APMP Supplementary Comparison on Fiber Optic Power Responsivity APMP.PR-S2 Final Report Seung Kwan Kim, Dong-Hoon Lee, and Seung-Nam Park Division of Physical Metrology, Korea Research Institute of Standards and Science 267 Gajeong-Ro, Yuseong-Gu, Daejeon 305-340, Republic of Korea Correspondence to: [email protected] APMP.PR-S2 Fiber Optic Power Responsivity APMP Supplementary Comparison on Fiber Optic Power Responsivity Seung Kwan Kim, Dong-Hoon Lee, and Seung-Nam Park Division of Physical Metrology, Korea Research Institute of Standards and Science 267 Gajeong-Ro, Yuseong-Gu, Daejeon 305-340, Republic of Korea [email protected] Abstract KRISS, NMISA, CMS/ITRI, NMC-A*STAR, NMIJ/AIST, NMIA, NML-SIRIM, NIM, and VNIIOFI conducted a supplementary comparison on the fiber optic power responsivity at 1310 nm and 1550 nm. The aim of this comparison is to examine the equivalence of the fiber optic power responsivity among participating laboratories and to provide supporting evidence for associated CMC claims in BIPM KCDB. 2 APMP.PR-S2 Fiber Optic Power Responsivity Table of Contents 1. Introduction ........................................................................................................................... 4 2. Organization of the comparison ............................................................................................ 5 2.1. Participants .................................................................................................................. 5 2.2. Participants’ details ..................................................................................................... 5 2.3. Form of the comparison .............................................................................................. 7 2.4. Timetable..................................................................................................................... 8 3. Description of the artifact .................................................................................................... 10 4. Measurement Capability and Results of Pilot Laboratory ................................................... 13 5. 6. 7. 4.1. Traceability ............................................................................................................... 13 4.2. Description of measurement facility ......................................................................... 14 4.3. Laboratory conditions ............................................................................................... 16 4.4. Measurement procedure ............................................................................................ 16 4.5. Measurement results ................................................................................................. 17 4.6. Uncertainty ................................................................................................................ 18 Measurement Capabilities and Results of Participants ........................................................ 21 5.1. NMISA ...................................................................................................................... 21 5.2. CMS/ITRI ................................................................................................................. 28 5.3. NMC-A*STAR ......................................................................................................... 31 5.4. NMIJ/AIST ............................................................................................................... 39 5.5. NMIA ........................................................................................................................ 56 5.6. NML-SIRIM ............................................................................................................. 73 5.7. NIM ........................................................................................................................... 76 5.8. NIM (Second Measurements) ................................................................................... 80 5.9. VNIIOFI .................................................................................................................... 84 Results and Discussions ...................................................................................................... 87 6.1. Artifact Drift ............................................................................................................. 87 6.2. Difference from Pilot ................................................................................................ 90 6.3. Comparison Reference Value .................................................................................... 94 6.4. Degree of Equivalence .............................................................................................. 99 6.5. Discussions.............................................................................................................. 103 Conclusions ....................................................................................................................... 105 3 APMP.PR-S2 Fiber Optic Power Responsivity 1. Introduction Under the Mutual Recognition Arrangement (MRA) the metrological equivalence of national measurement standards will be determined by a set of key comparisons chosen and organized by the Consultative Committees of the CIPM working closely with the Regional Metrology Organizations (RMOs). At its meeting in November 2004, the Technical Committee for Photometry and Radiometry (TCPR) of the Asia Pacific Metrology Programme (APMP) proposed several regional comparisons in the field of optical radiation metrology. Fiber optic power responsivity was one of them and was agreed to be conducted as supplementary comparison. The present report concerns the supplementary comparison APMP.PR-S2, international comparison of fiber optic power responsivity measurements at the wavelength of 1310 nm and 1550 nm, piloted by KRISS. The technical protocol was prepared by KRISS and agreed by all the other participants. The comparison was carried out through the calibration of a fiber optic power meter chosen as the comparison artifact. The comparison was organized in a star format as [pilot]-[participant]-[pilot]. The comparison measurement began in January, 2006 with eight participants. While measurements were being carried out, VNIIOFI joined under the agreement by all participants. It was agreed that VNIIOFI’s result would be added in the appendix of the report in order not to affect the original comparison schedule. However, measurements were delayed due to several unexpected reasons even after VNIIOFI’s participation. Therefore, VNIIOFI’s result was also included in the report since all the reports from participants including VNIIOFI were available at the time of report preparation. For more details, the Technical Protocol of the APMP.PR-S2 comparison can be referred. 4 APMP.PR-S2 Fiber Optic Power Responsivity 2. Organization of the comparison 2.1. Participants The participants of this supplementary comparison were: KRISS (Republic of Korea), CSIRNML (now NMISA, South Africa), CMS/ITRI (Chinese Taipei), SPRING (now NMC-A*STAR, Singapore), NMIJ/AIST (Japan), NMIA (Australia), NML-SIRIM (Malaysia), NIM (People’s Republic of China), and VNIIOFI (Russia); KRISS acted as the pilot laboratory. All the participants were able to demonstrate traceability to an independent realization of the quantity or make clear the route of traceability to the quantity via another named laboratory at the time of comparison measurements. 2.2. Participants’ details Table 2-2-1. Contact list of participants. NMI Name (Country) Personnel KRISS (Republic of Korea) Seung Kwan Kim Seung-Nam Park NMISA (South Africa) Bertus Theron* Mariesa Nel Natasha NelSakharova CMS/ITRI (Republic of China) Min-Jay Huang* Mao-Sheng Huang* Hsueh-Ling Yu NMC-A*STAR (Singapore) Huang Xuebo Xu Gan Contact information Center for Photometry and Radiometry Division of Physical Metrology Korea Research Institute of Standards and Science 1 Doryong-dong, Yuseong-gu Daejeon 305-340, Republic of Korea Tel: +82 42 868-5701, 5200 Fax: +82 42 868-5022 E-mail: [email protected]; [email protected] Fiber Optics Laboratory National Metrology Institute of South Africa Private Bag X34, Lynnwood Ridge, 0040 South Africa Tel: +27 12 841 2561, 3618 Fax: +27 86 509 6171, +27 12 841 2131 E-mail: [email protected]; [email protected] Center for Measurement Standards, ITRI 321 Kuang Fu Rd., Sec. 2, Bldg. 16 30042 Hsinchu, Taiwan, R.O.China Tel: +886 3 5743746 Fax: +886 3 5716231 E-mail: [email protected]; [email protected] National Metrology Centre Agency for Science, Technology and Research (A*STAR) 1 Science Park Drive, Singapore 118221 Tel: +65 6279 1939, 1937 Fax: +65 6279 1995 5 APMP.PR-S2 Fiber Optic Power Responsivity E-mail: NMIJ/AIST (Japan) Kuniaki Amemiya Terubumi Saito* NIMA (Australia) Errol Atkinson Philip Lukins* Peter Manson NML-SIRIM (Malaysia) Mohd Nizam Abdullah NIM (People’s Republic of China) Lin Yandong Zhang Zixin VNIIOFI (Russia) Alexey Svetlichny Vladimir Kravtsov [email protected] [email protected] Laser Standard Laboratory NMIJ Tsukuba Center 3-9, AIST 1-1-1 Umezono, Tsukuba 305-8563, Japan Tel: +81 29 861 4191 Fax: +81 29 861 4259 E-mail: [email protected] Optical Standards National Measurement Institute Department of Innovation, Industry, Science and Research Bradfield Road, West Lindfield NSW 2070, Australia Tel: +61 2 8467 3858 Fax: +61 2 8467 3752 E-mail: [email protected] [email protected] National Metrology Laboratory SIRIM Berhad Lot PT 4803 Bandar Baru Salak Tinggi 43900 Sepang Selangor Darul Ehsan, Malaysia Tel: +603-87781644 Fax: +603-87781616 E-mail: [email protected] Optical Measurement Division National Institute of Metrology 18 Bei San Huan Dong Lu 100013 Beijing, China Tel: +86 10 64218651 Fax: +86 10 64218651 E-mail: [email protected]; [email protected] Laboratory of low-intensity laser radiation and fiberoptical systems metrology All Russian Research Institute for Optical and Physical Measurements (VNIIOFI) 46 Ozernaya street, Moscow 119361, Russia Tel: +7 495 7814587, 7814586 Fax: +7 495 7814587, 4373147 E-mail: [email protected]; [email protected] * Their affiliation changed and they are not related with this work any longer. 6 APMP.PR-S2 Fiber Optic Power Responsivity 2.3. Form of the comparison The comparison was carried out through the calibration of a fiber optic power meter prepared by KRISS. A detailed description of the fiber optic power meter used in this comparison is given in section 3. The fiber optic power meter consists of an optical head, a unit for control and display, and an electrical cable connecting them. KRISS further prepared two FC/PC type fiber optic patch cords labeled as FC-1 and FC-2 to reduce the uncertainty from using different kinds of fiber optic connector. FC-2 was prepared only in the case that FC-1 would be damaged. FC-1 had been used without any problem throughout the measurements and therefore FC-2 was not actually used for comparison. It was recommended that the participants would report the measurement results both with the prepared fiber optic patch cords and with their own patch cords in order to investigate how large the deviation could occur owing to the use of different fiber connector. The comparison was organized in a star type format. KRISS calibrated the artifact first and then sent it to a participant. The participant calibrated it and returned the artifact to KRISS. KRISS re-calibrate it to check the drift during the period of transportation and measurements in a different country. The process was repeated until all the participants finished their calibration. It was agreed that each participant should report its correction factor at 1310 nm and 1550 nm at the radiant power level of -10 dBm (0.1 mW), and it was strongly recommended that the correction factors at the radiant power level of -20 dBm (0.01 mW), and -30 dBm (0.001 mW) be reported if available. In addition, it was agreed that each participant should specify the type of the optical source used, center wavelength with uncertainty defined in the technical protocol, and FWHM. Finally, it was agreed that it is the participants’ responsibility to report the actual wavelengths used, corrections to be made to the measurement results for the center wavelength offsets and uncertainties associated with such corrections. The participants should make corrections based on the spectral responsivity data of the transfer power meter determined by its own means. 7 APMP.PR-S2 Fiber Optic Power Responsivity 2.4. Timetable Timetable of the original plan of the comparison as given in the technical protocol is shown in Table 2-4-1. Table 2-4-1. Scheduled timetable of the comparison in the beginning. Activity Circulation of technical protocol and invitation of participants Confirmation of participation and revision of protocol Submission of technical protocol to TCPR chair for approval Final revision and announcement of kick-off Calibration of NMI 1 (KRISS, Rep. of Korea) Calibration of NMI 2 (CSIR, South Africa) Calibration of NMI 3 (CMS/ITRI, Rep. of China) Calibration of NMI 4 (SPRING, Singapore) Calibration of NMI 5 (NMIJ/AIST, Japan) Calibration of NMI 6 (NMIA, Australia) Calibration of NMI 7 (NML-SIRIM, Malaysia) Calibration of NMI 8 (NIM, P.R. of China) Draft A report Draft B report Start Date 1 Jun, 2005 1 Jul, 2005 1 Sep, 2005 1 Nov, 2005 1 Jan, 2006 1 Mar, 2006 1 May, 2006 1 Jul, 2006 1 Sep, 2006 1 Nov, 2006 1 Jan, 2007 1 Mar, 2007 1 May, 2007 1 July, 2007 End Date 30 Jun, 2005 31 Aug, 2005 31 Oct, 2005 31 Dec, 2005 28 Feb, 2006 30 Apr, 2006 30 Jun, 2006 31 Aug, 2006 31 Oct, 2006 31 Dec, 2006 28 Feb, 2007 30 Apr, 2007 30 Jun, 2007 31 Aug, 2007 However, the actual measurements were delayed from the above plan due to each of the laboratory's specific circumstance, such as customs clearance, re-measurements, etc. Table 2-4-2 lists the actual time sequence. Table 2-4-2. History of the comparison measurements. Activity KRISS, NMISA, CMS/ITRI, NMC-A*STAR, NMIJ/AIST, NMIA, NML-SIRIM, NIM, VNIIOFI Pre-draft A process NIM KRISS, 1st measurements 2nd measurements 3rd measurements 4th measurements 5th measurements 6th measurements 7th measurements 8th measurements 9th measurements Re-measurements Final measurements Occupied period 01 Jan. 2006 ~ 09 Mar. 18 Mar. 2006 ~ 19 Apr. 11 May 2006 ~ 28 Jun. 18 Jul. 2006 ~ 13 Sep. 06 Oct. 2006 ~ 23 Nov. 18 Dec. 2006 ~ 06 Mar. 28 Mar. 2007 ~ 21 Jun. 28 Jul. 2007 ~ 18 Oct. 01 May 2008 ~ 31 Oct. 20 Nov. 2008 ~ 30 Jan. 13 Nov. 2009 ~ 15 Apr. 20 May 2010 ~ 31 Jan. 2006 2006 2006 2006 2006 2007 2007 2007 2008 2009 2010 2011 All the comparison reports from original 8 participants arrived to KRISS by the end of July, 2008 while VNIIOFI conducted its measurements. Since VNIIOFI’s results were agreed to append in the appendix section, the pre-draft A process began on 20 November, 2008 without VNIIOFI by circulating the uncertainty budgets of all participants blinded and distributing the 8 APMP.PR-S2 Fiber Optic Power Responsivity relative data of each participant to each of them. When participants were confirming their relative data, NIM claimed its re-measurement because the correction factor change of the artifact before and after NIM’s measurements was relatively larger compared to the other times. The coordinator postponed the decision until checking the status of the artifact when VNIIOFI returned it. It took almost a year until the status of the artifact was checked because the artifact did not return to KRISS for a while due to the internal problems of VNIIOFI’s administration and long occupation by Russian customs office. Then, NIM’s re-measurement was decided when the correction factor change of the artifact before and after VNIIOFI’s measurements was identified to be much smaller than that of NIM’s. After NIM’s re-measurements finished, the artifact returned to KRISS in May, 2010. 9 APMP.PR-S2 Fiber Optic Power Responsivity 3. Description of the comparison artifact The comparison artifact was a fiber optic power meter consisting of a control unit and an optical head to collect radiant flux coming from the FC/PC type fiber optic connector end as shown in Fig. 3-1 and 3-2. It was manufactured by ILX Lightwave, Inc. in 2005 with the model number of FPM-8210 and the serial number of 82103878. KRISS purchased this product with its own budget but later received reimbursement through APEC-TILT fund via APMP in 2005. It was agreed that the artifact should be safely preserved in the pilot laboratory after completion of comparison measurements for the future application. Acknowledgement to APMP and APECTILT The optical head consisted of an InGaAs photodiode and a small integrating sphere that enabled this power meter to be independent of the state of polarization from the fiber optic connector end, which gave the reason to select it as the comparison artifact. The optical head were connected to the control unit with an electrical cable. The control unit had a display to indicate the radiant power level either in linear scale (W) or logarithmic scale (dBm or dB) and wavelength in nm. A printed manual was included in the artifact package so that participants could refer to it when they need to set wavelength, gain range, power unit, GPIB address, and so on. Two FC/PC type fiber optic patch cords were also included in the artifact package as described in Section 2.3. FOPM Contoller/Display Unit 102.351 1310 Mains cable plug Optical head FC receptacle Electrical cable Fiber optic patch cord (FC/PC to FC/PC) Fig. 3-1. A schematic of the comparison artifact. 10 APMP.PR-S2 Fiber Optic Power Responsivity Fig. 3-2. Photographs of the artifact. Fig. 3-3. Photographs of the artifact package. 11 APMP.PR-S2 Fiber Optic Power Responsivity Fig. 3-3 shows the artifact package to transport from one country to another. The control unit and the optical head were put into transparent plastic bags with desiccants (silica gel) and securely tied with strings around the electrical cable, respectively. They were securely placed in a polystyrene plate in a thick paper box and covered with another polystyrene plate. The two fiber optic patch cords, the mains cable and the manual were placed on the cover plate, and then the paper box was sealed with packing tape. Finally, the paper box was put into a wooden box and all the necessary information sheets were attached to it. Transportation fees were shared by all participants. KRISS paid the cost of shipment to each participant and each participant paid the individual cost from customs clearance to shipment to KRISS. The costs were partially reimbursed by APMP in 2006 only. 12 APMP.PR-S2 Fiber Optic Power Responsivity 4. Measurement Capability and Results of Pilot Laboratory 4.1. Traceability The KRISS reference standard of the fiber optic power responsivity is an electrically calibrated pyroelectric radiometer (ECPR). The ECPR is a thermal detector coated with a radiation absorbing material that enables the detector to be spectrally insensitive over the wavelength region from visible to mid-IR. The absorbed radiant power causes temperature change and the radiant power is then substituted by the electrical power through pyroelectricity that causes the same temperature change. The correction factor of the ECPR is calibrated using the radiant power of a laser beam measured by the KRISS Si-trap detector at 633 nm in an underfill condition. The responsivity of the KRISS Si-trap detector is calibrated using the KRISS absolute cryogenic radiometer. The correction factor of the ECPR at 633 nm is then expanded to near IR region using the spectral flatness of the ECPR. The correction factor of the KRISS working standard or a fiber optic power meter (FOPM) can be calibrated at -10 dBm using the radiant power of a laser diode delivered through a fiber optic patch cord measured by the ECPR with an appropriate fiber optic receptacle attached to the ECPR. Together with the linearity of the fiber optic power meter calibrated using a superposition method, the correction factor of the fiber optic power meter can be calibrated in the range between -50 dBm and 5 dBm. Therefore, the traceability of the fiber optic power responsivity measurements at KRISS is as shown in Fig. 4-1-1. KRISS Absolute Cryogenic Radiometer Si-trap dector Electrically Calibrated Pyroelectric Radiometer -10 dBm KRISS Working Standard Fiber Optic Power Meter Fiber Optic Power Linearity (Superposition method) -50 ~ +5 dBm Fiber Optic Power Meter Fig. 4-1-1. Traceability of fiber optic power responsivity measurements at KRISS. 13 APMP.PR-S2 Fiber Optic Power Responsivity 4.2. Description of measurement facility The KRISS fiber optic power responsivity measurement facility is as shown in Fig. 4-2-1. Tunable laser sources made by external cavity laser diodes or DFB laser diodes were used as optical sources. The optical beams from the sources were collimated out from the fiber optic patch cords and in to another fiber optic patch cords using appropriate lenses to make 20 cmlong free space gap between them in order to move the chopper of the ECPR into the optical beam when the ECPR measured the radiant power at the corresponding wavelength. Variable optical attenuators (VOA’s) adjusted the radiant power levels to be -10 dBm at the final output end. A broadband fiber optic coupler with a splitting ratio of 90:10 was used to tap 10 % of light out of the optical path and fed into the multi-wavelength meter in order to measure the source wavelengths. A motorized polarization controller was inserted optionally in case that the state of polarization was required to be changed. Fiber optic isolators were used to reduce the radiant power fluctuation caused by interferences due to reflections possibly occurring at the fiber optic connector interfaces. In Fig. 4-2-1, the vertical line in the small rectangle indicates FC/PC to FC/PC interface and the slanted line FC/APC to FC/APC interface. MWM TLS or DFB-LD 1310 nm VOA Broadband Coupler 1310 nm chopper 90/10 Coupler 1550 nm TLS or DFB-LD 1550 nm MPC ECPR FOI (1550 nm) Comparison Artifact FOI (1310 nm) Fig. 4-2-1. Schematic diagram of the KRISS fiber optic power measurement facility. DFB-LD, distributed feedback laser diode; ECPR, electrically calibrated pyroelectric radiometer; MPC, motorized polarization controller; MWM, multi-wavelength meter; FOI, fiber optic isolator; TLS, tunable laser source; VOA, variable optical attenuator. Fig. 4-2-1 can be regarded as a snap shot when the fiber optic power was being measured 14 APMP.PR-S2 Fiber Optic Power Responsivity with the ECPR at 1550 nm. After the ECPR measurement, the chopper moved out of 1550 nm beam path and the fiber output end was connected to the FOPM that was a comparison artifact, after the position of the FOPM head was shifted to where the ECPR had been. Then, the radiant power was measured with the FOPM. The correction factor of the FOPM at the radiant power level of about 0.1 mW (-10 dBm) was then determined by the ratio of measured value with the ECPR to that of the FOPM and the correction factor of the ECPR as in Eq. (4-2-1), P k f ke ke e P f , (4-2-1) where kf, ke, , Pe, and Pf are the correction factor of FOPM, the correction factor of ECPR, power ratio, measured value with ECPR, and measured value with FOPM, respectively. For 1310 nm, the measurement procedure was the same but the fiber optic isolator for 1550 nm was replaced by that of 1310 nm. Fig. 4-2-2 shows the fiber optic power linearity measurement facility using a superposition method. The laser from a DFB laser diode was split into two paths by a broadband fiber optic coupler. The VOA in each path could shut the laser or change the attenuation level precisely. The two laser beams after the VOA’s were then combined into a fiber with another broadband fiber optic coupler and delivered to the fiber optic power meter. In order to remove interference effect between the two laser beams when combining, a single mode optical fiber with a length of about 20 km was inserted in one of the two paths since the line width of the DFB laser diode was known to be a few MHz. VOA-1 Broadband Coupler DFB-LD 50/50 Broadband Coupler SMF 20 km 50/50 VOA-2 1310 nm 1550 nm Detector Head Comparison Artifact Fig. 4-2-2. Schematic diagram of the KRISS fiber optic power linearity measurement facility using superposition method. DFB-LD, distributed feedback laser diode; SMF, single mode fiber; VOA, variable optical attenuator. Using this facility, a partial nonlinearity factor f defined by Eq. (4-2-2) could be measured, 15 APMP.PR-S2 Fiber Optic Power Responsivity where R is the responsivity of the artifact. D1 is the measured power when only VOA-1 is open. Likewise D2 is the measured power when only VOA-2 is open with D1 D2. Then D3 is the measured power when both VOA-1 and VOA-2 are open. The partial nonlinearity factor f can be measured every 3 dB step by changing the attenuators such that D3 can become equal to D1 in the previous step. The total nonlinearity factor F can then be calculated according to Eq. (4-23) and the correction factor at a certain level, e.g. -30 dBm, can be determined using the correction factor at -10 dBm (reference level) and the total nonlinearity factor F according to Eq. (4-2-4). If the level is not exactly the same as (-10–3j) dBm (j=0, 1, 2,), the correction factor can be assumed to be equal to that of the nearest neighboring level unless the gain range is changed. f ( 2 1 P) D3 R( P) R( P) P 1 1 1 1 1 R(2 P) R(2 P)2 P R(2 P)2 P D1 D2 F ( P 2 n Pr ) n f (2 k Pr ) k 1 R( Pr ) k f ( P ) R ( P ) k f ( Pr ) k f ( P) k f ( Pr ) F ( P ) (4-2-2) (4-2-3) (4-2-4) 4.3. Laboratory conditions The laboratory temperature was controlled to be (23 2) C and the humidity (45 15) % throughout the calibration and measurements. 4.4. Measurement procedure Before measurements, all the equipments were turned on and they were left to get stabilized at least for one hour. The detailed procedure for the calibration of the fiber optic power responsivity at -10 dBm is as follows: (1) Configure the calibration setup as shown in Fig. 4-2-1 to operate at 1310 nm. (2) Adjust the height of the detector heads of the ECPR and the artifact to be the same. (3) Set the wavelength of the artifact to 1310 nm. (4) Adjust the zero point of the ECPR and the artifact. (5) Slide the beam chopper of the ECPR to the collimated optical beam. (6) Connect the fiber end to the detector head of the ECPR. 16 APMP.PR-S2 Fiber Optic Power Responsivity (7) Set the radiant power to be -10 dBm (0.1 mW) using the variable optical attenuator. (8) Measure the radiant power with the ECPR. (9) Disconnect the fiber end from the ECPR. (10) Slide the beam chopper out from the collimated optical beam. (11) Connect the fiber end to the detector head of the artifact. (12) Measure the radiant power with the artifact. (13) Repeat the step from (5) to (12) at least four times more. (14) If the measurement is finished at 1310 nm, change the source to 1550 nm and conduct the step (3) to (13), where 1310 nm is replaced by 1550 nm. The detailed procedure for the calibration of the fiber optic power responsivity at -20 dBm and -30 dBm is as follows: (1) Configure the calibration setup as shown in Fig. 4-2-2 to operate at 1310 nm. (2) Set the wavelength of the artifact to 1310 nm. (3) Adjust the zero point of the artifact. (4) Open VOA-1 and adjust the attenuation level so that the artifact can indicate -13 dBm while VOA-2 is closed. (5) Open VOA-2 and adjust the attenuation level so that the artfact can indicate the same -13 dBm while VOA-1 is closed. (6) Record the radiant power with VOA-1 open and VOA-2 closed. (7) Record the radiant power with VOA-1 closed and VOA-2 open. (8) Record the radiant power with both VOA-1 and VOA-2 open. (9) Increase the attenuation level of VOA-1 and VOA-2 by 3 dB. (10) Repeat the step from (6) to (7) until the radiant power with either VOA open becomes less than -30 dBm. (11) Repeat the step from (4) to (10) at least four times more. (12) If the measurement is finished at 1310 nm, change the source to 1550 nm and conduct the step (2) to (11), where 1310 nm is replaced by 1550 nm. 4.5. Measurement results Table 4-5-1 summarized the measurement results using KRISS’ own fiber connector that was the fiber connector of the fiber optic isolator in Fig. 4-2-1 and the common fiber connector labeled as FC-1. 17 APMP.PR-S2 Fiber Optic Power Responsivity Table 4-5-1. Correction factor of the comparison artifact measured at KRISS. Wavelength (nm) Power level (dBm) Fiber connector Correction factor Uncertainty (Type A) 1310 1310 1310 1310 1310 1310 1550 1550 1550 1550 1550 1550 -10 -10 -20 -20 -30 -30 -10 -10 -20 -20 -30 -30 KRISS FC-1 KRISS FC-1 KRISS FC-1 KRISS FC-1 KRISS FC-2 KRISS FC-3 1.01413 1.01164 1.01292 1.01043 1.01443 1.01193 0.99736 0.99484 0.99574 0.99323 0.99701 0.99450 0.00015 0.00012 0.00008 0.00008 0.00012 0.00012 0.00018 0.00022 0.00004 0.00004 0.00011 0.00011 Relative uncertainty (Type A) (%) 0.015 0.012 0.008 0.008 0.012 0.012 0.018 0.022 0.004 0.004 0.011 0.011 The relative deviation of correction factors in case of FC-1 from that of KRISS’ own fiber connector at -10 dBm level was -0.246 % at 1310 nm and -0.252 % at 1550 nm. Note that these values were the same at different radiant power levels since we determined the correction factors at different levels through nonlinearity measurements, not through comparison with reference. The above measurements of KRISS were conducted using auto range function of the artifact and the range was always 4 (1 A) for -10 dBm, 5 (100 nA) for -20 dBm, and 6 (10 nA) for -30 dBm regardless of wavelength. 4.6. Uncertainty From Eq. (4-2-1), we can derive the uncertainty propagation equation as shown in Eq. (4-6-1) since the correction factor of ECPR ke is uncorrelated with the radiant power ratio . 2 ur2 (k f 2 2 u (k f ) u (ke ) u ( ) 2 2 ) ur (ke ) ur ( ) k k e f (4-6-1) The uncertainty of the correction factor of ECPR at the calibration wavelength (633 nm), spectral dependence of ECPR, and the uncertainty caused by chopper alignment were major sources of the uncertainty for the correction factor of ECPR when using it near IR region. The sources of uncertainty for the radiant power ratio were repeatability, temporal stability of optical source including the optical circuits, resolution of ECPR and the artifact, wavelength mismatch between the optical source and set wavelength of the artifact, and temperature 18 APMP.PR-S2 Fiber Optic Power Responsivity dependence of the artifact. The uncertainty budgets of KRISS are as shown in Table 4-6-1 and Table 4-6-2 in case of using the common fiber connector, FC-1. In case of using KRISS’ own fiber connector, only the repeatability component is slightly different. Table 4-6-1. Uncertainty budget of correction factor at 1310 nm. 1310 nm, -10 dBm Source of uncertainty Relative standard uncertainty Probability distribution Sensivity coefficient Correction factor of reference standard Correction factor at cal. wavelength 0.200 % normal Spectral dependence 0.191 % rectangular Alignment 0.0577 % rectangular Ratio of ref.std. to artifact Repeatability 0.0120 % t Source stability 0.0195 % rectangular Resolution Resolution of ref.std 0.0288 % rectangular Resolution of artifact 0.00285 % rectangular Wavelength mismatch 0.0303 % t Temperature dependence of artifact 0.231 % rectangular Relative Combined Uncertainty Relative Expanded Uncertainty (Coverage factor, k = 2; Level of confidence, approx. 95 %) Relative Standard uncertainty Degree of freedom 1 1 1 0.200 % 0.191 % 0.0577 % 1 1 0.0120 % 0.0195 % 1 1 1 1 % % % % % % 1.3E+06 3.5E+06 Relative Standard uncertainty 0.368 % Degree of freedom 0.00803 0.0693 0.374 0.75 % % % % 2.4E+07 Relative Standard uncertainty 0.368 % Degree of freedom 0.0288 0.00285 0.0303 0.231 0.368 0.74 1310 nm, -20 dBm Source of uncertainty Relative standard uncertainty 0.368 % Probability distribution Sensivity coefficient Correction factor at -10 dBm normal 1 Nonlinearity Repeatability 0.00803 % t 1 Nonlinearity factor 0.0693 % rectangular 1 Relative Combined Uncertainty Relative Expanded Uncertainty (Coverage factor, k = 2; Level of confidence, approx. 95 %) 1310 nm, -30 dBm Source of uncertainty Relative standard uncertainty 0.368 % Probability distribution Sensivity coefficient Correction factor at -10 dBm normal 1 Nonlinearity Repeatability 0.0115 % t 1 Nonlinearity factor 0.0167 % rectangular 1 Relative Combined Uncertainty Relative Expanded Uncertainty (Coverage factor, k = 2; Level of confidence, approx. 95 %) 19 0.0115 0.0167 0.368 0.74 % % % % 5.3E+06 APMP.PR-S2 Fiber Optic Power Responsivity Table 4-6-2. Uncertainty budget of correction factor at 1550 nm. 1550 nm, -10 dBm Source of uncertainty Relative standard uncertainty Probability distribution Sensivity coefficient Correction factor of reference standard Correction factor at cal. wavelength 0.200 % normal Spectral dependence 0.191 % rectangular Alignment 0.0577 % rectangular Ratio of ref.std. to artifact Repeatability 0.0225 % t Source stability 0.0415 % rectangular Resolution Resolution of ref.std 0.0288 % rectangular Resolution of artifact 0.00280 % rectangular Wavelength mismatch 0.123 % t Temperature dependence of artifact 0.231 % rectangular Relative Combined Uncertainty Relative Expanded Uncertainty (Coverage factor, k = 2; Level of confidence, approx. 95 %) Relative Standard uncertainty Degree of freedom 1 1 1 0.200 % 0.191 % 0.0577 % 1 1 0.0225 % 0.0415 % 1 1 1 1 % % % % % % 6.0E+06 3.6E+05 Relative Standard uncertainty 0.389 % Degree of freedom 0.00386 0.0938 0.400 0.80 % % % % 4.6E+08 Relative Standard uncertainty 0.389 % Degree of freedom 0.0288 0.00280 0.123 0.231 0.389 0.78 1550 nm, -20 dBm Source of uncertainty Relative standard uncertainty 0.389 % Probability distribution Sensivity coefficient Correction factor at -10 dBm normal 1 Nonlinearity Repeatability 0.00386 % t 1 Nonlinearity factor 0.0938 % rectangular 1 Relative Combined Uncertainty Relative Expanded Uncertainty (Coverage factor, k = 2; Level of confidence, approx. 95 %) 1550 nm, -30 dBm Source of uncertainty Relative standard uncertainty 0.389 % Probability distribution Sensivity coefficient Correction factor at -10 dBm normal 1 Nonlinearity Repeatability 0.0107 % t 1 Nonlinearity factor 0.0202 % rectangular 1 Relative Combined Uncertainty Relative Expanded Uncertainty (Coverage factor, k = 2; Level of confidence, approx. 95 %) 20 0.0107 0.0202 0.389 0.78 % % % % 7.0E+06 APMP.PR-S2 Fiber Optic Power Responsivity 5. Measurement Capabilities and Results of Participants 5.1. NMISA 5.1.1. Introduction This report contains NMISA’s results for comparison APMP.PR-S2 of Fibre Optic Power Responsivity. The measurements at NMISA were performed over the period 13 to 20 April 2006. 5.1.2. Reference Standards, Equipment and Experimental Set-up & Method The primary reference used for the comparison measurements was a room temperature absolute radiometer. Literature reference [1] contains some details about the absolute radiometer, and Chapter 6 of literature reference [2] contains details on the theory and determination of instrumental corrections particular to it. For fibre optic purposes the absolute radiometer is fitted with an insert with a fibre optic port, which reaches to within close proximity of the sensor cavity of the absolute radiometer. This enables feeding of radiant power via optical fibre, directly to the absolute radiometer, for absolute measurement. Therefore a fibre optic power meter requiring calibration can be calibrated by comparison to the absolute radiometer by moving the fibre between them. This is the approach that was used to calibrate the comparison transfer detector (comparison artifact). Fig. 5-1-1 shows the measurement set-up (photograph) and Fig. 5-1-2 is a simple diagrammatic representation of the set-up and measurement process. The optical sources were FP lasers, for which the wavelength can be optimised by adjusting its power. For the 1550 nm FP laser a centre wavelength within 0.1 nm of nominal could be achieved. For the 1310 nm FP laser the closest centre wavelength that could be achieved was ≈1307 nm. The laser radiation was fed to the detectors via a variable optical attenuator, which served both to set the desired power level to the detectors, and to limit back-reflections to the laser. 5.1.3. Results The results are expressed as a correction factor, as defined by the protocol, i.e. the “ratio of the optical power determined by the participating laboratory to the reading displayed by the artifact (Watt per reading in Watt)”. The results are given in Table 5-1-1. Uncertainty budget details are given in Table 5-1-2 to Table 5-1-5, and further discussion about the contributors in §5.1.4. The results are for powers 0.1 mW and 0.01 mW. No result is reported for power 0.001 mW. 21 APMP.PR-S2 Fiber Optic Power Responsivity The reason is that the measurements at 0.1 mW and 0.01 mW were done directly against our primary reference (absolute radiometer), BUT measurements for 0.001 mW not. Measurements for 0.001 mW were done via a linearity measurement approach but were found to be unsuitable for determining the correction factor at this power level. The actual centre wavelengths of the FP sources were calculated from spectral traces taken with an optical spectrum analyzer. Fig. 5-1-1. Photograph of measurement set-up for calibration of comparison artifact: (1) Absolute radiometer optical head. (2) Absolute radiometer preamplifier and bridge unit. (3) Absolute radiometer control unit. (4). ILX Lightwave FPM-8210 optical head. (5) ILX Lightwave FPM-8210 readout unit. (6) Mainframe unit containing FP laser source module and variable optical attenuator. The other three instruments at the top of the photograph are digital multimeters used with the absolute radiometer for measurement and monitoring. 22 APMP.PR-S2 Fiber Optic Power Responsivity Fig. 5-1-2. Measurement set-up and comparison of unit under calibration with absolute radiometer. 5.1.4. Uncertainties The detailed uncertainty budgets are given in Table 5-1-2 to Table 5-1-5. The following potential contributions were considered negligible or not relevant: Uncertainties: · Linearity of reference detector: Because the reference detector works on the electrical substitution principle non-linearity is negligible. · Drift of reference detector: This is implicitly contained in the ESDM. · Connector tightening effects: Owing to the design of the optical port on both our reference detector and the comparison artifact, tightening effects is negligible. The tip of the fibre is open, unconstrained. · Linearity of comparison artifact: Not relevant because the reported results apply to a specific radiant power level. · Optical fibre connector effects / Inter-reflection (detector / connector). The nature of the comparison artifact’s optical head, i.e. a sphere, causes such effects to be negligible. The following is explains the basis of the uncertainty contributions in the uncertainty budgets: · Uncertainty contributions associated with the reference detector (absolute radiometer). Lead heating effect, Substitution non-equivalence correction, Reflection correction, Uncertainty of spatial uniformity correction: The corrections had been empirically measured and the uncertainties associated with the corrections. 23 APMP.PR-S2 Fiber Optic Power Responsivity · Uncertainty contributions associated with the reference detector (absolute radiometer). Electrical power measurement: Uncertainty derived from electrical measurands. · Uncertainty contributions associated with the reference detector (absolute radiometer). Resolution: Its resolution is 0.001 uW, which translates to relative resolutions of 0.001% and 0.01% at measured radiant powers of 0.1 mW and 0.01 mW respectively. · Fibre flexing (in-fibre back-reflection/polarisation / laser feedback effects / Coherence effects): Based on a set of fibre flexing measurements by keeping the fibre connected to a photodiode and performing movements that flexes the fibre in a way equivalent to that during actual calibration measurements. · Effect of wavelength offset, wavelength uncertainty & detector relative spectral responsivity. Our reference detector has a flat response, but the comparison artifact not. The “Input quantity” in the uncertainty budget was derived as (offset) 2 ( wavelength uncertainty) 2 and the sensitivity coefficients at 1310 nm and 1550 nm was derived from the sample responsivity plot available in the instrument manual on page 22. · Temperature sensitivity of UUT responsivity. The worst case deviation from the 23°C environmental condition required by the protocol was 1.2°C and the temperature measurement uncertainty was 0.4°C, which can be combined as (1.2) 2 (0.4) 2 C 1.27 C The sensitivity coefficient was taken as the manufacturer specification for temperature coefficient, 0.2 %/°C. · ESDM of the readings: The ESDM was calculated from measurement data. 24 APMP.PR-S2 Fiber Optic Power Responsivity Table 5-1-1. Results of comparison artifact calibration. Table 5-1-2. Uncertainty budget for correction factor: Source wavelength 1310 nm, instrument range setting 4, instrument wavelength setting 1310.0 nm. The input quantities are all uncorrelated. 25 APMP.PR-S2 Fiber Optic Power Responsivity Table 5-1-3. Uncertainty budget for correction factor: Source wavelength 1310 nm, instrument range setting 5, instrument wavelength setting 1310.0 nm. The input quantities are all uncorrelated. Table 5-1-4. Uncertainty budget for correction factor: Source wavelength 1550 nm, instrument range setting 4, instrument wavelength setting 1550.0 nm. The input quantities are all uncorrelated. 26 APMP.PR-S2 Fiber Optic Power Responsivity Table 5-1-5. Uncertainty budget for correction factor: Source wavelength 1550 nm, instrument range setting 5, instrument wavelength setting 1550.0 nm. The input quantities are all uncorrelated. 5.1.5. Literature References [1] F. Hengstberger, R.E. Dressler, L.A.G. Monard, C.J. Kok, and R. Turner, “Further advances with the fully automated absolute radiometer developed at the NPRL”, Proc. of an International Meeting on Advances in Absolute Radiometry (1985), Cambridge, Massachusetts, P.V. Foukal, ed., Atmospheric and Environmental Research Inc., Cambridge, Mass., pp.34-37. [2] F. Hengstberger, ed, Absolute Radiometry – Electrically calibrated detectors of optical radiation, Academic Press (1989). 27 APMP.PR-S2 Fiber Optic Power Responsivity 5.2. CMS/ITRI 5.2.1. Description of the measurement facility and traceability in CMS/ITRI Fig. 5-2-1 illustrates the measurement system configuration of optical fiber power measurement. The system consists of laser source, fiber isolator, fiber attenuator (Anritsu ), 12 fiber coupler, and monitor detector. All fibers of system are single-mode. The fiber pigtailed laser diode (Thorlabs/LPS-SMF28-1310-FC) and DFB laser diode (NEL/NLK1556STG-BX) are used as standard laser sources. The wavelengths of sources are adjusted to 1310.46 nm and 1550.01 nm by wavemeter (Berleigh/WA-1550). The monitor detector is used to observe the stability of light source and the attenuator controls the power level. The output power of KC fiber is measured by absolute radiometer, and then measured by the artifact. Fig. 5-2-2 shows the traceability of optical fiber power measurements. Micro-current meter Fiber 12 fiber coupler Monitor Detector pigtailed Fiber Temperature isolator controller Fiber attenuator KC Fiber Absolute Fiber adaptor radiometer Laser diode/DFB laser diode Laser driver Fiber adaptor artifact Fig. 5-2-1. Optical fiber power meter measurement system configuration. 28 diode APMP.PR-S2 Fiber Optic Power Responsivity Room temperature absolute radiometer artifact Fig. 5-2-2. Traceability. 5.2.2. Calibration results The calibration results for 1310 nm and 1550 nm are shown in the following tables. The ambient temperature and relative humidity are (23.0 1.5) C and (45 10) %, respectively. Table 5-2-1. Calibration results for 1310 nm. Gain range Calibration factor (W/reading in W) Relative expanded uncertainty (%) (k=1.97) 1310 auto 1.027 1.4 FC-1 1310 auto 1.025 1.4 1.005-1.08 FC-1 1310 auto 1.020 1.4 110-120 CMS/ITRI 1310 auto 1.029 1.4 Fiber used Wavelength setting (nm) 107-120 FC-1 10.3-10.9 Meter power range (W) Table 5-2-2. Uncertainty budget for 1310 nm. Source Type Relative standard uncertainty (%) Degree of freedom Repeatability A 0.26 12 Laser power drift B 0.38 200 0.50 0.10 200 0.69 eff =466 1.4 k=1.97 Room temperature B absolute radiometer Artifact spectral B responsivity Relative combined standard uncertainty Relative expanded uncertainty 29 APMP.PR-S2 Fiber Optic Power Responsivity Table 5-2-3. Calibration results for 1550 nm. Gain range Calibration factor (W/reading in W) Relative expanded uncertainty (%) (k=1.96) 1550 auto 1.014 1.2 FC-1 1550 auto 1.010 1.2 1.1-1.2 FC-1 1550 auto 1.006 1.2 115-130 CMS/ITRI 1550 auto 1.019 1.2 Fiber used Wavelength setting (nm) 105-120 FC-1 10.8-11.5 Meter power range (W) Table 5-2-4. Uncertainty budget for 1550 nm. Source Type Relative standard uncertainty (%) Degree of freedom Repeatability A 0.12 12 Laser power drift B 0.25 200 0.50 0.10 200 0.58 eff = 3032 1.2 k=1.96 Room temperature B absolute radiometer Artifact spectral B responsivity Relative combined standard uncertainty Relative expanded uncertainty 30 APMP.PR-S2 Fiber Optic Power Responsivity 5.3. NMC-A*STAR NMC-A*STAR is a new name of national metrology institute of Singapore. It was SPRING at the time of the measurement and reporting. Therefore, the following measurement report contains the name SPRING. 5.3.1. Measurement facility The measurement was carried out by using following reference standard, intensity stabilized tunable laser sources, variable attenuator and other equipment in SPRING Singapore: a) Laboratory reference standard: InGaAs photodiode (s/n: InGaAs-05) (900-1640nm) calibrated on 5 July 2006. b) Tunable laser sources: ANDO AQ4321 tunable laser source (s/n: 10158008) (1520 nm to 1620nm) and Santec ECL-210 tunable laser source (s/n: 6010002) (1270nm to 1350nm). c) Variable attenuator: EXFO IQ-3100 variable attenuator (s/n:118320-35) d) Dual stage isolators: COPENETI isolators (p/n:IS-D-13/15-P-L-10-FC) e) Current-to-voltage converter: Vinculum E755 I-V converter (s/n:OP002) calibrated on 3 April 2006. f) Digital multimeter: Keithley 2000 DVM (s/n: 0687186) calibrated on 28 March 2006. 5.3.2. Measuring technique The artifact (the fiber optic power meter, FOPM, provided by the pilot lab) was calibrated by a SPRING’s reference standard, an InGaAs photodiode (RS-PD), under intensity-stabilized laser beams from tunable laser sources at wavelengths of 1310 nm and 1550 nm. The detector of the FOPM and the RS-PD were connected through either the fiber patch cord provided by the pilot lab or the fiber isolator of SPRING Singapore to the tunable laser source alternatively. The laser power level of -10 dBm, -20 dBm and -30 dBm were obtained from laser sources through a variable attenuator. The short-circuit photocurrents from InGaAs photodiode was measured using calibrated current-to-voltage converter and digital multimeter. The correction factor [CF()] defined as the ratio of the optical power determined by SPRING Singapore [PSPRING()] to the reading displayed by the artifact [PArtifact()] was calculated by Eq. (5-3-1). CF ( ) PSPRING ( ) PArtifact ( ) 31 (5-3-1) APMP.PR-S2 Fiber Optic Power Responsivity As the wavelength accuracy of both laser sources is better than 0.1nm, no correction was made to the measurement results for the central wavelength offsets. A schematic diagram of the measurement setup is shown in Fig. 5-3-1 as follow. Fig. 5-3-1. Schematic diagram of measurement setup in SPRING Singapore. 5.3.3. Traceability and uncertainty budget The traceability of SPRING’s fibre optic power measurement is based on our spectral responsivity scale as shown in Fig. 5-3-2. The laser wavelength measurement is traceable to the primary standard of laser wavelength maintained in SPRING Singapore. The electrical measurement is traceable to the primary standards of current and voltage maintained in SPRING Singapore. The breakdown uncertainty budget of measurement was estimated and its results are shown in the Table 5-3-2 ~ 5-3-5. 32 APMP.PR-S2 Fiber Optic Power Responsivity Fig. 5-3-2. Traceability chart for APMP.PR-S2 comparison (All uncertainty values in the chart refer to combined standard uncertainty, k=1). 5.3.4. Laboratory Conditions Temperature: (23±2) C and Relative Humidity: (60±10) %. 5.3.5. Measurement Results The measurement results of SPRING Singapore was summarized in Table 5-3-1. 33 APMP.PR-S2 Fiber Optic Power Responsivity Table 5-3-1. Calibration result of SPRING Singapore. 5.3.6. Uncertainty budgets Table 5-3-2 and 5-3-3 shows the uncertainty budget when the FC/PC output end of SPRING’s fibre isolator was used, whereas Table 5-3-4 and Table 5-3-5 shows the uncertainty budget when the FC-1 was used. 34 APMP.PR-S2 Fiber Optic Power Responsivity Table 5-3-2. Uncertainty budget for measurement at 1310nm by using SPRING’s FC/PC fibre isolator. 35 APMP.PR-S2 Fiber Optic Power Responsivity Table 5-3-3. Uncertainty budget for measurement at 1550nm by using SPRING’s FC/PC fibre isolator. 36 APMP.PR-S2 Fiber Optic Power Responsivity Table 5-3-4. Uncertainty budget for measurement at 1310nm by using given FC/PC patch cord (s/n:FC-1). 37 APMP.PR-S2 Fiber Optic Power Responsivity Table 5-3-5. Uncertainty budget for measurement at 1550nm by using given FC/PC patch cord (s/n:FC-1). 38 APMP.PR-S2 Fiber Optic Power Responsivity 5.4. NMIJ/AIST 5.4.1. NMIJ Working Standard for Optical Fiber Power: Optical Fiber Power Calorimeter As schematically illustrated in Fig. 5-4-1, the NMIJ working standard for optical fiber power, optical fiber power calorimeter, consists of the main body and a detachable adaptor for optical fiber power input. The structure of the main body is similar to the Japan’s national standard of open beam laser power [1]. We measure optical power with the calorimeter by electrothermal substitution technique under isothermal temperature control. The advantage of the electrothermal substitution is that we can translate input optical power into electrical power output, which is traceable to much more precise standards of electricity. Isothermal temperature control of the optical absorber with heater and Pertier element enables us to eliminate the fluctuation driven by convectional or radiation loss of heat on the optical absorber since the temperature of the optical absorber is kept same with the ambient temperature, therefore measurement uncertainty would be more reduced than the system without isothermal temperature control. This type of calorimeter is equipped with NiP ultra-black absorber [2]; its reflectance is less than 0.2 %. The calorimeter also has the compensative absorber [3] to eliminate the effect from ambient temperature and/or atmospheric pressure fluctuation, so that optical fiber power of less than 100 microwatt level can be determined with high accuracy. The adaptor for optical fiber power input is attached in front of the NiP absorber, which enables us to introduce the divergent beam from optical fiber. The sensitivity of the calorimeter to optical power is determined using collimated beam by comparison with the calorimeter so called H-3, which is Japan’s national standard for open beam laser power. When the calorimeter is used as a standard for calibration of detectors under test (DUT, c.f. optical power meters) for optical fiber power, we use the calibration measurement system as shown in Fig. 5-4-2. To reduce the effect of light source (LD) fluctuation, the optical fiber power is splitted and the power in one branch is monitored by photodetector such as Ge or InGaAs photodiode. Using the optical fiber power calorimeter, we can calibrate DUT directly without any transfer standards such as semiconductor photodiodes, between national standard of optical power and DUT, therefore the calibration uncertainty can be reduced. There are several uncertainty factors in the calibration measurement of DUT using the optical fiber power calorimeter as mentioned in the following section. 39 APMP.PR-S2 Fiber Optic Power Responsivity Fig. 5-4-1: The schematic illustration of the optical fiber calorimeter: (a) structure of main body, (b) detailed structure of absorber unit and block diagram of measurement system. Fig. 5-4-2: The schematic diagram of the system for calibration of DUT with the optical fiber power. 5.4.2. Uncertainty Analysis Calibration measurement uncertainty using the NMIJ optical fiber power calorimeter was evaluated for 100 uW, 1310/1550 nm. The uncertainties were evaluated in accordance with international document standards [4]. The results are described in Table 5-4-1 ~ 5-4-4. First, the calorimeter was calibrated with open beam of 1550 nm from laser diode at 1 mW using the laser power national standard, therefore there are sensitivity calibration uncertainties, including the uncertainty of the national standard and standard deviation of the measurement for the calibration; 0.068%. To measure the fiber optical power at 100 uW with the calibrated fiber calorimeter, the uncertainty arises for non-linearity of the calorimeter between 1 mW and 100 uW. The 40 APMP.PR-S2 Fiber Optic Power Responsivity nonlinearity was measured using small heater buried at the center of NiP absorber of the calorimeter, applying known power to the heater. The uncertainty to determine the non-linearity was 0.070 %. When measuring the power of 1310 nm and so on in wavelength, the wavelength dependence of NiP absorber affects the measurements. In manufacturer specification [2], the reflectance of NiP absorber is ranging between 0.1 – 0.2 % for near infra-red region. The uncertainty due to the reflectance fluctuation is calculated into 0.029 % assuming rectangular distribution. Beam incident position also causes another uncertainty because of the non-uniformity of NiP absorber. Detachable adapter would be exchanged periodically (typically once a year) for sensitivity calibration with open beam using laser power national standard H-3, therefore the position of beam center from optical fiber on NiP absorber may be fluctuated. The uniformity of sensitive area of the absorber was examined by measuring open beam power with scanning 0.5 mm x 0.5 mm area on the absorber. The result was translated into the uncertainty of 0.067 %. These uncertainties mentioned above are common to the uncertainty of open beam laser power calorimeter. There are other uncertainty factors unique for the measurement of fiber optical power, because of the divergent nature of its beam. One is the divergent incidence on the NiP absorber. Sensitivity calibration of the calorimeter is performed with collimated beam; therefore, divergent incidence from optical fiber to the absorber would cause uncertainty since the reflectance of NiP would vary with incident angle of optical power. Relation between reflectance of NiP and incident angle of optical power was measured using the setup shown in Fig. 5-4-3 (boxed). Collimated beam was introduced into integrating sphere, equipped with NiP absorber at the center of the sphere. Rotating the direction of NiP absorber surface, we measure the optical power reflected by the NiP with InGaAs photodiode. The results were shown in Fig. 5-4-3; Reflectance was normalized by the value at 0 degree (normal incidence). The reflectance goes up to 1.7 with 30 degree incidence. However, according to the measurement of beam pattern emitted from optical fiber end, as shown in Fig. 5-4-4, optical power of more than 99.99% is within +/- 10 degree direction from normal incidence, therefore the difference of the reflectance is only about 10 % between beam center and edge. Since the reflectance itself is quite small (0.1 - 0.2 %), the uncertainty driven by the angular incident of optical power is less than 0.01%. Another factor is multi-reflection between NiP absorber and the inner wall of the fiber adaptor, which also arises from the divergent incidence. If the NiP absorber shows completely diffusive reflection, the multi-reflection is negligible. However, actual NiP absorber reflects a part of incident optical power to the specular direction rather than diffusively. That causes 41 APMP.PR-S2 Fiber Optic Power Responsivity another uncertainty for the fiber optical power measurements. The uncertainty calculated with the beam pattern as shown in Fig. 5-4-4 was 0.139 %. The correction factor is -0.122 %. The uncertainty due to DC voltage meter used to measure the heater power in electrical substitution technique was 0.023 % according to the specification of manufacturer. The optical fiber power calorimeter is operated in isothermal temperature control with proportional feedback; therefore there is deviation due to the control. The uncertainty from the control was found to be 0.014 % by the experiment. Uncertainty due to temperature or wavelength dependence of the APMP artifact was determined using data about ambient temperature obtained with a calibrated thermometer and center wavelength of LD source measured with a calibrated spectrum analyzer during the comparison measurements (See table 5-4-5 – 5-4-7). Combining all of the uncertainty mentioned above and standard deviation of comparison measurements (0.014 ~ 0.017 %, n=15), the expanded uncertainty for the calibration measurement of the APMP artifact for 100 uW, 1310/1550 nm with APMP or NMIJ patch cord using the optical fiber power calorimeter was 0.49 ~ 0.52 % (k=2). Fig. 5-4-3: Relation between relative reflectance of NiP absorber and incident angle of optical power. The reflectance at normal incident (0 degree) is normalized to be unity. Boxed: schematic setup for the measurement. 42 APMP.PR-S2 Fiber Optic Power Responsivity Fig. 5-4-4: Beam profile of divergent optical power emitted from optical fiber end. Boxed: schematic setup for the measurement. 5.4.3. Low Fiber-Optic-Power (1, 10 W) Calibration With Optical Attenuation Standard By Incremental Attenuation Method Linearity of fiber-optic power meters is usually calibrated by the superposition method [5], where desired attenuations are realized by summing up many 3 dB attenuation steps. For cases where a gradual variation of linearity over a wide range is concerned, it is more convenient to use the attenuation steps larger than 3 dB ones. Therefore we used incremental attenuation method based on 10 dB steps. In this method a narrow range of calibrated linear response of a reference power meter is sufficient to perform the wide dynamic range calibration of a test meter. The measurement setup is illustrated in Fig.5-4-5. The tunable LD source operates in the 1550/1310 nm band. Two attenuators, Att.1 and Att.2, are used; Att.1 is for level shift and Att.2 for step attenuation. The output port of Att.2 is connected to one end of a fiber optical patch cord. The other end of the fiber is switched onto a reference meter (STD), or a test power meter (DUT = APMP artifact in the comparison measurement), as in the following steps. Firstly, it is connected to STD. The nominal 0 dB to 10 dB attenuation step of Att.2 is then calibrated (ACAL(1)) at power level PCAL with STD, whose linearity has been calibrated beforehand by the superposition method over a power range just wide enough to perform this calibration. Secondly, the fiber end is connected to DUT. DUT’s uncorrected readings, AD(k), for the same nominal 43 APMP.PR-S2 Fiber Optic Power Responsivity steps are recorded at a series of power levels, P(k), each level shifted from its previous level by the same amount (in dB) as the step attenuation, A(k), at P(k). Thirdly, the fiber end is switched back to STD and the attenuation step is calibrated again (ACAL(2)). Steps 1 to 3 are repeated to evaluate experimental deviations. The relationship among AD(k), A(k), and P(k) are illustrated in Fig.5-4-6. The nonlinearity of DUT, NL(n) (in dB), at power P(n) (in dBm) is given as: (5-4-1) Here, ADC(k)'s are hypothetical attenuation step readings with DUT and are calculated from recorded readings AD(k)'s by: (5-4-2) where -SDPLΔPL2 corrects for the effect that the 0 dB to 10 dB switching of Att.2 changes the polarization state of its output light by ΔPL2, which then affects the reading of DUT (AD(k)) through its sensitivity to polarization SDPL. Similarly, -SPSΔPS corrects for an error ΔPS in setting P(k), which affects AD(k) through DUT’s sensitivity SPS to power setting errors. On the other hand, A(k)'s in (5-4-1) are given by: (5-4-3) where ACAL is calibrated value of the attenuation step and is equal to (ACAL(1)+ACAL(2))/2: SAPWΔPW corrects for Att.2's power dependence; note that ΔPW here is power difference between P(k) and PCAL both expressed in W (not in dBm): SAPLΔPL1 corrects for the effect that the setting of Att.1 changes the polarization state of its output light by ΔPL1, which then affects attenuation step of Att.2 through its polarization dependence. Temperature variation, which is found to affect the values of both ADC(k) and A(k) seriously, are not corrected but its effect is treated as a random error component in AD(k). 44 APMP.PR-S2 Fiber Optic Power Responsivity Fig. 5-4-5. Measurement setup for the incremental attenuation method. Fig.5-4-6. Nonlinearity (NL) of DUT power meter. P(0) is the reference power (P(0)=100uW in the comparison measurements. 5.4.4. Uncertainties of Linearity Calibration The uncertainties of NL(n)'s in (5-4-1) are calculated as the root-sum-square of UAD(n) and n UA(n), which represent uncertainties of A k 1 DC ( k ) and n A(k ) , respectively. UAD(n) and k 1 UA(n) are obtained by accumulating uncertainty components of ADC(k) and A(k) over k as follows: 45 APMP.PR-S2 Fiber Optic Power Responsivity (5-4-4) (5-4-5) where UAD, UPS, and UDPL are uncertainties of AD(k), SPSΔPS and SDPLΔPL2 in (5-4-2), while UAC, UAPL, and U(SAPW) are uncertainties of ACAL, SAPLΔPL1 and SAPW in (5-4-3). Note that, UDPL, UAC, and U(SAPW) are independent of k and thus that uncertainties involving them cannot be calculated as the root-sum-square of corresponding uncertainties for each k-th step. The contributions of these uncertainties to NL(n) for several power levels representative of very low (pW), intermediate (nW – μW), and high (mW) powers are summarized as follows: At the lowest power, by far the largest contribution comes from UAD, i.e., experimental deviations of raw readings with DUT, which is due to the limit of S/N performance of DUT at very low powers. For intermediate to high powers the largest uncertainty component is nUAC. At the n highest power level the second largest contribution, arising from U ( S APW ) P k 1 W , also becomes significant, which indicate the importance of selecting a less power-sensitive attenuator as a function of power. For powers P(n) > -90 dBm (nW), the expanded uncertainty increases almost linearly with the difference between P(n) and P(0). The linear variation of UNL is due to the fact that nUAC in (5-4-5) is the dominant uncertainty component, as stated above. Note that UAC is the calibration uncertainty of the Att.2's attenuation step, and this calibration uncertainty arises mainly from uncertainties of temperature dependence of both Att.2 and the standard power meter, shown in Fig.5-4-5. For power levels of APMP-PR.S2 comparison (1 μW – 100 μW), main contribution to the uncertainty was arisen from UAC and UAD, while other components of the uncertainties as described above were quite less than one tenth of those two components. Therefore we considered only UAC and UAD for the uncertainty estimation. That is reasonable because the uncertainty itself of linearity measurements (~ 0.01 %) is usually less than one tenth of that of optical power responsivity calibration (~ 0.2 %). Uncertainty due to temperature or wavelength dependence of APMP artifact was determined using data about ambient temperature and center wavelength during the comparison measurements as mentioned in the section for 100 μW calibration. The uncertainty due to such environmental parameters at 1 μW was determined as 2 u because the NL between 1 μW and 100 W was calculated through the results for 10 W and 100 μW. The uncertainty budgets 46 APMP.PR-S2 Fiber Optic Power Responsivity for the linearity calibration of the APMP artifact are summarized in Table 5-4-8 – 5-4-15. Using measured non-linearity NL (dB) for each power level, that is, 1 and 10 μW and correction factors at 100 μW measured by previous experiment mentioned above, we can derive the correction factors for 1 and 10 μW. The uncertainty for determining the correction factors for 1 and 10 μW was calculated by combining the uncertainty to determine the correction factors at 100 μW and that for the linearity calibration. 5.4.5. Correction factors and its uncertainties with data for environmental parameters 5.4.5.1. 100 W Used range of APMP artifact: 4 (=1 A) for 100 W Type of LD source: ECL (External Cavity Laser) 5.4.5.2. 10 W Used range of APMP artifact: 5 (=100 nA) for 10 W Type of LD source: ECL (External Cavity Laser) 47 APMP.PR-S2 Fiber Optic Power Responsivity 5.4.5.3. 1 W Used range of APMP artifact: 6 (=10 nA) for 1 W Type of LD source: ECL (External Cavity Laser) 5.4.6. Uncertainty Budgets Table 5-4-1: Uncertainty budget for the calibration measurement of APMP artifact for optical fiber power at 100 W, 1550 nm with APMP patch cord (FC-1) using the NMIJ optical fiber calorimeter. 48 APMP.PR-S2 Fiber Optic Power Responsivity Table 5-4-2: Uncertainty budget for the calibration measurement of APMP artifact for optical fiber power at 100 W, 1550 nm with NMIJ patch cord using the NMIJ optical fiber calorimeter. Table 5-4-3: Uncertainty budget for the calibration measurement of APMP artifact for optical fiber power at 100 W, 1310 nm with APMP patch cord (FC-1) using the NMIJ optical fiber calorimeter. 49 APMP.PR-S2 Fiber Optic Power Responsivity Table 5-4-4: Uncertainty budget for the calibration measurement of APMP artifact for optical fiber power at 100 W, 1310 nm with NMIJ patch cord using the NMIJ optical fiber calorimeter. Table 5-4-5: Derivation of uncertainty for temperature dependence of APMP artifact. Table 5-4-6: Derivation of uncertainty for wavelength dependence of APMP artifact (1550nm). 50 APMP.PR-S2 Fiber Optic Power Responsivity Table 5-4-7: Derivation of uncertainty for Wavelength dependence of APMP artifact (1310nm). Table 5-4-8: Uncertainty budget for the linearity calibration of APMP artifact for optical fiber power at 10 – 100 W, 1550 nm with APMP patch cord (FC-1) using the NMIJ linearity calibration system for fiber optic power meter. 51 APMP.PR-S2 Fiber Optic Power Responsivity Table 5-4-9: Uncertainty budget for the linearity calibration of APMP artifact for optical fiber power at 1 – 100 W, 1550 nm with APMP patch cord (FC-1) using the NMIJ linearity calibration system for fiber optic power meter. Table 5-4-10: Uncertainty budget for the linearity calibration of APMP artifact for optical fiber power at 10 – 100 W, 1550 nm with NMIJ patch cord using the NMIJ linearity calibration system for fiber optic power meter. 52 APMP.PR-S2 Fiber Optic Power Responsivity Table 5-4-11: Uncertainty budget for the linearity calibration of APMP artifact for optical fiber power at 1 – 100 W, 1550 nm with NMIJ patch cord using the NMIJ linearity calibration system for fiber optic power meter. Table 5-4-12: Uncertainty budget for the linearity calibration of APMP artifact for optical fiber power at 10 – 100 W, 1310 nm with APMP patch cord (FC-1) using the NMIJ linearity calibration system for fiber optic power meter. 53 APMP.PR-S2 Fiber Optic Power Responsivity Table 5-4-13: Uncertainty budget for the linearity calibration of APMP artifact for optical fiber power at 1 – 100 W, 1310 nm with APMP patch cord (FC-1) using the NMIJ linearity calibration system for fiber optic power meter. Table 5-4-14: Uncertainty budget for the linearity calibration of APMP artifact for optical fiber power at 10 – 100 W, 1310 nm with NMIJ patch cord using the NMIJ linearity calibration system for fiber optic power meter. 54 APMP.PR-S2 Fiber Optic Power Responsivity Table 5-4-15: Uncertainty budget for the linearity calibration of APMP artifact for optical fiber power at 1 – 100 W, 1310 nm with NMIJ patch cord using the NMIJ linearity calibration system for fiber optic power meter. 5.4.7. REFERENCES [1] T. Inoue, I. Yokoshima and A. Hiraide, “Highly Sensitive Calorimeter for Microwatt-Level Laser Power Measurements,” IEEE Trans. Instrum. Meas., vol. IM-36, no. 2, pp. 623-626, Jun. 1987. [2] S. Kodama, M. Horiuchi, T. Kunii and K. Kuroda, “Ultra-Black Nickel-Phosphorus Alloy Optical Absorber,” IEEE Trans. Instrum. Meas., vol. 39, no. 1, pp. 230-232, Feb. 1990. [3] Y. Suzuki, A. Murata, M. Aragai and T. Inoue, “Calorimeter with Compensative Absorber for Measuring Microwatt Level Optical Power,” IEEE Trans. Instrum. Meas., vol. 40, no. 2, pp. 219-221, Apr. 1991. [4] “ISO, Guide to the Expression of Uncertainty in Measurement,” International Organization for Standardization, Geneva, Switzerland, 1993.” [5] I. Vayshenker, S. Yang, X. Li, and T.R. Scott, "Automated measurement of nonlinearity of optical fiber power meters," in Proc. SPIE, Vol. 2550, pp. 12-19, 1995. 55 APMP.PR-S2 Fiber Optic Power Responsivity 5.5. NMIA 5.5.1. Measurement Setup and Method 5.5.1.1. Traceability: 5.5.1.2. Working Standard Detector See NMIA APMP presentation on fibre power uncertainties from 2006 APMP TCPR workshop. 5.5.1.3. Comparison Setup 56 APMP.PR-S2 Fiber Optic Power Responsivity 5.5.1.4. Method Each source used was allowed a period of at least 1 hour to stabilise after activation before measurements commenced. The source wavelengths were measured by Yokogawa AQ6370 OSA s/n 91FC27793. The effective wavelengths of each source were determined as described in Report RN070010. The ILX Lightwave fibre optic power meter was manually set to the nearest integer value of the effective wavelength determined for each source (or the wavelength setting was recorded and later corrected to the response of the ILX at the nearest effective integer value of wavelength). The reference detector (TD3) was connected to a Keithley 486 picoammeter (s/n 0576891) which was read via IEEE from a PC. Similarly the ILX Lightwave was read via IEEE from the same PC. For each meter range and wavelength tested: 1. Radiant flux levels were adjusted to values near the limit of each range tested using the Anritsu attenuator. 2. The ILX range was selected manually. 3. NMIA laser power meter calibration software was run taking groups of 10 readings for each of the detection systems beginning with zero levels for each detector (on the fixed range to be calibrated for the ILX). 4. With the radiant flux propagating through fibre FC1, the patch cable was then transferred between the reference detector TD3 and the ILX, exposing each detector for a minimum of five sets of readings for each range tested, taking readings of the signal current produced for the reference detector and the indicated power level for the ILX. Note: For the reference detector measurements, patch cable FC1 was supported in a cork lined chemical retention clamp so that the end was between 5 and 15 mm from the surface of the reference detector and the axis of the fibre was at an angle between 2 and 8 degrees from the normal to the surface of the detector to avoid inter-reflection errors. The uncertainty in transfer from the multiple transfers performed will correspondingly contain some component of the uncertainty from spatial non-uniformity and angular responsivity variation because the fibre is aligned slightly differently each time.) Selected ranges were recalibrated on different days to check previously determined results. Uncertainty note: NMIA Uncertainties for this intercomparison are dominated by noise introduced into the 57 APMP.PR-S2 Fiber Optic Power Responsivity measurements by the NMIA Anritsu attenuator, which is not normally used for client calibrations. 5.5.2. Measurement Results The Laser Power Meter was tested to determine flux responsivity to fibre-optically propagated coherent radiation at nominal wavelengths 1310 nm and 1550 nm using a fibre optic patch cord, labelled “FC1”, terminated in a ceramic FC connector with end marked “out” to the detector. Fig. 5-5-1. Spectral Distribution of NMI nominal 1310 nm laser source. Fig. 5-5-2. Spectral Distribution of NMI nominal 1550 nm laser source. The relative spectral radiant flux distributions for the laser sources are shown in Fig. 5-5-1 and 5-5-2. Using the data presented, the effective wavelengths for the sources, based on the 58 APMP.PR-S2 Fiber Optic Power Responsivity responsivity weighting of the NMI reference InGaAs detector, were determined to be 1295.4 nm and 1539.4 nm. Using the laser sources described above, the results obtained for the responsivity of the Laser Power Meter are given in Table 5-5-1. Table 5-5-1. Results for the Radiant Power Responsivity of ILX FPM-8210 s/n 82103878 using fibre optic patch cable “FC-1”. 59 APMP.PR-S2 Fiber Optic Power Responsivity 60 APMP.PR-S2 Fiber Optic Power Responsivity 5.5.3. Uncertainty Budgets 5.5.3.1. 100 W at 1295 nm (Range 3) 61 APMP.PR-S2 Fiber Optic Power Responsivity 5.5.3.2. 100 W at 1295 nm (Range 4) 62 APMP.PR-S2 Fiber Optic Power Responsivity 5.5.3.3. 10 W at 1295 nm (Range 4) 63 APMP.PR-S2 Fiber Optic Power Responsivity 5.5.3.4. 10 W at 1295 nm (Range 5) 64 APMP.PR-S2 Fiber Optic Power Responsivity 5.5.3.5. 1 W at 1295 nm (Range 5) 65 APMP.PR-S2 Fiber Optic Power Responsivity 5.5.3.6. 1 W at 1295 nm (Range 6) 66 APMP.PR-S2 Fiber Optic Power Responsivity 5.5.3.7. 100 W at 1539 nm (Range 3) 67 APMP.PR-S2 Fiber Optic Power Responsivity 5.5.3.8. 100 W at 1539 nm (Range 4) 68 APMP.PR-S2 Fiber Optic Power Responsivity 5.5.3.9. 10 W at 1539 nm (Range 4) 69 APMP.PR-S2 Fiber Optic Power Responsivity 5.5.3.10. 10 W at 1539 nm (Range 5) 70 APMP.PR-S2 Fiber Optic Power Responsivity 5.5.3.11. 1 W at 1539 nm (Range 5) 71 APMP.PR-S2 Fiber Optic Power Responsivity 5.5.3.12. 1 W at 1539 nm (Range 6) 72 APMP.PR-S2 Fiber Optic Power Responsivity 5.6. NML-SIRIM 5.6.1. Measurement Setup This document sets out the results of NML-SIRIM, Malaysia in APMP key comparison of fiber optic power responsivity. It also describes the description of the facilities involved as shown in Fig. 5-6-1. The measurement is performed in a laboratory environmental conditions of (23 3) C and (65 5) % R.H.. The measurement system consists of the items as listed in Table 5-6-1. This calibration set-up covers the calibration of the artifact at the wavelengths of 1310 nm and 1550 nm. Model IQ 1500 Calibration Power Meter manufactured by EXFO is used as reference standard/national standard in order to carry out measurement on power meter. It has reliable performance wise towards stability and also reproducibility. The reference standard which being traceable to KRISS with absolute power reference uncertainty 0.9 % for two wavelengths 1310 nm and 1550 nm. The national reference standards are biennially calibrated at NIST until 2007. The traceability route now has been changed to KRISS. Traceability chart as shown in Fig. 5-6-2. 1310 nm DFBLD Variable Optical Attenuator 1550 nm DFBLD Artefact Artefact Head NML-SIRIM Working Standard Fig. 5-6-1. Measurement system setup. 73 APMP.PR-S2 Fiber Optic Power Responsivity Table 5-6-1. List of standards/equipment in the measurement system. Equipment Maker Model Serial # Calibration Power Meter Calibration Power Meter Variable Attenuator Splitter 1X2B WDM Laser Source WDM Laser Source EXFO EXFO EXFO EXFO EXFO EXFO IQ 1500 IQ 1500 IQ 3100 IQ 9600 IQ 2400 IQ 2400 230777 230778 232087 232786 232279 204431 5.6.2. Traceability NIST Since 2003 KRISS since 2007 Optical Power Meter at 1310 nm & 1550 nm Power Meters Fig. 5-6-2. Traceability chart. 5.6.3. Results Wavelength, Correction factor Correction factor Correction Factor Expanded nm -10dBm -20dBm -30dBm Uncertainty (%) 1310 1.0114 1.0108 1.0197 1.3 1550 1.0013 1.0018 1.0102 1.3 74 APMP.PR-S2 Fiber Optic Power Responsivity 5.6.4. Contribution towards expanded uncertainty Source of Uncertainty Value, % Reference Power Meter 0.6 Spectral responsivity 0.5 Correction Factor 0.9 Power linearity 0.05 Power uncertainty 0.3 Power flatness 0.1 Expanded Uncertainty, k=2 1.3 75 APMP.PR-S2 Fiber Optic Power Responsivity 5.7. NIM 5.7.1. Main instrument used in the measurement The Agilent 8164A lightwave measurement system is used as standard optical fiber power meter which has been traced to NIM Cryogenic Radiometer. The detailed information of the 8164A lightwave measurement system is shown in the table below: Model Description Information (Measured by NIM) 81654A LD Module Central wavelength: 1301.4 nm/1543.4 nm FWHM: 4.1 nm/5.6 nm Stability(30min): ±0.002 dB/±0.002 dB Peak wavelength uncertainty :0.1 nm 81618A Single Channel Interface/ Sensor InGaAs Power Range : (10 to -80) dBm Linearity (0dBm to -40dBm): ±0.002 dB 81566A Attenuator Attenuation Adjust Range: 0 to 60 dB 5.7.2. Traceability Fig. 5-7-1 shows the reference standard optical fiber power which is traceable to the NIM Laser Cryogenic Radiometer based on the electrical substitution method. The laboratory standard is an optical fiber power meter based on photodiode sensor. The optical fiber power meter (81618A) is applied to carry out the comparison. 5.7.3. Environmental condition The environment temperature is (21.6 ~ 23.1) ℃ and the humidity is (31 ~ 45) % in the measurement process (6 days). 76 APMP.PR-S2 Fiber Optic Power Responsivity Fig. 5-7-1. Traceability chain. 5.7.4. Results 5.7.4.1. Given FC/PC type fiber (FC-1) Wavelength set 1301nm 1543nm gain range autorange autorange gain Power Level correction factor 4 0.1mW 1.0416 4 0.01mW 1.0421 5 0.001mW 1.0409 4 0.1mW 1.0335 4 0.01mW 1.0344 5 0.001mW 1.0330 77 APMP.PR-S2 Fiber Optic Power Responsivity 5.7.4.2. Given FC/PC type fiber (FC-2) Wavelength set 1301nm 1543nm gain range autorange autorange gain Power Level correction factor 4 0.1 mW 1.0445 4 0.01 mW 1.0450 5 0.001 mW 1.0439 4 0.1 mW 1.0359 4 0.01 mW 1.0367 5 0.001 mW 1.0360 gain Power Level correction factor 4 0.1 mW 1.0442 4 0.01 mW 1.0434 5 0.001 mW 1.0433 4 0.1 mW 1.0359 4 0.01 mW 1.0368 5 0.001 mW 1.0354 5.7.4.3. NIM’s own FC/PC type fiber Wavelength set 1301nm 1543nm gain range autorange autorange 78 APMP.PR-S2 Fiber Optic Power Responsivity 5.7.5. Uncertainty Budgets Source Type Standard uncertainty (%) 0.22 Uncertainty associated with the reference standard used uncertainty associated with the source central wavelength offset B Repeatability of the measurement A 0.1 Uncertainty associated with linearity of the reference standard used Combined uncertainty Expanded uncertainty (k=2) B 0.06 Information The laser source used in the comparison is F-P type, which central wavelengths are 1301.4nm and 1543.4nm. The artifact(FPM-8240) wavelength is set to 1301nm and 1543 nm in the whole comparison process. There is no correction to central wavelength offset. It includes uncertainty associated with drift and environmental condition viration during the measurement process (6 days). 0.25 0.5 Note: For the NIM laboratory standard is an optical fiber power meter based on photodiode sensor and it directly read out the optical power, so there is no any uncertainty associated with the current measurement. 79 APMP.PR-S2 Fiber Optic Power Responsivity 5.8. NIM (Second Measurements) Since the comparison artifact was found to have large drift when it was checked by the pilot after NIM’s measurements, NIM conducted second measurements after VNIIOFI’s measurements. It was conducted two years later from the first measurements due to delivery process and customs problem in Russia. During NIM’s second measurements, significant artifact drift was observed even without transportation. Therefore, the following report contains the results before and after drift. 5.8.1. Main instrument used in the measurement The Agilent 8164A lightwave measurement system is used as reference standard optical fiber power meter which has been traced to NIM Cryogenic Radiometer. The detailed information of the 8164A lightwave measurement system is shown in the table below: Model Description Information (Measured by NIM) 81654A LD Module 81618A/81623A Single Channel Interface/ Sensor InGaAs Central wavelength: 1301.2 nm/1542.4 nm FWHM: 4.1 nm/5.6 nm Stability(30min): ±0.002 dB/±0.002 dB Central wavelength uncertainty :0.1 nm Power Range : (10 to -80) dBm Linearity (0 dBm to -40 dBm): ±0.002 dB 81566A Attenuation Adjust Range: Attenuator (0 to 60) dB 5.8.2. Traceability Fig. 5-8-1 shows the reference standard optical fiber power which is traceable to the NIM Laser Cryogenic Radiometer based on the electrical substitution method. The laboratory standard is an optical fiber power meter based on photodiode sensor. The optical fiber power meter (81618A) is applied to carry out the comparison. 5.8.3. Environmental condition of the measurements The environment temperature is (23 ~ 24) C and the humidity is (25 ~ 29) % before drift and (15 ~ 26) % after drift in the measurement process. 80 APMP.PR-S2 Fiber Optic Power Responsivity Fig. 5-8-1. Traceability chain. 5.8.4. Measurement Results 5.8.4.1. Before drift gain range FC-1 FC-2 NIM fiber autorange 100 1.0651 1.0711 1.0699 4 10 1.0644 1.0693 1.0679 5 1 1.0690 1.0735 1.0719 100 1.0575 1.0605 1.0590 4 10 1.0553 1.0592 1.0571 5 1 1.0600 1.0625 1.0604 gain 1301nm 4 1542nm Correction factor of artifact Power Level(μW) Wavelength set 4 autorange 81 APMP.PR-S2 Fiber Optic Power Responsivity 5.8.4.2. After drift gain range FC-1 FC-2 NIM fiber autorange 100 1.0764 1.0825 1.0813 4 10 1.0758 1.0807 1.0792 5 1 1.0804 1.0850 1.0833 100 1.0679 1.0709 1.0695 4 10 1.0657 1.0696 1.0676 5 1 1.0704 1.0730 1.0708 Relative standard uncertainty Degree of freedom gain 1301nm 4 1542nm Correction factor of artifact Power Level(μW) Wavelength set 4 autorange 5.8.5. Uncertainty Budgets 5.8.5.1. Before drift Source of uncertainty Correction factor of reference standard Correction factor at cal. wavelength Ratio of ref.std. to artifact Reproducibility (5 groups and 3 observers) Source stability Linearity of reference standard Relative Combined Uncertainty Relative standard uncertainty Probability distribution Sensitivity coefficient 0.32 % normal 1 0.32 % 51 0.1 % t 1 0.1 % 14 0.06 % rectangular 1 0.06 % 100 0.04 % rectangular 1 0.04 % 60 0.343 % 64 0.69 % Relative Expanded Uncertainty ( Coverage factor: k = 2) 82 APMP.PR-S2 Fiber Optic Power Responsivity 5.8.5.2. After drift Source of uncertainty Relative standard uncertainty Probability distribution Sensitivity coefficient Relative standard uncertainty Degree of freedom Correction factor of reference standard Correction factor at cal. wavelength Ratio of ref.std. to artifact Reproducibility (5 groups and 3 observers) 0.32 % normal 1 0.32 % 51 0.1 % t 1 0.1 % 14 Source stability 0.06 % rectangular 1 0.06 % 100 Linearity of reference standard 0.04 % rectangular 1 0.04 % 60 Correction factor drift 0.14 % rectangular 1 0.14 15 Relative Combined Uncertainty 0.37 % Relative Expanded Uncertainty ( Coverage factor: k = 2) 0.74 % 77 Note: NIM reference standard is an optical fiber power meter with photodiode sensor and it directly read out the optical power. There is no uncertainty component contributed by electric current measurement. 83 APMP.PR-S2 Fiber Optic Power Responsivity 5.9. VNIIOFI 5.9.1. Laboratory Standard The VNIIOFI primary standard is a compact thermal detector operating at room temperature and capable of electrical calibration. It incorporates two sensitive cavity-type absorbers (receiving and compensating) with a substitution heater for electrical calibration. Calibration is accomplished by direct substitution of electrically injected power using techniques to reduce drift in ambient conditions. A high fraction of the incident power is absorbed by the cavity with little spectral dependence. Input to the detector is achieved trough an optical-fiber connector. Reference: S.V. Tikhomirov, A.I. Glasov, M.L.Kozatchenko, V.E Kravtsov, A.B. Svetlichny, I.Vayshenker, T.R. Scott, D.I. Franzen. Comparison of reference standards for measurements of optical- fiber power. Metrologia, № 37, 2000, pp. 347-348. 5.9.2. Measurement Conditions Source: ANDO AQ2140 with AQ4213(131/155) LD UNIT, Variable attenuator EXFO FVA-60B. Patch cord: No 1. Temperature: ( 23 ± 1 ) C 5.9.3. Measurement Results Table 5-9-1. Comparison data at 1310 nm. Number 1 2 3 4 5 6 7 8 9 10 VNIIOFI standard, W 106.36 106.32 106.4 106.36 106.47 106.47 106.29 107.41 107.52 107.42 Mean value Standard deviation, % ILX, W 101.38 101.38 101.37 101.43 101.45 101.49 101.35 102.23 102.38 102.27 84 PVNIIOFI / PILX 1.04912 1.04873 1.04962 1.04860 1.04948 1.04907 1.04874 1.05067 1.05021 1.05036 1.0495 0.022 APMP.PR-S2 Fiber Optic Power Responsivity Table 5-9-2. Comparison data at 1550 nm. Number 1 2 3 4 5 6 7 8 9 10 VNIIOFI standard, W 106.07 106.14 106.14 105.92 105.42 105.56 105.60 105.74 105.34 105.45 Mean value Standard deviation, % ILX, W 103.02 102.76 102.78 102.63 102.62 102.63 102.38 102.44 102.48 102.45 PVNIIOFI / PILX 1.02959 1.03290 1.03270 1.03209 1.02724 1.02855 1.03142 1.03223 1.02793 1.02930 1.0304 0.065 5.9.4. Wavelength Correction Central wavelengths: 1308.8 nm and 1548.5 nm. Table 5-9-3. Spectral responsivity of ILX. (nm) S (%) (nm) S (%) 1290 98,66 1530 100 1300 98,81 1540 98,83 1310 99,14 1550 98,48 1320 99,72 1560 98,42 1330 100 1570 97,83 Correction factor 1310 nm: S(1308.8nm) / S(1310nm) = 0.99960 Correction factor 1550 nm: S(1548.5nm) / S(1550nm) = 1.00053 Resulting ratio 1310 nm: 1.0490 Resulting ratio 1550 nm: 1.0309 85 APMP.PR-S2 Fiber Optic Power Responsivity Table 5-9-4. Measurement uncertainties. Source Standard uncertainty Repeatability 1310 nm 1550 nm 0.022 0.065 Laser stability 0.1% - B Laser wavelength 0.05% - B ILX spectral responsivity 0.1% - B Connector 0.1% - B Temperature stability 0.1% - B Laboratory standard 0.085% - A Laboratory standard 0.06% - B -A Table 5-9-5. Comparison results. Wavelength, nm Ratio Standard deviation, % Expanded uncertainty, % 1310 1.0490 0.022 0.44 1550 1.0309 0.065 0.45 86 APMP.PR-S2 Fiber Optic Power Responsivity 6. Results and Discussions 6.1. Artifact Drift Artifact drift was checked by the pilot after the artifact was delivered to the pilot from the participating lab and before it was delivered to the next participating lab. Therefore, there were 10 data sets on the deviation of correction factor of the artifact at -10 dBm level for both 1310 nm and 1550 nm with respect to the reference detector of the pilot. Simultaneously, the working standard of the pilot (the same model as the artifact) was also checked with respect to the reference detector of the pilot in order to monitor how stably the scale was maintained at the pilot. Table 6-1-1 and 6-1-2 show the accumulative deviation of correction factors using the two different fiber connectors and they are plotted in Fig. 6-1-1 and 6-1-2. From Fig. 6-1-1, we could identify that a significant drift took place before and after NIM’s measurements in both the first and the second measurements. As it was mentioned in NIM’s second measurement results in the previous section, it also drifted during their measurements, which led to report the results twice. However, since it was delivered to the pilot, the correction factors did not change for a month or so. Table 6-1-1. Artifact drift check results using the pilot’s own fiber connector. Deviation of Correction factor of Artifact (%) Deviation of Correction factor of working standard of pilot (%) 1310 nm 1550 nm 1310 nm 1550 nm 1 0.00 0.00 0.000 2 0.08 0.12 3 0.66 4 Fiber connector Date Remark (checked after this NMI) 0.000 KRISS 2006-03-06 KRISS 0.002 0.156 KRISS 2006-04-27 NMISA 0.69 N/A N/A KRISS 2006-07-10 CMS 1.20 1.13 -0.062 0.106 KRISS 2006-09-27 NMC 5 0.62 0.51 0.027 0.027 KRISS 2006-11-30 NMIJ 6 0.67 0.64 -0.070 0.118 KRISS 2007-03-16 NMIA 7 0.59 0.56 -0.091 -0.039 KRISS 2007-07-09 NML 8 2.80 2.49 0.351 0.424 KRISS 2008-01-15 NIM 9 3.42 2.35 0.510 0.568 KRISS 2009-10-07 VNIIOFI 10 4.73 4.21 0.495 0.383 KRISS 2011-01-04 NIM 87 APMP.PR-S2 Fiber Optic Power Responsivity Table 6-1-2. Artifact drift check results using the fiber connector labeled as FC-1. Deviation of Correction factor of Artifact (%) Fiber connector Date Remark (checked after this NMI) 1310 nm 1550 nm 1 0.00 0.00 FC-1 2006-03-06 KRISS 2 0.01 0.03 FC-1 2006-04-27 NMISA 3 0.63 0.59 FC-1 2006-07-10 CMS 4 1.15 1.13 FC-1 2006-09-27 NMC 5 0.61 0.55 FC-1 2006-11-30 NMIJ 6 0.70 0.67 FC-1 2007-03-16 NMIA 7 0.75 0.72 FC-1 2007-07-09 NML 8 2.76 2.44 FC-1 2008-01-15 NIM 9 3.36 2.76 FC-1 2009-10-07 VNIIOFI 10 4.79 4.20 FC-1 2011-01-04 NIM Although the reason of the drift was not visible because the optical head was an integrating sphere with its detector firmly fixed as shown in Fig. 3-1 and 3-2, it is clear that something happened during the transportation to NIM or from NIM. It is also clear that the spectral responsivity of the artifact was also changed after VNIIOFI although the drift in each wavelength was not as significant as the one after NIM. The correction factors of the working standard of the pilot did not show deviation beyond the expanded uncertainty of the pilot in Fig. 6-1-1, which was a good evidence of stable maintenance of the scale. From Fig. 6-1-2, the effect of fiber connector difference was negligible at the pilot. 88 APMP.PR-S2 Fiber Optic Power Responsivity Fig. 6-1-1. Accumulative deviation of correction factors of artifact and working standard of KRISS using KRISS fiber connector. Fig. 6-1-2. Accumulative deviation of correction factors of artifact for the two different fiber connectors. 89 APMP.PR-S2 Fiber Optic Power Responsivity 6.2. Difference from Pilot To calculate the difference of measured correction factors between each participant (index i) and the pilot (index p), the two values of the pilot, before (p1) participant and after (p2) participant, was averaged by C ip Cip1 Cip 2 , 2 (6-2-1) for two different wavelengths and three different power levels. Since the two values of the pilot were measured only at -10 dBm level for both 1310 nm and 1550 nm, we applied the same deviation between the two values at -10 dBm to the values at -20 dBm and -30 dBm as well. The relative standard uncertainty of the averaged value Cip is then given by u r (Cip ) u 2 p r ,co 1 p1 2 1 p 2 ur ,un u r ,un 4 4 2 , (6-2-2) 2 where u rp,co , u rp,1un , and u rp,un are relative standard uncertainties of the correlated components (scale uncertainty), uncorrelated components (transfer uncertainty) of measurements before participant, and uncorrelated components of measurements after participant, respectively. Since the uncorrelated components are much smaller than overall combined standard uncertainty of the pilot from Table 4-6-1 and 4-6-2, we used the following assumption. u r (Cip ) u r (Cip1 ) u r (Cip 2 ) (6-2-3) The relative difference i of correction factors between the participant i and the pilot is then calculated by i Ci 1 Cip (6-2-4) and its uncertainty u ( i ) by u ( i ) u r2 (Ci ) 1 p1 u r ,un 4 2 1 p2 u r ,un 4 2 u r2,ad (Ci ) (6-2-5) where ur ,ad (Ci ) denotes the additional uncertainty of the correction factor by the participant i due to non-ideal characteristics of the artifact. We used the drift of the artifact for the corresponding participant as the value of ur ,ad (Ci ) that can be calculated by Eq. (6-2-6). u r ,ad (Ci ) C ip 2 1 Cip1 (6-2-6) Again, we ignored the uncorrelated components of the pilot in Eq. (6-2-5) because they were 90 APMP.PR-S2 Fiber Optic Power Responsivity negligible for all participants. For the pilot lab (i=0), 0 0 and the uncertainty u ( 0 ) is calculated by u ( 0 ) 1 N N u i 1 r (Cip ) , (6-2-7) which is the average total relative uncertainty of all measurements at the pilot lab. Since the pilot did not evaluate the uncertainty every time that the drift was checked, the reported uncertainty of the pilot was used for all measurements, which means u ( 0 ) ur (C pilot ) . The calculated results are summarized in Table 6-2-1 ~ 6-2-6 and Fig. 6-2-1 ~ 6-2-3. Please note that we only used the data measured using the fiber connector labeled as FC-1 in calculation. Later, we discussed about the effect of fiber connector. Table 6-2-1. Difference from Pilot (1310 nm, -10 dBm). Participant Ci Cip ur (Ci ) ur ,ad (Ci ) i u ( i ) KRISS NMISA CMS/ITRI NMC-A*STAR NMIJ/AIST NMIA NML-SIRIM NIM VNIIOFI NIM(2) 1.0116 1.016 1.027 1.0309 1.0287 1.0278 1.0114 1.0416 1.0490 1.0651 1.0116 1.0117 1.0149 1.0206 1.0205 1.0183 1.0190 1.0294 1.0426 1.0529 0.00368 0.00315 0.00690 0.00820 0.00247 0.00368 0.00650 0.00250 0.00220 0.00343 0 0.000125 0.006180 0.005116 0.005253 0.000880 0.000456 0.019996 0.005817 0.013861 0.0000 0.0042 0.0119 0.0101 0.0080 0.0093 -0.0074 0.012 0.0061 0.012 0.0037 0.0032 0.0093 0.0097 0.0058 0.0038 0.0065 0.0202 0.0062 0.014 Table 6-2-2. Difference from Pilot (1310 nm, -20 dBm). Participant Ci Cip ur (Ci ) ur ,ad (Ci ) i u ( i ) KRISS NMISA CMS/ITRI NMC-A*STAR NMIJ/AIST NMIA NML-SIRIM NIM NIM(2) 1.0104 1.016 1.025 1.0307 1.0279 1.0259 1.0108 1.0421 1.0651 1.0104 1.0105 1.0137 1.0194 1.0193 1.0171 1.0178 1.0282 1.0516 0.00374 0.00550 0.00690 0.00820 0.00307 0.00317 0.00650 0.00250 0.00343 0 0.000125 0.006180 0.005116 0.005253 0.000880 0.000456 0.019996 0.013861 0.0000 0.0055 0.0112 0.0111 0.0085 0.0087 -0.0068 0.014 0.012 0.0037 0.0055 0.0093 0.0097 0.0061 0.0033 0.0065 0.020 0.014 91 APMP.PR-S2 Fiber Optic Power Responsivity Table 6-2-3. Difference from Pilot (1310 nm, -30 dBm). Participant Ci Cip ur (Ci ) ur ,ad (Ci ) i u ( i ) KRISS CMS/ITRI NMC-A*STAR NMIJ/AIST NMIA NML-SIRIM NIM NIM(2) 1.0119 1.020 1.0301 1.0298 1.0282 1.0197 1.0409 1.0690 1.0119 1.0152 1.0209 1.0208 1.0186 1.0193 1.0297 1.0532 0.00368 0.00690 0.00820 0.00356 0.00323 0.00650 0.00250 0.00343 0 0.006180 0.005116 0.005253 0.000880 0.000456 0.019996 0.013861 0.0000 0.0047 0.0090 0.0088 0.0094 0.0004 0.011 0.015 0.0037 0.0093 0.0097 0.0063 0.0033 0.0065 0.020 0.014 Table 6-2-4. Difference from Pilot (1550 nm, -10 dBm). Participant Ci Cip ur (Ci ) ur ,ad (Ci ) i u ( i ) KRISS NMISA CMS/ITRI NMC-A*STAR NMIJ/AIST NMIA NML-SIRIM NIM VNIIOFI NIM(2) 0.9948 1.002 1.014 1.0199 1.0148 1.0240 1.0013 1.0335 1.0309 1.0575 0.9948 0.9950 0.9979 1.0034 1.0032 1.0009 1.0018 1.0106 1.0207 1.0295 0.00389 0.00415 0.00580 0.00820 0.00258 0.00552 0.00650 0.00250 0.00225 0.00343 0 0.000347 0.005544 0.005380 0.005715 0.001189 0.000512 0.017045 0.003116 0.014005 0.0000 0.0070 0.0161 0.0164 0.0115 0.0230 -0.0005 0.023 0.0100 0.027 0.0039 0.0042 0.0080 0.0098 0.0063 0.0056 0.0065 0.017 0.0038 0.014 Table 6-2-5. Difference from Pilot (1550 nm, -20 dBm). Participant Ci Cip ur (Ci ) ur ,ad (Ci ) i u ( i ) KRISS NMISA CMS/ITRI NMC-A*STAR NMIJ/AIST NMIA NML-SIRIM NIM NIM(2) 0.9932 1.005 1.010 1.0196 1.0140 1.0245 1.0018 1.0344 1.0553 0.9932 0.9934 0.9963 1.0018 1.0016 0.9993 1.0002 1.0089 1.0278 0.00400 0.00700 0.00580 0.00820 0.00314 0.00445 0.00650 0.00250 0.00343 0 0.000347 0.005544 0.005380 0.005715 0.001189 0.000512 0.017045 0.014005 0.0000 0.0117 0.0137 0.0178 0.0124 0.0252 0.0016 0.025 0.027 0.0040 0.0070 0.0080 0.0098 0.0065 0.0046 0.0065 0.017 0.014 Table 6-2-6. Difference from Pilot (1550 nm, -30 dBm). Participant Ci Cip ur (Ci ) ur ,ad (Ci ) i u ( i ) KRISS CMS/ITRI NMC-A*STAR NMIJ/AIST NMIA NML-SIRIM NIM NIM(2) 0.9945 1.006 1.0186 1.0158 1.0290 1.0102 1.0330 1.0600 0.9945 0.9976 1.0030 1.0029 1.0006 1.0014 1.0102 1.0291 0.00389 0.00580 0.00820 0.00361 0.00747 0.00650 0.00250 0.00343 0 0.005544 0.005380 0.005715 0.001189 0.000512 0.017045 0.014005 0.0000 0.0084 0.0155 0.0129 0.0284 0.0088 0.023 0.030 0.0039 0.0080 0.0098 0.0068 0.0076 0.0065 0.017 0.014 92 APMP.PR-S2 Fiber Optic Power Responsivity 0.05 0.06 1310 nm, -10 dBm Difference from pilot Difference from pilot 0.06 0.04 0.03 0.02 0.01 0.00 -0.01 0.04 0.03 0.02 0.01 0.00 -0.01 -0.02 N N KR IS S M IS A C M S N M C N M IJ N M IA N M L N VN IM IIO N FI IM (2 ) KR IS S M IS A C M S N M C N M IJ N M IA N M L N I M VN IIO N FI IM (2 ) -0.02 1550 nm, -10 dBm 0.05 Fig. 6-2-1. Difference of correction factors of participants from the pilot at -10 dBm. 0.05 0.06 1310 nm, -20 dBm Difference from pilot Difference from pilot 0.06 0.04 0.03 0.02 0.01 0.00 -0.01 1550 nm, -20 dBm 0.04 0.03 0.02 0.01 0.00 -0.01 -0.02 N N KR IS S M IS A C M S N M C N M IJ N M IA N M L N I M VN IIO N FI IM (2 ) KR IS S M IS A C M S N M C N M IJ N M IA N M L N VN IM IIO N FI IM (2 ) -0.02 0.05 Fig. 6-2-2. Difference of correction factors of participants from the pilot at -20 dBm. 0.06 1310 nm, -30 dBm Difference from pilot 0.05 0.04 0.03 0.02 0.01 0.00 -0.01 0.05 1550 nm, -30 dBm 0.04 0.03 0.02 0.01 0.00 -0.01 -0.02 KR IS S M IS A C M S N M C N M IJ N M IA N M L N VN IM IIO N FI IM (2 ) KR IS S M IS A C M S N M C N M IJ N M IA N M L N I M VN IIO N FI IM (2 ) -0.02 N N Difference from pilot 0.06 Fig. 6-2-3. Difference of correction factors of participants from the pilot at -30 dBm. 93 APMP.PR-S2 Fiber Optic Power Responsivity 6.3. Comparison Reference Value In calculation of comparison reference value, that is SCRV (supplementary comparison reference value), we chose NIM’s second result only because the artifact drift was less in the second measurement than the first one as shown in Fig. 6-1-2 (FC-1). At first, the cut-off value of the uncertainty is determined by u cut off averageu r Ci for u r Ci medianu r Ci (i 0 to N ) , (6-3-1) where N is the number of participants excluding the pilot. Then the reported uncertainty of each NMI is adjusted by the cu-off as u r ,adj (Ci ) u r Ci u r ,adj (Ci ) u cut off u r Ci u cut off for u r Ci u cut off (i 0 to N ) . (6-3-2) The uncertainty of the relative difference i after cut-off is also adjusted by u adj ( i ) u r2,adj (Ci ) uT2 ( i ) (6-3-3) where the transfer uncertainty component, uT ( i ) in u ( i ) is separated by uT ( i ) u 2 ( i ) u r2 (Ci ) . (6-3-4) The weights wi is then calculated by N 2 2 wi u adj ( i ) / u adj ( j ) . (6-3-5) j 0 Now the SCRV, SCRV is determined by N SCRV wi i , (6-3-6) i 0 and the uncertainty of the SCRV is given by u 2 ( i ) u SCRV 4 i 0 u adj ( i ) N N u i 0 2 adj ( i ) , (6-3-7) and the expanded uncertainty of the SCRV is U ( SCRV ) ku ( SCRV ) (k=2). The calculated values are summarized in Table 6-3-1 ~ 6-3-6 based on the summarized results in Table 6-2-1 ~ 6-2-6. 94 APMP.PR-S2 Fiber Optic Power Responsivity Table 6-3-1. SCRV and its uncertainty (1310 nm, -10 dBm). u cut off =0.00310. Participant i u ( i ) u r ,adj (Ci ) u adj ( i ) wi KRISS 0.0000 0.0037 0.00368 0.0037 0.2140 NMISA 0.0042 0.0032 0.00315 0.0032 0.2916 CMS 0.0119 0.0093 0.00690 0.0093 0.0338 NMC 0.0101 0.0097 0.00820 0.0097 0.0310 NMIJ 0.0080 0.0058 0.00310 0.0061 0.0779 NMIA 0.0093 0.0038 0.00368 0.0038 0.2025 NML -0.0074 0.0065 0.00650 0.0065 0.0683 NIM 0.0116 0.0143 0.00343 0.0143 0.0142 VNIIOFI 0.0061 0.0062 0.00310 0.0066 0.0667 SCRV U ( SCRV ) 0.0045 0.0034 Table 6-3-2. SCRV and its uncertainty (1310 nm, -20 dBm). u cut off =0.00335. Participant i u ( i ) u r ,adj (Ci ) u adj ( i ) wi KRISS 0.0000 0.0037 0.00374 0.0037 0.2706 NMISA 0.0055 0.0055 0.00550 0.0055 0.1250 CMS 0.0112 0.0093 0.00690 0.0093 0.0441 NMC 0.0111 0.0097 0.00820 0.0097 0.0405 NMIJ 0.0085 0.0061 0.00335 0.0062 0.0975 NMIA 0.0087 0.0033 0.00335 0.0035 0.3150 NML -0.0068 0.0065 0.00650 0.0065 0.0891 NIM 0.0122 0.0145 0.00343 0.0145 0.0181 SCRV U ( SCRV ) 0.0048 0.0038 Table 6-3-3. SCRV and its uncertainty (1310 nm, -30 dBm). u cut off =0.00348. Participant i u ( i ) u r ,adj (Ci ) u adj ( i ) wi KRISS 0.0000 0.0037 0.00368 0.0037 0.3249 CMS 0.0047 0.0093 0.00690 0.0093 0.0513 NMC 0.0090 0.0097 0.00820 0.0097 0.0471 NMIJ 0.0088 0.0063 0.00356 0.0063 0.1093 NMIA 0.0094 0.0033 0.00348 0.0036 0.3424 NML 0.0004 0.0065 0.00650 0.0065 0.1036 NIM 0.0150 0.0143 0.00348 0.0143 0.0215 95 SCRV U ( SCRV ) 0.0052 0.0041 APMP.PR-S2 Fiber Optic Power Responsivity Table 6-3-4. SCRV and its uncertainty (1550 nm, -10 dBm). u cut off =0.00326. Participant i u ( i ) u r ,adj (Ci ) u adj ( i ) wi KRISS 0.0000 0.0039 0.00389 0.0039 0.2346 NMISA 0.0070 0.0042 0.00415 0.0042 0.2047 CMS 0.0161 0.0080 0.00580 0.0080 0.0552 NMC 0.0164 0.0098 0.00820 0.0098 0.0369 NMIJ 0.0115 0.0063 0.00326 0.0066 0.0820 NMIA 0.0230 0.0056 0.00552 0.0056 0.1114 NML -0.0005 0.0065 0.00650 0.0065 0.0835 NIM 0.0272 0.0144 0.00343 0.0144 0.0171 VNIIOFI 0.0100 0.0038 0.00326 0.0045 0.1746 SCRV U ( SCRV ) 0.0086 0.0037 Table 6-3-5. SCRV and its uncertainty (1550 nm, -20 dBm). u cut off =0.00376. Participant i u ( i ) u r ,adj (Ci ) u adj ( i ) wi KRISS 0.0000 0.0040 0.00400 0.0040 0.3040 NMISA 0.0117 0.0070 0.00700 0.0070 0.0990 CMS 0.0137 0.0080 0.00580 0.0080 0.0756 NMC 0.0178 0.0098 0.00820 0.0098 0.0506 NMIJ 0.0124 0.0065 0.00376 0.0068 0.1040 NMIA 0.0252 0.0046 0.00445 0.0046 0.2293 NML 0.0016 0.0065 0.00650 0.0065 0.1144 NIM 0.0268 0.0144 0.00376 0.0145 0.0231 SCRV U ( SCRV ) 0.0110 0.0044 Table 6-3-6. SCRV and its uncertainty (1550 nm, -30 dBm). u cut off =0.00418. Participant i u ( i ) u r ,adj (Ci ) u adj ( i ) wi KRISS 0.0000 0.0039 0.00418 0.0042 0.3844 CMS 0.0084 0.0080 0.00580 0.0080 0.1045 NMC 0.0155 0.0098 0.00820 0.0098 0.0699 NMIJ 0.0129 0.0068 0.00418 0.0071 0.1341 NMIA 0.0284 0.0076 0.00747 0.0076 0.1175 NML 0.0088 0.0065 0.00650 0.0065 0.1582 NIM 0.0300 0.0144 0.00418 0.0146 0.0315 96 SCRV U ( SCRV ) 0.0094 0.0050 APMP.PR-S2 Fiber Optic Power Responsivity 2 When the Chi-square value obs is calculated for consistency check using Eq. (6-3-8) where i=0 represents the pilot lab, N i RV 2 i 0 2 u adj ( i ) 2 obs , (6-3-8) the values are as shown in Table 6-3-7. Table 6-3-7. Calculated Chi-square values. Wavelength (nm) 1310 1550 Power level (dBm) -10 -20 -30 -10 -20 -30 (= N 1 ) 2 obs 2 0.05 ( ) 7 6 5 7 6 5 8.105 7.604 4.880 16.995 20.964 14.012 14.067 12.592 11.070 14.067 12.592 11.070 2 2 0.05 For the comparison results at 1310 nm, the consistency is satisfied because obs ( ) for all power levels. However, the consistency fails for the comparison results at 1550 nm because 2 2 obs 0.05 ( ) . Therefore, we attempted to make the consistency satisfied in the case of 1550 nm by adding s 2 term in Eq. (6-3-3) following the Mandel-Paule method as u adj ( i ) u r2,adj (Ci ) uT2 ( i ) s 2 (6-3-9) 2 2 0.05 ( ) . and iteratively increase s from zero until obs The new SCRV and its uncertainty in the case of 1550 nm are summarized in Table 6-3-8 ~ 63-10 based on the new calculated u adj ( i ) . When we compare Table 6-3-4 ~ 6-3-6 and Table 63-8 ~ 6-3-10, we can notice that the SCRV increased by 5.1 %, 5.2 %, and 11.4 % for -10 dBm, -20 dBm, and -30 dBm, respectively, with the uncertainty of SCRV almost unchanged. 97 APMP.PR-S2 Fiber Optic Power Responsivity Table 6-3-8. SCRV and its uncertainty (1550 nm, -10 dBm). u cut off =0.00326. 2 s 0.00244, obs 14.067 Participant i u ( i ) u r ,adj (Ci ) u adj ( i ) wi KRISS 0.0000 0.0039 0.00389 0.0046 0.2113 NMISA 0.0070 0.0042 0.00415 0.0048 0.1913 CMS 0.0161 0.0080 0.00580 0.0084 0.0633 NMC 0.0164 0.0098 0.00820 0.0101 0.0436 NMIJ 0.0115 0.0063 0.00326 0.0070 0.0905 NMIA 0.0230 0.0056 0.00552 0.0061 0.1177 NML -0.0005 0.0065 0.00650 0.0070 0.0919 NIM 0.0272 0.0144 0.00343 0.0146 0.0208 VNIIOFI 0.0100 0.0038 0.00326 0.0051 0.1695 SCRV U ( SCRV ) 0.0091 0.0037 Table 6-3-9. SCRV and its uncertainty (1550 nm, -20 dBm). u cut off =0.00376. 2 s 0.00388, obs 12.592 Participant i u ( i ) u r ,adj (Ci ) u adj ( i ) wi KRISS 0.0000 0.0040 0.00400 0.0056 0.2387 NMISA 0.0117 0.0070 0.00700 0.0080 0.1155 CMS 0.0137 0.0080 0.00580 0.0089 0.0933 NMC 0.0178 0.0098 0.00820 0.0105 0.0666 NMIJ 0.0124 0.0065 0.00376 0.0079 0.1199 NMIA 0.0252 0.0046 0.00445 0.0060 0.2043 NML 0.0016 0.0065 0.00650 0.0076 0.1288 NIM 0.0268 0.0144 0.00376 0.0150 0.0329 SCRV U ( SCRV ) 0.0115 0.0045 Table 6-3-10. SCRV and its uncertainty (1550 nm, -30 dBm). u cut off =0.00418. 2 s 0.00307, obs 11.070 Participant i u ( i ) u r ,adj (Ci ) u adj ( i ) wi KRISS 0.0000 0.0039 0.00418 0.0052 0.3212 CMS 0.0084 0.0080 0.00580 0.0086 0.1171 NMC 0.0155 0.0098 0.00820 0.0103 0.0818 NMIJ 0.0129 0.0068 0.00418 0.0077 0.1451 NMIA 0.0284 0.0076 0.00747 0.0082 0.1297 NML 0.0088 0.0065 0.00650 0.0072 0.1664 NIM 0.0300 0.0144 0.00418 0.0149 0.0387 98 SCRV U ( SCRV ) 0.0104 0.0051 APMP.PR-S2 Fiber Optic Power Responsivity 6.4. Degree of Equivalence The unilateral degree of equivalence (DoE) of the participant i is definded by Di i SCRV , (6-4-1) and the uncertainty of DoE is given by u 2 ( ) u i u 2 ( i ) u 2 ( SCRV ) 2 2 i u adj ( i ) N u j 0 2 adj ( i ) , (6-4-2) and U i kui (6-4-3) with the coverage factor k=2 at the level of confidence of approximately 95 %. Table 6-4-1 and 6-4-2 summarize the calculation results and they are plotted in Fig. 6-4-1 and 6-4-6. Table 6-4-1. Unilateral degree of equivalence and its uncertainty of each participant at 1310 nm. Participant KRISS NMISA CMS NMC NMIJ NMIA NML NIM VNIIOFI 1310 nm, -10 dBm Di (%) Ui (%) -0.45 0.65 -0.03 0.53 0.74 1.8 0.55 1.9 0.35 1.1 0.48 0.67 -1.2 1.3 0.71 2.8 0.16 1.2 1310 nm, -20 dBm Di (%) Ui (%) -0.48 0.63 0.07 1.0 0.64 1.8 0.63 1.9 0.37 1.2 0.39 0.55 -1.2 1.2 0.74 2.9 1310 nm, -30 dBm Di (%) Ui (%) -0.52 0.60 -0.05 0.38 0.36 0.42 -0.48 0.98 1.8 1.9 1.2 0.56 1.2 2.8 Table 6-4-2. Unilateral degree of equivalence and its uncertainty of each participant at 1550 nm. Participant KRISS NMISA CMS NMC NMIJ NMIA NML NIM VNIIOFI 1550 nm, -10 dBm Di (%) Ui (%) -0.91 0.70 -0.20 0.75 0.70 1.5 0.74 1.9 0.25 1.2 1.4 1.1 -0.95 1.2 1.8 2.9 0.093 0.73 1550 nm, -20 dBm Di (%) Ui (%) -1.2 0.73 0.013 1.3 0.22 1.5 0.63 1.9 0.084 1.2 1.4 0.84 -0.99 1.2 1.5 2.8 99 1550 nm, -30 dBm Di (%) Ui (%) -1.0 0.69 -0.20 0.51 0.25 1.8 -0.17 2.0 1.5 1.9 1.2 1.4 1.2 2.8 APMP.PR-S2 Fiber Optic Power Responsivity 4.0% 1310 nm, -10 dBm 3.0% Unilateral DoE 2.0% 1.0% 0.0% -1.0% -2.0% -3.0% KRISS NMISA CMS NMC NMIJ NMIA NML NIM VNIIOFI Participant Fig. 6-4-1. Unilateral degree of equivalence and its uncertainty of each participant (1310 nm, 10 dBm). Red dotted lines indicate the uncertainty boundaries of SCRV. 4.0% 1310 nm, -20 dBm 3.0% Unilateral DoE 2.0% 1.0% 0.0% -1.0% -2.0% -3.0% KRISS NMISA CMS NMC NMIJ NMIA NML NIM VNIIOFI Participant Fig. 6-4-2. Unilateral degree of equivalence and its uncertainty of each participant (1310 nm, 20 dBm). Red dotted lines indicate the uncertainty boundaries of SCRV. 100 APMP.PR-S2 Fiber Optic Power Responsivity 5.0% 1310 nm, -30 dBm 4.0% Unilateral DoE 3.0% 2.0% 1.0% 0.0% -1.0% -2.0% -3.0% KRISS NMISA CMS NMC NMIJ NMIA NML NIM VNIIOFI Participant Fig. 6-4-3. Unilateral degree of equivalence and its uncertainty of each participant (1310 nm, 30 dBm). Red dotted lines indicate the uncertainty boundaries of SCRV. 6.0% 5.0% 1550 nm, -10 dBm Unilateral DoE 4.0% 3.0% 2.0% 1.0% 0.0% -1.0% -2.0% -3.0% KRISS NMISA CMS NMC NMIJ NMIA NML NIM VNIIOFI Participant Fig. 6-4-4. Unilateral degree of equivalence and its uncertainty of each participant (1550 nm, 10 dBm). Red dotted lines indicate the uncertainty boundaries of SCRV. 101 APMP.PR-S2 Fiber Optic Power Responsivity 5.0% 4.0% 1550 nm, -20 dBm Unilateral DoE 3.0% 2.0% 1.0% 0.0% -1.0% -2.0% -3.0% KRISS NMISA CMS NMC NMIJ NMIA NML NIM VNIIOFI Participant Fig. 6-4-5. Unilateral degree of equivalence and its uncertainty of each participant (1550 nm, 20 dBm). Red dotted lines indicate the uncertainty boundaries of SCRV. 6.0% 5.0% 1550 nm, -30 dBm Unilateral DoE 4.0% 3.0% 2.0% 1.0% 0.0% -1.0% -2.0% -3.0% KRISS NMISA CMS NMC NMIJ NMIA NML NIM VNIIOFI Participant Fig. 6-4-6. Unilateral degree of equivalence and its uncertainty of each participant (1550 nm, 30 dBm). Red dotted lines indicate the uncertainty boundaries of SCRV. 102 APMP.PR-S2 Fiber Optic Power Responsivity 6.5. Discussions 6.5.1. Range discontinuity When we collected the reported values to make Table 6-2-1 ~ 6-2-6, we tried to compare the values with the same gain range of the artifact at each optical power levels. However, there were the cases that this was not so available. Table 6-5-1 shows the gain range of the artifact used by each participant when it measured the values reported at different optical power levels for both wavelengths. Table 6-5-1. Gain range of the artifact reported by each participant. Participant Range at -10 dBm Range at -20 dBm Range at -30 dBm KRISS 4 5 6 NMISA 4 5 N/A CMS/ITRI 3 or 4 (not specified) 4 or 5 (not specified) 5 or 6 (not specified) NMC-A*STAR 3 4 5 NMIJ/AIST 4 5 6 NMIA 4 5 6 NML-SIRIM 3 or 4 (not specified) 4 or 5 (not specified) 5 or 6 (not specified) NIM 4 4 5 VNIIOFI 4 N/A N/A When the pilot measured the same stable optical power with the two different ranges of the artifact, the displayed values show deviations of less than 0.2 % at all optical power levels and wavelengths. It agrees with the values reported by NMIA, where they reported two correction factors with different range at each optical power level for each wavelength. Therefore, we can conclude that the range discontinuity did not significantly affect SCRV’s and the unilateral DoE’s. 6.5.2. Effect of fiber optic connector Six participants reported their correction factors measured with their own fiber connector as well as FC-1. Note that FC-2 was prepared as a backup in case of damage of FC-1, but the quality of FC-1 was sustained until the end of measurements so we did not include the case of FC-2 here. The relative deviation of correction factor in case of FC-1 from that of NMI’s own 103 APMP.PR-S2 Fiber Optic Power Responsivity fiber connector for each participant at each optical power level and wavelength was summarized in Table 6-5-2. The maximum deviation was -0.49 % but it was well within 0.3 % for most cases as shown in the table. Consequently, the effect of using different fiber connectors is well under the uncertainty of fiber optic power meter calibration for all participants. Table 6-5-2. Relative deviation of correction factor in the case of FC-1 from that of NMI’s own fiber connector. Relative deviation of correction factor (%): Participant Ci ,FC-1 / Ci ,own 1 1310 nm -10 dBm 1310 nm -20 dBm 1310 nm -30 dBm 1550 nm -10 dBm 1550 nm -20 dBm 1550 nm -30 dBm KRISS -0.25 -0.25 -0.25 -0.25 -0.25 -0.25 CMS -0.19 N/A N/A -0.49 N/A N/A NMC -0.19 -0.16 -0.16 0.05 0.15 0.08 NMIJ -0.18 -0.17 -0.16 -0.12 -0.12 -0.12 NIM-1st -0.25 -0.12 -0.23 -0.23 -0.23 -0.23 NIM-2nd -0.45 -0.33 -0.27 -0.14 -0.17 -0.04 104 APMP.PR-S2 Fiber Optic Power Responsivity 7. Conclusions We have reported the results of the supplementary comparison of APMP TCPR on fiber optic power responsivity at optical power levels of -10 dBm, -20 dBm, and -30 dBm and at wavelengths of 1310 nm and 1550 nm. We selected an artifact with an integrating sphere type optical head in order to suppress polarization dependence and to reduce multiple reflection, which might unfortunately lead to large drift in the later part of this comparison. Relatively large uncertainty of DoE compared to the reported uncertainty of each participant was mainly due to the artifact drift. Another bad thing was that we were unable to look inside the optical head and determine what was wrong in the artifact. In order to examine the cause of the drift, destruction of the optical head may be inevitable. Although our choice of artifact was not quite satisfactory, we obtained quite consistent result for comparison at 1310 nm. In case of 1550 nm, relatively larger deviations of DoE than 1310 nm were observed, which indicated that an effort is required to improve the scale by finding out unknown sources of uncertainty. The degrees of equivalence calculated from the data are to be used within the framework of the Mutual Recognition Arrangement, for example, as the supporting evidence for the item 7.1.0 of the CCPR service category that is Responsivity, Fiber optic power meter. 105
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