15 % Solids @ 2.5 GPM Mass meter to regulate whole stillage to centrifuge #A Centrisys decanter centrifuge adjustable bowl & scroll speed 50 GPM maximum capacity. Thin stillage exits from weir of centrifuge 4% solids Whole stillage from beer column bottoms From Page 6 Operation-data logging of the decanting centrifuge, drying, and evaporation equipment is preformed by a Siemens PCS 7 system. 65 % moisture wet cake, 50 - 300 #/hr. Whole Stillage Tank 100 Gallon Thin Stillage Tank 100 Gallon Wet cake discharge rates and weight totalizer data from the centrifuge is integrated by a weigh belt. Wet cake to co-product separation conveyor To Page 8 #A Mass Meter Thin stillage to evaporator feed tank To Page 9 #A CO PRODUCT DE-WATERING AND DRYING PAGE 7 NATIONAL CORN TO ETHANOL RESEARCH CENTER APRIL 16, 13 BY TERRY LASH 8 - 12% Moisture NCERC uses weigh belt feeders to control the rate of the previously dried product to be recycled & mixed with the co-product wet – cake before it enters the dryers. 8 % Moisture 320 pounds/hr. 8 - 12% Moisture product to storage 8 % Moisture 50 pounds/hr. 8 - 12% Moisture 1000 pounds/hr. 63 % Moisture Separation screw divides wet – cake flow to either the drum dryer or the ring dryer or both at once. T o #A From Page 7 Wet Cake Weigh Belt P a g e The weigh belt scale is used to measure wet – cake feed rate to the ring dryer. 8 65 % Moisture #B From Page 9 Syrup Pump The paddle mixer receives dried co-product from the recycle control weigh feeder & syrup pump and blends with wet cake from the centrifuge. Davenport drum dryer receives 1800 pounds/hr. 30% moisture co-product 175-325 F. drying temp. produces 5 – 15 % moisture co-product. 8 % Moisture 250 pounds/hr. 65 % Moisture 65 % Moisture 30 % Moisture The Barr Rosin steam heated ring dryer can process 100 pounds/hr. of 65 % moisture wet – cake at lower temperatures than the drum dryer. Dried co-products are weighed as they are filling the bulk storage bags. #C From Page 9 Syrup Pump CO PRODUCT DRYING EQUIPMENT PAGE 8 NATIONAL CORN TO ETHANOL RESEARCH CENTER APRIL 16, 13 BY TERRY LASH PROCESS WATER OR BACKSET HOLD TANK To Page 2 VAPOR CONDENSER “BACKSET” To Page 8 #B 35 % solids syrup @ 1 – 2½ pounds/min. Metered by mass to drum dryer mixer. VAPOR SEPERATOR Backset To Slurry Makeup Syrup Flow (Brown) To Page 8 #C 35 % solids syrup @ .5 – 1½ pounds/min. metered by mass to ring dryer mixer. Alfa Lavel small volume (75 Gallon) uses a plate & frame heat exchanger. Didert large volume evaporator (750 Gallon) uses a shell & tube heat exchanger. #A From Page 7 Thin Stillage THIN STILLAGE HOLDING HEATED SYRUP TANK Evaporator Feed Tank STILLAGE EVAPORATION & SYRUP PRODUCTION Thin Stillage Flow (Yellow) PAGE 9 NATIONAL CORN TO ETHANOL RESEARCH CENTER APRIL 16, 13 BY TERRY LASH The NCERC fermentation lab is able to propagate cultures from plates to shake flasks to transfer to the 5 – 30 liter cultivation vessels. Two 5 liter fully automated cultivation/fermentation systems. 30 liter steam in place cultivation/ fermentation system with distillation capabilities. 300 & 3000 LITER CIP/SIP CULTIVATION/FERMENTATION SUITE 400 – 1200 liter steam in place cultivation/fermentation system. P-66 P-65 Pharma grade cell cultivation/biofermentation equipment is highly instrumented & automated for precise control. Fermenter and transfer system piping utilize a sterilization validation system to eliminate contamination. All process control data captured by data historian. 40 – 120 liter steam in place cultivation/fermentation system. Dual PH/DO, load cells, mass air flow sparge control, cell growth, off gas concentration FOUR 22,000 LITER CLEAN IN PLACE PRODUCTION FERMENTERS CULTIVATION/FERMENTATION SUITE PAGE 5-2 NATIONAL CORN TO ETHANOL RESEARCH CENTER APRIL 16, 13 BY TERRY LASH OFF GAS MEASUREMENT SYSTEMS Additional 250, 500, 1300 & 5000 liter vessels available for hydration, fermentation and cultivation. 30 liter cultivation unit equipped with reflux column to remove products from a finished fermentation. CULTIVATION/FERMENTATION SUITE PAGE 5-2 NATIONAL CORN TO ETHANOL RESEARCH CENTER APRIL 16, 13 BY TERRY LASH
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