MODEL TX-RSA TX - NDT Systems X-ray Residual Stress analysers Industrial metallurgists have been using X-ray residual stress analysis for many years as the preferred method for measuring unwanted or actual residual stresses in crystalline materials, but the technology available has always been based on simple manually operated, often floor mounted XRD systems employing relatively insensitive detectors which always require a high power X-ray source with a water cooling supply. Such systems work well enough although there can sometimes be safety issues to consider when high power X-ray tubes are employed. Water cooling supplies are always a problem and high X-ray power means a high power mains voltage supply There is however an urgent need in industry for automated high speed systems with very high sensitivity allowing a complete analysis to be made in just a few seconds plus a need for systems that can handle larger components that just will not fit into a safety enclosure and it is these requirements that our new universal multi use NDT systems address. RSA-10 - Mobile X-Ray Residual Stress Analyser RSA-20 - Portable X-Ray Residual Stress Analyser RSA 30 - Industrial X-Ray Residual Stress Analyser RSA-40 - Robotic X-Ray Residual Stress Analyzer To improve the analytical method for large and or massive components we have developed a very high precision computer controlled robotic X-ray residual stress analyser designed to substantially improve accuracy of stress measurements both in terms of defining residual stress parameters within a sample in addition to measuring Austenite phases and the absolute location of those parameters about or within the sample. The new TX Robo-Stress analyser ( RSA-40 ) is based on an extremely robust computer controlled robot that can be programmed to accurately position a compact stress analyser within or about a defined 3D volume and automatically measure residual stresses located about an object by analysing the Xray diffraction peaks associated with stresses retained in a material after a manufacturing process. Powerful software operating in real time allows the robot to automatically position the X-ray probe about any 3D object within or about practically any sample no matter how large. Such samples can be aerospace components, turbine blades, gears, bearings, motor car components and other large structures. Absolute positional accuracy is assured by an integrated laser position finder that can determine an objects 3D profile and locate an exact location for analysis and repeatedly reposition to that location to within just a few microns without manual intervention. RSA-40 robotic residual stress analyser Robotic Safety The RSA-10 Robotic Stress Analyser is the safest instrument in town and the reason why is that the robot does all the work and the operator simply controls the measurement from a computer console at a distance. All parameters being under software control. The X-ray power supply is just 4 watts making TX NDT systems the safest in the world to use. Many commercial stress systems require high power X-ray sources ranging from 200W to 2KW. Ours is just 4W Robotic software is able to control the position of the stress probe by accurately and automatically finding the correct Eulerian coordinates about any type of sample and so measuring the correct X-ray diffraction stress parameters in 2 or 3D space. By employing a free spatial probe under robotic control it is no longer necessary to employ manually operated or fixed position goniometers allowing massive or exceptionally large samples to be analysed with ease Applications for our robot stress analysers are industry wide and include aerospace, motor industry, bearing manufacturers and most other manufacturers of large critical assemblies and components including structural engineering.. Other but similar applications include aircraft undercarriage components, airframe, high pressure or critical pipe assemblies as well as alloy metal components, engine and turbine parts and assemblies and similar technologies. MODEL TX-RSA TX stress systems can employ many types of X-ray source but for safety reasons we choose to use low power AIR COOLED high radiance X-ray sources designed specifically for stress analysers. Because of the exceptional sensitivity provided by our solid state strip detector technology, compact air cooled high radiance sources to be used as standard and with a power of just 4 Watts we achieve truly excellent S:N ratios in just a few seconds. An integrated collimator and laser profiler ensures that the maximum Xray intensity is available in the exact position required for the sample under test. Our ultra high sensitivity position sensitive detector does the rest ensuring both high accuracy and short measure times in the region of just a few seconds and in “real time “. The design also ensures that the requirements of most world standards for NDT are always exceeded Solid state “ultra high sensitivity” 1280 channel PSD detector TX stress analysers employ a remarkable ultra fast solid state detector with 1028 separate elements or channels, each providing a count rate of 1 X106 cps and therefore an overall max count rate >1.2 X 109 cps. Efficiency is optimised for Cr Ka energy. In addition the detector is single photon counting plus energy discrimination and a net photon efficiency that exceeds 90% , making it the perfect detector for stress analysis. By employing a wide angle position sensitive detector with energy discrimination and single photon counting sensitivity we are able to measure stress parameters with exceptionally low backgrounds. We have also designed the stress head in such a way that we are not limited to measuring just two diffraction profiles but can analyse up to ten or more separate diffraction profiles about the stressed location so allowing exceptionally good stress data to be obtained from both low or wide angles. By employing a “state of the art” strip detector we are also able to improve system reliability by providing a stress analyser that is both rugged and accurate. Notes on retained Austenite When steel is heated as part of a manufacturing process, phases present in the structure at ambient temperatures can change in such a way that they become transformed into a face centred cubic structure generally known as Austenite. When steel is heat treated as part of a manufacturing process such as hardening, the metal is first heated and then rapidly cooled by quenching, This causes the Austenite to transform to Martinsite which is a very brittle and hard phase. When this phase is undesirable, metals can be tempered in such a way so as to reduce the brittleness but retain most of its hardness In fact when steel is tempered or quenched it is always likely that Austenitic phases will be retained and so may seriously effect the design performance requirements of the alloy over time, in that stresses can cause the retained Austenite phase to slowly change to Martensite, which may cause dimensional instability or failure. Clearly control of Martensitic and Austenitic phases are extremely important when manufacturing high performance alloys and it is for this reason that TX stress analysers allow the user to simultaneously or otherwise measure these critical phases.. See ASTM E975 and SAE SP-453 How is this achieved TX Stress systems are sophisticated, mini X-ray diffractometers designed to spatially measure diffraction peak intensities associated with residual stresses and are retained within a crystalline matrix, using technology that allows diffracted X-rays to be measured in real time and at high sensitivity. To achieve this we employ a rugged very high sensitivity X-ray detector placed at the side of a low power X-ray source and this constitutes the Xray diffractometer. The detector measures the diffraction pattern associated with that particular sample over a small or if necessary a large angular range as determined by the experiment. Our Software plus Reitveld refinement Residual stress tensors are measured using X-ray Diffraction technology and we have manufactured a range of XRD systems now for several years. During this time we have developed sophisticated software for all XRD applications including full profile stress analysis using the Reitveld whole pattern method. This allows stress and texture analysis to be made at high speed on a wide range of materials and alloys measuring critical microstructures or multi phase components using either multi - bi axial or mono axial geometry plus Sine2 Psi. This means that residual stress analysis can be made on any polycrystalline material using a variety of methods including plane or triaxial stress using chord, Marquardt and centroid analysis with both linear and elliptical interpolation. The Reitveld whole pattern method allows stress values to be evaluated from each phase both with or without texture and is not limited to analysing stress tensors from just two or three diffraction peaks The unique multi use TX Goniometer Our goniometers are exceptionally compact and are ideally suited for use as mobile stress analysers or integrated into a console or robot. They have a large angular 2 theta range of 40 degrees and have options for a motorised phi axis. The multi RSA-20 portable residual stress analyser channel detector provides a typical measure time of just a few seconds per psi position allowing fast analysis to be made on any sample. The overall measurement angle in “real time “is over 40 degrees ( 125 – 165 degrees 2 theta. The Psi Angular range is 90 degrees ( -45 to +45 ) degrees and the Phi range is 360 degrees about a radius of 80mm. This exceptional goniometer allows the measurement of stress tensors in many different alloys without the need to adjust the goniometer allowing retained Austenite also to be measured in a single measurement with stress and in “real time “ . This compares favourably with any other commercial instrument which may offer typically only 20 degrees in a single measurement and must be readjusted every time the sample alloy type is changed. RSA-20 portable residual stress analyser RSA-20 This remarkable portable “go anywhere” stress analyser weighs just 3 Kgs including a high speed solid state multi channel detector and X-ray source and is one of the most compact stress analysers available today. It features a solid state single photon counting high speed detector that allows accurate stress measurements to be made in just a few seconds including retained Austenite. The stress probe can be fixed to any object by way of a simple adjustable arm or clamp including a simple magnetic clamp which is very useful for out of doors applications such as bridge structures or pipelines. The measuring head is very small allowing stress measurements to be made inside bearings or gears or other objects with complex shapes. RSA-30 Is a console based stress analyser designed for laboratory environments where both large and small structures require analysis and certification. Large or heavy samples can be positioned about the stress measurement head with ease and provides an extremely accurate and fast stress measurement system that is easy to use and very robust 3D measurements using our electrolytic depth profiler Sometimes it is interesting to measure stress as a function of depth within a sample which means that material must be removed to expose stressed crystalline layers under the surface. Normal machining is not possible as this would introduce further stresses within the material. To overcome this difficulty we have developed a small easy to use electro etching process that allows material to be removed without inducing further stress An analytical service to our customers with 2Effe engineering We provide both an on site and an in house analysis service for all stress / NDT requirements as well as offering a certification programme for finished parts. We have several types of residual stress and X-ray diffraction instruments available and this service is available in any country on demand. In Europe we are able to provide a stress relieving service for finished products including shot peening and product certification for residual stress and Austenite phases System Specifications Goniometer Psi Angular range Phi angular range Radius Solid State strip detector range Sample alignment Sample 3D profiling Motorised phi axis option Double 2D inclinometer option Can be used in any orientation Type 2 Goniometer Super lightweight sress probe designed for use as a mobile analyser or robotic probe. A rugged multi access goniometer designed for laboratory applications and interfaced to an adjustable tripod mount. Communication System Control Retained Austenite Method Detector Option 1 Alloys Xray Power supply Xray Source Ethernet or wireless communication Automatic under software control Simultaneous analysis + stress Single direction - bi-axial – tri-axial analysis Sine2 Psi using the Rietveld method Mythen ultra fast detector with single photon counting Type strip detector, 320 microns thick with low background Overall max count rate 1.2 X 109 cps Strip width each 50 microns. Total number of strips 1280. Efficiency 90% @5KeV. Allows analysis over 40 degrees (125 – 165) degrees 2 theta Analysed with standard detector include St - Steel, Al. , Austenitic steels etc 0-35KV 0-100uA air cooled 4Watt Cr Air cooled long life Light weight stand Console System Multi Axis Robot Stress Software A compact portable stress stand that can be used in the lab or out side. For use with both small and very large structures A standard safety enclosure console for stress measurements in the lab. Suitable for small and large structures Multi axis Robot providing centre less sampling All positions under software control Full profile analysis using Rietveld method Multi material program Weight stress head Water Power Net 3Kgs according to detector and model Not Required Mains operation 110 – 240V AC standard Or Battery Operated for mobile use Type 10 Goniometer System RSA-30 industrial residual stress analyser 90˚ ( - 45 to + 45 ) degrees 360˚ degrees 80mm 40˚ degrees ( 125˚ – 165˚ degrees 2 theta Laser controlled height adjustment Laser 3D analyser Portable Tri Axis Services CAT412050 Representative In association with TNX srl and 2EFFE srl International X-Ray Associates, Suite 5 Enterprise Centre, Shrivenham Business Park, Swindon Wiltshire UK Tel 44(0) 1793 783666 E [email protected] www.spectrolab.co.uk www.xrayassociates.co.uk
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