FINITE ELEMENT SIMULATION OF STRUCTURAL ADHESIVES AND ADHESIVELY BONDED JOINTS AND EXPERIMENTAL VERIFICATION BY NONCONTACTING STRESS-STRAIN ANALYSIS P. L. Geiss, S. Gramsch, D. Vogt University of Kaiserslautern, Workgroup for Materials and Surface Technologies, Gottlieb-Daimler-Strasse, D-67663 Kaiserslautern, Germany, [email protected] ABSTRACT The thick-adherend tensile–shear test according to ISO 11003-2 is widely used to characterize adhesively bonded joints. However, the accurate measurement of deformations close to the bondline is still a challenge, especially for structural adhesives with high moduli. In this paper a method of using finite element simulation to evaluate and adjust data from non-contacting video extensometry strain-measurements is discussed. FEM, simulation of adhesives, bonded joints, non-contacting stress-strain-analysis, compensation INTRODUCTION A widely used method to analyze the shear-stress strain behaviour of adhesives is the thick-adherend tensile-shear test according to ISO 11003-2. To determine shear strains, optical or mechanical extensometers are usually applied on the front side of both parts of the specimen close to the end of the overlap area. The overall extension reading thus includes deformation of the adhesive as well as deformation of the adherend. In this paper a new method (dot measurement) is used and the results are compared to the strain measurement using simple gauge marks. The finite element simulation (FEM) is applied to correlate the results of both different measurement methods and to derive a correction function. EXPERIMENTAL METHODS Non-contacting videoextensometry To measure shear strain the non-contacting video extensometry is used. This technique is based on an optical displacement-measurement using high resolution CCD-cameras. The deformation of a sample can either be measured by the application of gauge marks at the joints edges or the application of a grit of dots close to the adhesive layer (fig. 1). Fig. 1: Gauge mark and dot measurement – measuring point positions FE-simulation The finite element simulation (FEM) is a widely spread and effective tool to analyze and predict stress-strain distributions. Its use related to adhesive joints is already discussed in [1] and [2]. In this study the MARC/Mentat 2005r software package from MSC was used. The mesh was composed of 10 hexahedral 8-node elements across the thickness of the adhesive layer (d=0.2mm), 50 elements covering the width of the joint (25mm) and 400 elements in the longitudinal direction of the overlap area (12.5mm). To avoid mesh-dependent effects the number of elements in the cross section of the adhesive layer varies to maintain a constant element size independent of the bondline thickness. On the basis of data obtained from bulk specimen the material properties of a one-component epoxy based structural adhesive were characterized by Young’s modulus and the Poisson ratio. For plasticity a workhardening function σ = σ(εplastic) is determined from shear tests, using the dot measurement variant. The bonded parts are simulated as linear-elastical applying the von Mises yield criterion. RESULTS AND DISCUSSION Experimental results Depending on the measurement method different results are obtained leading to differences in the τ-γ-behaviour (fig. 2). Linear gauge marks result in a lower shear modulus (GGM = 206 MPa) compared to the use of the dot measurement (GDM = 640 MPa). A comparison with the shear modulus G = E/2(1+µ) = 615 MPa determined from uniaxial tensile tests (bulk specimen) reveals the dot measurement to be more accurate because the measurement takes place closer to Fig. 2: τ-γ-behaviour at different the bondline. Despite this advantage the gauge strain measurements variants mark variant is more popular due to the easiness in application and less scattering leading to a higher resolution due to the possibility of integration along the length of the marker. Simulation results and validation Fig. 3 compares experimental and simulated σ-ε-curves from uniaxial tension tests. Fig. 4 displays experimental and simulated τ-γ-curves from thick-adherend tensile sheartests for two different bondline thicknesses (d=0.2mm and d=3mm). Correlating with [3] the shear modulus increases with an increasing bondline thickness (fig 4). Furthermore the results feature a good correlation between simulation and experiment. Fig. 3: Correlation experiment/simulation at uniaxial tension Fig. 4: Correlation experiment/simulation at different bondline strength (shear) Correction of the experimental shear strain data by FE-simulation Simulated τ-γ-curves are determined at marker positions (fig. 5) similar to the experimental measurement via gauge marks and dots. Fig. 6 illustrates how simulated τγ-curves correlate with the experimental data for different positions of the marker. Fig. 5: Positions of the markers Fig. 6: Correlation experiment/simulation at different positions of the markers The simulated results allow the generation of a correction function as follows: ξ (τ ) = γ GM (τ ) γ DM (τ ) γDM(τ): shear strain, analogue to dot measurement γGM(τ): shear strain, analogue to gauge mark measurement The function ξ( τ) depends on the thickness of the adhesive layer, so a FE-based correction function can be derived for various bondline thicknesses (see fig. 7). Below the yield point the correction factors remain constant. After the yield point they decline linearly until reaching a threshold value ξ( τmax) = 1. By this approach it is possible to reduce the FE-model to a simple linear-elastic model with a single load step correlating to a shear stress within the range 0<τ<τyield and to approximate the Fig. 7: Correction functions complete correction function by a bilinear function. In return only Young’s modulus, Poisson ratio, the yield point and bond strength need to be experimentally predetermined. The thickness dependent value of ξ( τ<τyield) is derived directly from the FE-simulation. The function above the yield point can be derived by linear regression between the starting point (ξ( τ<τyield); τyield) and the end point (1; τmax). As depicted in fig. 8 the application of the correction function with the Fig. 8: Corrected characteristics experimental data from gauge mark measurements leads to a similar characteristics, as using the dot measurement variant. CONCLUSION In this paper a method of using finite element simulation to evaluate and adjust data from non-contacting video extensometry strain-measurements is discussed and applied to data from thick-adherend tensile–shear tests. By using sample specific correction functions obtained from finite element simulation the accuracy of measurements with linear markers on the surface of the specimen could be enhanced to match the results of more sophisticated but more laborious dot-measurements on the edge of the specimen close to the bondline. References [1] Adams, R. D.; Wake, W. C.: “Structural Adhesive Joints in Engineering”; Elsevier Applied Science Publishers, 1984 [2] Schlimmer, M. u.a.; „Berechnung und Auslegung von Klebverbindungen“; Teil 19, Adhäsion – Kleben & Dichten, Jahrgang 2004 Heft 5-12, Jahrgang 2005 Heft 1-3 [3] Habenicht, G.; „Kleben - Grundlagen, Technologie, Anwendung“; Springer-Verlag 2006
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