2015 Laboratory Results: As shown in our most recent independent laboratory results (enclosed), Dowser Spring Water meets all applicable Federal and New York State health standards (NYS Dept of Health Certificate #135). The FDA regulates bottled water as a food product while the EPA regulates tap water as provided by water utilities. Standards of quality enacted by the FDA for bottled water must be as protective of the public health as EPA's standards (known as Maximum Contaminant Levels) for tap water. Ensuring the safety of the spring water is Dowser's primary objective in providing our product to the consumer. OUR SOURCES FOR OUR WATER Dowser's bottling facilities use protected springs as the source of our water--specifically, those located at Shawangunk Bulk Spring Water in Pine Bush, NY (NYS Dept of Health Certificate #232). These springs bring water to the surface from aquifers far below the surface. The water in these aquifers begins as rain and snow higher up in the mountains and it remains underground until we bring it to the surface. Layers of solid rock and clay provide an impervious (not-passable) protective cover for the aquifer water. This source water is completely safe to drink -- right at the springhead. We test our sources regularly to verify that they are of extremely high quality...and that they remain suitable for bottled water. HOW BOTTLED WATER IS PREPARED Dowser Spring Water is protected by a multi-barrier approach during its journey to our customers. These barriers include steps such as source protection and monitoring, and treatment such as one micron filtration, ozonation, the application of ultraviolet light or other appropriate processing measures. By law, all bottled water products labeled as spring water, well water, artesian water, and mineral water must come from protected sources which are monitored frequently. Some bottled waters may also come from treated municipal supplies; however, Dowser does not. Dowser is a natural spring water as defined by law. Regardless of their source, all United States water bottlers must employ processing methods such as reverse osmosis, micron filtration, distillation and/or ozonation to remove any chemical and microbiological contaminants, including Cryptosporidium, from their product. For our Distilled Water, the water is heated to produce steam. The minerals are left behind and the steam is condensed for a pure, mineral-free distilled product. All of our bottled water products are ozonated. We use ozone instead of chlorine because it leaves no residual, and it does not cause a taste and odor problem. Ozone is oxygen (O3 to be exact) which is bubbled through the water just before it goes into a clean, sanitized bottle. Within a few hours after the bottle has been filled and capped, the ozone dissipates or converts back to the same form of oxygen that we breathe (O2). DOWSER'S WATER TESTING: As required by law, our company regularly tests for organic, radiological, and inorganic constituents that are regulated by the FDA. No contaminant was detected above FDA's limits in third-party testing as demonstrated by our most recent independent lab results for 2015. There have been no Dowser violations of any FDA or New York State Standard of Quality. Unlike municipal waters, Dowser bottled water is not allowed to "average out" any test results that are not (in each and every instance) in full compliance with the regulations. To assist you in reading the attached laboratory analysis the following explanations may be of help: MDL or DL stands for minimum detection limit and is a measure of the sensitivity of the analytical methods used by the lab for the substances under examination--a variant of this will be RL, or Reporting Level. mg/L stands for milligrams per liter and means parts per million (e.g., 7 mg/L translates to 7 parts per million, and 0.007 mg/L translates to 7 parts per billion). MCL means Maximum (allowable) Contamination Level and is the legal limit established by the FDA (and EPA) above which bottled water may not contain any regulated substance. More properly, since bottled water is regulated as a food product, the FDA term, SOQ (Standard of Quality) should apply to bottled water analyses rather than the EPA term, MCL. In one of those instances in which the FDA regulates bottled water more stringently than the EPA regulates tap water, the SOQ for lead in bottled water is 5 parts per billion; tap water has an MCL "action level" for lead of 15 parts per billion. If you have any questions about the enclosed analytical results you may contact Dowser directly at (800)724-1084. We will be pleased to speak with you about the many ways in which we ensure the quality of Dowser's products. Yours truly, Glenn Barnes General Manager encl. 2015 Laboratory Analysis from Compliance Designs Compliance Designs CLIENT: Dowser, LLC 1 Pepsi Way Newburgh, NY 12550 NOTE: “*” “ND” “MCL” “RL” Units Quarter 1, 2015 010-043 514398 indicates that maximum levels have been exceeded, or in the case of pH, is either too high or too low indicates that none of this analyte has been detected at or above the specified detection level indicates maximum contaminant level as established by US FDA for bottled water indicates laboratory reporting limit for method results are reported in mg/L unless other wise noted ANALYSIS PERFORMED Primary Inorganics Antimony Arsenic Asbestos Barium Beryllium Cadmium Chromium Cyanide Fluoride Lead Mercury Nickel Nitrogen, Nitrate Nitrogen, Nitrite Nitrogen - NO3/NO2 (NOX) Selenium Thallium Secondary Inorganics Alkalinity Aluminum Bicarbonate Boron Bromide Calcium Carbonate Chloride Copper Corrosivity Foaming Agents Hardness, Calcium Hardness, Total Hydroxide Iron Magnesium Manganese Orthophosphate pH Phenol Potassium Silver Sodium Specific Conductance Sulfate TDS Zinc DATE OF REPORT: REPORT #: LABORATORY ID#: MCL1 (mg/L) 0.006 0.01 7 MFL 2 0.004 0.005 0.1 0.2 See endnote2 0.005 0.002 0.1 10 1.0 10 0.05 0.002 -0.2 -----2503 1 -----0.33 -0.053 -See endnote4 0.001 -0.1 --- umho/cm 250 5003,5 53 RL (mg/L) SPRING FINISHED PRODUCT (Produced from Shawangunk Spring, 5 Gallon, L1) 010-043 (mg/L) 0.001 0.002 0.2 0.002 0.001 0.0005 0.005 0.025 0.05 0.0005 0.0002 0.005 0.1 0.05 0.1 0.005 0.001 ND ND ND 0.017 ND ND ND ND ND ND ND ND 0.58 ND 0.58 ND ND 2 0.02 2 0.05 0.005 1 2 0.5 0.002 -14 0.05 5 3 2 0.02 0.1 0.002 0.01 0.1 0.001 1 0.0005 1 2 0.5 10 0.02 36 0.048 44 ND 0.0087 14 ND 16 ND -1.6 ND 35 48 ND 0.027 3.1 ND ND 7.1 ND ND ND 11 150 9.2 96 ND 159 South Stark Highway, The Governor Wentworth Building, Weare, New Hampshire 03281 Phone: (603) 529-4977 / Fax: (603) 529-4988 Page 2 of 6 ANALYSIS PERFORMED MCL (mg/L) RL (mg/L) SPRING FINISHED PRODUCT (Produced from Shawangunk Spring, 5 Gallon, L1) 010-043 (mg/L) Physical Color Odor Turbidity 153 CU 33 TON 5 NTU 3 1 0.05 ND 1.0 0.54 Microbiological Total Coliform E. Coli. Standard Plate Count Absence Absence -- cfu/mL 1.1 1.1 1 ND ND ND Radiologicals Gross Alpha Gross Beta Radium 226/228 Uranium 15 pCi/L 50 pCi/L5 5 pCi/L 0.030 3 3 0.7 / 0.23 0.001 Volatile Organic Compounds EPA 524.2: Total Trihalomethanes tert-Amyl Methyl Ether (TAME) tert-Butyl-Ethyl Ether (TBEE) Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethylene cis-1,2-Dichloroethylene trans-1,2-Dichloroethylene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene 0.080 --0.005 --------0.005 0.1 -------0.6 -0.075 --0.005 0.007 0.07 0.1 0.005 ------ 0.0005 0.003 0.003 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 ND ND ND / ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Page 3 of 6 ANALYSIS PERFORMED MCL (mg/L) RL (mg/L) SPRING FINISHED PRODUCT (Produced from Shawangunk Spring, 5 Gallon, L1) 010-043 (mg/L) EPA 524.2 continued: Di-Isopropyl Ether Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene 4-Methyl-2-Pentanone (MIBK) Methyl tert-Butyl Ether (MTBE) Methyl Ethyl Ketone (MEK) Methylene Chloride Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethylene Trichlorofluoromethane Trichlorotrifluoroethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Chloride m+p-Xylenes ortho-Xylene Total Xylene -0.7 ------0.005 --0.1 --0.005 1 -0.07 0.2 0.005 0.005 -----0.002 --10 0.003 0.0005 0.0005 0.0005 0.0005 0.005 0.0005 0.005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0003 0.0005 0.0005 0.0005 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Add'l Organics EPA 551.1: Ethylene Dibromide Dibromochloropropane 0.00005 0.0002 0.00001 0.00001 ND ND EPA 505: Alachlor Aldrin Chlordane (alpha and gamma) Dieldrin Endrin Heptachlor Heptachlor Epoxide Lindane Methoxychlor Total PCBs PCB 1016 PCB 1221 PCB 1232 PCB 1242 PCB 1248 PCB 1254 PCB 1260 Toxaphene 0.002 -0.002 -0.002 0.0004 0.0002 0.0002 0.04 0.0005 -------0.003 0.0001 0.00001 0.0001 0.00001 0.00001 0.00001 0.00001 0.00001 0.00005 0.0001 0.00008 0.0001 0.0001 0.0001 0.0001 0.0001 0.0001 0.0005 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Page 4 of 6 ANALYSIS PERFORMED MCL (mg/L) RL (mg/L) SPRING FINISHED PRODUCT (Produced from Shawangunk Spring, 5 Gallon, L1) 010-043 (mg/L) EPA 515.4: Acifluorfen Bentazon 2,4-D 2,4-DB Dalapon DCPA (total Mono & Di acid degradate) Dicamba 3,5-Dichlorobenzoic Acid Dichlorprop Dinoseb Pentachlorophenol Picloram 2,4,5-T 2,4,5-TP (Silvex) --0.07 -0.2 ----0.007 0.001 0.5 -0.05 0.0002 0.0005 0.0001 0.002 0.001 0.0001 0.0001 0.0005 0.0005 0.0002 0.00004 0.0001 0.0002 0.0002 ND ND ND ND ND ND ND ND ND ND ND ND ND ND EPA 525.2: Acenaphthene Acenaphthylene Acetochlor Alpha-BHC Anthracene Atrazine Benz(a)Anthracene Benzo(a)Pyrene Benzo(b)Fluoranthene Benzo(g,h,i)Perylene Benzo(k)Fluoranthene Beta-BHC Bromacil Butylbenzylphthalate Butachlor Caffeine Chlordane (alpha) Chlordane (gamma) Chlorobenzilate Chloroneb Chlorothalonil Chlorpyrifos Chrysene Delta-BHC 4,4-DDD 4,4-DDE 4,4-DDT Diazinon (Qualitative) Dichlorvos (DDVP) Dieldrin Di(2-ethylhexyl)Adipate Dibenz(a,h)Anthracene Di(2-ethylhexyl)Phthalate Diethylphthalate Dimethylphthalate Dimethoate Di-n-Butylphthalate Di-n-Octylphthalate -----0.003 -0.0002 --------0.002 0.002 ------------0.4 -0.006 ------ 0.0001 0.0001 0.0001 0.0001 0.00002 0.00005 0.00005 0.00002 0.00002 0.00005 0.00002 0.0001 0.0002 0.0005 0.00005 0.00005 0.00005 0.00005 0.0001 0.0001 0.0001 0.00005 0.00002 0.0001 0.0001 0.0001 0.0001 0.0001 0.00005 0.0002 0.0006 0.00005 0.0006 0.0005 0.0005 0.0001 0.001 0.0001 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Page 5 of 6 MCL (mg/L) ANALYSIS PERFORMED RL (mg/L) SPRING FINISHED PRODUCT (Produced from Shawangunk Spring, 5 Gallon, L1) 010-043 (mg/L) EPA 525.2 continued: 2,4-Dinitrotoluene 2,6-Dinitrotoluene Endosulfan I (Alpha) Endosulfan II (Beta) Endosulfan Sulfate Endrin Aldehyde EPTC Fluoranthene Fluorene Heptachlor Hexachlorobenzene Hexachlorocyclopentadiene Indeno(1,2,3-cd)Pyrene Isophorone Malathion Metolachlor Metribuzin Molinate Naphthalene trans-Nonachlor Parathion Pendimethalin Permethrin Phenanthrene Propachlor Pyrene Simazine Terbacil Terbuthylazine Thiobencarb Trifluralin ---------0.0004 0.001 0.05 --------------0.004 ----- 0.0001 0.0001 0.0001 0.0001 0.0001 0.0001 0.0001 0.0001 0.00005 0.00003 0.00005 0.00005 0.00005 0.0005 0.0001 0.00005 0.00005 0.0001 0.0003 0.00005 0.0001 0.0001 0.0001 0.00004 0.00005 0.00005 0.00005 0.0001 0.0001 0.0002 0.0001 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND EPA 531.2: Aldicarb (TEMIK) Aldicarb sulfone Aldicarb sulfoxide Baygon (PROPOXUR) Carbaryl Carbofuran (FURADAN) 3-Hydroxycarbofuran Methiocarb Methomyl Oxamyl (VYDATE) -----0.04 ---0.2 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 ND ND ND ND ND ND ND ND ND ND EPA 547: Glyphosate 0.7 0.006 ND EPA 548.1: Endothall 0.1 0.005 ND EPA 549.2: Diquat Paraquat 0.02 -- 0.0004 0.002 ND ND Page 6 of 6 MCL (mg/L) ANALYSIS PERFORMED EPA 1613: 2,3,7,8-TCDD (DIOXIN) RL (mg/L) SPRING FINISHED PRODUCT (Produced from Shawangunk Spring, 5 Gallon, L1) 010-043 (mg/L) 3x10-8 5.0x10-9 ND Disinfection Byproducts EPA 317: Bromate EPA 300.1B: Chlorite 0.010 0.005 ND 1.0 0.01 ND EPA 6251B: Bromochloroacetic acid Dibromoacetic acid Dichloroacetic acid Monobromoacetic acid Monochloroacetic acid Trichloroacetic acid Haloacetic Acids, Total ------0.060 0.001 0.001 0.001 0.001 0.002 0.001 0.002 ND ND ND ND ND ND ND EPA 524.2: Total Trihalomethanes Bromodichloromethane Bromoform Chloroform Chlorodibromomethane 0.080 ----- 0.0005 0.0005 0.0005 0.0005 0.0005 ND ND ND ND ND Residual Disinfectants SM4500-CL G: Residual Chlorine, Free Residual Chlorine, Total Chloramines -4.0 4.0 0.1 0.1 0.1 ND ND ND 0.8 0.24 ND SM4500-CIO2-D: Chlorine Dioxide EPA approved methods were used in all of the analyses and a listing is available upon request. These test results may be used for compliance purposes as required. The EPA, some State agencies and/or the IBWA may have established alternate MCLs for some of these analytes. Please refer to Federal, State and Industry codes. Fluoride MCL is determined by annual average of maximum daily air temperatures where the bottled water is sold. Refer to tables found in 21 CFR 165. 3 Mineral water is exempt from allowable levels per 21 CFR 165.110(b)(3) and (4). The exemptions are aesthetically based allowable levels and do not relate to a health concern. 4 MCL established by US FDA for waters that meet the US FDA definition of “Purified” is 5-7 pH Units per the USP XXIII Standards, as referenced in 21 CFR 165. 5 The bottled water shall not contain beta particle and photon radioactivity from man-made radionuclides in excess of that which would produce an annual dose equivalent to the total body or any internal organ of 4 millirems per year calculated on the basis of an intake of 2 liters of the water per day (= 50 pCi/L). 1 2 750 Royal Oaks Drive, Suite 100 Monrovia, California 91016-3629 Tel: (626) 386-1100 Fax: (626) 386-1101 1 800 566 LABS (1 800 566 5227) Laboratory Report for Dowser, LLC 1 Pepsi Way Newburgh, NY 12550 Attention: (010) Water Quality Manager Date of Issue 03/06/2015 EUROFINS EATON ANALYTICAL LXG: Linda Geddes Report: 514398 Project: 010-DOW Group: Finished Product Project Manager * Accredited in accordance with TNI 2009 and ISO/IEC 17025:2005. * Laboratory certifies that the test results meet all TNI 2009 and ISO/IEC 17025:2005 requirements unless noted under the individual analysis. * Following the cover page are State Certification List, ISO 17025 Accredited Method List, Acknowledgement of Samples Received, Comments, Hits Report, Data Report, QC Summary, QC Report and Regulatory Forms, as applicable. * Test results relate only to the sample(s) tested. Page 1 of 39 pages STATE CERTIFICATION LIST State Certification Number State Certification Number Alabama 41060 Mississippi Certified Alaska CA00006 Montana Cert 0035 Arizona AZ0778 Nebraska Certified Arkansas Certified Nevada CA00006-2014-1 California-MonroviaELAP 2813 New Hampshire * 2959 California-Colton- ELAP 2812 New Jersey * CA 008 California-Folsom- ELAP 2820 New Mexico Certified Colorado Certified New York * 11320 Connecticut PH-0107 North Carolina 06701 Delaware CA 006 North Dakota R-009 Florida * E871024 Oregon (Primary AB) * ORELAP 4034 Georgia 947 Pennsylvania * 68-565 Guam 14-003r Rhode Island LAO00326 Hawaii Certified South Carolina 87016 Idaho Certified South Dakota Certified Illinois * 200033 Tennessee TN02839 Indiana C-CA-01 Texas * T104704230-14-7 Kansas * E-10268 Utah * CA000062014-7 Kentucky 90107 Vermont VT0114 Louisiana * LA140009 Virginia * 460260 Maine CA0006 Washington C838 Maryland 224 West Virginia 9943 C Commonwealth of Northern Marianas Is. MP0004 Wisconsin 998316660 Massachusetts M-CA006 Wyoming 8TMS-L Michigan 9906 EPA Region 5 Certified Los Angeles County Sanitation Districts 10264 * NELAP/TNI Recognized Accreditation Bodies Page 2 of 39 pages ISO 17025 Accredited Method List The tests listed below are accredited and meet the requirements of ISO 17025 as verified by the ANSI-ASQ National Accreditation Board/ACLASS. Refer to Certificate and scope of accreditation (AT 1807) found at: http://www.eatonanalytical.com SPECIFIC TESTS 1,4-Dioxane 2,3,7,8-TCDD Acrylamide Alkalinity Ammonia Ammonia Anions and DBPs by IC Anions and DBPs by IC Asbestos Bicarbonate Alkalinity as HCO3 METHOD OR TECHNIQUE USED EPA 522 Modified EPA 1613B In House Method SM 2320B EPA 350.1 SM 4500-NH3 H (18th) EPA 300.0 EPA 300.1 EPA 100.2 SM 2330B BOD / CBOD Drinking Water x x x x x x x x Food & Beverage x x x x x x x x Waste Water x x x SM 5210B SPECIFIC TESTS Hormones Hydroxide as OH Calc. x x x x x Kjeldahl Nitrogen Mercury Metals Microcystin LR NDMA Nitrate/Nitrite Nitrogen OCL, Pesticides/PCB Ortho Phosphate Ortho Phosphate and Total Phosphorous Ortho Phosphorous Oxyhalides Disinfection Byproducts Perchlorate Perchlorate In House Method x x Carbamates EPA 531.2 x x Carbonate as CO3 Carbonyls SM 2330B EPA 556 x x x x x x Perfluorinated Alkyl Acids x pH pH Bromate COD EPA 410.4 / SM 5220D x x x x x x x x x x x x x x SM 4500P E x x EPA 317.0 x x EPA 331.0 EPA 314.0 x x x x x EPA 539 SM 2330B EPA 351.2 EPA 245.1 EPA 200.7 / 200.8 ELISA EPA 521 EPA 353.2 EPA 505 EPA 365.1 x EPA 365.1/SM 4500-P E x In House Method x x Pseudomonas IDEXX Pseudalert x x Radium-226 RA-226 GA x x RA-228 GA SM 7500RN x x x x Residue, Filterable SM 2540C x x x Residue, Non-filterable Residue, Total Residue, Volatile SM 2540D SM 2540B EPA 160.4 x x x x EPA 555 x x Chlorine Dioxide SM 4500-CLO2 D x x SM 4500-Cl G x x x EPA 120.1 SM 2510B x x x x Radium-228 Radon-222 x SM 2330B x SM 4500-CN G SM 4500CN F EPA 335.4 x x x x x In House Method x x Semi-VOC EPA 525.2 x x EPA 549.2 SM 6251B SM 4500-O G (MTF/EC+MUG) x x x x x Semi-VOC Silica Silica Sulfide EPA 625 SM 4500-Si D SM 4500-SiO2 C x x x x x E. Coli CFR 141.21(f)(6)(i) E. Coli SM 9223 x x x x Sulfite x Surfactants SM 4500-S= D x x x x x SM 9221B.1/ SM 9221F x x Taste and Odor Analytes SM 6040E x x SM 9223B x x SM 9221 A, B x x EDB/DCBP EPA 504.1 x SM 9221 A, B, C x x EPA 551.1 In House Method x x x x Colisure SM 9221B x x x Total Coliform Total Coliform (Enumeration) Total Coliform / E. coli Total Coliform Total Coliform with Chlorine Present Total Coliform / E.coli TOC EPA 548.1 x Enterococci Fecal Coliform SM 9230B SM 9221 E (MTF/EC) x x Fecal Coliform SM 9221C, E (MTF/EC) Fecal Coliform (Enumeration) Fecal Coliform with Chlorine Present Fecal Streptococci Fluoride Glyphosate Gross Alpha/Beta HAAs/ Dalapon Hardness Heterotrophic Bacteria Heterotrophic Bacteria Hexavalent Chromium Hexavalent Chromium Hexavalent Chromium SM 9221E (MTF/EC) x x SM 3500-Cr B or C (20th) x x x x x x x x x x x x x x x x x x x x SM 9221B x x x TOC/DOC SM 5310C x x TOX SM 5320B x Total Phenols EPA 420.1 x x Total Phenols Total Phosphorous Turbidity Turbidity Uranium by ICP/MS UV 254 VOC VOC VOC VOC Yeast and Mold x SM 9221E SM 9230B SM 4500-F C EPA 547 EPA 900.0 EPA 552.3 SM 2340B In House Method SM 9215 B EPA 218.6 EPA 218.7 x SM 9223 SM 5310C x x x x x x x x x x E. Coli (Enumeration) Endothall x SM 4500-SO3B SM 5540C E. Coli (Enumeration) EDB/DBCP and DBP EDTA and NTA x Phenylurea Pesticides/ Herbicides Chlorinated Acids x x x x x x x x x x Corrosivity (Langelier Index) Waste Water x x x Cyanide, Amenable Cyanide, Free Cyanide, Total Cyanogen Chloride (screen) Diquat and Paraquat DBP/HAA Dissolved Oxygen E. Coli Food & Beverage x x EPA 537 SM 4500-CL G EPA 515.4 Conductivity Conductivity Drinking Water x x EPA 150.1 SM 4500-H+B Chloramines Chlorinated Acids Chlorine -Total/Free/ Combined Residual METHOD OR TECHNIQUE USED EPA 420.4 SM 4500 P F EPA 180.1 SM 2130B EPA 200.8 SM 5910B EPA 524.2/EPA 524.3 EPA 624 EPA SW 846 8260 In House Method SM 9610 x x x x x x x x x x x x x x x x x x x x x x x x x x 750 Royal Oaks Dr., Ste 100, Monrovia, CA 91016 Tel (626) 386-1100 Fax (626) 386-1101 http://www.EatonAnalytical.com Version 002. Issued: 06/03/2014 Page 3 of 39 pages Acknowledgement of Samples Received Addr: Dowser, LLC 1 Pepsi Way Newburgh, NY 12550 Client ID: Folder #: Project: Sample Group: Attn: (010) Water Quality Manager Phone: CDI 514398 010-DOW Finished Product Project Manager: Linda Geddes Phone: (626) 386-1163 The following samples were received from you on January 29, 2015 at 1150. They have been scheduled for the tests listed below each sample. If this information is incorrect, please contact your service representative. Thank you for using Eurofins Eaton Analytical. Sample # Sample ID Sample Date 201501050135 010-043 Spring Finished Product 01/28/2015 1030 Well ID: 1 Static ID: Shawangunk Spring Prod Code: 0847 012615 201501050134 size: 5 Gallon @505 @515.4 @525 @531 @549 @551SODA @ANIONS28 @ANIONS48 @DBP_28 @ICP @ICPMS @VOA Alkalinity in CaCO3 units Apparent Color Bicarb.Alkalinity as HCO3,calc Calcium Hardness as CACO3 Carbonate as CO3, Calculated Cyanide Endothall Fluoride Glyphosate Hydroxide as OH, Calculated Langelier Index - 25 degree Mercury Odor at 60 C (TON) Orthophosphate as P (OPO4) PH (H3=past HT not compliant) pH of CaCO3 saturation(25C) Phenolic Compounds-low level Specific Conductance Surfactants Total Dissolved Solid (TDS) Total Hardness as CaCO3 by ICP Turbidity @900 @ICPMS @HAA Chloramines Chlorine Dioxide Free Chlorine Residual Total Chlorine Residual @2378-TCDD_Dioxin @COLI10 @R226EDD by SM7500-Ra B @R228EDD by SM7500-Ra D Asbestos by TEM - >10 microns Heterotrophic Plate Count 01/28/2015 1030 Trip Blanks @VOASDWA TB 201502110448 02/10/2015 0700 010-043 Spring Finished Product Well ID: 1 Static ID: Shawangunk Spring Prod Code: 0846 01 2615 @DBP_14 size: 3 Gallon Bromate by UV/VIS Freight - Retest Test Description @505 -- Organochlorine Pesticides/PCBs @515.4 -- Chlorophenoxy Herbicides @525 -- Semivolatiles by GCMS @531 -- Aldicarbs @549 -- Diquat and Paraquat @551SODA -- EDB/DBCP/HAN by EPA 551.1 Reported: 03/06/2015 Page 1 of 2 750 Royal Oaks Drive, Suite 100, Monrovia, CA 91016 Tel (626) 386-1100 Fax (626) 386-1101 http://www.EatonAnalytical.com Page 4 of 39 pages Acknowledgement of Samples Received Addr: Dowser, LLC 1 Pepsi Way Newburgh, NY 12550 Client ID: Folder #: Project: Sample Group: Attn: (010) Water Quality Manager Phone: CDI 514398 010-DOW Finished Product Project Manager: Linda Geddes Phone: (626) 386-1163 The following samples were received from you on January 29, 2015 at 1150. They have been scheduled for the tests listed below each sample. If this information is incorrect, please contact your service representative. Thank you for using Eurofins Eaton Analytical. Sample # Sample ID Sample Date @ANIONS28 -- Chloride, Sulfate by EPA 300.0 @ANIONS48 -- Nitrate, Nitrite by EPA 300.0 @DBP_28 -- Disinfection ByProducts by 300.0 @ICP -- ICP Metals @ICPMS -- ICPMS Metals @VOA -- Volatile Organics by GCMS @900 -- Gross Alpha/Beta Radiation @ICPMS -- ICPMS Metals @DBP_14 -- Chlorite by 300.0 @HAA -- Haloacetic Acids @2378-TCDD_Dioxin -- 2,3,7,8-TCDD_Dioxin @COLI10 -- Total & Fecal Coliform, 24 Hour @R226EDD by SM7500-Ra B -- Radium 226 @R228EDD by SM7500-Ra D -- Radium 228 @VOASDWA TB -- Volatile Organics by GCMS Reported: 03/06/2015 Page 2 of 2 750 Royal Oaks Drive, Suite 100, Monrovia, CA 91016 Tel (626) 386-1100 Fax (626) 386-1101 http://www.EatonAnalytical.com Page 5 of 39 pages Page 6 of 39 pages Page 7 of 39 pages Page 8 of 39 pages Page 9 of 39 pages Page 10 of 39 pages Page 11 of 39 pages Page 12 of 39 pages Page 13 of 39 pages Laboratory Data Report: 514398 750 Royal Oaks Drive, Suite 100 Monrovia, California 91016-3629 Tel: (626) 386-1100 Fax: (626) 386-1101 1 800 566 LABS (1 800 566 5227) Client: Dowser, LLC 1 Pepsi Way Newburgh, NY 12550 (010) Water Quality Manager Attention: Parameter Sample ID: Report Date: 03/06/2015 Method Reporting Limit 010-043 Spring Finished Product Result Sample #: 201501050135 Primary Inorganics Antimony, Total, ICAP/MS EPA 200.8 0.001 ND Arsenic, Total, ICAP/MS EPA 200.8 0.002 ND Asbestos by TEM - >10 microns, MFL EPA 100.2 0.2 ND Barium, Total, ICAP/MS EPA 200.8 0.002 0.017 Beryllium, Total, ICAP/MS EPA 200.8 0.001 ND Cadmium, Total, ICAP/MS EPA 200.8 0.0005 ND Chromium, Total, ICAP/MS EPA 200.8 0.005 ND Cyanide SM4500CN-F 0.025 ND Fluoride SM 4500F-C 0.05 ND Lead, Total, ICAP/MS EPA 200.8 0.0005 ND Mercury EPA 245.1 0.0002 ND Nickel, Total, ICAP/MS EPA 200.8 0.005 ND Nitrate as Nitrogen by IC EPA 300.0 0.1 0.58 Nitrite, Nitrogen by IC EPA 300.0 0.05 ND Selenium, Total, ICAP/MS EPA 200.8 0.005 ND Thallium, Total, ICAP/MS EPA 200.8 0.001 ND Alkalinity in CaCO3 units SM 2320B 2 36 Aluminum, Total, ICAP/MS EPA 200.8 0.02 0.048 Bicarb.Alkalinity as HCO3,calc SM2330B 2 44 Boron, Total, ICAP EPA 200.7 0.05 ND Bromide EPA 300.0 0.005 0.0087 Calcium, Total, ICAP EPA 200.7 1 14 Carbonate as CO3, Calculated SM2330B 2 ND Chloride EPA 300.0 0.5 16 Copper, Total, ICAP/MS EPA 200.8 0.002 ND Corrosivity, Units SM 2330B -14 -1.6 Foaming Agents (MBAS) SM 5540C/EPA 425.1 0.05 ND Calcium Hardness as CACO3 EPA 200.7 5 35 Hardness, Total SM 2340B 3 48 Hydroxide as OH, Calculated SM2330B 2 ND Iron, Total, ICAP EPA 200.7 0.02 0.027 Secondary Inorganics All results reported in milligrams per liter unless otherwise noted. ND - Not detected at the specified limit Data - Page 1 of 12 Page 14 of 39 pages Laboratory Data Report: 514398 750 Royal Oaks Drive, Suite 100 Monrovia, California 91016-3629 Tel: (626) 386-1100 Fax: (626) 386-1101 1 800 566 LABS (1 800 566 5227) Client: Dowser, LLC 1 Pepsi Way Newburgh, NY 12550 (010) Water Quality Manager Attention: Parameter Sample ID: Report Date: 03/06/2015 Method Reporting Limit 010-043 Spring Finished Product Result Sample #: 201501050135 Magnesium, Total, ICAP EPA 200.7 0.1 3.1 Manganese, Total, ICAP/MS EPA 200.8 0.002 ND Orthophosphate-P 4500P-E/365.1 0.01 ND pH SM4500-HB 0.1 7.1 Phenolic Compounds-low level (units) EPA 420.4 0.001 ND Potassium, Total, ICAP EPA 200.7 1 ND Silver, Total, ICAP/MS EPA 200.8 0.0005 ND Sodium, Total, ICAP EPA 200.7 1 11 Specific Conductance, umho/cm SM2510B 2 150 Sulfate EPA 300.0 0.5 9.2 Total Dissolved Solids (TDS) E160.1/SM2540C 10 96 Uranium, Total, ICAP/MS EPA 200.8 0.001 ND Zinc, Total, ICAP/MS EPA 200.8 0.02 ND Physical Color SM 2120B 3 ND Odor at 60C (TON) (ACU) SM 2150B 1 1.0 Turbidity EPA 180.1 0.05 0.54 Benzene EPA 524.2 0.0005 ND Bromobenzene EPA 524.2 0.0005 ND Bromochloromethane EPA 524.2 0.0005 ND Bromodichloromethane EPA 524.2 0.0005 ND Bromoform EPA 524.2 0.0005 ND Bromomethane EPA 524.2 0.0005 ND n-Butylbenzene EPA 524.2 0.0005 ND sec-Butylbenzene EPA 524.2 0.0005 ND tert-Butylbenzene EPA 524.2 0.0005 ND Carbon Tetrachloride EPA 524.2 0.0005 ND Chlorobenzene EPA 524.2 0.0005 ND Chloroethane EPA 524.2 0.0005 ND Chloroform (Trichloromethane) EPA 524.2 0.0005 ND Chloromethane(Methyl Chloride) EPA 524.2 0.0005 ND 2-Chlorotoluene EPA 524.2 0.0005 ND (NTU) Volatile Organic Compounds All results reported in milligrams per liter unless otherwise noted. ND - Not detected at the specified limit Data - Page 2 of 12 Page 15 of 39 pages Laboratory Data Report: 514398 750 Royal Oaks Drive, Suite 100 Monrovia, California 91016-3629 Tel: (626) 386-1100 Fax: (626) 386-1101 1 800 566 LABS (1 800 566 5227) Client: Dowser, LLC 1 Pepsi Way Newburgh, NY 12550 (010) Water Quality Manager Attention: Parameter Sample ID: Report Date: 03/06/2015 Method Reporting Limit 010-043 Spring Finished Product Result Sample #: 201501050135 4-Chlorotoluene EPA 524.2 0.0005 ND Chlorodibromomethane EPA 524.2 0.0005 ND Dibromomethane EPA 524.2 0.0005 ND 1,2-Dichlorobenzene (1,2-DCB) EPA 524.2 0.0005 ND 1,3-Dichlorobenzene EPA 524.2 0.0005 ND 1,4-Dichlorobenzene EPA 524.2 0.0005 ND Dichlorodifluoromethane EPA 524.2 0.0005 ND 1,1-Dichloroethane EPA 524.2 0.0005 ND 1,2-Dichloroethane EPA 524.2 0.0005 ND 1,1-Dichloroethylene EPA 524.2 0.0005 ND cis-1,2-Dichloroethylene EPA 524.2 0.0005 ND trans-1,2-Dichloroethylene EPA 524.2 0.0005 ND 1,2-Dichloropropane EPA 524.2 0.0005 ND 1,3-Dichloropropane EPA 524.2 0.0005 ND 2,2-Dichloropropane EPA 524.2 0.0005 ND 1,1-Dichloropropene EPA 524.2 0.0005 ND cis-1,3-Dichloropropene EPA 524.2 0.0005 ND trans-1,3-Dichloropropene EPA 524.2 0.0005 ND Di-Isopropyl ether EPA 524.2 0.003 ND Ethyl benzene EPA 524.2 0.0005 ND Hexachlorobutadiene EPA 524.2 0.0005 ND Isopropylbenzene EPA 524.2 0.0005 ND 4-Isopropyltoluene EPA 524.2 0.0005 ND 4-Methyl-2-Pentanone (MIBK) EPA 524.2 0.005 ND Methyl Tert-butyl ether (MTBE) EPA 524.2 0.0005 ND Methyl Ethyl Ketone (MEK) EPA 524.2 0.005 ND Methylene Chloride (Dichloromethane) EPA 524.2 0.0005 ND Naphthalene EPA 524.2 0.0005 ND n-Propylbenzene EPA 524.2 0.0005 ND Styrene EPA 524.2 0.0005 ND Tert-Amyl Methyl Ether (TAME) EPA 524.2 0.003 ND Tert-Butyl Ethyl Ether (TBEE) EPA 524.2 0.003 ND 1,1,1,2-Tetrachloroethane EPA 524.2 0.0005 ND 1,1,2,2-Tetrachloroethane EPA 524.2 0.0005 ND Tetrachloroethylene (PCE) EPA 524.2 0.0005 ND All results reported in milligrams per liter unless otherwise noted. ND - Not detected at the specified limit Data - Page 3 of 12 Page 16 of 39 pages Laboratory Data Report: 514398 750 Royal Oaks Drive, Suite 100 Monrovia, California 91016-3629 Tel: (626) 386-1100 Fax: (626) 386-1101 1 800 566 LABS (1 800 566 5227) Client: Dowser, LLC 1 Pepsi Way Newburgh, NY 12550 (010) Water Quality Manager Attention: Parameter Sample ID: Report Date: 03/06/2015 Method Reporting Limit 010-043 Spring Finished Product Result Sample #: 201501050135 Toluene EPA 524.2 0.0005 ND 1,2,3-Trichlorobenzene EPA 524.2 0.0005 ND 1,2,4-Trichlorobenzene EPA 524.2 0.0005 ND 1,1,1-Trichloroethane EPA 524.2 0.0005 ND 1,1,2-Trichloroethane EPA 524.2 0.0005 ND Trichloroethylene (TCE) EPA 524.2 0.0005 ND Trichlorofluoromethane (Freon 11) EPA 524.2 0.0005 ND Trichlorotrifluoroethane(Freon 113) EPA 524.2 0.0005 ND 1,2,3-Trichloropropane EPA 524.2 0.0005 ND 1,2,4-Trimethylbenzene EPA 524.2 0.0005 ND 1,3,5-Trimethylbenzene EPA 524.2 0.0005 ND Vinyl chloride (VC) EPA 524.2 0.0003 ND Total xylenes EPA 524.2 0.0005 ND m,p-Xylenes EPA 524.2 0.0005 ND o-Xylene EPA 524.2 0.0005 ND Carbon Disulfide EPA 524.2 0.0005 ND Dibromochloropropane (DBCP) EPA 551.1 0.00001 ND Ethylene Dibromide (EDB) EPA 551.1 0.00001 ND Alachlor (Alanex) EPA 505 0.0001 ND Aldrin EPA 505 0.00001 ND Chlordane EPA 505 0.0001 ND Dieldrin EPA 505 0.00001 ND Endrin EPA 505 0.00001 ND Heptachlor EPA 505 0.00001 ND Heptachlor Epoxide EPA 505 0.00001 ND Lindane (gamma-BHC) EPA 505 0.00001 ND Methoxychlor EPA 505 0.00005 ND Total PCBs EPA 505 0.0001 ND PCB 1016 Aroclor EPA 505 0.00008 ND PCB 1221 Aroclor EPA 505 0.0001 ND PCB 1232 Aroclor EPA 505 0.0001 ND EDB and DBCP Pesticides and PCBs All results reported in milligrams per liter unless otherwise noted. ND - Not detected at the specified limit Data - Page 4 of 12 Page 17 of 39 pages Laboratory Data Report: 514398 750 Royal Oaks Drive, Suite 100 Monrovia, California 91016-3629 Tel: (626) 386-1100 Fax: (626) 386-1101 1 800 566 LABS (1 800 566 5227) Client: Dowser, LLC 1 Pepsi Way Newburgh, NY 12550 (010) Water Quality Manager Attention: Parameter Sample ID: Report Date: 03/06/2015 Method Reporting Limit 010-043 Spring Finished Product Result Sample #: 201501050135 PCB 1242 Aroclor EPA 505 0.0001 ND PCB 1248 Aroclor EPA 505 0.0001 ND PCB 1254 Aroclor EPA 505 0.0001 ND PCB 1260 Aroclor EPA 505 0.0001 ND Toxaphene EPA 505 0.0005 ND 2,4,5-T EPA 515.4 0.0002 ND 2,4,5-TP (Silvex) EPA 515.4 0.0002 ND 2,4-D EPA 515.4 0.0001 ND 2,4-DB EPA 515.4 0.002 ND Dichlorprop EPA 515.4 0.0005 ND Acifluorfen EPA 515.4 0.0002 ND Bentazon EPA 515.4 0.0005 ND Dalapon EPA 515.4 0.001 ND 3,5-Dichlorobenzoic acid EPA 515.4 0.0005 ND Tot DCPA Mono&Diacid Degradate EPA 515.4 0.0001 ND Dicamba EPA 515.4 0.0001 ND Dinoseb EPA 515.4 0.0002 ND Pentachlorophenol EPA 515.4 0.00004 ND Picloram EPA 515.4 0.0001 ND Acenaphthene EPA 525.2 0.0001 ND Acenaphthylene EPA 525.2 0.0001 ND Acetochlor EPA 525.2 0.0001 ND Alpha-BHC EPA 525.2 0.0001 ND alpha-Chlordane EPA 525.2 0.00005 ND Anthracene EPA 525.2 0.00002 ND Atrazine EPA 525.2 0.00005 ND Benz(a)Anthracene EPA 525.2 0.00005 ND Benzo(a)pyrene EPA 525.2 0.00002 ND Benzo(g,h,i)Perylene EPA 525.2 0.00005 ND Benzo(b)Fluoranthene EPA 525.2 0.00002 ND Benzo(k)Fluoranthene EPA 525.2 0.00002 ND Herbicides Semivolatile Organic Compounds All results reported in milligrams per liter unless otherwise noted. ND - Not detected at the specified limit Data - Page 5 of 12 Page 18 of 39 pages Laboratory Data Report: 514398 750 Royal Oaks Drive, Suite 100 Monrovia, California 91016-3629 Tel: (626) 386-1100 Fax: (626) 386-1101 1 800 566 LABS (1 800 566 5227) Client: Dowser, LLC 1 Pepsi Way Newburgh, NY 12550 (010) Water Quality Manager Attention: Parameter Sample ID: Report Date: 03/06/2015 Method Reporting Limit 010-043 Spring Finished Product Result Sample #: 201501050135 Beta BHC EPA 525.2 0.0001 ND Butachlor EPA 525.2 0.00005 ND Butylbenzylphthalate EPA 525.2 0.0005 ND Caffeine EPA 525.2 0.00005 ND Chlorobenzilate EPA 525.2 0.0001 ND Chloroneb EPA 525.2 0.0001 ND Chlorothalonil EPA 525.2 0.0001 ND Chlorpyrifos EPA 525.2 0.00005 ND Chrysene EPA 525.2 0.00002 ND Bromacil EPA 525.2 0.0002 ND 4,4-DDD EPA 525.2 0.0001 ND 4,4-DDE EPA 525.2 0.0001 ND 4,4-DDT EPA 525.2 0.0001 ND Delta BHC EPA 525.2 0.0001 ND Dibenz(a,h)Anthracene EPA 525.2 0.00005 ND Diethylphthalate EPA 525.2 0.0005 ND Di(2-Ethylhexyl)phthalate EPA 525.2 0.0006 ND Diazinon (Qualitative) EPA 525.2 0.0001 ND Dieldrin EPA 525.2 0.0002 ND Dichlorvos (DDVP) EPA 525.2 0.00005 ND Dimethoate EPA 525.2 0.0001 ND Di-n-Butylphthalate EPA 525.2 0.001 ND 2,4-Dinitrotoluene EPA 525.2 0.0001 ND Di-n-octylphthalate EPA 525.2 0.0001 ND 2,6-Dinitrotoluene EPA 525.2 0.0001 ND Di-(2-Ethylhexyl)adipate EPA 525.2 0.0006 ND Dimethylphthalate EPA 525.2 0.0005 ND Endosulfan I (Alpha) EPA 525.2 0.0001 ND Endosulfan II (Beta) EPA 525.2 0.0001 ND Endosulfan Sulfate EPA 525.2 0.0001 ND Endrin Aldehyde EPA 525.2 0.0001 ND EPTC EPA 525.2 0.0001 ND Fluoranthene EPA 525.2 0.0001 ND Fluorene EPA 525.2 0.00005 ND gamma-Chlordane EPA 525.2 0.00005 ND All results reported in milligrams per liter unless otherwise noted. ND - Not detected at the specified limit Data - Page 6 of 12 Page 19 of 39 pages Laboratory Data Report: 514398 750 Royal Oaks Drive, Suite 100 Monrovia, California 91016-3629 Tel: (626) 386-1100 Fax: (626) 386-1101 1 800 566 LABS (1 800 566 5227) Client: Dowser, LLC 1 Pepsi Way Newburgh, NY 12550 (010) Water Quality Manager Attention: Parameter Sample ID: Report Date: 03/06/2015 Method Reporting Limit 010-043 Spring Finished Product Result Sample #: 201501050135 Heptachlor EPA 525.2 0.00003 ND Hexachlorobenzene EPA 525.2 0.00005 ND Hexachlorocyclopentadiene EPA 525.2 0.00005 ND Indeno(1,2,3,c,d)Pyrene EPA 525.2 0.00005 ND Isophorone EPA 525.2 0.0005 ND Malathion EPA 525.2 0.0001 ND Metolachlor EPA 525.2 0.00005 ND Metribuzin EPA 525.2 0.00005 ND Molinate EPA 525.2 0.0001 ND Naphthalene EPA 525.2 0.0003 ND trans-Nonachlor EPA 525.2 0.00005 ND Parathion EPA 525.2 0.0001 ND Pentachlorophenol EPA 525.2 0.001 ND Pendimethalin EPA 525.2 0.0001 ND Permethrin EPA 525.2 0.0001 ND Phenanthrene EPA 525.2 0.00004 ND Propachlor EPA 525.2 0.00005 ND Pyrene EPA 525.2 0.00005 ND Simazine EPA 525.2 0.00005 ND Terbuthylazine EPA 525.2 0.0001 ND Terbacil EPA 525.2 0.0001 ND Thiobencarb EPA 525.2 0.0002 ND Trifluralin EPA 525.2 0.0001 ND Aldicarb (Temik) EPA 531.2 0.0005 ND Aldicarb sulfone EPA 531.2 0.0005 ND Aldicarb sulfoxide EPA 531.2 0.0005 ND Baygon (Propoxur) EPA 531.2 0.0005 ND Carbaryl EPA 531.2 0.0005 ND Carbofuran (Furadan) EPA 531.2 0.0005 ND 3 Hydroxycarbofuran EPA 531.2 0.0005 ND Methiocarb EPA 531.2 0.0005 ND Methomyl EPA 531.2 0.0005 ND Oxamyl (Vydate) EPA 531.2 0.0005 ND Carbamates All results reported in milligrams per liter unless otherwise noted. ND - Not detected at the specified limit Data - Page 7 of 12 Page 20 of 39 pages Laboratory Data Report: 514398 750 Royal Oaks Drive, Suite 100 Monrovia, California 91016-3629 Tel: (626) 386-1100 Fax: (626) 386-1101 1 800 566 LABS (1 800 566 5227) Client: Dowser, LLC 1 Pepsi Way Newburgh, NY 12550 (010) Water Quality Manager Attention: Parameter Sample ID: Report Date: 03/06/2015 Method Reporting Limit 010-043 Spring Finished Product Result Sample #: 201501050135 Other Organics Glyphosate EPA 547 0.006 ND Endothall EPA 548.1 0.005 ND Diquat EPA 549.2 0.0004 ND Paraquat EPA 549.2 0.002 ND Total Haloacetic Acids SM 6251B 0.002 ND Bromochloroacetic acid SM 6251B 0.001 ND Dibromoacetic acid SM 6251B 0.001 ND Dichloroacetic acid SM 6251B 0.001 ND Monobromoacetic acid SM 6251B 0.001 ND Monochloroacetic acid SM 6251B 0.002 ND Trichloroacetic acid SM 6251B 0.001 ND Total Trihalomethanes EPA 524.2 0.0005 ND Total Chlorine Residual SM 4500-CL G 0.1 ND Chloramines SM 4500CL-G/HACH 0.1 ND Chlorine Dioxide SM 4500-CLO2-D/HACH 0.24 ND Free Chlorine Residual SM 4500CL-G/HACH 0.1 ND Alpha, Gross, pCi/L EPA 900.0 3 ND Beta, Gross, pCi/L EPA 900.0 3 ND Radium 226, pCi/L SM7500-Ra B 0.7 ND Radium 228, pCi/L SM7500-Ra D 0.23 ND 2,3,7,8-TCDD EPA 1613B 0.000000005 ND Disinfection By-products Other Compounds All results reported in milligrams per liter unless otherwise noted. ND - Not detected at the specified limit Data - Page 8 of 12 Page 21 of 39 pages Laboratory Data Report: 514398 750 Royal Oaks Drive, Suite 100 Monrovia, California 91016-3629 Tel: (626) 386-1100 Fax: (626) 386-1101 1 800 566 LABS (1 800 566 5227) Client: Dowser, LLC 1 Pepsi Way Newburgh, NY 12550 (010) Water Quality Manager Attention: Parameter Sample ID: Report Date: 03/06/2015 Method Reporting Limit 010-043 Spring Finished Product Result Sample #: 201501050135 Microbiologicals Heterotrophic Plate Count, CFU/ml SM 9215B 1 ND Total Coliform Bacteria, MPN/100 ml SM 9223 1.1 ND E. Coli Bacteria, MPN/100 ml SM 9223 1.1 ND All results reported in milligrams per liter unless otherwise noted. ND - Not detected at the specified limit Data - Page 9 of 12 Page 22 of 39 pages Laboratory Data Report: 514398 750 Royal Oaks Drive, Suite 100 Monrovia, California 91016-3629 Tel: (626) 386-1100 Fax: (626) 386-1101 1 800 566 LABS (1 800 566 5227) Client: Dowser, LLC 1 Pepsi Way Newburgh, NY 12550 (010) Water Quality Manager Attention: Parameter Sample ID: Report Date: 03/06/2015 Method Reporting Limit 010-043 Spring Finished Product Result Sample #: 201502110448 Disinfection By-products Bromate EPA 317 0.005 ND Chlorite EPA 300.0 0.01 ND All results reported in milligrams per liter unless otherwise noted. ND - Not detected at the specified limit Data - Page 10 of 12 Page 23 of 39 pages Laboratory Data Report: 514398 750 Royal Oaks Drive, Suite 100 Monrovia, California 91016-3629 Tel: (626) 386-1100 Fax: (626) 386-1101 1 800 566 LABS (1 800 566 5227) Client: Dowser, LLC 1 Pepsi Way Newburgh, NY 12550 (010) Water Quality Manager Attention: Parameter Sample ID: Report Date: 03/06/2015 Method Reporting Limit Trip Blanks Result Sample #: 201501050134 Volatile Organic Compounds Benzene EPA 524.2 0.0005 ND Bromobenzene EPA 524.2 0.0005 ND Bromochloromethane EPA 524.2 0.0005 ND Bromodichloromethane EPA 524.2 0.0005 ND Bromoform EPA 524.2 0.0005 ND Bromomethane EPA 524.2 0.0005 ND n-Butylbenzene EPA 524.2 0.0005 ND sec-Butylbenzene EPA 524.2 0.0005 ND tert-Butylbenzene EPA 524.2 0.0005 ND Carbon Tetrachloride EPA 524.2 0.0005 ND Chlorobenzene EPA 524.2 0.0005 ND Chloroethane EPA 524.2 0.0005 ND Chloroform (Trichloromethane) EPA 524.2 0.0005 ND Chloromethane(Methyl Chloride) EPA 524.2 0.0005 ND 2-Chlorotoluene EPA 524.2 0.0005 ND 4-Chlorotoluene EPA 524.2 0.0005 ND Chlorodibromomethane EPA 524.2 0.0005 ND Dibromomethane EPA 524.2 0.0005 ND 1,2-Dichlorobenzene (1,2-DCB) EPA 524.2 0.0005 ND 1,3-Dichlorobenzene EPA 524.2 0.0005 ND 1,4-Dichlorobenzene EPA 524.2 0.0005 ND Dichlorodifluoromethane EPA 524.2 0.0005 ND 1,1-Dichloroethane EPA 524.2 0.0005 ND 1,2-Dichloroethane EPA 524.2 0.0005 ND 1,1-Dichloroethylene EPA 524.2 0.0005 ND cis-1,2-Dichloroethylene EPA 524.2 0.0005 ND trans-1,2-Dichloroethylene EPA 524.2 0.0005 ND 1,2-Dichloropropane EPA 524.2 0.0005 ND 1,3-Dichloropropane EPA 524.2 0.0005 ND 2,2-Dichloropropane EPA 524.2 0.0005 ND 1,1-Dichloropropene EPA 524.2 0.0005 ND cis-1,3-Dichloropropene EPA 524.2 0.0005 ND trans-1,3-Dichloropropene EPA 524.2 0.0005 ND Di-Isopropyl ether EPA 524.2 0.003 ND All results reported in milligrams per liter unless otherwise noted. ND - Not detected at the specified limit Data - Page 11 of 12 Page 24 of 39 pages Laboratory Data Report: 514398 750 Royal Oaks Drive, Suite 100 Monrovia, California 91016-3629 Tel: (626) 386-1100 Fax: (626) 386-1101 1 800 566 LABS (1 800 566 5227) Client: Dowser, LLC 1 Pepsi Way Newburgh, NY 12550 (010) Water Quality Manager Attention: Parameter Sample ID: Report Date: 03/06/2015 Method Reporting Limit Trip Blanks Result Sample #: 201501050134 Ethyl benzene EPA 524.2 0.0005 ND Hexachlorobutadiene EPA 524.2 0.0005 ND Isopropylbenzene EPA 524.2 0.0005 ND 4-Isopropyltoluene EPA 524.2 0.0005 ND 4-Methyl-2-Pentanone (MIBK) EPA 524.2 0.005 ND Methyl Tert-butyl ether (MTBE) EPA 524.2 0.0005 ND Methyl Ethyl Ketone (MEK) EPA 524.2 0.005 ND Methylene Chloride (Dichloromethane) EPA 524.2 0.0005 ND Naphthalene EPA 524.2 0.0005 ND n-Propylbenzene EPA 524.2 0.0005 ND Styrene EPA 524.2 0.0005 ND Tert-Amyl Methyl Ether (TAME) EPA 524.2 0.003 ND Tert-Butyl Ethyl Ether (TBEE) EPA 524.2 0.003 ND 1,1,1,2-Tetrachloroethane EPA 524.2 0.0005 ND 1,1,2,2-Tetrachloroethane EPA 524.2 0.0005 ND Tetrachloroethylene (PCE) EPA 524.2 0.0005 ND Toluene EPA 524.2 0.0005 ND 1,2,3-Trichlorobenzene EPA 524.2 0.0005 ND 1,2,4-Trichlorobenzene EPA 524.2 0.0005 ND 1,1,1-Trichloroethane EPA 524.2 0.0005 ND 1,1,2-Trichloroethane EPA 524.2 0.0005 ND Trichloroethylene (TCE) EPA 524.2 0.0005 ND Trichlorofluoromethane (Freon 11) EPA 524.2 0.0005 ND Trichlorotrifluoroethane(Freon 113) EPA 524.2 0.0005 ND 1,2,3-Trichloropropane EPA 524.2 0.0005 ND 1,2,4-Trimethylbenzene EPA 524.2 0.0005 ND 1,3,5-Trimethylbenzene EPA 524.2 0.0005 ND Vinyl chloride (VC) EPA 524.2 0.0003 ND Total xylenes EPA 524.2 0.0005 ND m,p-Xylenes EPA 524.2 0.0005 ND o-Xylene EPA 524.2 0.0005 ND Carbon Disulfide EPA 524.2 0.0005 ND EPA 524.2 0.0005 ND Disinfection By-products Total Trihalomethanes All results reported in milligrams per liter unless otherwise noted. ND - Not detected at the specified limit Data - Page 12 of 12 Page 25 of 39 pages Laboratory Comments Report: 514398 750 Royal Oaks Drive, Suite 100 Monrovia, California 91016-3629 Tel: (626) 386-1100 Fax: (626) 386-1101 1 800 566 LABS (1 800 566 5227) Dowser, LLC (010) Water Quality Manager 1 Pepsi Way Newburgh, NY 12550 Folder Comments Analytical results for Radium 226 and Radium 228 are submitted by Eurofins Eaton Analytical in South Bend IN The Comments Report may be blank if there are no comments for this report. Comments - Page 1 of 1 Page 26 of 39 pages LABORATORY REPORT 13 This report contains pages. (including the cover page) If you have any questions concerning this report, please do not hesitate to call us at (800) 332-4345 or (574) 233-4777. This report may not be reproduced, except in full, without written approval from Eurofins Eaton Analytical, Inc. Page 27 of 39 pages NELAC NARRATIVE PAGE Client: Eurofins Eaton Analytical Report #: 333462NP Eurofins Eaton Analytical, Inc. is a NELAP accredited laboratory. All reported results meet the requirements of the NELAC standards, unless otherwise noted. EEA contact person: Kelly Trott NELAP requires complete reporting of deviations from method requirements, regardless of the suspected impact on the data. Quality control failures not reported within the report summary are noted here. There were no quality control failures. Note: This report may not be reproduced, except in full, without written approval from EEA. EEA is accredited by the National Environmental Laboratory Accreditation Program (NELAP). 02/20/2015 Authorized Signature Title Date Page 1 of 1 Page 28 of 39 pages 110 South Hill Street South Bend, IN 46617 Tel: (574) 233-4777 Fax: (574) 233-8207 1 800 332 4345 Laboratory Report Client: Attn: Copies to: Report: 333462 Priority: Standard Written 750 Royal Oaks Drive Status: Final Suite 100 Monrovia, CA 91016 PWS ID: Not Supplied Eurofins Eaton Analytical Jackie Contreras None Sample Information EEA ID # Client ID Method Collected Date / Time Collected By: Received Date / Time 3181111 3181111 201501050135 7500-Ra B 01/28/15 10:30 Client 02/04/15 09:45 201501050135 7500-Ra D 01/28/15 10:30 Client 02/04/15 09:45 Report Summary Note: See attached page for additional comments. EEA Folder #514398 / Sub PO #99-32945 / Job #1000014 Note: Sample containers were provided by the client. Detailed quantitative results are presented on the following pages. The results presented relate only to the samples provided for analysis. We appreciate the opportunity to provide you with this analysis. If you have any questions concerning this report, please do not hesitate to call Kelly Trott at (574) 233-4777. Note: This report may not be reproduced, except in full, without written approval from EEA. EEA is accredited by the National Environmental Laboratory Accreditation Program (NELAP). 02/20/2015 Authorized Signature Client Name: Eurofins Eaton Analytical Report #: 333462 Title Date Page 1 of 3 Page 29 of 39 pages Client Name: Sampling Point: Report #: 333462 Eurofins Eaton Analytical PWS ID: Not Supplied 201501050135 Radionuclides Analyte ID # Analyte Method Reg Limit MDA 95** MRL Result Units Preparation Date Analyzed EEA ID # 13982-63-3 Radium-226 7500-Ra B --- 0.7 1.0 -1.6 ± 1.5 pCi/L 02/09/15 16:29 02/16/15 09:25 3181111 15262-20-1 Radium-228 7500-Ra D --- 0.23 1.0 0.17 ± 0.23 pCi/L 02/09/15 19:20 02/13/15 14:24 3181111 calc. 5* 0.7 --- -1.43 ± 1.52 pCi/L 02/09/15 16:29 02/16/15 09:25 3181111 --- Combined Radium ** Minimum Detectable Activity (MDA95) shall be that concentration which can be counted with a precision of plus or minus 100% at the 95 % confidence level. † EEA has demonstrated it can achieve these report limits in reagent water, but can not document them in all sample matrices. Reg Limit Type: MCL SMCL AL Symbol: * ^ ! Page 2 of 3 Page 30 of 39 pages Client Name: Report #: 333462 Eurofins Eaton Analytical Lab Definitions Continuing Calibration Check Standard (CCC) / Continuing Calibration Verification (CCV) / Initial Calibration Verification Standard (ICV) / Initial Performance Check (IPC) - is a standard containing one or more of the target analytes that is prepared from the same standards used to calibrate the instrument. This standard is used to verify the calibration curve at the beginning of each analytical sequence, and may also be analyzed throughout and at the end of the sequence. The concentration of continuing standards may be varied, when prescribed by the reference method, so that the range of the calibration curve is verified on a regular basis. Internal Standards (IS) - are pure compounds with properties similar to the analytes of interest, which are added to field samples or extracts, calibration standards, and quality control standards at a known concentration. They are used to measure the relative responses of the analytes of interest and surrogates in the sample, calibration standard or quality control standard. Laboratory Duplicate (LD) - is a field sample aliquot taken from the same sample container in the laboratory and analyzed separately using identical procedures. Analysis of laboratory duplicates provides a measure of the precision of the laboratory procedures. Laboratory Fortified Blank (LFB) / Laboratory Control Sample (LCS) - is an aliquot of reagent water to which known concentrations of the analytes of interest are added. The LFB is analyzed exactly the same as the field samples. LFBs are used to determine whether the method is in control. Laboratory Method Blank (LMB) / Laboratory Reagent Blank (LRB) - is a sample of reagent water included in the sample batch analyzed in the same way as the associated field samples. The LMB is used to determine if method analytes or other background contamination have been introduced during the preparation or analytical procedure. The LMB is analyzed exactly the same as the field samples. Laboratory Trip Blank (LTB) / Field Reagent Blank (FRB) - is a sample of laboratory reagent water placed in a sample container in the laboratory and treated as a field sample, including storage, preservation, and all analytical procedures. The FRB/LTB container follows the collection bottles to and from the collection site, but the FRB/LTB is not opened at any time during the trip. The FRB/LTB is primarily a travel blank used to verify that the samples were not contaminated during shipment. Matrix Spike Duplicate Sample (MSD) / Laboratory Fortified Sample Matrix Duplicate (LFSMD) - is a sample aliquot taken from the same field sample source as the Matrix Spike Sample to which known quantities of the analytes of interest are added in the laboratory. The MSD is analyzed exactly the same as the field samples. Analysis of the MSD provides a measure of the precision of the laboratory procedures in a specific matrix. Matrix Spike Sample (MS) / Laboratory Fortified Sample Matrix (LFSM) - is a sample aliquot taken from field sample source to which known quantities of the analytes of interest are added in the laboratory. The MS is analyzed exactly the same as the field samples. The purpose is to demonstrate recovery of the analytes from a sample matrix to determine if the specific matrix contributes bias to the analytical results. Quality Control Standard (QCS) / Second Source Calibration Verification (SSCV) - is a solution containing known concentrations of the analytes of interest prepared from a source different from the source of the calibration standards. The solution is obtained from a second manufacturer or lot if the lot can be demonstrated by the manufacturer as prepared independently from other lots. The QCS sample is analyzed using the same procedures as field samples. The QCS is used as a check on the calibration standards used in the method on a routine basis. Reporting Limit Check (RLC) / Initial Calibration Check Standard (ICCS) - is a procedural standard that is analyzed each day to evaluate instrument performance at or below the minimum reporting limit (MRL). Surrogate Standard (SS) / Surrogate Analyte (SUR) - is a pure compound with properties similar to the analytes of interest, which is highly unlikely to be found in any field sample, that is added to the field samples, calibration standards, blanks and quality control standards before sample preparation. The SS is used to evaluate the efficiency of the sample preparation process. Page 3 of 3 Page 31 of 39 pages Page 32 of 39 pages Page 33 of 39 pages 3186271 3186272 LRB LFB Page 1 of 2 Sample Id Type Sample Site Run ID: 199611 RW RW Matrix Method: DU DU Instrument ID 7500-Ra B Eurofins Eaton Analytical Run Log Calibration File EEA Run ID 199611 / EEA Report # 333462 02/12/2015 09:39 02/12/2015 09:39 Analysis Date Page 34 of 39 pages Radium-226 Radium-226 LRB LFB Page 2 of 2 Analyte Sample Type True False 7500-Ra B 7500-Ra B Method 0.2 0.25 MRL --- --- Client ID Result Flag 20.8600 0.14 Amount 18.0 Target QC Summary Report % Recovery pCi/L Units 116 --- % Recovery --- --- RPD --- --- RPD Limit 1.0 1.0 Dil Factor 02/09/2015 16:29 02/09/2015 16:29 Extracted 02/12/2015 09:39 02/12/2015 09:39 Analyzed EEA Run ID 199611 / EEA Report # 333462 30 - 160 --- Recovery Limits 3186272 3186271 EEA ID # Page 35 of 39 pages 3181111 FS Page 1 of 2 Sample Id Type 201501050135 Sample Site Run ID: 199712 DW Matrix Method: DU Instrument ID 7500-Ra B Eurofins Eaton Analytical Run Log Calibration File EEA Run ID 199712 / EEA Report # 333462 02/16/2015 09:25 Analysis Date Page 36 of 39 pages Radium-226 FS Page 2 of 2 Analyte Sample Type True 7500-Ra B Method 0.7 MRL 201501050135 Client ID Result Flag -1.6 Amount Target QC Summary Report pCi/L Units --- % Recovery --- --- RPD --- RPD Limit 1.0 Dil Factor 02/09/2015 16:29 Extracted 02/16/2015 09:25 Analyzed EEA Run ID 199712 / EEA Report # 333462 Recovery Limits 3181111 EEA ID # Page 37 of 39 pages 201501050135 3181111 3187768 3187769 FS LRB LFB Page 1 of 2 Sample Site Sample Id Type Run ID: 199672 RW RW DW Matrix Method: DU DU DU Instrument ID 7500-Ra D Eurofins Eaton Analytical Run Log Calibration File EEA Run ID 199672 / EEA Report # 333462 02/13/2015 14:24 02/13/2015 14:24 02/13/2015 14:24 Analysis Date Page 38 of 39 pages Radium-228 Radium-228 Radium-228 FS LRB LFB Page 2 of 2 Analyte Sample Type True True False 7500-Ra D 7500-Ra D 7500-Ra D Method 0.22 0.24 0.23 MRL --- --- 201501050135 Client ID Result Flag 6.6400 0.17 0.17 Amount 8.14 Target QC Summary Report % Recovery pCi/L pCi/L Units 82 --- --- % Recovery --- --- --- RPD --- --- --- RPD Limit 1.0 1.0 1.0 Dil Factor 02/09/2015 19:20 02/09/2015 19:20 02/09/2015 19:20 Extracted 02/13/2015 14:24 02/13/2015 14:24 02/13/2015 14:24 Analyzed EEA Run ID 199672 / EEA Report # 333462 48 - 139 --- --- Recovery Limits 3187769 3187768 3181111 EEA ID # Page 39 of 39 pages Field Sample Laboratory Fortified Blank Laboratory Reagent Blank FS LFB LRB Page 1 of 1 Sample Type Type (Abbr.) Type (Abbr.) Sample Type Key Sample Type EEA Run ID 199672 / EEA Report # 333462
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