APPLICATION NOTE An Atlas of ESD Failure Signatures in Vertical Cavity Surface Emitting Lasers ABSTRACT AOC herein describes a collection of material degradation features observed in Vertical Cavity Surface Emitting Lasers (VCSELs) that have been intentionally degraded with a range of electrostatic discharge (ESD) stress conditions. Failure analysis techniques employed include emission microscopy, Focused Ion Beam (FIB) microscopy and Transmission Electron Microscopy (TEM). The results have enabled higher confidence in root-cause determination for failed VCSEL devices. INTRODUCTION The application of sophisticated characterization techniques (e.g. emission microscopy, FIB, and TEM) to understanding VCSEL failure mechanisms has been well documented1, and analysts continue to add to3 and improve on these techniques4. Typically, in the absence of gross mechanical or electrical overstress damage, these techniques often reveal that the active layers of a failed VCSEL contain a complex patterned dislocation array1,5 . Acting as nonradiative recombination sites these arrays degrade the optical and electrical properties of the laser device. However, while visually imposing, the dislocation arrays represent only the final cause, not root cause of failure. Rather, nonradiative recombination of minority carriers at a defect site in the active layers of a light emitting diode provides a positive feedback mechanism that typically leads to the self-supporting growth of a dislocation array from that defect site. Consequently, a single defect such as a dislocation propagating from the substrate is able to generate a dense dislocation array that covers the entire active region of the device. Thus, the goal in the analysis of many failed VCSELs is to find the source defect of the dislocation array. Once discovered, the next challenge is to attribute that defect to some outside event, design flaw, or growth anomaly. The emphasis of this paper is on the characterization of defects caused by outside events, primarily Electrostatic Discharge (ESD) and minor Electrical Overstress (EOS) events. The data shown below was generated with AOC’s 14um oxide confined devicesi though the principles described are applicable to other VCSEL designs. i Human Body Model and Machine Model pulses were generated using an Oryx 700 System. BACKGROUND The 2004 annual Electrostatic Discharge Association (ESDA) Symposium included no obvious representation from the optical semiconductor device community in either the tutorial or technical programs. Nevertheless, optical devices are susceptible to ESD events and many of the concepts discussed in the ESDA community are as applicable to the manufacturers and users of VCSELs as they are to the silicon IC industry6. The following data show a range of material degradation features in oxide confined VCSELs intentionally exposed to ESD under laboratory conditions, the characteristics of which depend on the type of ESD stress applied. Several texts7,8 describe in detail these various forms of ESD and AOC has previously shown the application of these models to the oxide VCSEL9. Briefly, the Human Body Model (HBM) describes the discharge of a fully charged capacitor (~100pf ), through an inductor (~10uH) and resistor (~1500Ω) in series with the device (where the values of the components used are intended to represent the electrical properties of the average human). The Machine Model (MM) describes the discharge of a fully charged capacitor (~100pf ) through a smaller inductor (~100nH) in series with the device. Here the component values typify the circuit when a device is contacted by a charged metal object. In the Charged Device Model (CDM), the device discharges through a zero ohm, zero inductance circuit. Figure 1 shows a comparison of the electrical signals that a device would experience via these models. Historically, pinpointing the exact cause of ESD damage so that improved controls can be implemented has proven to be notoriously difficult. However, if it is possible to determine which type of ESD event (HBM, MM, or CDM) is associated with a particular failure, it is then possible to determine how the part is being exposed to ESD, thereby making it possible to correct the issue. For example, a failure with HBM-type damage would lead to better controls on factory employees – e.g. wrist straps, heel straps, etc. Damage induced by MM would indict equipment fixtures or handling tools (tweezers for example). CDM failures would most likely be caused by automated equipment or improper device handling which induces charging on the devices. Thus, a means of narrowing the search for the ESD source can lead to much faster actions to prevent future failures. VCSELS DAMAGED BY CHARGED HUMANS – THE HBM EVENT The electrostatic discharge pulse from a charged human is slow and of lower magnitude relative to other models. Under these conditions, current is restricted by the oxide aperture and the highest fluxes occur in the active area, near the oxide aperture9. Reverse bias ESD events dissipate more power than forward bias events (i.e. due to the fact that the reverse breakdown voltage is about an order of magnitude greater than the forward voltage of the device) and thus, the VCSEL has a lower threshold of damage from reverse bias events. 1.00E-05 Reverse Current (-A) 1.00E-06 1.00E-07 1.00E-08 1.00E-09 1.00E-10 1.00E-11 1.00E-12 0 5 10 15 Reverse Bias (-V) Figure 1. Comparison of the signals from three common ESD events. Image courtesy of Joe Bernier, Intersil Corp. Figure 2. Reverse Bias IV trace from a device subjected to a RB HBM event of 500V (red) and a known good device. Fused quantum wells Oxide tip Figure 5. Cross-section TEM micrograph of device subjected to 500V RB HBM ESD event. Figure 3. Electroluminescence image from a device subjected to a RB HBM event of 500V. The power dissipation for a reverse bias event should occur in the plane of the junction as is demonstrated below by the failure analysis of a device subjected to an event slightly above the threshold (500V in this case) which causes immediate output degradation. Electrical characterization (Figure 2) shows excessive reverse bias leakage current and sub-threshold forward bias electroluminescence, or emission, imaging (Figure 3) shows dark areas in the emission patterns. Both results demonstrate a degradation of the diode properties of the device. Planview TEM analysis shows that the dark areas observed in the emission image correspond to large defects (i.e. dislocation tangles) within the active area of the device (Figure 4). Crosssection analysis of this type of defect (Figure 5) shows that the quantum well layers have fused in, and adjacent to, the damage center and that a dense dislocation tangle exists there. Dislocation tangles and loss of architecture also occur in other nearby high gallium-containing layers presumably due in part to the lower melting temperature and greater optical energy absorption in those lower bandgap layers. Electrical characterization (Figure 6) of a device subject to a forward bias HBM ESD event (1800V; just above the threshold for output degradation) reveals no significant change in the diode properties of the device. Furthermore, there are no 1.00E-05 Reverse Current (-A) 1.00E-06 1.00E-07 1.00E-08 1.00E-09 1.00E-10 1.00E-11 1.00E-12 0 5 10 15 Reverse Bias (-V) Figure 4. Plan-view TEM micrograph showing the oxide and quantum well active layers from a reverse bias HBM degraded VCSEL. Figure 6. Reverse bias IV trace from device subjected to a FB HBM event of 1800V (red) and a known good device. Oxide tip Figure 9. Cross-section TEM micrograph of device subjected to FB HBM event. Figure 7. Sub-threshold forward-bias electroluminescence image of device subjected to a FB HBM event of 1800V. easily recognizable dark area defects in the electroluminescence image (Figure 7). Plan-view TEM analysis (Figure 8) shows that the damage areas are located close to the oxide aperture where current densities are expected to be greatest. The damaged area is smaller relative to the reverse bias case, presumably due to the lower power dissipation under forward bias. Cross-section TEM analysis (Figure 9) of a similar defect shows relatively high mechanical stress (dark contrast) at the oxide tip and a single dislocation arching through the otherwise preserved active layers. Thus, the forward bias HBM event may not cause sufficient damage to the active layers to be reflected in immediate degradation of the electrical properties, though subsequent operation can extend the dislocations (i.e. by the growth of an array) in the active layers and lead to early failure. Reverse Current (-A) 1.00E-05 1.00E-06 1.00E-07 1.00E-08 1.00E-09 1.00E-10 1.00E-11 1.00E-12 0 5 10 Reverse Bias (-V) Figure 8. Plan-view TEM micrograph showing the oxide and quantum well active layers from a forward bias HBM degraded VCSEL. The arrow indicates a dislocation tangle. Figure 10. Reverse bias IV trace from a device subjected to a 100V MM ESD event (red) and a known good device. 15 DAMAGE CAUSED BY THE VCSEL ITSELF – THE CDM EVENT Figure 11. Electroluminescence image from a device subjected to a 100V MM ESD event. Mishandling of a packaged VCSEL may lead to the triboelectric buildup of a charge on the device. A CDM event may result upon subsequent contact with another body at a different potential. Among ESD events, CDM pulses are of the highest magnitude and shortest duration. Thus, the power dissipation is greater than for other ESD models and the damage threshold for VCSELs is expected to be low. For the high speed of the pulse, normally insulating elements of the VCSEL (e.g. the oxide layer) will become more conductive. Furthermore, SPICE modeling of ESD events in oxide VCSELs has shown that for a CDM event, the voltage expressed across the oxide layer is easily sufficient to cause dielectric breakdown9. To intentionally induce a CDM event for this work, a VCSEL was charged with an ion gun and subsequently discharged to a metal block. Electrical characterization (Figure 14) shows degradation of the diode properties of the device (e.g. increased reverse bias leakage and a soft-knee) while the electroluminescence image (Figure 15) shows no significant dark area defects. This data suggests that there is some degradation of the active layers of the device but does not indicate the location. However, plan-view TEM analysis (Figure 16) shows numerous damage sites in the oxide. The damage occurs in circles of two different radii which may reflect an initial discharge pulse (larger circle) and a subsequent pulse from the metal block back to the chip (smaller circle). The damage-type observed in the circle of greater radius has never been observed in devices that were subjected to HBM 1.00E-05 Figure 12. Plan-view TEM micrograph of device subjected to MM ESD event. Reverse Current (-A) oxide tip 1.00E-06 1.00E-07 1.00E-08 1.00E-09 After zap 1.00E-10 Before zap 1.00E-11 1.00E-12 0 5 10 15 Reverse Bias (-V) Figure 13. Cross-section TEM image of a section lifted from the planview membrane shown in Figure 12 (dotted line box). Figure 14. Reverse bias IV trace from a device subjected to a relatively strong CDM ESD event (red) and a known good device. Figure 15. Electroluminescence image from a device subjected to a relatively strong CDM ESD event. Figure 17. Cross-section TEM micrograph through a defect caused by a CDM event. or MM events. Cross-section TEM analysis of one of these damage sites in the oxide (Figure 17) shows dielectric breakdown for which the crystallinity of the site is disrupted (likely due to local melting and freezing). The damage extends vertically through the oxide layer even physically moving a section of the oxide in the image shown. Other cross-section analyses have shown damage sites that extend vertically to the active layers of the device which is consistent with the increased leakage current. In contrast, cross-section analysis (not shown) of the damage near the oxide aperture edge shows junction damage similar to, and in roughly the same location as, damage caused by MM ESD events. DAMAGE FROM LONGER DURATION ELECTRICAL PULSES Within the broader class of electrical overstress occurrences (of which the relatively short ESD events comprise a subset) the more severe cases of abuse are often detected with an optical microscope (e.g. by the presence of cavities where the active area should be). However, weaker EOS events may generate outward characteristics that are similar to those observed in ESD-degraded devices. Figure 16. Plan-view TEM micrograph showing the oxide and quantum well active layers from a CDM degraded VCSEL. The oxide layer is populated by two circular distributions of damage sites. Reverse Current (-A) 1.00E-05 1.00E-06 1.00E-07 1.00E-08 1.00E-09 1.00E-10 1.00E-11 1.00E-12 0 5 10 15 Reverse Bias (-V) Figure 18. Reverse bias IV trace from a device subjected to a short pulse EOS event (red) and a known good device. Electrical characterization (Figure 18) of a device subjected to 5 minutes of 1% duty cycle 100ns 300mA pulses shows increased leakage current and a lower breakdown voltage. Electroluminescence imaging (Figure 19) shows a nonuniform emission pattern with a “dim” area defect. Plan-view TEM imaging (Figure 20) reveals punched-out dislocations Figure 20. Plan-view TEM micrograph showing the oxide and quantum well active layers from a forward bias EOS pulse degraded VCSEL. Several punched-out dislocations have moved through the active area, segments of which have experienced recombination enhanced dislocation growth. which have undergone some recombination enhanced dislocation growth. Thus, whereas the ESD causes localized damage sites, the short pulse EOS event appears to create a broader thermal stress, that acting on the active area generates dislocations at the oxide terminus. ESD IN CUSTOMER-RETURNED DEVICES Thus far, we have shown how the location and characteristics of ESD damage in VCSELs depends on the electrical properties of the ESD source. The data shown (with the exception of the CDM example) was generated using standardized test circuits. In the field, VCSELs will be subjected to ESD sources that may closely resemble these circuit models but there will likely be some variation in the real-world circuit values from those specified in the models. To conclude, we show evidence that the intentionally generated ESD damage mechanisms explored here are found in field returns and that these ESD damage sites can act as the nucleation centers for dislocation arrays. Figure 19. Electroluminescence image from a device subjected to a short pulse EOS event. Similarly, the plan-view TEM data shown in Figure 22 demonstrates that a dislocation array can nucleate on damage created by a what appears to be a CDM ESD event. SUMMARY Figure 21. Plan-view TEM micrograph showing the oxide and quantum well active layers from a field-failed VCSEL that was subjected to an HBM ESD event. The plan-view TEM data in Figure 21 shows that the dislocation array found in a field return device was nucleated on damage that appears to be due to a reverse bias HBM ESD. The fact that the centers of the damage occur at the oxide edge suggests that the power was dissipated in a faster pulse than the HBM example shown in Figure 4. Figure 22. Plan-view TEM micrograph of a field-failed device subjected to a CDM event. In this paper we have shown how the degradation present in an ESD damaged oxide VCSEL depends on the electrical properties of the ESD source and subsequent pulse characteristics. The damage resulting from relatively slow ESD models (e.g. HBM) occurs well within the oxide confinement aperture. As the speed of the ESD pulse increases, the damage occurs in a wider circumference as the impendence of the oxide layer decreases and as greater bias is expressed across the oxide layer. In general, the damage can extend from the mirror layers above the oxide layer though the quantum wells to the mirrors layers below. Where the damage does intersect the quantum wells, it is possible for a dislocation array to grow. Laterally, the dislocation arrays nucleated on ESD damage sites generally grow towards the active area where carrier concentrations are high. AOC has not observed dislocation array growth from the oxide trenches due to ESD or any other defect. The ESD failure signatures revealed by this work have been observed in field returned devices. An understanding of the failure signatures has improved AOC’s ability to assign a more precise root cause to those field returned devices. Knowing which the type of ESD caused the failure has greatly aided in determining the source of the event and in implementing appropriate corrective action. REFERENCES 1 D.T. Mathes, R. Hull, Kent Choquette, K. Geib, A. Allerman, J. Guenter, B. Hawkins, R. Hawthorne, “Nanoscale Materials Characterization of Degradation in VCSELs”, Proc. of SPIE, vol. 4994, pp 67-83, (2003). 2 R. W. Herrick, Degradation in Vertical Cavity Lasers, Dissertation, Department of Electrical and Computer Engineering, University of California, Santa Barbara, CA (1997). 3 R.W. Herrick, “Failure Analysis and Reliability of Optoelectronic Devices,” published in “Microelectronics Failure Analysis Desk Reference, 5th ed.,” by ASM International, Materials Park Ohio, pp. 230-254 (2004). 4 Terence J. Stark, Phillip E. Russell, and Corey Nevers, “3-D defect characterization using plan view and crosssectional TEM / STEM analysis,” to be published in the proceedings of ISTFA 2005 (this volume). 5 F. Siegelin, C. Brillert, “Failure Analysis of Vertical Cavity Surface Emission Laser Diodes”, Proceedings from the 29th International Symposium for Testing and failure Analysis, p. 426, 2003. 6 J. Krueger, R. Sabharwal, S. McHugo, K. Nguyen, N.X. Tan, N. Janda, M. Mayonte, M. Heidecker, D. Eastley, M. Keever, and C. Kocot, "Studies of ESD-related failure patterns of Agilent oxide VCSELs," Proc of SPIE, vol. 4994, pp. 162-172, (2003). 7 O. Mcateer, Electrostatic Discharge Control, (Mcgraw-Hill Publishing Company, 1990). 8 S. Voldman, ESD Physics and Devices, (John Wiley and Sons, 2004). 9 James K. Guenter, Jim A. Tatum, Robert A. Hawthorne III, Ralph H. Johnson, David T. Mathes, Bobby M. Hawkins, “A plot twist: the continuing story of VCSELs at AOC, “ Proc of the SPIE, vol 5737, pp. 20-34, (2005). ADVANCED OPTICAL COMPONENTS AOC CAPABILITIES Finisar’s ADVANCED OPTICAL COMPONENTS division was formed through strategic acquisition of key optical component suppliers. The company has led the industry in high volume Vertical Cavity Surface Emitting Laser (VCSEL) and associated detector technology since 1996. VCSELs have become the primary laser source for optical data communication, and are rapidly expanding into a wide variety of sensor applications. VCSELs’ superior reliability, low drive current, high coupled power, narrow and circularly symmetric beam and versatile packaging options (including arrays) are enabling solutions not possible with other optical technologies. 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