Arlington, TX 76012 Pocomoke City, MD 21851 Batesville, IN 47006 http://www.riccachemical.com 1-888-GO-RICCA [email protected] Certificate of Analysis Nickel Standard Stock Solution, 1000 ppm Ni Lot Number: 4302358 Product Number: 5302 Contains: Name Expiration Date: FEB 2014 Manufacture Date:2/9/2013 CAS# Grade Nickel Sulfate Hexahydrate, NiSO4·6H2O 10101-97-0 ACS Water, Deionized, H2O 7732-18-5 ACS, ASTM D 1193 (Type I), EP, USP Test Name Assay Method Specification Result Appearance Clarity, Color, Odor Clear, light green, odorless Passed Test Assay at 20 °C (traceable to NIST SRM 915) Titrimetric vs. EDTA (Murexide Indicator) 1000 ± 1 ppm Ni 999 ppm Ni Specification Reference Method Number ACS Nickel Stock Solution, for preparation of N/A Nickel Standard Solution (0.01 mg of Ni in 1 mL) EP Nickel stock solution (4.78 g NiSO4.7H2O in N/A 1000 mL), for preparation of R 5002000 Volumetric glassware complies with Class A tolerance requirements of ASTM E 288 and NIST Circular 434; it is calibrated before first use and recalibrated regularly in accordance with ASTM E 542 and NIST Procedure NBSIR 74-461. Balances are calibrated regularly with weights certified traceable to the NIST national mass standard. Thermometers and temperature probes are calibrated before first use and recalibrated regularly with a thermometer traceable to NIST standards. All products are prepared according to master documents that assure manufacture according to validated methods. Batch records document raw material traceability and production and testing history for each lot manufactured. Shelf Life (unopened container): Part Number 5302-4 5302-16 Recommended Storage: 15°C - 30°C (59°F - 86°F) Shelf Life 18 months 18 months LaNelle Ohlhausen Quality Assurance This Certificate of Analysis is designed to comply with ISO Guide 31 "Reference Materials -- Contents of Certificates and Labels." To determine manufacture site using lot number, visit http://www.riccachemical.com/Documents/lot.pdf. Version: 1
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