Journal of Advanced Applied Scientific Research - ISSN: 2454-3225
K. Irulandi et.al JOAASR-RTB-2016- February-2016: supplementary
GC-MS analysis and phytochemical studies of methanolic fruits extract of
Garcinia cambogia Hort. Ex Boerl and Ziziphus trinervia Roth
Garcinia cambogia
Ziziphus trinervia
Methanol extract
Methanol extract
Alkaloid
+
+
Catechin
-
-
Coumarin
+
-
Flavonoid
-
+
Phenol
+
+
Quinone
-
+
Saponin
+
-
Steroid
+
-
Tannin
+
-
Terpenoid
+
-
Phyto compounds
+ = indicates presence of phytochemicals, - = indicates absence of phytochemicals
Table 1. Results of Preliminary Phytochemical Evaluation of methanolic fruit extract of
Garcinia cambogia and Ziziphus trinervia
Journal of Advanced Applied Scientific Research - ISSN: 2454-3225
K. Irulandi et.al JOAASR-RTB-2016- February-2016: supplementary
GC-MS analysis and phytochemical studies of methanolic fruits extract of
Garcinia cambogia Hort. Ex Boerl and Ziziphus trinervia Roth
S.No
R.Time
Area
percentage
Chemical formula
1
1.667
19.30
C3H7ClO
Ethane, (chloromethoxy)-
2
1.924
1.37
C16H24N2
1H-Imidazole, 2,4-dimethyl-
3
1.975
1.01
C5H8O
4
2.224
0.74
C14H30O
5
2.480
1.07
6
2.531
7
Compound name
3-Pentyn-1-ol
2-Hexyl-1-octanol
C12H23ClO2
Acetic acid, 10-chlorodecyl ester
0.99
C19H31F7O2
Heptafluorobutyric acid, n-tetradecyl ester
3.476
18.74
C15H26O2
8
4.091
2.15
C5H8N2
Formaldehyde, methyl(2-propynyl)hydrazone
9
4.259
1.50
C8H14O
2-ethoxy-3,5-hexadiene
10
4.567
5.44
C14H42O7Si7
Cycloheptasiloxane, tetradecamethyl-
11
5.826
1.86
C15H26O2
2-Pentadecanone, 6,10,14-trimethyl-
12
6.068
3.44
C18H37
1-Octadecanesulphonyl chloride
13
6.317
3.04
C15H28Cl2O2
Dichloroacetic acid, tridecyl ester
14
6.434
1.62
C11H24
15
6.478
1.76
C10H9NO
16
6.558
0.99
C6H6S
17
6.617
0.58
C54H108Br2
Tetrapentacontane, 1,54-dibromo-
18
6.661
1.15
C13H20O3
3-Cyclopenteneethanal, 2-[[(tetrahydro-2pyranyl)oxy]methyl]-, (1r,2-cis)-
19
6.734
0.84
C5H6O4
1,1-Cyclopropanedicarboxylic acid
20
6.851
1.82
C8H16O
2-Hexen-1-ol, 2-ethyl-
21
6.932
1.29
C12H26
2,6-Dimethyldecane
22
7.005
0.85
C28H58O
Ditetradecyl ether
23
7.071
1.97
C20H40O2
9-Octadecene, 1,1-dimethoxy-, (Z)-
24
7.203
1.15
C20H41Cl
1-Chloroeicosane
25
7.247
1.52
C17H34O3
Methoxyacetic acid, 2-tetradecyl ester
Cyclohexanecarboxylic acid, 2-ethylcyclohexyl ester-
Undecane
8-Quinolinol, 4-methylDipropargyl sulfide
Journal of Advanced Applied Scientific Research - ISSN: 2454-3225
K. Irulandi et.al JOAASR-RTB-2016- February-2016: supplementary
GC-MS analysis and phytochemical studies of methanolic fruits extract of
Garcinia cambogia Hort. Ex Boerl and Ziziphus trinervia Roth
26
7.320
0.58
C11H24
Undecane
27
7.605
1.78
C26H54
Octadecane, 3-ethyl-5-(2-ethylbutyl)-
28
7.745
1.88
C28H48O
Cholest-4-ene, 3.beta.-(methoxymethoxy)-
29
8.096
1.00
C5H6N2O3
1,2,5-Oxadiazole-3-acetic acid, 4-methyl-
30
8.389
2.36
C13H21NO
N-Methyl-1-adamantaneacetamide
31
8.469
0.73
C16H48O7Si8
32
8.513
0.64
C13H21NO
33
8.638
1.58
C9H10O3
34
8.740
0.96
C16H14N2O4
35
8.850
3.34
C17H34O2
36
8.982
0.63
C16H48O7Si8
37
9.019
1.83
Octasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11,13,13,15,15hexadecamethylN-Methyl-1-adamantaneacetamide
3,5-Dimethylbenzaldehyde thiocarbamoylhydrazone
4-Dehydroxy-N-(4,5-methylenedioxy-2nitrobenzylidene)tyramine
Hexadecanoic acid, methyl ester
Octasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11,13,13,15,15hexadecamethyl3,5-Ethanoquinolin-10-one, decahydro-1,7-dimethyl-, [3R(3.alpha.,4a.beta.,5.alpha.,7.beta.,8a.beta.)]-
C11H11Bro4
38
9.348
0.64
C16H48O7Si8
39
9.824
4.53
C8H5N3O4
40
9.875
1.34
C15H13N
Octasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11,13,13,15,15hexadecamethyl1,4-Phthalazinedione, 2,3-dihydro-6-nitroTrimethylsilyl 3-methyl-4-[(trimethylsilyl)oxy]benzoate
Table 2. Compounds identified by the GC-MS analysis from methanolic fruit extract of Garcinia
cambogia.
Journal of Advanced Applied Scientific Research - ISSN: 2454-3225
K. Irulandi et.al JOAASR-RTB-2016- February-2016: supplementary
GC-MS analysis and phytochemical studies of methanolic fruits extract of
Garcinia cambogia Hort. Ex Boerl and Ziziphus trinervia Roth
S.No R.Time
1
2
3
Area
percentage
Chemical
formula
Compound name
4.633
31.06
C9H12O
benzenemethanol .alpha. .alpha.dimethyl-
15.111
21.30
C16H32O2
n-Hexadecanoic acid
18.215
44.64
C7HF4NS
2,3,4,6-tetrafluorophenyl
isothiocyanide
Table 3. Compounds identified by the GC-MS analysis from methanolic fruit extract of
Ziziphus trinervia
Journal of Advanced Applied Scientific Research - ISSN: 2454-3225
K. Irulandi et.al JOAASR-RTB-2016- February-2016: supplementary
GC-MS analysis and phytochemical studies of methanolic fruits extract of
Garcinia cambogia Hort. Ex Boerl and Ziziphus trinervia Roth
Figure 1. GC-MS chromatogram of methanolic extract of fruit of Garcinia cambogia
Journal of Advanced Applied Scientific Research - ISSN: 2454-3225
K. Irulandi et.al JOAASR-RTB-2016- February-2016: supplementary
GC-MS analysis and phytochemical studies of methanolic fruits extract of
Garcinia cambogia Hort. Ex Boerl and Ziziphus trinervia Roth
Figure 2. GC-MS chromatogram of methanolic extract of fruit of Ziziphus trinervia