
12 15
6,7,8 16,17
6,7,8
16,17
16,17
14,15
16,17
6,7,8
12
10,11
10,11
14,15
16,17
6,8
14,15
10,11
16
14
17
15
16
17
12
10,11
14
12 15
16
17
6,8
4
5,9
4
7
2
2D HMQC shows single-bond
2
2D HMQC
shows
single-bondcorrelations.
proton-carbon
proton-carbon correlations.
2D HMQC
shows shows
single-bond
2D HMQC
single-bond
2D HMQCcorrelations.
shows single-bond
proton-carbon
proton-carbon correlations.
2
14,15
14,15
5,9
4
5,9
6,7,8
12
10,11
proton-carbon correlations.
14
12 15
16
17
12
10,11
7
6,8
4
5,9
14,15
15
10,11
16,1714,15
12
10,11
6,8
15
10,11
16,17
14,15
7
2
6,8
16,17
16,17
12
7
7
7
6,8
2 4 6,8
4
5,9
5,9
Spectral editing using DEPT
selects
signals of
10,11
10,11
16
16
16,17
14
14
6,7,8 CH groups (rows
CH3, 6,7,8
CH2 and
2-4).
17
17
12
12
10,11
14,15
17 12 15
12 15
12
5,9
12
12 15
14,15
12
10,11
10,11
14
12 15 12
10,11
10,11
17
7
4
7 12
7 2
6,8
6,8
2
4
4
5,9
5,9
2D HMBC shows long-range
2
2
2D HMBC
shows
long-range
proton-carbon
correlations.
7
proton-carbon
correlations.
6,8
4
5,92D
HMBC
shows long-range
2D HMBC
shows long-range
2D
HMBC
shows long-range
proton-carbon
correlations.
proton-carbon
correlations.
2
proton-carbon correlations.
Carbon
Software
The power of simplicity
• Uncomplicated one-button operation
• Minimal user controlled parameters
• Simple intuitive graphical interface
• Traditional NMR complexities are hidden
• Automated and easy to use
DEPT-135 spectrum of 2 M lidocaine in d-chloroform. The inverted peaks are the CH2 carbons.
Features
• 1D 1H, 19F and 13C experiments
• Standard 5 mm NMR tubes
• 2D COSY and homonuclear j-resolved
spectroscopy
• T1 and T2 relaxation experiments
• Spectral editing with DEPT
• Composite pulse decoupling
• 2D heteronuclear correlation experiments
HETCOR, HMQC, HMBC
R
Specifications
• Frequency: 42.5 MHz Proton, 10.8 MHz Carbon
• Resolution: 50% linewidth < 0.5 Hz (12 ppb)
• Lineshape: 0.55% linewidth < 20 Hz
• Dimensions: 58 x 43 x 40 cm
• Weight: 55 kg
• Magnet: Permanent and cryogen free
• Stray field: < 2 G all around system
Other Spinsolve products
Spinsolve for education
R
Spinsolve
R
• 1D Proton only system
• 1H and 19F nuclei
• Budget friendly price
• Relaxation time experiments
• Upgradeable
• 2D COSY and JRES
• Reaction monitoring
“Now the students are able to acquire their own NMR spectra as well as carry out the analysis of the compounds they
have made. This makes their undergraduate experiment more applicable to both research and industry settings and
increases their enthusiasm for Chemistry.”
Professor Frances Separovic, Head of Chemistry, University of Melbourne
Contact us now for a quote, or to arrange a demo or sample measurement.
CONTACT INFORMATION
For further information, please contact: [email protected]
GERMANYNEW ZEALAND
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Tel: +49 (241) 70525-6000
Tel: +64 4 477 7096
Fax: +49 (241) 963 1429
Fax: +64 4 471 4665
Or visit our website www.magritek.com
UNITED STATES
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San Diego, CA 92121, USA
Tel: +1 (855) 667-6835
+1 (866) NMR-MTEK