Canadian Grain Commission 17. Corn Determination of dockage ........................................................................................... 17-2 Definitions ................................................................................................................ 17-2 Dockage not reported .............................................................................................. 17-2 Normal cleaning procedures: .................................................................................. 17-2 Composition of dockage .......................................................................................... 17-3 Estimating test weight of well-matured corn after drying ....................................... 17-4 Grading ......................................................................................................................... 17-5 Important definitions ................................................................................................ 17-5 Net weight of sample ............................................................................ 17-5 Hazardous substances in samples ........................................................ 17-5 Representative portions for grading ........................................................................ 17-5 Grading factors ........................................................................................................ 17-6 Blue-eye mould .................................................................................... 17-6 Caramelized kernels ............................................................................. 17-6 Classes ................................................................................................ 17-6 Contaminated grain .............................................................................. 17-6 Cracked corn and foreign material (CCFM) ........................................... 17-7 Damage (DMG) .................................................................................... 17-7 Earth pellets ......................................................................................... 17-7 Excreta (EXCR) .................................................................................... 17-8 Fertilizer pellets (FERT PLTS) .............................................................. 17-8 Fireburnt (FBNT) .................................................................................. 17-8 Foreign material (FM) ........................................................................... 17-8 Heated (HTD) ....................................................................................... 17-9 Odour (ODOR) ..................................................................................... 17-9 Rotted (ROT) ....................................................................................... 17-9 Stones (STNS) ................................................................................... 17-10 Treated seed and other chemical substances ...................................... 17-12 Varieties ............................................................................................ 17-12 Primary and export grade determinants table ........................................................ 17-13 Corn, Canada Western/Canada Eastern Yellow, White or Mixed (CW/CE) ......... 17-13 Export shipments ....................................................................................................... 17-14 Grading .................................................................................................................. 17-14 Cracked corn and foreign material (CCFM) .......................................................... 17-14 Official Grain Grading Guide Corn 17-1 August 1, 2016 Canadian Grain Commission Determination of dockage Definitions In Eastern Canada the terms of delivery or terms of a contract will determine if dockage is to be assessed. In Western Canada dockage may only be assessed on tough, damp, moist or wet corn. The CGC will only assess dockage upon request. Dockage is assessed to the nearest 0.1%. Once dockage material has been removed it will not be reintroduced to the sample to determine the grade. Cracked Corn and Foreign Material (CCFM) is a grading factor and will be assessed when determining the grade. Dockage is defined under the Canada Grain Act as “any material intermixed with a parcel of grain, other than kernels of grain of a standard of quality fixed by or under this Act for a grade of that grain that must and can be separated from the parcel of grain before that grade can be assigned to the grain.” Dockage is removed by following the cleaning procedures described in this section of the manual. The sample as it arrives is referred to as the uncleaned or dirty sample. Its weight is the gross weight of the sample. Dockage is assessed on the gross weight of the sample. Dockage not reported ▲ Important: Dockage is not reported when corn is graded • Corn, Sample CE Account Fireburnt • Corn, Sample Salvage • Corn, Sample Condemned Normal cleaning procedures: ▲ Important: Wear gloves and a mask to handle any sample which you suspect may contain hazardous substances. Assess dockage before assessing test weight. Procedures for normal cleaning of corn require • No. 12 round-hole hand sieve for corn with 25% moisture or less • No. 14 round-hole hand sieve for corn over 25% moisture 1. Using a Boerner-type divider, divide the uncleaned sample to obtain a representative portion. • Official samples shall be at least 1kg. • Unofficial samples shall be at least 1 kg. 2. Sieve approximately 250 g at a time on the appropriate hand sieve until all possible material has fallen through the sieve. 3. Handpick material remaining on top of the sieve as described under Composition of dockage. Official Grain Grading Guide Corn 17-2 August 1, 2016 Canadian Grain Commission Composition of dockage • All material which passes through the No. 12 or No. 14 round-hole sieve • All foreign material and pieces of cob handpicked from the sample, excluding stones Official Grain Grading Guide Corn 17-3 August 1, 2016 Canadian Grain Commission Estimating test weight of well-matured corn after drying Note: Test weight is determined on corn prior to removal of cracked corn and foreign material. When the Terms of Delivery or terms of a contract state that dockage can be deducted then test weight is determined after the removal of dockage. Corn samples that contain a high percentage of moisture typically show an increase in test weight after drying. Use the following table to predict the test weight of well-matured corn before drying. ▲ Important: This is only a guide, and works only with well matured corn. Samples should be checked yearly to ensure that the formula applies for that crop condition. Amount to add Moisture range kg/hl g/0.5 L 15.8 - 16.4 0.5 2.6 16.5 - 16.9 1.0 5.2 17.0 - 17.3 2.0 10.5 17.4 - 17.6 2.1 11.0 17.7 - 17.9 2.2 11.5 18.0 - 18.3 2.3 12.0 18.4 - 18.6 2.4 12.5 18.7 - 18.9 2.5 13.0 1. Find the moisture range for the test weight of the sample. 2. Add the amount for that moisture range in the appropriate units, either kg/hl or g/l. ▲ Important: Corn samples are not to be downgraded on the basis of an “estimated” test weight. Questionable samples must be dried by exposure and then have the test weight determined. For example, The moisture for the tested sample is 17.5%, and the test weight is in kg/hl. Amount to add Moisture range kg/hl g/0.5 L 17.4 - 17.6 2.1 11.0 Add 2.1 to the test weight in kg/hl. Official Grain Grading Guide Corn 17-4 August 1, 2016 Canadian Grain Commission Grading Important definitions Net weight of sample The sample after cleaning and removal of dockage is referred to as the cleaned sample. Its weight is the net weight of the sample. Percentages by weight for grading refer to percentages of the net weight. Hazardous substances in samples Wear gloves and a mask to handle any samples that you suspect may contain hazardous substances. Hazardous substances are defined in the Regulations as “any pesticide, herbicide, desiccant or inoculant.” Representative portions for grading All grading is done on representative portions divided down from the cleaned sample, using a Boerner-type divider. Values in the following table represent a range of recommended portions of samples for grading. Refer to definition of “Representative portion” in the glossary for a complete description of the terms “Minimum”, “Optimum” and “Export”. Representative portion of corn for grading, grams Grading factor Minimum Optimum Export Caramelized kernels 100 500 500 Classes 100 working sample working sample working sample working sample working sample Damage 100 500 500 Excreta working sample working sample working sample Fireburnt working sample working sample working sample 100 500 500 Odour working sample working sample working sample Stones 500 working sample working sample Cracked corn and foreign material Heated and rotted Official Grain Grading Guide Corn 17-5 August 1, 2016 Canadian Grain Commission Grading factors Blue-eye mould Germs of kernels appear dark blue with mould, or there may be just a visible mouldy blue streak under the hull of the germ. In the second case, peel back the hull from the germ to examine the germ. Blue-eye mould is included in the tolerance for Damage. Representative portion for analysis Minimum—100 g Optimum—500 g Export—500 g Caramelized kernels Caramelized kernels are kernels that were very immature when dried at a high temperature in a dryer, and the heat has turned the kernel to a scorched colour similar to that of heated kernels. The outer hull of the kernel may be peeled off showing a slightly damaged kernel inside. These kernels are classed as Damaged. Representative portion for analysis Minimum—100 g Optimum— 500 g Export— 500 g Classes Corn is classed as yellow, white, or mixed. The class forms part of the grade name; for example, Corn, Sample CW Yellow Account Heated. Samples of yellow and white corn containing less than 95.0% of one class are designated Mixed; for example, Corn No. 1 CE Mixed. Representative portion for analysis Minimum—100 g Optimum— working sample Export— working sample Contaminated grain ▲ Important: Wear gloves and a mask to handle any sample that is suspected of containing contaminated grain. Contaminated is defined in the “Canada Grain Act” as; “Contaminated means, in respect of grain, containing any substance in sufficient quantity that the grain is unfit for consumption by persons or animals or is adulterated within the meaning of the regulations made pursuant to sections B.01.046(1), B.15.001 and B.15.002(1) of the Food and Drugs Act.” Samples deemed to be contaminated by the Grain Research Laboratory in consultation with the Chief Grain Inspector for Canada are graded Corn, Sample Condemned. Official Grain Grading Guide Corn 17-6 August 1, 2016 Canadian Grain Commission Cracked corn and foreign material (CCFM) Cracked corn and foreign material includes any of the following: • All material including kernels and pieces of kernels of corn or any other grains which pass through a No. 12 round-hole sieve or, for samples with a moisture level over 25.0%, through the No. 14 round-hole sieve • All foreign material other than stones handpicked from the sample, including pieces of cobs that were not removed by sieving Representative portion for analysis Minimum—working Optimum— working sample sample Export— working sample Procedures ▲ Important: Follow procedures for assessing dockage. Note: Because breakage occurs during handling at terminal elevators, round down percentages by weight of CCFM to the nearest whole number on all officially sampled and inspected domestic or export shipments from a terminal elevator. For example, a sample containing 4.7% CCFM by weight is recorded as containing 4.0% CCFM for grading purposes only on officially sampled and inspected shipments from a terminal elevator. Damage (DMG) Damaged kernels include whole kernels or pieces of kernels which are • Affected by blue-eye mould and other types of moulds • Sprouted • Ground-damaged • Weathered • Diseased • Frosted • Scorched, from a drier • Heated, naturally, or from a drier, or caramelized • Rotted Representative portion for analysis Minimum—100 g Optimum—500 g Export—500 g Earth pellets • • Hard earth pellets are pellets that do not crumble under light pressure. See Stones. Soft earth pellets are pellets that crumble under light pressure. See Cracked corn and foreign material. Official Grain Grading Guide Corn 17-7 August 1, 2016 Canadian Grain Commission Excreta (EXCR) ▲ Important: Wear gloves and a mask to handle any samples that you suspect may contain excreta. Representative portion for analysis Minimum—working Optimum— working sample sample Export— working sample Fertilizer pellets (FERT PLTS) Fertilizer pellets are a manufactured plant nutrient product used by producers in the production of grain. They are typically small, round or irregular shaped and usually white, grey, brown, pink or reddish in colour. Note: Canadian Grain Commission personnel should refer to ISO national work instruction “Suspect Contaminated Grain, Handling Procedures” for procedures to be followed when handling samples containing fertilizer pellets. Representative portion for analysis Minimum—working Optimum—working sample sample Export—working sample Procedures • Handpick any fertilizer pellets and determine the concentration basis the net working sample. • Fertilizer pellets are assessed as stones when the concentration does not exceed 1.0% of the net sample weight. • Samples containing fertilizer pellets in excess of 1.0% of the net sample weight are graded Corn, Held IP Suspect Contaminated Grain. Fireburnt (FBNT) Fireburnt kernels are kernels charred or scorched by fire. A cross-section of a fireburnt kernel resembles charcoal with numerous air holes. The air holes result in a low weight kernel which crumbles easily under pressure. Representative portion for analysis Minimum—working Optimum— working sample sample Export— working sample Procedures Samples of corn containing fireburnt kernels are graded Corn, Sample CW/CE (class) Account /Fireburnt. Foreign material (FM) See Cracked corn and foreign material (CCFM). Official Grain Grading Guide Corn 17-8 August 1, 2016 Canadian Grain Commission Heated (HTD) Heated kernels have at least one of the following characteristics: • Whole kernels or pieces of kernels which range in colour from amber to dark brown over the entire kernel • Kernels which are totally discoloured by fermentation and show no natural colour on the crowns or dorsals, or both • The germ of the kernel is amber to dark brown and is severely puffed in the germ area when heated in a drier • Heated seeds of other grains are included in the tolerance for Heated If kernels exhibit none of the above characteristics, but are not whole or sound, they are classed as Damaged. Note: Cracked corn and foreign material that is heated is included with heated corn for grade assessment. Representative portion for analysis Minimum—100 g Optimum—500 g Export—500 g Odour (ODOR) There is no numeric tolerance for odour. Consider • The basic quality of the sample • The type and degree of the odour • The presence of visible residue causing the odour Grains grading No. 1 through 4 must be cool and sweet. Corn grading No. 5 may have a slight odour associated with the low quality, but the odour cannot be sour or musty. Representative portion for analysis Minimum—working Optimum— working sample sample If odour is the grade determinant and there is . . . Export— working sample Then the grade is . . . An excessive objectionable odour not associated with the quality of the grain, but not heated or fireburnt Corn, Sample CW/CE Account Odour An excessive heated odour Corn, Sample CW/CE Account Heated An excessive fireburnt odour Corn, Sample CW/CE Account Fireburnt Rotted (ROT) Rotted kernels are whole kernels or pieces of kernels which are visibly in advanced stages of decomposition and feel spongy under pressure. Rotted kernels are included in the percentage of heated kernels for grade assessment. Representative portion for analysis Minimum—100 g Optimum—500 g Official Grain Grading Guide Corn 17-9 Export—500 g August 1, 2016 Canadian Grain Commission Stones (STNS) Stones are hard shale, coal, hard earth pellets, and any other non toxic materials of similar consistency. Fertilizer pellets are assessed as stones when constituting 1.0% or less of the net sample weight. (See Fertilizer pellets for specific procedures to be followed when samples contain fertilizer pellets.) Representative portion for analysis Minimum—500 g Optimum—1000 g Export—1000 g Procedures 1. Handpick stones from a representative portion of the cleaned sample. 2. Determine stone concentration in the net sample. • • • In western Canada samples of grain containing stones in excess of “basic grade” tolerances, up to 2.5% are graded Corn, Rejected “basic grade” Account Stones. The “basic grade” refers to a grade established in the Canada Grain Regulations (grades listed in the first column in grade determinant tables) that would have been assigned to the sample if it contained no stones. In eastern Canada samples of grain containing stones in excess of grade tolerances are degraded to lower grades. Samples containing stones in excess of the tolerance of the lowest grade established by regulation up to 2.5% are graded Corn, Sample CE (class) Account Stones. In western and eastern Canada grain containing more than 2.5% stones is graded Corn, Sample Salvage. Official Grain Grading Guide Corn 17-10 August 1, 2016 Canadian Grain Commission Examples: Western Canada Excerpt from grade determinant tables for Corn, Canada Western, White, Yellow or Mixed Grade name Stones % No. 1 CW 0.15 No. 2 CW 0.15 No. 3 CW 0.15 No. 4 CW 0.15 No. 5 CW 0.15 Basic grade:......................... Corn, No. 2 CW Yellow Reason for basic grade: ....... 3.0% Cracked corn and foreign material If the above sample contained Grade in Western Canada 0.5% stones Corn, Rejected No. 2 CW Yellow Account Stones 3.0% stones Corn, Sample Salvage Examples: Eastern Canada Excerpt from grade determinants table for Corn, Canada Eastern, White, Yellow or Mixed Grade name Stones % No. 1 CE 0.15 No. 2 CE 0.15 No. 3 CE 0.15 No. 4 CE 0.15 No. 5 CE 0.15 Basic grade:......................... Corn, No. 2 CE Yellow Reason for basic grade: ....... 3.0% Cracked corn and foreign material Official Grain Grading Guide Corn If the above sample contained Grade in Eastern Canada 0.5% stones Corn, Sample CE Yellow Account Stones 3.0% stones Corn, Sample Salvage 17-11 August 1, 2016 Canadian Grain Commission Treated seed and other chemical substances Treated seed Treated seed is grain that has been coated with an agricultural chemical for agronomic purposes. These seed dressings contain a dye to render the treated seed visually conspicuous. The colour of the dye varies depending upon the type of treatment and the type of grain. The current Canadian colour standards for pesticide seed treatments are: cereals–pink or red, canola–baby blue or green. Seed treated with an inoculant may have a green stain. The coatings or stains may appear greasy or powdery and surface area distribution ranges from tiny flecks to complete coverage. Other chemical substances Other chemical substances refers to any chemical residues either adhering to the kernel or remaining in the sample and to samples having a chemical odour of any kind. ▲ Important: Wear gloves and a mask to handle any samples that you suspect may contain contaminated grain. Representative portion for analysis Minimum—working Optimum—working sample sample Export—working sample If a sample is suspected of being coated with a pesticide, desiccant, inoculant or if the sample contains evidence of any foreign chemical substance other than fertilizer pellets, the sample shall be graded Corn, Held IP Suspect Contaminated Grain. Note: Canadian Grain Commission personnel should refer to ISO national work instruction “Suspect Contaminated Grain, Handling Procedures” for specific procedures to be followed when handling samples suspected of containing treated seed or other chemical substances. Varieties Corn is graded without reference to variety. Official Grain Grading Guide Corn 17-12 August 1, 2016 Canadian Grain Commission Primary and export grade determinants table Corn, Canada Western/Canada Eastern Yellow, White or Mixed (CW/CE) Standard of quality Grade name Minimum test weight kg/hL (g/0.5 L) Degree of soundness Damage Foreign material Heated % Total % Stones % Excreta % Total Cracked corn and foreign material % Other classes % No. 1 CW/CE 68 (343) Cool and sweet, uniform size 0.1 3 0.15 0.02 2 5 No. 2 CW/CE 66 (333) Cool and sweet 0.2 5 0.15 0.02 3 5 No. 3 CW/CE 64 (322) Cool and sweet 0.5 7 0.15 0.02 5 5 No. 4 CW/CE 62 (311) Cool and sweet 1 10 0.15 0.02 7 5 No. 5 CW/CE 58 (291) May have a slight odour, not sour or musty 3 15 0.15 0.02 12 5 Grade, if No. 5 specs not met Corn, Sample CW/CE (class) Account Light Weight Corn, Sample CW/CE (class) Account Heated Corn, Sample CW/CE (class) Account Damaged 2.5% or less—Corn, Corn, Sample CW/CE Rejected (grade) (class) (class) Account Account Stones or Corn, Excreta Sample CE (class) Account Stones Over 2.5%—Corn, Sample Salvage 50% or less – Corn Sample CW/CE (class) Account CCFM Over 50% - sample Cracked Corn and Foreign Material Over 5%—Use all other grading criteria and grade as Corn (grade) Mixed Note: The colour is added to the grade name. Official Grain Grading Guide Corn 17-13 August 1, 2016 Canadian Grain Commission Export shipments Grading Corn on export is graded in accordance with primary grade standards and specifications. Cracked corn and foreign material (CCFM) Because breakage occurs during handling at terminal elevators, round down percentages by weight of CCFM to the nearest whole number on all officially sampled and inspected domestic or export shipments from a terminal elevator. For example, a sample containing 4.7% CCFM by weight is recorded as containing 4.0% CCFM for grading purposes only on officially sampled and inspected shipments from a terminal elevator. Official Grain Grading Guide Corn 17-14 August 1, 2016
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