Initiation of damage in composite plates under transverse central static loading N.K. Naik *, Bulliraju Nemani Department of Aerospace Engineering, Indian Institute of Technology, Powai, Mumbai 400 076, India Abstract Experimental and analytical studies have been carried out on transverse static central load threshold for damage initiation. Experiments have been carried out on a typical plain weave E-glass/epoxy laminated plate. A good correlation is observed between the experimental results and ®nite element analysis predictions. Further, analytical studies have been carried out on the eect of reinforcement architecture on the load threshold for damage initiation. It is observed that transverse static central load threshold for damage initiation is higher for woven fabric composites compared to those of cross-ply laminates made of unidirectional layers and unidirectional composites. Keywords: Damage initiation; Transverse static loading; Experimental results; Prediction; Woven fabric composites 1. Introduction Polymer matrix composite materials are ®nding increasing use in high performance applications because of their high inplane speci®c stiness and speci®c strength. For eective use of composite structures, they should be able to withstand multidirectional loading also. Composite structures under transverse static loading are one of the important design requirements. For laminated composites made of unidirectional (UD) layers dierent failure modes are: matrix cracking/ lamina splitting, ®bre debonding, delamination and ®bre breakage. Normally, the macro damage initiation takes place in the form of matrix cracking/lamina splitting and delamination. Stress analysis of laminated composite plates subjected to transverse loading has received considerable attention of researchers, and many articles are available [1±8]. The objective of the present work is to look into the initiation of damage in composite plates under transverse central static loading. Experimental studies have been carried out on a typical plain weave E-glass/ epoxy laminate. The damage initiation has also been predicted using the inhouse ®nite element analysis code. Further, a parametric study has been carried out on damage initiation with dierent reinforcement architectures. Speci®cally, the studies have been carried out on balanced symmetric cross-ply laminates made of UD layers, woven fabric (WF) composites and three-dimensional (3D) composites. 2. Stress and damage analysis A three-dimensional linear elastic ®nite element analysis has been used to predict the initiation of damage in composite plates. A 3D eight-noded brick element was used in the analysis, with three degrees of freedom at each node u; v; w. The aspect ratio considered in the present analysis is inbetween 1 and 2. By taking symmetry into consideration, quarter plate analysis was used for the present study. Convergence study was carried out for the mesh size. Based on this study, a mesh size of 32 32 5 was chosen for the quarter plate. The co-ordinate system for the composite plate is shown in Fig. 1. The boundary conditions for quarter plate are as given below: (a) Simply supported boundary conditions: At X 0; u 6 0; v 0; w 0; At X LX =2; u 0; v 6 0; w 6 0; At Y 0; u 0; v 6 0; w 0; At Y LY =2; u 6 0; v 0; w 6 0: 168 3. Damage evolution during transverse central quasi-static loading Fig. 1. Composite plate co-ordinate system. (b) Clamped boundary conditions: At X 0; At X LX =2; u 0; v 0; w 0; u 0; v 6 0; w 6 0; At Y 0; u 0; v 0; w 0; At Y LY =2; u 6 0; v 0; w 6 0: Based on the nodal displacements obtained, the stress state has been evaluated throughout the composite plate. An inplane failure criterion by Tsai±Hill [9] has been used for damage initiation studies. An inplane failure function, I based on Tsai±Hill criterion is de®ned as follows: 2 2 2 r1 r2 s12 r1 r2 1: XT YT S12 XT XT Here r1 ; r2 , and s12 are the induced inplane stress components and XT ; YT , and S12 are the normal and inplane shear strength values. The damage initiation takes place in the form of matrix cracking/lamina failure when the value of the inplane failure function, I just exceeds unity. Initiation of delamination due to rZ and other interlaminar shear stresses is determined using an interlaminar failure function. For this, an interlaminar failure function based on through-the-thickness quadratic failure criterion as proposed by Brewer±Lagace has been used [10]. An interlaminar failure function is de®ned as follows: 2 2 2 2 r3t r3c s23 s31 1: Zt Zc S23 S31 Here, r3 ; s23 and s31 are the induced stress components and Z, S23 and S31 are the corresponding strength values. Subscripts t and c indicate tensile and compressive, respectively. Superscript indicates average values over a certain area. The delamination initiates when the value of the interlaminar failure function, I just exceeds unity. The damage initiation in laminated composite plates subjected to transverse loading can be in the form of matrix cracking/lamina splitting, debonding and initiation of delamination. Upon further loading, the major damage propagation mode can be the delamination growth, and the cracking of the adjacent layers, ®nally leading to ®bre breakage and ®bre pull out. Matrix micro-cracking and the debonding are the micro-failure mechanisms, and can take place at very early stages. For UD-laminated composites the ®rst macro damage occurs in the form of lamina splitting on the tensile side of the laminates during transverse loading because of the inplane stresses [11]. This is because of the lower transverse tensile strength properties of the UD lamina. Lammerant and Verpoest [11] carried out transverse quasi-static loading experiments on cross-ply laminate 904 =04 S made of toughened carbon/epoxy prepreg HTA/6376. In the experiments, they used plate-like composite specimens clamped in a square ®xture and loaded at a speed of 0.01 mm/sec with a hemispherical tup at a central loading point. The laminates could still slide in the ®xture because of the ¯at polished surface of the ®xture. So, at the edges the ®xture only prevented the plate from translating in the loading direction or rotating. The unsupported area of the composite plate was 80 mm 80 mm and the thickness 1.8 mm. Using the acoustic emission technique and ultrasonic testing, they monitored initiation and propagation of damage. They observed that the ®rst damage in the laminate was matrix cracking/lamina splitting in the bottom layer right under the loading point at a displacement of 1 mm. They experimentally observed that the ®rst matrix crack initiated only a small delamination in the centre of the plate at the lower interface. The WF composites are characterised by balanced inplane properties. Hence, inplane elastic and strength properties are equal along both warp and ®ll directions. Hence, early lamina splitting may not take place. It was observed that the failure initiates in the top layer for WF laminates because of inplane stresses [12]. This is because of lower inplane compressive strength of the WF laminate compared to its inplane tensile strength. The damage can also initiate in the form of delamination at dierent interfaces because of interlaminar stresses for WF composites. 4. Experimental studies: transverse quasi-static loading Composite plates of dimension 150 mm 150 mm 5 mm made of a typical plain weave E-glass/epoxy laminate GLE-12 were used for the experimental studies under transverse quasi-static loading. Loading was 169 Fig. 2. Experimental load±displacement behaviour for E-glass/epoxy, WF, 0s , GLE-12 under transverse static central loading-clamped. performed on the clamped specimen at the rate of 0.2 mm/min. The unsupported area of the plate was 128 mm 128 mm. Loading was continued till the damage initiated. Tests were planned at loads at which the damage just initiated and at loads at which substantial damage occurred. Experimental load±displacement behaviour is presented in Fig. 2. In the ®rst test, loading was continued till a substantial damage was visible on the top and bottom surfaces of the specimen. The maximum load in this case was 5.12 kN. In the second test, loading of the specimen was continued until damage was clearly visible on the top surface. The corresponding load was 4.06 kN. Cscans also showed damage at this load. The other two tests were carried out at comparatively lesser loads of 2.3 and 2.56 kN. No clear damage was visible on any of the surfaces. However when viewed against a strong source of light, these specimens showed a dense region below the point of contact. The C-scans did not show any damage. It can be taken that the point damage initiated at a load below 2.3 kN. Typical C-scans are shown in Fig. 3. 4.1. Validation Using the inhouse ®nite element analysis code [13,14], the central point displacement and the inplane failure function have been evaluated in the present study for the composite plate used in [11]. It was observed that, the failure had just initiated in the form of matrix cracking/ lamina splitting in the bottommost layer as in the case of Lammerant and Verpoest experimental observations. Lammerant and Verpoest considered quasi-static load- Fig. 3. Damage shapes and sizes under transverse quasi-static central loading: C-scan results. ing condition, whereas in the analytical predictions static loading is considered. For the plate geometry and materials considered, inplane failure function at the bottom (at point b), I1 1:049 at a central static load of 380 N for simply supported case. The corresponding displacement of the plate at the centre, dm 1.221 mm. Again, for the simply supported boundary condition, dm 1:06 mm at a load of 330 N. The corresponding inplane failure function, I1 0:791. On the other hand, for clamped boundary condition, inplane failure function, I1 1:042 at a central static load of 460 N. The corresponding displacement of the plate at the centre, dm 0:57 mm. As seen earlier, the boundary condition was not simply supported or clamped realistically for the experimental studies of Lammerant and Verpoest [11]. Hence, the displacement predicted should be in between the limiting case of 1.221 mm for simply supported case and 0.57 mm for the clamped case at I1 1:04. Realistically, the transverse central loading can be treated as a small patch load rather than a point load. Hence the transverse load was distributed over a central patch for the predictions. The patch area considered was 0.097% of the plate area. Further, the experimental and predicted results have been compared for plain weave E-glass/epoxy laminate GLE-12. The prediction was carried out with mechani- 170 Table 1 Elastic properties of composites: E-glass/epoxya Material E11 (GPa) E22 (GPa) E33 (GPa) G12 (GPa) G13 (GPa) G23 (GPa) m12 m13 m23 Vf0 q (kg/m3 ) UD UD GLE-12 WG02G 3D-O 3D-OO 48.0 30.9 20.8 20.8 20.1 16.9 15.3 8.3 20.8 20.8 19.9 19.5 15.3 8.3 8.7 8.7 14.0 11.7 5.1 2.8 3.92 3.9 4.0 3.9 5.1 2.8 4.2 4.2 4.0 3.9 5.8 3.0 4.2 4.2 4.0 3.9 0.32 0.33 0.17 0.17 0.20 0.19 0.32 0.33 0.28 0.28 0.29 0.36 0.33 0.40 0.28 0.28 0.30 0.36 0.65 0.40 0.44 0.40 0.40 0.40 2112 1750 1808 1750 1750 1750 6.9b 6.9b 3.2 0.28b 0.28b 0.39b Toughened carbon/epoxy HTA/6376 148.0 9.9 a b 9.9b 1430b Densities of E-glass ®bre 2620 kg/m3 and epoxy resin 1170 kg/m3 ; 3D-OO: considering possible undulations in stuers, ®llers and warp weavers. Estimated values. Table 2 Strength properties of composites: E-glass/epoxya Material XT (MPa) YT (MPa) ZT (MPa) UD UD GLE-12 WG02G 3D-O 3D-OO 1297 798 360 250b 359 253 27.8 27.1 360 250b 340 333 27.8 27.1 32.0 27.1 83.0 22.0 Toughened carbon/epoxy HTA/6376 2000 70 70c YC (MPa) ZC (MPa) Vfo 820 480 225 183 215 152 150 140 225 183 204 200 150 140 445 140 170 170 0.65 0.4 0.44 0.4 0.4 0.4 1892c 260c 260c ) S12 (MPa) S13 (MPa) S23 (MPa) XC (MPa) 39.2 36.8 28.0 28.0 36.8 36.8 39.2 36.8 28.0 28.0 36.8 36.8 38 36 28 28 36 36 100c 105 105c a 3D-OO: considering possible undulations in stuers, ®llers and warp weavers. At pure matrix block failure. c Estimated values. b cal properties given in Tables 1 and 2 [12]. Peak stresses were at the top layer right below the point of loading. With a load of 2 kN and clamped boundary condition on all the four sides, the following stress state has been obtained: rX 227 MPa; rZ 140 MPa: rY 227 MPa; The maximum tensile rZ at some distance away from the point of loading is 6 MPa, and the central de¯ection d 1 mm. The same plate was analysed for simply supported boundary condition on all the four sides with a central load of 2 kN. The results are: rX 263 MPa; rZ 140 MPa: rY 263 MPa; The maximum tensile rZ at some distance away from the point of loading is 6 MPa, and the central de¯ection d 2:28 mm. For the clamped boundary condition, rX or rY is )227 MPa. The corresponding strength value YC is 225 MPa. So, this indicates that the damage would initiate at a load of 2 kN on the upper surface right below the point of loading. For static loading, the predictions showed that the point damage initiates at a transverse central patch loading of 2 kN. The experimental study also showed that the point damage would initiate at about 2 kN load. The corresponding central de¯ection, d was 1.7 mm. The prediction shows d 1:0 mm for clamped boundary condition and d 2:28 mm for simply supported boundary condition. It was observed during experimentation that the composite plate could still slide even though clamped boundary condition was adopted. At the edges the clamping ®xture only prevented the composite plate from translating in the loading direction or rotating. Hence, during experimentation, the boundary condition was not exactly clamped. The prediction of central de¯ection is based on clamped boundary condition. Hence, the central de¯ection predicted should be in between the limiting cases of 1.0 mm for clamped case and 2.28 mm for simply supported case. 5. Parametric studies A parametric study has been carried out on the eect of reinforcement architecture on transverse static central load for damage initiation. Studies have been carried 171 Table 3 Stress and failure behaviour of composites under transverse central static loadinga Material Load, P (kN) Central displacement, dm (mm) UD1b UD2c CP1b CP2c GLE-12 WG02G 3D-O 3D-OO 0.49 0.51 0.55 0.58 2.00 1.60 1.85 1.40 0.172 0.301 0.189 0.334 1.006 0.805 0.938 0.767 rX (MPa) 51.2 55.8 56.8 62.5 ())227.0 ())182.0 ())206.0 ())154.0 rY (MPa) rZ (MPa) 27.6 27.5 27.8 27.4 ())227.0 ())182.0 ())204.0 ())165.0 ())16.3 ())1.8 ())2.3 ())2.5 ())139.0 ())112.0 ())136.0 ())102.0 Failure function I1 Failure function I2 0.99 1.03 1.00 1.03 ± ± ± ± ± ± ± ± 1.02 0.99 1.00 1.01 a Plate dimensions: LX 128 mm, LY 128 mm, LZ 5 mm, clamped. 1. Vf0 0.65. c 2. Vf0 0.40. b 3D composites. This is because of lower inplane compressive strength of WF and 3D composites compared to the corresponding tensile strength. It may be noted that through-the-thickness stress rZ does not lead to initiation of delamination. From Table 3 and Fig. 4 it can be seen that transverse static central load threshold for damage initiation is higher for WF and 3D composites compared to those of CP laminates made of UD layers and UD composites. This is because of balanced inplane properties of WF and 3D composites. 6. Conclusions Fig. 4. Transverse static central load threshold for damage initiation for E-glass/epoxy composites ± clamped. out on E-glass/epoxy composites clamped on all four sides using the inhouse ®nite element analysis code [13,14]. The plate dimension: 128 mm 128 mm 5 mm. The central patch area is 0.097% of the plate area. Studies have been carried out on balanced symmetric cross-ply laminate (CP) made of UD layers and UD composites with ®bre volume fraction, Vf0 0:65 and 0.4. Studies have also been carried out on two types of plain weave E-glass/epoxy composites (GLE-12 and WG02G) and two types of 3D orthogonal through-thethickness interlock woven composites (3D-O and 3DOO). The mechanical properties are given in Tables 1 and 2 [12,15]. Transverse static central load threshold for damage initiation (P), central displacement dm ) and peak stress values rX ; rY and rZ ) are given in Table 3 and Fig. 4. It may be noted that the corresponding failure function values are equal to one. Damage initiates at the bottom surface (Fig. 1, point b) for CP and UD composites. This is because of lower transverse tensile strength of the unidirectional composites. On the other hand, failure initiates at the top surface (Fig. 1, point a) for WF and Experimental studies have been carried out on a typical plain weave E-glass/epoxy composite, and the transverse quasi-static central load threshold for damage initiation has been determined. The damage initiation has been predicted using the inhouse ®nite element analysis code. A good correlation is observed between the experimental and predicted results. The transverse static central load threshold for damage initiation is higher for WF and 3D composites compared to those of CP laminates made of UD layers and UD composites. Acknowledgements This work was supported by the Structures Panel, Aeronautics Research and Development Board, Ministry of Defence, Government of India, Grant No. Aero/ RD-134/100/10/95-96/890. References [1] Kapania RK, Reciti S. Recent advances in analysis of laminated beams and plates: part ± I. AIAA J 1989;27:923±34. 172 [2] Kapania RK, Reciti S. Recent advances in analysis of laminated beams and plates: part ± II. AIAA J 1989;27:935±46. [3] Reddy JN. On the generalisation of displacement - based laminate theories. Appl Mech Rev 1989;42:S213±22. [4] Finn SR, Springer GS. Delaminations in composite plates under transverse static or impact loads ± a model. Compos Struct 1993;23:177±90. [5] Doxsee LE, Rubbrecht P, Li L, Verpoest I. Delamination growth in composite plates subjected to transverse loads. 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