PALLET CARD PROGRAM LABORATORY REPORT PROSOCO, Inc. Page 4 PURPOSE OF TESTING Seven different dolomitic limestone veneer samples were submitted to PROSOCO, Inc.’s Testing Laboratory with a request to determine if application of the cleaning products evaluated will produce any surface alterations during new construction cleaning operations. Additionally, the effectiveness of water repellents, stain repellents, and graffiti control products suitable for dolomitic limestone as well as treatments for color enhancement will be evaluated. ® ® ® A. New Construction Cleaning – Sure Klean Vana Trol and Sure Klean Burnished Custom Masonry ® Cleaner were evaluated for removal of laboratory applied Ash Grove Type S mortar. To simulate new construction soiling, the samples are placed on a bench with finished surface facing upward. Hollow cylinders measuring 50 mm in diameter and 75 mm tall are positioned on top of each ® sample and filled with a wet mixture of Ash Grove Type S mortar. The wet mortar-filled cylinder is allowed to remain in contact with the sample for 10 minutes before removal. Soiled samples are allowed to dry before test cleaning. Heavy deposits of mortar are removed with dry scraping after 24 hours. Prepared cleaning solutions are then evaluated for their effectiveness in removing residual mortar staining after 3, 7, and 14 days of curing. ® ® B. Surface Alteration Testing – Sure Klean Vana Trol® and Sure Klean Burnished Custom Masonry Cleaner were tested to determine if a cleaning program implemented to remove excess mortar and related new construction soiling would otherwise alter the appearance of cleaned surfaces. Surface Alteration was evaluated visually based upon perceived discoloration or erosion/etching of the samples. Surface Finish Removal is the visual examination of the sample comparing the surface finish of the untreated control surface to the surface finish cleaned with selected product(s) at given dilutions. Substrate Deterioration is the visual examination of the sample comparing the surface of the untreated control to surfaces cleaned with selected product(s) at given dilutions looking for any potential erosion/digestion of the sample. Color Change is the visual examination comparing the color of the untreated control surface to color of surfaces cleaned with selected products at given dilutions. Staining is the visual examination for changes that are the result of a chemical reaction that leaves a staining precipitate. ® ® C. Water Repellent Evaluation – Sure Klean Weather Seal Natural Stone Treatment, Sure Klean ® ® Weather Seal Blok-Guard & Graffiti Control, and Stand Off Paver Enhancer were evaluated on the submitted samples for their ability to provide water repellency using RILEM Test Method No. II.4. ® D. Stain Repellent Evaluation – Stand Off Stone, Tile, & Masonry Protector was evaluated on the submitted samples for its ability to provide stain repellency to the submitted samples. E. Graffiti Control – Sure Klean® Weather Seal Blok-Guard® & Graffiti Control was evaluated for its ability to ® control graffiti on the submitted samples. Defacer Eraser® Graffiti Wipe and Sure Klean Fast Acting Stripper were evaluated for their ability to remove graffiti from the submitted samples. ® ® ® F. Color Enhancement – Sure Klean Weather Seal Blok-Guard & Graffiti Control and Stand Off Paver Enhancer were evaluated on the submitted samples for their ability to enhance the natural color of the submitted samples in relative comparison to the untreated surface’s water-saturated appearance. PROSOCO, Inc. • 3741 Greenway Circle • Lawrence, Kansas 66046 • (785) 865-4200 • Fax (785) 830-9176 PALLET CARD PROGRAM LABORATORY REPORT PROSOCO, Inc. Page 5 CLEANING PRODUCTS SAMPLE PRODUCT ® All types of dolomitic limestone veneer DILUTION ® 1:10 Sure Klean Vana Trol ® Sure Klean Burnished Custom Masonry Cleaner 1:3 SURFACE ALTERATION PRODUCTS EVALUATED SAMPLE PRODUCT ® All types of dolomitic limestone veneer DILUTION ® 1:10 Sure Klean Vana Trol ® Sure Klean Burnished Custom Masonry Cleaner 1:3 WATER REPELLENT PRODUCTS EVALUATED SAMPLE PRODUCT ® Sure Klean Weather Seal Natural Stone Treatment All types of dolomitic limestone veneer ® ® Sure Klean Weather Seal Blok-Guard & Graffiti Control ® Stand Off Paver Enhancer STAIN REPELLENT PRODUCTS EVALUATED SAMPLE PRODUCT All types of dolomitic limestone veneer Stand Off Stone, Tile, & Masonry Protector ® NOTE: Dilution ratios refer to mixtures of concentrated product : fresh water. PROSOCO, Inc. • 3741 Greenway Circle • Lawrence, Kansas 66046 • (785) 865-4200 • Fax (785) 830-9176 PALLET CARD PROGRAM LABORATORY REPORT PROSOCO, Inc. Page 6 GRAFFITI CONTROL PRODUCTS EVALUATED SAMPLE PRODUCT All types of dolomitic limestone veneer Sure Klean® Weather Seal Blok-Guard® & Graffiti Control GRAFFITI REMOVAL PRODUCTS EVALUATED SAMPLE PRODUCT Defacer Eraser® Graffiti Wipe All types of dolomitic limestone veneer ® Sure Klean Fast Acting Stripper COLOR ENHANCING PRODUCTS EVALUATED SAMPLE PRODUCT All types of dolomitic limestone veneer Sure Klean Weather Seal Blok-Guard & Graffiti Control ® ® ® Stand Off Paver Enhancer PROSOCO, Inc. • 3741 Greenway Circle • Lawrence, Kansas 66046 • (785) 865-4200 • Fax (785) 830-9176 PALLET CARD PROGRAM LABORATORY REPORT PROSOCO, Inc. Page 26 SECTION F – COLOR ENHANCEMENT The testing described below evaluates the degree of color enhancement that the treatments provide to the samples. The surface treatments evaluated were selected for their suitability for application based on the following selection criteria: 1. 2. 3. Ease of application Color change Removal of staining substances DESCRIPTIONS OF PRODUCT EVALUATED – Color Enhancement Sure Klean® Weather Seal Blok-Guard® & Graffiti Control – A clear, solvent-based silicone elastomer formulated to weatherproof custom masonry units, cast stone, and concrete block without altering the natural appearance. Blok-Guard® & Graffiti Control penetrates and fills pores to prevent water penetration through exterior walls exposed to normal weathering as well as long-lasting protection against many types of graffiti. Stand Off® Paver Enhancer – A solvent-based blend of high-quality siloxanes modified to provide excellent water repellency and color enhancement to interlocking concrete, fired clay, porous tile and many types of natural stone surfaces. Penetrates and reacts with the surface to form a chemical bond, provided long-term durability, alkali resistance and superior breathability. SAMPLE PREPARATION – Color Enhancement The submitted samples were allowed to dry, and reabsorb atmospheric humidity for 24 hours prior to treatment. ® ® Method of treatment consisted of a wet-on-wet brush application for Sure Klean Weather Seal Blok-Guard & ® Graffiti Control and one saturating application for Stand Off Paver Enhancer. All treatments were allowed to cure at least 72 hours prior to testing. TEST METHODS – Color Enhancement Color enhancement is evaluated visually based on the appearance of the treatment applied. This includes color changes and/or darkening. For purpose of this evaluation, treatments that produce “no enhancement” do not alter the natural appearance of the substrate and are rated with a value of 1. Untreated substrates are rated a value of 0. Treatments that provide the same degree of darkening as water-saturated examples of the substrate are rated with a value of 5. A value of 2 is estimated to be 25% of the water-saturated degree of darkening. A value of 3 is estimated to be 50% of the water-saturated degree of darkening. A value of 4 is estimated to be 75% of the water-saturated degree of darkening. PROSOCO, Inc. • 3741 Greenway Circle • Lawrence, Kansas 66046 • (785) 865-4200 • Fax (785) 830-9176 PALLET CARD PROGRAM LABORATORY REPORT PROSOCO, Inc. Page 27 Test Results – Color Enhancement “Wisconsin Castle Rock (Gray Buff)” Treatment Untreated Control Enhancement 0 4 3 ® Blok-Guard & Graffiti Control Paver Enhancer “Wisconsin Castle Rock (Full Color)” Treatment Untreated Control Enhancement 0 4 3 ® Blok-Guard & Graffiti Control Paver Enhancer “Chilton Rustic” Treatment Untreated Control Enhancement 0 2 2 ® Blok-Guard & Graffiti Control Paver Enhancer “Chilton Country Squire” Treatment Untreated Control Enhancement 0 4 4 ® Blok-Guard & Graffiti Control Paver Enhancer “Fond du Lac Castle Rock” Treatment Untreated Control Enhancement 0 4 4 ® Blok-Guard & Graffiti Control Paver Enhancer “Fond du Lac Rustic” Treatment Untreated Control Enhancement 0 2 2 ® Blok-Guard & Graffiti Control Paver Enhancer “Fond du Lac Country Squire” Treatment Untreated Control ® Blok-Guard & Graffiti Control Paver Enhancer Enhancement 0 4 2 Scale used for reporting results: 0 – Untreated Control 3 – 50% Darkening 1 – No Enhancement 4 – 75% Darkening 2 – 25% Darkening 5 – 100% Darkening PROSOCO, Inc. • 3741 Greenway Circle • Lawrence, Kansas 66046 • (785) 865-4200 • Fax (785) 830-9176 PALLET CARD PROGRAM LABORATORY REPORT PROSOCO, Inc. Page 28 CONCLUSIONS – Color Enhancement ® ® Based upon laboratory evaluations, Sure Klean Weather Seal Blok-Guard & Graffiti Control was most effective at providing color enhancement. Stand Off® Paver Enhancer also enhanced the color of the dolomitic ® ® limestone veneer samples, but to a much lesser degree than the Sure Klean Weather Seal Blok-Guard & Graffiti Control. NOTE: See Attachment #2 “PHOTO C”. RECOMMENDATIONS – COLOR ENHANCEMENT ® ® Based on evaluations, Sure Klean Weather Seal Blok-Guard & Graffiti Control and Stand Off® Paver Enhancer can be recommended for job-site testing to provide color enhancement to the samples submitted by Buechel Stone Corporation, Chilton, WI. Apply all products in accordance with the manufacturer's recommendation provided on container labels and product data sheets. On-site testing should be conducted to determine the most appropriate color enhancing product and procedures for a particular project. See product literature for additional application and product information. Jason L. Anderson Materials Testing Technician JLA/ PROSOCO, Inc. • 3741 Greenway Circle • Lawrence, Kansas 66046 • (785) 865-4200 • Fax (785) 830-9176 PALLET TAG PROGRAM LABORATORY REPORT PROSOCO, Inc. Page 2 Purpose of Testing Seven types of dolomitic limestone were submitted to PROSOCO, Inc.’s Testing Laboratory with a request to determine the optimum dilution of the new construction cleaning products evaluated for complete removal of laboratory applied mortar while limiting any surface alterations. Additionally, the effectiveness of water repellents, graffiti control products and color and sheen enhancing treatments suitable for limestone were evaluated. New Construction Cleaning – Sure Klean® Vana Trol® and Sure Klean® Burnished Custom Masonry Cleaner were evaluated for removal of laboratory applied mortar. The surface alteration evaluation was visually determined based upon perceived discoloration or erosion/etching of the samples. To simulate new construction soiling, the samples were placed on a bench with finished surface facing upward. Hollow cylinders measuring 50 mm in diameter and 75 mm tall were positioned on top of the samples and filled with a wet mixture of Type S cementitious mortar. The wet mortar-filled cylinder was allowed to remain in contact with the samples for 10 minutes before removal. Heavy deposits of mortar were removed with dry scraping after 24 hours. Prepared cleaning solutions were then evaluated for their effectiveness in removing residual Type S mortar after 3, 7, and 14 days of curing. A visual examination was also made to determine if the tested cleaners caused any surface alterations to the submitted samples based on the following: Surface Finish Removal is the visual examination of the sample comparing the surface finish of the untreated control surface to the surface finish cleaned with selected product(s) at given dilutions. Substrate Deterioration is the visual examination of the sample comparing the surface of the untreated control to surfaces cleaned with selected product(s) at given dilutions looking for any potential erosion/digestion of the sample. Color Change is the visual examination comparing the color of the untreated control surface to color of surfaces cleaned with selected products at given dilutions. Staining is the visual examination for changes that are the result of a chemical reaction that leaves a staining precipitate. Protective Water Repellents – Sure Klean® Paver Enhancer, Sure Klean® Weather Seal Blok-Guard® & Graffiti Control, Sure Klean® Weather Seal Natural Stone Treatment, Sure Klean® Weather Seal Natural Stone Treatment WB, and Stand Off® Limestone & Marble Protector were evaluated for their ability to provide water repellency on the submitted samples. Graffiti Control – Sure Klean® Weather Seal Blok-Guard® & Graffiti Control and Defacer Eraser® Graffiti Barrier S were evaluated for their ability to repel graffiti from the submitted samples. Sure Klean® Fast Acting Stripper and Defacer Eraser® Graffiti Wipe were evaluated for their ability to remove graffiti from the submitted samples. Color and Sheen Enhancement – Sure Klean® Paver Enhancer, Stand Off® Gloss ‘N Guard, and Stand Off® Gloss ‘N Guard WB were evaluated for their ability to provide color and sheen enhancement to the submitted samples. PROSOCO, Inc. • 3741 Greenway Circle • Lawrence, Kansas 66046 • (785) 865-4200 • Fax: (785) 830-9176 PALLET TAG PROGRAM LABORATORY REPORT PROSOCO, Inc. Page 3 Products Evaluated New Construction Cleaning Products Evaluated Sample Treatment ® All Submitted Samples Dilution ® Sure Klean Vana Trol 1:6, 1:8 Sure Klean® Burnished Custom Masonry Cleaner 1:2, 1:3 Protective Water Repellent Products Evaluated Sample All Submitted Samples Treatment Dilution Sure Klean® Paver Enhancer Concentrate Sure Klean® Weather Seal Blok-Guard® & Graffiti Control Concentrate Sure Klean® Weather Seal Natural Stone Treatment Concentrate Sure Klean® Weather Seal Natural Stone Treatment WB Concentrate Stand Off® Limestone & Marble Protector Concentrate Graffiti Repellent Products Evaluated Sample Product Dilution Sure Klean® Weather Seal Blok-Guard® & Graffiti Control Concentrate Defacer Eraser® Graffiti Barrier S Concentrate Product Dilution Sure Klean® Fast Acting Stripper Concentrate Defacer Eraser® Graffiti Wipe Concentrate All Submitted Samples Graffiti Removal Products Evaluated Sample All Submitted Samples Color and Sheen Enhancement Products Evaluated Sample All Submitted Samples Treatment Dilution Sure Klean® Paver Enhancer Concentrate Stand Off® Gloss ‘N Guard Concentrate Stand Off® Gloss ‘N Guard WB Concentrate PROSOCO, Inc. • 3741 Greenway Circle • Lawrence, Kansas 66046 • (785) 865-4200 • Fax: (785) 830-9176 PALLET TAG PROGRAM LABORATORY REPORT PROSOCO, Inc. Page 23 Color and Sheen Enhancement These trials were conducted to determine the product(s) that provide the best color and sheen enhancement to the submitted dolomitic limestone. Description of Products Evaluated – Color and Sheen Enhancement Sure Klean® Paver Enhancer – A solvent-based blend of high-quality siloxanes modified to provide excellent water repellency and color enhancement to interlocking concrete, fired clay, porous tile and many types of natural stone surfaces. Paver Enhancer penetrates and reacts with the surface to form a chemical bond, providing long-term durability, alkali resistance and superior breatheability. Stand Off® Gloss ‘N Guard – A highly durable protective coating for tile, pavers, terrazzo and other polished and unpolished masonry. Gloss ‘N Guard dries to a high-gloss finish that enhances the natural beauty of treated surfaces. Stand Off® Gloss ‘N Guard WB – A highly durable protective coating for tile, pavers, terrazzo and other polished and unpolished masonry. Gloss ‘N Guard WB dries to a satin-gloss finish which enhances the natural beauty of treated surfaces. The water-borne acrylic formula complies with all known AIM VOC regulations nationwide. Sample Preparation – Color and Sheen Enhancement Samples were cleaned with Enviro Klean® 2010 All Surface Cleaner diluted with 10 parts water and allowed to dry for 24 hours prior to treatment. Test Method – Color and Sheen Enhancement All treatments were applied by brush in accordance with the application instructions in the current PROSOCO, Inc. Product Data Sheets. Visual examinations for color and sheen enhancement were then made, comparing the treated surfaces to an untreated surface. PROSOCO, Inc. • 3741 Greenway Circle • Lawrence, Kansas 66046 • (785) 865-4200 • Fax: (785) 830-9176 PALLET TAG PROGRAM LABORATORY REPORT PROSOCO, Inc. Page 24 Test Results – Color and Sheen Enhancement “Frontier Gray” Treatment Sure Klean Paver Enhancer Stand Off® Gloss ‘N Guard Stand Off® Gloss ‘N Guard WB Color Enhancement 3 3 1 “Millcreek – Rock-face” Sheen Enhancement 1 3 3 Treatment Sure Klean® Paver Enhancer Stand Off® Gloss ‘N Guard Stand Off® Gloss ‘N Guard WB Color Enhancement 2 3 2 “Sandcastle Dark” Sheen Enhancement 0 2 3 Treatment Sure Klean® Paver Enhancer Stand Off® Gloss ‘N Guard Stand Off® Gloss ‘N Guard WB Color Enhancement 3 3 1 “Sandcastle Light” Sheen Enhancement 0 2 3 Treatment Sure Klean® Paver Enhancer Stand Off® Gloss ‘N Guard Stand Off® Gloss ‘N Guard WB Color Enhancement 3 2 1 “Silverdale” Sheen Enhancement 0 2 3 Treatment Sure Klean Paver Enhancer Stand Off® Gloss ‘N Guard Stand Off® Gloss ‘N Guard WB Color Enhancement 2 3 1 “Texas Cream” Sheen Enhancement 0 1 3 Treatment Color Enhancement Sure Klean Paver Enhancer 2 Stand Off® Gloss ‘N Guard 3 Stand Off® Gloss ‘N Guard WB 1 “Thermal New York Bluestone” Sheen Enhancement 0 1 3 Treatment Sure Klean Paver Enhancer Stand Off® Gloss ‘N Guard Stand Off® Gloss ‘N Guard WB Sheen Enhancement 0 2 3 ® ® ® ® Color Enhancement 3 3 3 Scale: 0- No Enhancement; Dull 1- Slight Enhancement 2- Moderate Enhancement 3- Significant Enhancement PROSOCO, Inc. • 3741 Greenway Circle • Lawrence, Kansas 66046 • (785) 865-4200 • Fax: (785) 830-9176 PALLET TAG PROGRAM LABORATORY REPORT PROSOCO, Inc. Page 25 Photographs – Color and Sheen Enhancement “New York Thermal Bluestone”; Treatments Applied Stand Off® Gloss ‘N Guard Untreated Control Stand Off® Gloss ‘N Guard WB Sure Klean® Paver Enhancer PROSOCO, Inc. • 3741 Greenway Circle • Lawrence, Kansas 66046 • (785) 865-4200 • Fax: (785) 830-9176 PALLET TAG PROGRAM LABORATORY REPORT PROSOCO, Inc. Page 26 Recommendations – Color and Sheen Enhancement Recommendations for color and sheen enhancement for the dolomitic limestone submitted by Buechel Stone Corporation, Chilton, WI are provided in the chart below. Recommendations are based on the treatment or treatments that proved most effective in providing color and sheen enhancement to the submitted samples. Sample Color Enhancement Sheen Enhancement “Frontier Gray” “Sandcastle Dark” “Sandcastle Light” Sure Klean® Paver Enhancer OR Stand Off® Gloss ‘N Guard Stand Off® Gloss ‘N Guard OR Stand Off® Gloss ‘N Guard WB “Millcreek – Rock-face” “Thermal New York Bluestone” Sure Klean® Paver Enhancer OR Stand Off® Gloss ‘N Guard OR Stand Off® Gloss ‘N Guard WB Stand Off® Gloss ‘N Guard OR Stand Off® Gloss ‘N Guard WB “Silverdale” “Texas Cream” Sure Klean® Paver Enhancer OR Stand Off® Gloss ‘N Guard Stand Off® Gloss ‘N Guard WB Apply all products in accordance with the manufacturer's recommendation provided on container labels and product data sheets. On-site testing should be conducted to determine the most appropriate product and procedures for a particular project. See product literature for additional application and product information. Christopher A. Moore Project Testing Laboratory Technician CAM PROSOCO, Inc. • 3741 Greenway Circle • Lawrence, Kansas 66046 • (785) 865-4200 • Fax: (785) 830-9176
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