One-pot Synthesis of Oil Dispersible Ultra Fine Manganese (II

80
Manganese-oleate
manganese-oleatecomplex
complex
78
76
aged
sample
Aged
sample
1740
74
1740,,-C=O
–C = O
Transmittance (a.u.)
145145cm?¹
cmG 1
2852
2852
72
2957
,-CH3
2957,
-CH 3
2922, -CH2
2922, -CH 2
70
68
precursor
Precursor
66
64
62
60
0
500
1000
1500
2000
2500
Wavenumber (cmG 1)
3000
3500
4000
4500
425
(200)
(200)
375
(220)
(220)
Counts
325
(111)
(111)
275
(311)
(311)
(222)
(222)
225
175
1251 0
10
20
20
30
30
40
50
40
50
22
60
60
70
70
80
80
10 nm
(111)
(111)
(200)
(200)
(220)
(220)
(311)
(311)
(222)
(222)
1 1/nm
(a)
(a)
(b)
(b)
(c)
(c)