LAB REPORT OUTLINE Title: Date: (Be sure to label each section of the report) Purpose The purpose of any experiment is a concise statement as to why we are performing such an exercise and what we are trying to prove or learn from it. EXAMPLE: The purpose of this experiment is to discover differences between physical and chemical changes. Materials All the materials and apparatus needed to perform the experiment should be listed in column form. Knowing the concentrations of solutions is vital. You often need this information to perform calculations and to answer the questions at the end of the experiment. EXAMPLE: 250 mL beaker 100 mL graduated cylinder ring stand hot hands laboratory burner 6.0 M HCl Procedure The procedure used in the experiment should be written in brief, numbered steps. (Paraphrase the steps in the lab.) You should be able to do the lab based on your procedure. The procedure should not include instructions on how to do calculations. (Those instructions belong in the calculation section of the report.) EXAMPLE: 1. 2. Find the mass of a 250 mL beaker. Measure exactly 100 mL of tap water in a graduated cylinder. (etc.) Observations Observations are to be brief, descriptive statements. They are to be made at every possible interval of an experiment. They should be an honest record which does not always reflect the textbook content or what is reputedly “right". Remember, careful observations will make it easier for you to recognize chemical reactions. EXAMPLE: Reaction Observation CaCO3 + 6.0M HCl rapid bubbling CaCO3 + 1.0M HCl bubbling CaCO3 + 0.1M HCl slight bubbling 1 Data and Calculations Tables Data may be most efficiently arranged in a form of a table or tables. The columns of the table must be properly categorized and labeled. Always be sure to place labels on numerical values, such as 10.00 grams instead of 10. Make sure that all numerical values contain the correct number of significant figures. EXAMPLE: Sample Glass Rod Determining Density Original Final Water Mass (g) Water Level Level (mL) (mL) 10.00 50.00 51.00 Volume of Solid* (cm3) 1.00 1st irregular solid 15.00 50.00 60.00 10.00 2nd irregular solid 20.00 50.00 55.00 5.00 Regular metal object 25.00 50.00 80.00 30.00 *Calculation for the volume of the solid should be shown in the calculation section. Graphs In chemistry, data is often displayed o x-y graphs. There are many components that are important to a complete graph. They are listed below. • Title - brief description of the information that the graph represents, often given in the form y versus x. • Axis Labels – identification of the variable represented by each axis and the unit. The xaxis represents the independent variable. The y-axis represents the dependent variable. • Numbered Axes – Indication of the magnitude of the measurements must be provided for each axis. The distance between two marks must always represent the same difference in numbers. That is, the y-axis markings could represent 5, 10, 15, 20 etc., but they could not represent 1, 4, 9, 16 etc because the distance markings changes. • Data Points • Curve or Line of Best Fit – There are two basic ways to determine the curve on a graph: connect the data points, point-to point, or draw the best approximation of a smooth curve through the midst of the data points (though not necessarily through each data point). Sometimes this approximated curve will take form of a straight line; other times it will be a curve. In chemistry, since the data points often represent experimental measurements, the approximation method is preferred. If the data point fall along an approximate line, the “Line of Best Fit” is drawn. If the points approximate a curve, a smooth “Curve of Best Fit” is drawn. 2 EXAMPLE: Examine the following graph. This graph shows the amount of a sample of the radioactive isotope carbon-14 remaining after a given time. A “Curve of Best Fits” has been drawn. Calculations All mathematical computations should be recorded in the lab reports no matter how insignificant and simple they may seem. This is important for future reference to a particular laboratory experiment. EXAMPLE: (This example is based on information from the data table.) 1. 2. Determine the volume of each solid. Volume of the solid = final water volume – original water volume a. Volume of the glass rod = 51.00 mL – 50.00 mL = 1.00 mL = 1.00 cm3 b. volume of 1st irregular solid = 60.00 – 50.00 mL = 10.00 mL = 10.00 cm3 c. etc. Determine the density of each solid. Density = mass volume a. Density of the glass rod = b. etc. 10.00 g 1.00 cm 3 3 = 10.0 g/cm 3 Questions Based on the data and calculations, you should be able to develop a plausible explanation for the phenomena observed during the experiment. Specific questions are asked that require you to draw on the concepts you have learned. All questions accompanying a lab experiment should be answered by making complete statements. In making your response make sure you are restating the question you are answering. It is not necessary to write the question as stated in you lab manual. Equations should be included anytime they will help to explain a particular situation. EXAMPLE WHAT EVIDENCE WAS THERE TO PROVE THAT THERE WAS A CHEMICAL REACTION BETWEEN CaCO3 and HCl? There was evidence of a chemical reaction in the experiment involving CaCO3 and HCl because a gas was produced. CaCO3 + HCl → CaCl2 + H2O + CO2 Conclusion One of the most important aspects of a laboratory report is the conclusion. The purpose of any lab exercise is to learn about some particular area of science. In drawing a conclusion from such an experiment you should look again at the purpose for performing this experiment and then decide whether or not you established the validity of this hypothesis. Did you really accomplish what you started out to; did you get accurate results; and where was your source of error? What improvements would you make if you were repeat the lab or do further study? Specific examples should be cited from the lab in your conclusion. Again the conclusion should be as brief as possible but yet contain all the necessary correlation between data, observations, and the original purpose. EXAMPLE: The purpose of this experiment was to discover the differences between physical and chemical changes. Many physical and chemical changes were observed while completing this laboratory experiment. A physical change is one that involves a change in state or matter without changing the chemical composition. Ice melting and water evaporating are physical changes (example from lab). A chemical change is one in which the atoms are rearranged to form substances that have chemical formulas that are different from that of the reactants. Chemical changes may be observed whenever heat is absorbed or given off. They are also evident when a new phase is produced such as a precipitate or a gas. The reaction of calcium carbonate and hydrochloric acid was a chemical change because it produced carbon dioxide gas (example from lab). Sources of error include . . . Improvements that could be made include . . . 4
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