IEEE PHOTONICS TECHNOLOGY LETTERS, VOL. 16, NO. 2, FEBRUARY 2004 359 Mode Characteristics of Semiconductor Equilateral Triangle Microcavities With Side Length of 5–20 m Qiao-Yin Lu, Xiao-Hong Chen, Wei-Hua Guo, Li-Juan Yu, Yong-Zhen Huang, Senior Member, IEEE, Jian Wang, and Yi Luo Abstract—Semiconductor equilateral triangle microresonators (ETRs) with side length of 5, 10, and 20 m are fabricated by the two-step inductively coupled plasma (ICP) etching technique. The mode properties of fabricated InGaAsP ETRs are investigated experimentally by photoluminescence (PL) with the pumping source of a 980-nm semiconductor laser and distinct peaks are observed in the measured PL spectra. The wavelength spacings of the distinct peaks agree very well with the theoretical longitudinal mode intervals of the fundamental transverse modes in the ETRs, which verifies that the distinct peaks are corresponding to the enhancement of resonant modes. The mode quality factors are calculated from the width of the resonant peaks of the PL spectra, which are about 100 for the ETR with side length of 20 m. Index Terms—GaInAsP–InP, microresonator, photoluminescence (PL), quantum wells. I. INTRODUCTION O PTICAL microresonators have the potential applications in the fabrication of microlasers and optical add–drop filters. Optical microdisk or microring lasers as typical semiconductor microcavity lasers have achieved great success [1]–[6]. Recently, we have numerically shown that the equilateral triangle microresonator (ETR) is a good choice for realizing semiconductor microlasers with directional emission [7]–[9]. In this letter, we fabricated GaInAsP–InP ETRs by the inductively coupled plasma (ICP) etching technique, and studied the mode characteristics for the fabricated ETRs. Resonant peaks are observed in the photoluminescence (PL) spectrum with the wavelength spacings in good agreement with the analytical mode wavelength intervals. In addition, the mode quality factors are calculated from the width of the resonant peaks and the cavity losses are estimated accordingly. II. EXPERIMENTAL RESULTS A laser wafer with the active region composed of six quantum wells was grown by metal-organic chemical vapor deposition (MOCVD) technique. The thickness of the InGaAsP quaternary (Q) quantum wells and the 1.2- m-Q barrier layers are Manuscript received February 25, 2003; revised August 26, 2003. This work was supported by the National Nature Science Foundation of China under Grant 60225011, and Major State Basic Research Program under Grant G2000036606. Q.-Y. Lu, X.-H. Chen, W.-H. Guo, L.-J. Yu, and Y.-Z. Huang are with State Key Laboratory on Integrated Optoelectronics, Institute of Semiconductors, Chinese Academy of Sciences, Beijing 100083, China (e-mail: [email protected]). J. Wang and Y. Luo are with State Key Laboratory on Integrated Optoelectronics, Department of Electronical Engineering, Tsinghua University, Beijing 100084, China. Digital Object Identifier 10.1109/LPT.2003.821063 Fig. 1. SEM pictures of the GaInAsP-InP ETR microcavities fabricated by two-step ICP etching. (a) Oblique side view of an ETR with side length a 5 m. (b) Oblique side view of arrayed ETRs with side length a 20 m. = = 11 nm. To enhance the emission of the TM mode 0.3% tensile strain is introduced into the quantum wells. The active region is sandwiched by 80-nm-thick 1.1- m-Q confining layers, and the upper layers consist of 1.7- m-thick InP cladding layer and a p -InGaAs ohmic contact layer. An 800-nm SiN layer was deposited by plasma-enhanced chemical vapor deposition (PECVD) on the laser wafer as the mask for etching InGaAsP and InP. After forming the triangle patterns on the photoresist by the standard photolithography, we first transferred the patterns onto the SiN layer with the reaction gas of SF and then etched InP–GaInAsP with the CH –Cl –Ar gas mixtures by a Plasmalab100 ICP system. The etching depth is about 6 m that is larger than the range of the lateral field distribution. The scanning electron microscope (SEM) pictures of oblique side view of fabricated ETRs are shown in Fig. 1, Fig. 1(a) for an ETR with side length of 5 m and Fig. 1(b) for arrayed ETRs with side length of 20 m. The etched pillars are nearly vertical and the surface at the bottom is smooth, however, the vertices of the ETRs are round, which is mainly distorted in the 1041-1135/04$20.00 © 2004 IEEE 360 IEEE PHOTONICS TECHNOLOGY LETTERS, VOL. 16, NO. 2, FEBRUARY 2004 60 140 a = 5 µm 40 10 µm 120 20 µm 100 Quality Factor Intensity (a.u.) 50 30 20 (a) a=5µm 10µm 80 20µm 60 40 10 0 1300 20 1350 1400 1450 1500 1550 0 1300 1600 1350 1400 1450 Fig. 2. PL spectra for GaInAsP/InP ETRs with side length of 5, 10, and 20 m. 1550 1600 120 (b) a = 20µm λ=1523 nm 110 Quality Factor photolithography process. The ETR vertices are very difficult to keep during the photolithography and the ICP etching process especially for deep etching. The polymers formed in the etching process with CH gas mixture help to protect the sidewalls and result in smoother sidewalls in the lower layer than the upper layer as shown in Fig. 1(a). The fabricated ETRs were optically pumped by a 980-nm semiconductor laser at room temperature (RT) under continuous wave (CW) condition, with the pump beam focused onto the ETR through a tipped single-mode fiber. The output spectrum was collected by another tipped single-mode fiber and measured by an optical spectrum analyzer (OSA). The measured 5, 10, and PL spectra for the ETRs with the side length 20 m are shown in Fig. 2, distinct peaks are observed in the PL spectra and the peak wavelengths are not influenced by the position and angle of the detection fiber relative to the ETR. By Lorentzian fitting of the measured PL spectra, we can obtain the wavelength and width of each peak. In the next section, we will show that these distinct peaks are corresponding to the resonant peaks of different longitudinal modes of the fundamental transverse mode in the ETR and the peak wavelength is the mode wavelength. We can calculate the mode quality factor as the ratio of the peak wavelength to the width and estimate the cavity loss. In Fig. 3(a), the quality factors are plotted as functions of the mode wavelength at 5, 10, and 20 m. The calculated mode quality factors are about 35 and 60 at 5 and 10 m, respectively, as the wavelength increases from 1300 to 1550 nm. The results indicate that the cavity loss is much larger than the band-to-band transition absorption of the active region at 10 m, so its quality factor varies a little from 1400 to 1580 nm. For the ETR with the side length of 20 m, the quality factor increases from 101 to 142 as the wavelength increases from 1505 to 1580 nm, which corresponds to the mode loss decreasing from 1.8 10 to 1.2 10 cm . The mode loss difference of 6 10 cm can be considered mainly from the difference of the band-to-band transition absorption between 1505 and 1580 nm for the 20- m ETR. The increase of the mode quality factor in the short-wavelength side may be caused by the decrease of the cavity loss. Fig. 3(b) represents the mode quality factors versus pumping intensity for the modes with wavelength 1488, 1505, and 1523 nm at 20 m. With the increase of the pumping intensity the mode quality factor for 1505 nm increases from 86 to 106 and the corresponding mode loss 1500 Wavelength (nm) Wavelength (nm) 100 1505 nm 1488 nm 90 80 0 4 8 12 16 20 24 28 Pump Intensity (a.u.) Fig. 3. (a) Mode quality factors versus mode wavelengths for the ETRs with side length of 5, 10, and 20 m. (b) Mode quality factors versus pumping intensity for different longitudinal modes in an ETR with side length of 20 m. decreases from 2.1 10 to 1.7 10 cm . The cavity loss is too large for lasing in the ETRs. The imperfect vertices and rough sidewalls greatly reduce the mode quality factors of confined modes in the ETRs. III. COMPARISON WITH THEORETICAL RESULTS In this section, the mode wavelength intervals obtained from the PL spectra are compared with the theoretical results. The mode wavelength of the confined modes in the ETR can be written as [9] (1) where the phase shift for the TM mode is (2) is the side length of the ETR, is the effective index of the guided modes, and and are transverse and longitudinal mode numbers. The transverse and longitudinal propagation constant and and the decay constant satisfy (3) (4) (5) LU et al.: MODE CHARACTERISTICS OF SEMICONDUCTOR EQUILATERAL TRIANGLE MICROCAVITIES 80 IV. CONCLUSION Experiment Mode Spacing (nm) 70 In conclusion, we fabricated semiconductor equilateral triangle microcavities by the two-step ICP etching process. The PL spectra of the ETRs were measured at room temperature with the pump source of a 980-nm semiconductor laser. Distinct peaks are observed in the PL spectra for the ETRs with side length of 5, 10, and 20 m. Comparing with the theoretical results, we find that the distinct peaks in the PL spectra are resonant peaks of different longitudinal modes of the fundamental transverse modes. In addition, mode quality factors and cavity losses are estimated from the width of the resonant peaks. Theory 60 a = 5 µm 50 40 10 µm 30 20 µm 20 10 1300 1400 361 1500 1600 Mode Wavelength (nm) Fig. 4. Mode intervals versus mode wavelengths obtained from the PL spectra and the theoretical formulae for the ETRs with side length of 5, 10, and 20 m. where is the wavenumber in vacuum. Since the mode wavelength covers a wide wavelength range, the wavelength dependence of the mode refractive index should be accounted in calculating the mode wavelength. Assuming the effective index varying linearly with photon energy, we obtain the 0.8 eV from mode effective index as the group index obtained from the mode wavelength interval of a ridge-waveguide Fabry–Pérot laser fabricated from the same laser wafer. 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